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Highly Thermally Stable, Highly Electrolyte-Wettable Hydroxyapatite/Cellulose Nanofiber Hybrid Separators for Lithium-Ion Batteries

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ACS Applied Energy Materials 2023年第7期6卷 3862-3871页

作者： Liu, Yi Li, Chunxing Li, Chao Liang, Zhenye Hu, Xueshan Liu, Hao Zhang, Ze Cui, Meng Chen, Gang Wan, Jiayu Zhang, Xiangwu Tao, Jinsong State Key Lab of Pulp and Paper Engineering South China University of Technology Guangzhou510640 China SUSTech Energy Institute for Carbon Neutrality Southern University of Science and Technology Shenzhen518055 China Department of Mechanical and Energy Engineering Southern University of Science and Technology Shenzhen518055 China Fiber and Polymer Science Program Department of Textile Engineering Chemistry and Science Wilson College of Textiles North Carolina State University RaleighNC27695-8301 United States

Separators have an important influence on the safety and performance of lithium-ion batteries (LIBs). However, traditional polyolefin-based separators suffer from poor thermal stability and weak electrolyte wettability. Here, by using hydroxyapatite (HAP) and cellulose nanofibers (CNFs) as raw materials, we fabricated a unique HAP/CNF hybrid separator. The separators exhibit excellent thermal properties, with high thermal stability (up to 250 °C) and outstanding flame retardancy. The separators also demonstrate excellent electrolyte wettability. Compared to polypropylene (PP) separators, the HAP/CNF separators show a smaller contact angle with electrolytes, 17.2° for HAP/CNF and 45.5° for PP. Meanwhile, the HAP/CNF separators illustrate an excellent smoothness of 68.0 nm. In addition, the batteries assembled with the hybrid separators display a better performance compared with the batteries assembled with commercial PP separators. The raw materials are green, and the fabrication processes are free of organic solvents. We envision that the HAP/CNF hybrid separator could be a promising separator candidate for next-generation high-safety and high-performance LIBs. © 2023 American Chemical Society.

关键词： Thermodynamic stability

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Supertough spontaneously self-healing polymer based on septuple dynamic bonds integrated in one chemical group

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science China Chemistry 2022年第2期65卷 363-372页

作者： Luzhi Zhang Qingbao Guan Ao Shen Rasoul Esmaeely Neisiany Zhengwei You Meifang Zhu State Key Laboratory for Modification of Chemical Fibers and Polymer Materials Shanghai Belt and Road Joint Laboratory of Advanced Fiber and Low-dimension Materials(Donghua University)College of Materials Science and EngineeringShanghai Engineering Research Center of Nano-Biomaterials and Regenerative MedicineInstitute of Functional MaterialsDonghua UniversityResearch Base of Textile Materials for Flexible Electronics and Biomedical ApplicationsChina Textile Engineering SocietyShanghai 201620China Department of Materials and Polymer Engineering Hakim Sabzevari UniversitySabzevar ***Iran

The development of spontaneously self-healing materials with excellent mechanical properties remains a formidable challenge despite the extensive interest in such *** is because the self-healing and mechanical properties of a material are usually optimized via contradictory *** present study demonstrated a supertough spontaneously self-healing polymer,Fe-(2,6-diacetylpyridine dioxime)-urethane-based polyurethane(Fe-PPOU)based on septuple dynamic bonds integrated in one chemical group.A synergistic effect was induced by the presence of multiple dynamic crosslinking points,which comprised the integrated dynamic interactions,and the hidden lengths of the folded polymeric chains in ***,the mechanical and self-healing properties of the polymer were simultaneously ***-PPOU demonstrated the highest reported toughness(139.8 MJ m^(-3))among all the room-temperature spontaneously self-healing polymers with a nearly 100%healing ***-PPOU exhibited instant(30 s)self-healing to reach a strength of 1.6 MPa that was higher than the original strength of numerous recently reported self-healing polymers.

关键词： oxime-urethane bonds hydrogen bonds metal-coordination bonds 2 6-diacetylpyridine dioxime self-healing

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Flexible,anti-damage,and non-contact sensing electronic skin implanted with MWCNT to block public pathogens contact infection

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Nano Research 2022年第3期15卷 2616-2625页

作者： Duan-Chao Wang Hou-Yong Yu Lurong Jiang Dongming Qi Xinxing Zhang Lumin Chen Wentao Lv Weiqiang Xu Kam Chiu Tam National Engineering Lab for Textile Fiber Materials&Processing Technology College of Textile Science and EngineeringZhejiang Sci-Tech UniversityHangzhou 310018China College of Information Science and Technology Zhejiang Sci-Tech UniversityHangzhou 310018China State Key Laboratory of Polymer Materials Engineering Polymer Research Institute of Sichuan University Chengdu 610065China Department of Chemical Engineering Waterloo Institute for NanotechnologyUniversity of Waterloo200 University Avenue WestWaterlooOntario N2L 3G1Canada

If a person comes into contact with pathogens on public facilities,there is a threat of contact(skin/wound)*** urgently,there are also reports about COVID-19 coronavirus contact infection,which once again reminds that contact infection is a very easily overlooked disease exposure ***,we propose an innovative implantation strategy to fabricate a multi-walled carbon nanotube/polyvinyl alcohol(MWCNT/PVA,MCP)interpenetrating interface to achieve flexibility,anti-damage,and non-contact sensing electronic skin(E-skin).Interestingly,the MCP E-skin had a fascinating non-contact sensing function,which can respond to the finger approaching 0−20 mm through the spatial weak *** non-contact sensing can be applied urgently to human–machine interactions in public facilities to block *** scratches of the fruit knife did not damage the MCP E-skin,and can resist chemical corrosion after hydrophobic *** addition,the MCP E-skin was developed to real-time monitor the respiratory and cough for exercise detection and disease ***,the MCP E-skin has great potential for emergency applications in times of infectious disease pandemics.

关键词： prevent contact infection anti-damage sensors non-contact sensing respiratory sensing human–machine interaction

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Advanced Flexible Carbon‑Based Current Collector for Zinc Storage

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Advanced fiber Materials 2022年第6期4卷 1500-1510页

作者： Hao Jia Minghui Qiu Chunxia Tang Hongqi Liu Jinlin Xu Benjamin Tawiah Shou‑xiang Jiang Xiangwu Zhang Key Laboratory of Eco‑Textiles Ministry of EducationJiangnan UniversityWuxiJiangsuPeople’s Republic of China Institute of Textiles and Clothing The Hong Kong Polytechnic UniversityHong KongPeople’s Republic of China Department of Industrial Art(Textiles) Kwame Nkrumah University of Science and TechnologyKumasiGhana Fiber and Polymer Science Program Department of Textile EngineeringChemistry and ScienceWilson College of TextilesNorth Carolina State UniversityRaleighNC 27695‑8301USA

Carbon cloth(CC)-based electrodes have attracted extensive attention for next-generation wearable energy-storage devices due to their excellent electrical conductivity and mechanical ***,the application of conventional CC-based electrodes for zinc(Zn)storage severely hinders Zn ion transport and induces deleterious Zn dendrite growth,resulting in poor electrochemical ***,a novel oxygen plasma-treated carbon cloth(OPCC)is rationally designed as a current collector for flexible hybrid Zn ion supercapacitors(ZISs).The modified interface of OPCC with abundant oxygenated groups enables enhanced electrolyte wettability and uniform superficial electric field distribution.A prolonged working lifespan for Zn electrodeposition is achieved by the OPCC due to the improved interfacial kinetics and homogenized ion *** as-prepared hybrid ZIS also delivers excellent cycling endurance(98.5%capacity retention for 1500 cycles)with outstanding operation stability under various extreme *** facile surface modification strategy provides a new way for developing future flexible electrodes for wearable electronic products.

关键词： Zinc ion supercapacitor Carbon cloth Oxygen plasma treatment Interface kinetics

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A Review on Digital Simulation Strategies and Its Applications for Advanced Compression Garments

A Review on Digital Simulation Strategies and Its Applicatio...

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作者： Seonyoung Youn Ryan Darden Kavita Mathur Fiber and Polymer Science Ph.D.program North Carolina State University Department of Textile Engineering Chemistry and Sciences M.S.Textile Engineering program North Carolina State University Department of Textile and Apparel Technology and Management North Carolina State University

This paper presents a comprehensive review on the current state of digital simulation technology and its strategic application usages with a key focus on advanced compression garments. Although three-dimensional(3D) digital garment simulators have significantly impacted the apparel and textile industry, their use has been limited to visual prototyping, quality checking, or marketing. The physical properties of garment simulators have been overlooked in advanced functional manufacturing. This literature review investigates the possibility of strategically utilizing virtual physical properties to enhance garment functions, specifically in wearables and medical-grade compression fields. The first phase of this paper gives an overview of the current state of 3D garment simulation tools and their measurement features. This is followed by a gap analysis between simulated and physical property evaluations, focusing on minimizing the gaps. The literature is thoroughly examined to identify appropriate studies that uses digital tools for compressional garments and add value to wearables and healthcare applications. This paper provides valuable insights for apparel and textile engineers, enabling them to better understand the limitations and capabilities of garment simulators in improving advanced features for specific end users.

关键词： 3D Digital Garment Simulator Advanced Compression Garment Digital Strategy Medical-grade Compression Simulated Physical Property Virtual Evaluation

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A Braided Flexible Zn-MnO2 Yarn Battery Based on Cobweb-Like Carbonized Polypyrrole Modified Carbon fiber Electrodes

SSRN

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SSRN 2023年

作者： Chen, Lei Hu, Kairui Yang, Ke Yanilmaz, Meltem Han, Xu Liu, Yong Zhang, Xiangwu School of Textile Science and Engineering Tiangong University Tianjin300387 China Department of Textile Engineering Istanbul Technical University Istanbul Turkey Fiber and Polymer Science Program Department of Textile Engineering Chemistry and Science Wilson College of Textiles North Carolina State University RaleighNC27695 United States

Flexible zinc ion batteries (ZIBs) are promising candidate for energy storage devices because of high safety and low cost. Carbon fiber (CF) is an ideal current collector for ZIBs due to its good flexibility, electrical conductivity and corrosion resistance. Herein, a novel CF-based current collector is proposed. At first, the inertness and non-polarity of CF were significantly modified by activating and etching to obtain a multi-layered pore structure. After then, carbonized polypyrrole (CPPy) nanowire conductive networks were built up on etched carbon fiber (ECF) by electrochemical in-situ growing and carbonization. Based on the CPPy network, MnO2 nanoflowers were grown firmly by the hydrothermal method to construct a multilayer MnO2@CPPy@ECF composite electrode. The multi-layered three-dimensional CPPy conductive network is rooted in the interior of MnO2, providing a dedicated transmission path for both electrons and ions during electrochemical redox reactions. The MnO2@CPPy@ECF electrode had an initial capacity of 346.1 mAh·g-1 at 0.1 A·g-1 and 252.8 mAh·g-1 after 800 cycles. In addition, the integrated flexible Zn-MnO2 2D fabric battery with MnO2@CPPy@ECF fabric cathode shows a specific capacity of 254.7 mAh·g-1 at 0.1 A · g-1. Finally, a flexible Zn-MnO2 yarn battery with unique structural advantages of high flexibility, shape adaptability, structural integrity and good mechanical stability was fabricated by the 2D braid method. The initial specific capacity of the flexible Zn-MnO2 yarn battery is 111.7 mAh·g-1 at 0.1C, and the coulomb efficiency reaches more than 98%. This work opens up a new pathway for the rational design of flexible electrodes for wearable ZIBs. © 2023, The Authors. All rights reserved.

关键词： Yarn

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Elastomer-Based Soft Syntactic Foam with Broadly Tunable Mechanical Properties and Shapability

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SSRN 2024年

作者： Ghosh, Tushar K. Pragya, Akanksha Young, Natalie Department of Textile Engineering Chemistry and Science Wilson College of Textiles North Carolina State University RaleighNC27606 United States Fiber and Polymer Science Program Wilson College of Textiles North Carolina State University RaleighNC27695 United States

Fabrication of lightweight composites using thermally responsive expandable microspheres (EM) embedded in an elastomeric matrix to form syntactic foams offers significant opportunities to create functional and structural composites for diverse applications. The morphology of the EM-elastomer composite on the micro- and macro-scales is significantly influenced by the fabrication sequence and parameters (composition, expansion time/temperature, etc.). Herein, we report the morphological evolution of an EM-elastomer composite through the fabrication processes and elucidate the interaction of relevant fabrication parameters. Unlike the majority of published reports on hard EM composites, the in-situ expansion of the closed-cell foam structure within a soft matrix leads to larger void sizes, and the concomitant expansive force of the EM impacts the polymer chain mobility within the soft composite. At the same time, higher EM loading improves the mechanical properties;the evolved microstructure leads to a lightweight but stiff structure. For the first time, the report details the thermal expansion of EM under applied pretension, which leads to irreversible prestrain-dependent morphological changes toward anisotropic mechanical properties. Additionally, the composites are shaped under constrained expansion. The study provides a comprehensive guide and expands the pathways for the practical application of EM-embedded soft syntactic foams in aerospace, electronics, wearables, robotics, etc. © 2024, The Authors. All rights reserved.

关键词： Elastomers

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Graphene-functionalized textile composites for wearable Joule heating applications

Advanced Nanocomposites

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Advanced Nanocomposites 2025年 2卷 108-123页

作者： Omar Faruk Abbas Ahmed Ashfaqul Hoque Khadem Lu Jia Luyi Sun Department of Materials Science and Engineering Binghamton University State University of New York at Binghamton NY 13902 USA Polymer Program Institute of Materials Science and Department of Chemical & Biomolecular Engineering University of Connecticut Storrs CT 06269 USA Department Mechanical Engineering College of Engineering Computing and Applied Science Clemson University Clemson SC 29634 USA College of Textile Engineering Taiyuan University of Technology Jinzhong Shanxi 030600 China

Thermal comfort is essential for maintaining physiological well-being, with textile materials traditionally serving as the primary medium for regulating heat exchange between the body and its environment. However, conventional textiles often fall short of maintaining optimal thermal balance. So, there is an increasing demand for advanced thermoregulation systems that can effectively reduce heat loss and enhance warmth, ensuring consistent comfort. Recent research has highlighted the promise of advanced functional materials, especially graphene and its composites, for modifying textiles to improve thermal properties. This article comprehensively reviews recent advancements in graphene-functionalized textile composites, focusing on their applications in wearable Joule heaters designed for personalized thermal comfort or thermal therapy. Various graphene-functionalized textile composites are reviewed from the perspectives of material properties, processing strategies and device fabrication methods. Key challenges and future opportunities are summarized for graphene-functionalized textile-based Joule heaters as innovative solutions in wearable thermal regulation.

关键词： Graphene textile Composite Wearable electronics Joule heater

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Electrospinning of Neat Graphene Nanofbers

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Advanced fiber Materials 2022年第2期4卷 268-279页

作者： Zhanpo Han Jiaqing Wang Senping Liu Qinghua Zhang Yingjun Liu Yeqiang Tan Shiyu Luo Fan Guo Jingyu Ma Peng Li Xin Ming Chao Gao Zhen Xu MOE Key Laboratory of Macromolecular Synthesis and Functionalization Department of Polymer Science and EngineeringKey Laboratory of Adsorption and Separation Materials and Technologies of Zhejiang ProvinceZhejiang University38 Zheda RoadHangzhou 310027People’s Republic of China State Key Laboratory for Modifcation of Chemical Fibers and Polymer Materials Donghua UniversityShanghai 200051People’s Republic of China State Key Laboratory of Bio-Fibers and Eco-Textiles Collaborative Innovation Center of Marine Biobased Fiber and Ecological Textile TechnologySchool of Materials Science and EngineeringQingdao UniversityQingdao 266071People’s Republic of China

Macroscopic assembly of graphene sheets has renovated the preparation of neat carbonaceous fbers with integrating high performance and superior functionalities,beyond the pyrolysis of conventional polymeric *** date,graphene microfbers by the liquid crystalline wet-spinning method have been ***,how to reliably prepare continuous neat graphene nanofbers remains ***,we present the electrospinning of neat graphene nanofbers enabled by modulating colossally extensional fow state of graphene oxide liquid *** use polymer with mega molecular weight as transient additives to realize the colossal extensional fow and *** neat graphene nanofbers feature high electronic quality and crystallinity and exhibit high electrical conductivity of 2.02×10^(6) S/m that is to be comparable with single crystal graphite *** electrospinning of graphene nanofbers was extended to prepare large-area fabric with high fexibility and superior specifc electrical/thermal *** electrospinning of graphene nanofbers opens the door to nanofbers of rich two-dimensional sheets and the neat graphene nanofbers may grow to be a new species after conventional carbonaceous nanofbers and whiskers in broad functional applications.

关键词： Electrospinning Graphene nanofber Functional fabrics

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Inclusive Design of Advanced Wearable Health Monitoring Systems: Validating a Contact Pressure Prediction Model with a Sports Bra

SSRN

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SSRN 2024年

作者： Youn, Seonyoung Mathur, Kavita Mills, Amanda C. Fiber and Polymer Science Ph.D. candidate North Carolina State University RaleighNC27606 United States Department of Textile and Apparel Technology and Management North Carolina State University RaleighNC27606 United States Department of Textile Engineering Chemistry and Science North Carolina State University RaleighNC27606 United States

The integration of wearable biosignal monitoring systems into daily healthcare has marked a significant advancement in medical care. Yet, the design of these devices often neglects the anatomical specificity of individual bodies, compromising both functionality and comfort. This oversight is particularly pronounced in research on the effective placement of 3-lead electrodes, selecting suitable materials, and customizing fit for women's diverse body shapes. To address this gap, this research introduces a novel design methodology for the development of advanced wearable health-monitoring garments, focusing on smart sports bras as a case study. This approach emphasizes contact pressure (CP) optimization for electrode placement, material selection, and sizing to enhance biosignal acquisition and comfort for the wearer. The study identifies optimal horizontal 3-lead electrode placements and configurations, the most effective across three female participants with diverse body mass indices (BMIs). Furthermore, the research employs a simulation-based contact pressure model (CP model) to precisely engineer desired pressure levels through strategic material selection and sizing adjustments. Guided by the CP model, screen-printed silver/silver chloride electrodes are incorporated into single jersey knit fabric, adjusted by a 20% pattern size reduction for a tailored electrocardiogram (ECG) chest band in the optimized configuration. This achieves a signal-to-noise ratio of 40.9, closely comparable to the 41.9 ratio obtained with traditional wet electrodes, while also exhibiting a higher QRS amplitude above 0.84mV, benchmarked against 12-lead electrodes for reliability. The study further identifies an optimal contact pressure range of 0.56-1.24 kPa for ECG chest bands and a subjective pressure tolerance range of 0.93 to 1.8 kPa in the chest area across female subjects. Finally, the smart sports bra integration demonstrates clear QRS complexes and high biopotential amplitude, whi

关键词： Electrocardiograms

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