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Evaluation of Solubilization Time in Uncontrolled Atmosphere on Grain Growth, Phase Transformation Temperatures, and Mechanical Properties in a CuAlBe SMA

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Metallurgical and materials Transactions A: Physical Metallurgy and materials science 2025年

作者： da Silva Franco, Luiz Henrique Caluête, Rafael Evaristo de Lima, Bruno Alessandro Silva Guedes de Oliveira, Danniel Ferreira Brito, Ieverton Caiandre Andrade Department of Materials Engineering Federal University of Paraíba PB João Pessoa58051-900 Brazil Department of Mechanical Engineering Federal University of Paraíba PB João Pessoa58051-900 Brazil Graduate Program in Materials Science and Engineering Federal University of Paraíba PB João Pessoa58051-900 Brazil

Thermomechanical properties of SMAs are strongly affected by the metallurgical conditions imposed during their production. In this work, experiments were performed to investigate the behavior of the Cu–11.8Al–0.50Be (wt pct) SMA during solubilization at different times under an uncontrolled atmosphere. The results presented serve as a basis for predicting the macrostructure and thermomechanical properties in practical applications using CuAlBe SMAs. The grain growth evaluated by OM proved to be extremely sensitive to treatment time even after short intervals, tending to stabilize after 12 hours. Chemical analysis by EDS indicated a small variation in Al content produced during solidification, with 3 hours being enough to homogenize the Al concentration throughout the ingot despite producing a microstructure with non-uniform grain size. This variation in Al is not significant enough to influence the phase transformation temperatures, with the changes attributed to the grain growth and loss of Be by oxidation. ¼ hour resulted in the lowest values for maximum stress/strain, while 24 hours of solubilization showed the highest values of strain with small dispersion. The mixed fracture type (brittle/ductile) observed by SEM in the ¼ hour samples supports the hypothesis that ¼ hour is insufficient to dissolve the phases formed during solidification. This effect is aggravated by the strong elastic anisotropy, which contributes to embrittlement during quenching. © The Minerals, Metals & materials Society and ASM International 2025.

关键词： Setting

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Thermodynamic and Environmental Assessment of Low-GWP Alternative Refrigerants for Domestic Cooling

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Journal of The Institution of Engineers (India): Series C 2023年第2期104卷 377-383页

作者： Islam, Md. Amirul Rupam, Tahmid Hasan Hosan, Shahadat Saha, Bidyut Baran Institute for Materials Chemistry and Engineering Kyushu University Kasuga-Koen 6-1 Kasuga-Shi Fukuoka816-8580 Japan Department of Electrical and Electronics Engineering Bangabandhu Sheikh Mujibur Rahman Science and Technology University Gopalganj8100 Bangladesh Kyushu University 744 Motooka Nishi-Ku Fukuoka819-0395 Japan Kyushu University Program for Leading Graduate School Green Asia Education Center Kyushu University Fukuoka Japan Department of Mechanical Engineering Kyushu University 744 Motooka Nishi-Ku Fukuoka819-0395 Japan

Nearly two billion air-conditioning (AC) units are currently being used for space cooling worldwide. The majority of these ACs use R134a as the working fluid, a greenhouse gas (GHG) with a global warming potential (GWP) of 1300 kg-CO2-eq. According to the rules set by the world environment safety organizations, the GWP of domestic air-conditioning systems must not exceed 750 kg-CO2-eq. Hence, the R134a must be phased out by 2025, and an alternative refrigerant with similar thermodynamic properties yet low GWP is required. Therefore, the authors have investigated several potential binary/ternary refrigerant blends in this study. Among the studied refrigerants, R445A, R30A, and NPB2 (newly proposed blend: 8% R152a + 92% R1234yf) can reduce 90–99% global warming impact (more than 200 million tonnes of CO2 emission equivalent) caused by the domestic air-conditioning systems every year. © 2023, The Institution of Engineers (India).

关键词： Refrigerants

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Multi-objective parametrization of interatomic potentials for large deformation pathways and fracture of two-dimensional materials

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npj Computational materials 2021年第1期7卷 1042-1052页

作者： Xu Zhang Hoang Nguyen Jeffrey T.Paci Subramanian K.R.S.Sankaranarayanan Jose L.Mendoza-Cortes Horacio D.Espinosa Theoretical and Applied Mechanics Program Northwestern UniversityEvanstonILUSA Department of Chemistry University of VictoriaVictoriaBCCanada Center for Nanoscale Materials Argonne National LaboratoryLemontILUSA Department of Chemical Engineering&Materials Science Michigan State UniversityEast LansingMIUSA Department of Mechanical Engineering Northwestern UniversityEvanstonILUSA

This investigation presents a generally applicable framework for parameterizing interatomic potentials to accurately capture large deformation *** incorporates a multi-objective genetic algorithm,training and screening property sets,and correlation and principal component *** framework enables iterative definition of properties in the training and screening sets,guided by correlation relationships between properties,aiming to achieve optimal parametrizations for properties of ***,the performance of increasingly complex potentials,Buckingham,Stillinger-Weber,Tersoff,and modified reactive empirical bond-order potentials are *** MoSe_(2)as a case study,we demonstrate good reproducibility of training/screening properties and superior *** MoSe_(2),the best performance is achieved using the Tersoff potential,which is ascribed to its apparent higher flexibility embedded in its functional *** results should facilitate the selection and parametrization of interatomic potentials for exploring mechanical and phononic properties of a large library of two-dimensional and bulk materials.

关键词： materials apparent enable

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Adult dental epithelial stem cell-derived organoids deposit hydroxylapatite biomineral

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International Journal of Oral science 2023年第4期15卷 676-690页

作者： Hyun-Yi Kim Victoria Cooley Eun-Jung Kim Shujin Li Jong-Min Lee Dina Sheyfer Wenjun Liu Ophir D.Klein Derk Joester Han-Sung Jung NGeneS Inc. Ansan-siGyeonggi-doKorea Department of Materials Science and Engineering Northwestern UniversityEvanstonILUSA X-ray Science Division Advanced Photon SourceArgonne National LaboratoryLemontILUSA Division in Anatomy and Developmental Biology Department of Oral BiologyOral Science Research CenterBK21 FOUR ProjectYonsei University College of DentistrySeoulKorea Department of Orofacial Sciences and Program in Craniofacial Biology University of CaliforniaSan FranciscoCAUSA Department of Pediatrics Cedars-Sinai Guerin Children’sLos AngelesCAUSA

Ameloblasts are specialized cells derived from the dental epithelium that produce enamel,a hierarchically structured tissue comprised of highly elongated hydroxylapatite(OHAp)*** unique function of the epithelial cells synthesizing crystallites and assembling them in a mechanically robust structure is not fully elucidated yet,partly due to limitations with in vitro experimental ***,we demonstrate the ability to generate mineralizing dental epithelial organoids(DEOs)from adult dental epithelial stem cells(aDESCs)isolated from mouse incisor *** expressed ameloblast markers,could be maintained for more than five months(11 passages)in vitro in media containing modulators of Wnt,Egf,Bmp,Fgf and Notch signaling pathways,and were amenable to *** transplanted underneath murine kidney capsules,organoids produced OHAp crystallites similar in composition,size,and shape to mineralized dental tissues,including some enamel-like elongated *** are thus a powerful in vitro model to study mineralization process by dental epithelium,which can pave the way to understanding amelogenesis and developing regenerative therapy of enamel.

关键词： epithelium maintained specialized

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Z-Laminating Assembly of Graphene Nanoflakes for Super-Strong Membranes and Functional Coatings

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ACS Applied Nano materials 2024年第13期7卷 14957-14963页

作者： Santos, Ian Daniell Tjarks, Patrick Muthu, Jeyavelan Lin, You-Chen Yen, Zhi-Long Chand, Pradyumna Kumar Raman, Radha Nguyen, Dinh Tuan Rouhani, Mehdi Jeng, Yeau-Ren Hsieh, Ya-Ping Hofmann, Mario Department of Physics National Taiwan University Taipei 106 Taiwan Nano Science and Technology Program Taiwan International Graduate Program Academia Sinica and National Taiwan University Taipei 106 Taiwan J. Heyrovsky Institute of Physical Chemistry of the Czech Academy of Sciences Prague 18200 Czech Republic Institute of Atomic and Molecular Sciences Academia Sinica Taipei 106 Taiwan Department of Chemistry National Taiwan University Taipei 106 Taiwan Department of Physics National Central University Taoyuan 320 Taiwan Molecular Science and Technology Program Taiwan International Graduate Program Academia Sinica and National Central University Taipei 106 Taiwan Department of Biomedical Engineering National Cheng Kung University 1 University Road Tainan 70101 Taiwan Department of Materials Science and Engineering National Cheng Kung University Tainan 70101 Taiwan Academy of Innovative Semiconductor and Sustainable Manufacturing National Cheng-Kung University (NCKU) Tainan 70101 Taiwan

We demonstrate the strengthening of graphene, an atomically thin carbon allotrope, by out-of-plane folding. Through lateral confinement of graphene at the water-air interface, nanoscale buckling was induced in suspended flakes, leading to an unexpected folding transition beyond a critical surface pressure. The emergence of folding was confirmed by in situ Brewster angle reflectivity and ex situ microscopy, showing a unique “z-laminated” nanostructure. Molecular dynamics simulations indicate that z-lamination yields an enhanced adhesion between neighboring flakes compared to lateral sliding, which was confirmed by a surface pressure hysteresis during the folding process. Mechanical testing reveals superior Young’s modulus and yield strength when compared to conventional graphene assemblies and even compared to composites. We demonstrate the potential of the z-lamination approach for applications in graphene-based structural materials, tribological layers, and functional electrochemical coatings. Finally, the complete recyclability of z-laminated graphene opens up new routes toward sustainable nanostructured materials. © 2024 The Authors. Published by American Chemical Society

关键词： 2D materials composites laminated graphene membranes recyclable

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Quantifying Electrochemical Processes in Batteries and Beyond

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Energy & Environmental materials 2022年第4期5卷 1001-1004页

作者： Emma N.Antonio Michael F.Toney Materials Science and Engineering Program University of Colorado BoulderBoulderColorado 80309USA Joint Center for Energy Storage Research(JCESR) University of Colorado BoulderBoulderColorado 80309USA Department of Chemical and Biological Engineering University of Colorado BoulderBoulderColorado 80309USA Renewable and Sustainable Energy Institute University of Colorado BoulderBoulderColorado 80309USA

The correlation of electrochemical measurements with materials characterization has advanced our understanding of operation and degradation mechanisms in electrochemical energy storage and many other ***,often these correlations are qualitative,preventing the unambiguous identification of both operational principles and the root causes of performance *** we suggest quantitative approaches to define competing mechanisms and determine their relative *** illustrate the importance of quantitative methodologies over a range of electrochemical systems and highlight the need to consider the effect of the experimental design and measurement *** approaches will reveal the most detrimental degradation mechanisms and enable the development of strategies to suppress,stabilize or eliminate them,leading to materials and devices with longer lifetimes,reduced environmental impact,and improved performance.

关键词： electrochemistry in situ and operando characterization batteries quantification materials science

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Pulsing-Induced Healing of a Surface Crack of a Nickel-Based Alloy

SSRN

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SSRN 2024年

作者： Wang, Qian Quan, Mingming Tan, Zhen Liu, Ming Wang, Dianlong Yang, Xiao Liu, Ying Mao, Yaning Liang, Zhimin Yang, Fuqian Wang, Liwei School of Material Science and Engineering Hebei University of Science and Technology Shijiazhuang050018 China Hebei Key Laboratory of Material Near-Net Forming Technology Shijiazhuang050018 China School of Mechanical Engineering and Automation Fuzhou University Fuzhou350108 China HBIS Group Materials Institute HBIS Group Hebei Shijiazhuang050023 China Materials Program Department of Chemical and Materials Engineering University of Kentucky LexingtonKY40506 United States School of Material Science and Engineering Australia

In this work, we demonstrate the feasibility of applying electric pulses to heal surface cracks on Ni-based GH4169 alloy under compressive load. There exists an incubation time for the onset of the healing of a crack, which is associated with local temperature at the crack tip. The crack size decreases with increasing the pulsing time at a constant healing rate prior to complete healing of the crack. Increasing compressive load accelerates the healing process. The electric pulsing leads to the formation of an influential zone surrounding the crack with the finest grain sizes in the healed crack and the coarsest grain sizes away from the influential zone. The indentation hardness increases with the increase the distance to the crack tip of the healed crack. A model of viscous flow in the crack channel is proposed for the crack healing. The resultant force on the crack faces due to the crack healing increases with the increase of the healing time and the decrease of the crack width. © 2024, The Authors. All rights reserved.

关键词： Crack tips

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Ultrafast Treatment of Stainless Steel for Efficient and Stable Water Electrolysis

SSRN

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SSRN 2023年

作者： Ning, Minghui Wang, Yu Song, Shaowei Yang, Lun Ren, Zhifeng University of Houston HoustonTX77204 United States Materials Science and Engineering Program and TcSUH University of Houston HoustonTX77204 United States School of Materials Science and Engineering Hubei Normal University Hubei Huangshi435002 China

Stainless steel is widely utilized in industrial applications of alkaline water electrolysis due to its high anti-corrosion property, but it usually suffers from low catalytic activity. The complete activation of stainless steel to improve its efficiency while maintaining its excellent corrosion resistance is thus important for lowering the energy consumption of H2 production. Here, we developed an ultrafast one-step activation for stainless steel based on high-temperature heat treatment and quenching in an aqueous solution. After the activation, the resulting Ni-doped stainless-steel mat (Ni-SSM) exhibited significantly improved activity for both the hydrogen evolution reaction and the oxygen evolution reaction in comparison to pristine SSM. When assembled for overall water electrolysis, Ni-SSM delivered a current density of 100 mA/cm2 at a cell voltage of 1.72 V in 1 M KOH at 25 ℃, outperforming most of the stainless-steel-based electrodes reported thus far. Under a quasi-industrial environment of 6 M KOH at 60 ℃, Ni-SSM displayed extraordinary performance, producing a current density of 500 mA/cm2 at a low cell voltage of 1.615 V. Further durability testing showed that Ni-SSM maintains high performance at a current density of 500 mA/cm2 under this quasi-industrial environment for at least 150 h. Similar activation processes were applied to different substrates to verify the versatility of this strategy, and enhanced performance for alkaline water electrolysis was observed among all the selected substrates. Finally, 5×5 cm2 pieces of Ni-SSM were prepared and assembled in an anion exchange membrane (AEM) electrolyzer, in which they delivered a current of 12.5 A at a cell voltage of 1.93 V in 1 M KOH at 65 ℃. Therefore, the effectiveness of this activation strategy for improving activity and its feasibility and versatility together suggest its great potential for industrial application. © 2023, The Authors. All rights reserved.

关键词： Stainless steel

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Effective monitoring of environmental hazardous drug moxifloxacin hydrochloride using silver selenide on octadecyl amine modified reduced graphene oxide composite

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Journal of Environmental Chemical engineering 2024年第1期12卷

作者： Hwa, Kuo-Yuan Ganguly, Anindita Graduate Institute of Organic and Polymeric Materials National Taipei University of Technology Taipei China Department of Molecular Science and Engineering National Taipei University of Technology Taipei China International Graduate Program in Energy and Optoelectronic Materials National Taipei University of Technology China

The precise detection of antibiotics is very critical. Here, silver selenide (Ag2Se) nanorods are hydrothermally synthesized and ultrasonically treated with rGO surface modified with octadecylamine (rGO-ODA). The optical, structural, morphological, and functional analysis were performed which revealed the orthorhombic pattern of the P2221 E space group, the crystalline purity of Ag2Se, and the substantial composite formation. The morphological studies revealed nanorod like structure of the Ag2Se material and wrinkled sheets of rGO-ODA. A sensor that detects moxifloxacin hydrochloride (MOXH) antibiotic using the cyclic voltammetry (CV), differential pulse voltammetry (DPV) and UV-Vis absorbance was developed. For DPV analysis, a quite low value for detection limit 12.46 nM was exhibited with 0.199 μM – 425.16 μM linear range, and a sensitivity of 5.0439 μA M−1cm−2. For UV-Vis, the sensor demonstrated a very low limit of detection 17.42 nM over 0.12 μM – 7.7 μM working range. The use of this sensor was validated in real-time analysis with industrial waste water, fish, human blood, and urine samples. The results suggested an excellent rate of analyte recovery and enhanced efficiency for MOXH detection with a potential for commercialization in the future. © 2023

关键词： Nanorods

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Multi-Component Lubricant Additives Derived from Pickering Emulsion-Templated Ionic Liquid Microcapsules

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Journal of Molecular Liquids 2025年 422卷

作者： Yan, Jieming Lak, Sarah N. Pentzer, Emily B. Mangolini, Filippo Texas Materials Institute The University of Texas at Austin AustinTX78712 United States Materials Science and Engineering Program The University of Texas at Austin AustinTX78712 United States Department of Chemistry Texas A&M University College StationTX77843 United States Department of Materials Science and Engineering Texas A&M University College StationTX77843 United States Walker Department of Mechanical Engineering The University of Texas at Austin AustinTX78712 United States

Room-temperature ionic liquids (RTILs) have emerged as potential next-generation lubricants owing to their unique physico-chemical properties and promising lubricating behavior. However, their implementation in tribological applications has partly been hindered by their negligible solubility in hydrocarbon fluids. Here, encapsulated ionic liquids (ENILs) with a core of 1-hexyl-3-imidazolium bis(trifluoromethylsulfonyl)imide ([HMIM][TFSI]) and a composite shell of polyurea/graphene oxide were prepared via Pickering emulsion-templated interfacial polymerization using two approaches, namely an RTIL-in-water emulsion stabilized with graphene oxide (GO) nanosheets ([HMIM][TFSI]/GO) and an RTIL-in-oil emulsion-stabilized with octadecylamine-functionalized GO nanosheets ([HMIM][TFSI]/C18-GO). The synthesized ENILs were successfully dispersed in polyalphaolefin (PAO) synthetic oil and used as additives to lubricate 52100 steel-vs.-52100 steel sliding contacts. Tribological tests provided evidence that the addition of [HMIM][TFSI]/C18-GO and [HMIM][TFSI]/GO ENILs to PAO could reduce friction and wear owing to the release of the encapsulated [HMIM][TFSI] at the sliding interface after the mechanical breakage of the shell material at the contact inlet, but only if a significant fraction of the ENILs has a diameter smaller than 20 µm. Comparison of these results with the outcomes of sliding experiments performed with PAO containing ENIL obtained by mini-emulsion polymerization with poly(ethylene glycol dimethacrylate-co-buytl methacrylate) (poly(EGDM-c-BMA)) shells highlights the role of the shell material in reducing friction. These outcomes not only demonstrate that multiple parameters (i.e., size distribution, shell material) affect the tribological performance of ENILs, but also pave the way towards further systematic investigations for optimizing ENILs to be used as additives in oil formulations. © 2025 Elsevier B.V.

关键词： Emulsification

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