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Extraordinary Ultrahigh-Capacity and Long Cycle Life Lithium-Ion Batteries Enabled by Graphitic Carbon Nitride-Perylene Polyimide Composites

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Energy & Environmental Materials 2023年第6期6卷 199-226页

作者： Michael Ruby Raj Jungwon Yun Dong-kyu Son Gibaek Lee Advanced Energy Materials Design Lab School of Chemical EngineeringYeungnam University38541Gyeongsan-siKorea William G.Lowrie Chemical and Biomolecular Engineering The Ohio State UniversityColumbus OH 43210USA

Graphitic carbon nitride(g-C_(3)N_(4))is widely used in organic metal-ion batteries owing to its high porosity,facile synthesis,stability,and high-rate ***,pristine g-C_(3)N_(4)nanosheets exhibit poor electrical conductivity,irreversible metal-ion storage capacity,and short-term cycling owing to their high concentration of graphitic-N ***,a series of 3,4:9,10-perylenetetracarboxylic diimide-coupled g-C_(3)N_(4)composite anode materials,CN-PI_(x)(x=0.2,0.5,0.75,and 1),was investigated,which exhibited an unusually high surface nitrogen content(23.19-39.92 at.%)and the highest pyridinic-N,pyrrolic-N,and graphitic-N contents reported to *** CN-PI_(1)anode delivers an unprecedented and continuously increasing ultrahigh discharging capacity of exceeding 8400 mAh g^(-1)(1.96 mWh cm^(-2))at 100 mA g^(-1)with high specific energy density(E_(sp))of~7700 Wh kg^(-1)and the volumetric energy density(E_(v))of~14956 Wh L-1 and an excellent long-term stability(414 mAh g^(-1)or 0.579 mWh cm^(-2)at 1 A g^(-1)).Furthermore,the activation of the CN-PI_(x)electrodes contributes to their superior electrochemical performance,resulting from the fact that the Li+is not only stored in the CN-PI_(x)composites but also CN-PI_(x)activated the Li^(0)adlayer on the CN-PI_(1)-Cu heterojunction as an SEI layer to avoid the direct contact of Li^(0)phase and the *** CN-PI_(1)full cell with LiCoO_(2)as the cathode delivers a discharge capacity of~587 mAh g^(-1)at a 1 A g^(-1)after 250 cycles with a Coulombic efficiency nearly 99%.This study provides a strategy to develop N-doped g-C_(3)N_(4)-based anode materials for realizing long-lasting energy storage devices.

关键词： graphitic carbon nitride lithium-ion batteries organic electrode perylene polyimide semiconductor-metal heterojunction

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An automated design pipeline for transparent facial orthoses: A clinical study

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Journal of Prosthetic Dentistry 2024年第5期131卷 970-979页

作者： Willis, Samuel Waheed, Usman Coward, Trevor Myant, Connor Research Assistant Advanced Manufacturing Lab Dyson School of Design Engineering Imperial College London London United Kingdom Postdoctoral Research Associate Advanced Manufacturing Lab Dyson School of Design Engineering Imperial College London London United Kingdom Professor Maxillofacial Prosthetic Rehabilitation Academic Centre of Reconstruction Kings College London London United Kingdom Senior Lecturer & Assistant Professor Advanced Manufacturing Lab Dyson School of Design Engineering Imperial College London London United Kingdom

Statement of problem: Transparent facial orthoses (TFOs) are commonly used for the treatment of craniomaxillofacial trauma and burns to prevent hypertrophic and keloid scarring. A TFO is typically customized to the patient's facial contours and relies on a precise fit to ensure good rehabilitative performance. A smart method of TFO design and manufacture is needed which does not require an experienced prosthetist, allowing for rapidly produced, well-fitting TFOs. Whether the rapid application reduces the final level of patient scarring is unclear. Purpose: The purpose of this clinical study was to determine whether a scalable, automated design-through-manufacture pipeline for patient specific TFO fabrication would be successful. Material and methods: The automated pipeline received a 3-dimensional (3D) facial scan captured from a depth sensitive mobile phone camera. The scan was cleaned, aligned, and fit to a template mesh, with a known connectivity. The resultant fitted scan was passed into an automated design pipeline, outputting a 3D printable model of a custom TFO. The TFOs were fabricated with 3D printing and were both physically and digitally evaluated to test the fidelity of a digital fit testing system. Results: A total of 10 individuals were scanned with 5 different scanning technologies (STs). All scans were passed through an automated fitting pipeline and categorized into 2 groups. Each ST was digitally fitted to a ground truth scan. In this manner, a Euclidean distance map was built to the actual facial geometry for each scan. Heatmaps of 3D Euclidean distances were made for all participant faces. Conclusions: The ability to automatically design and manufacture a custom fitted TFO using commercially available 3D scanning and 3D printing technology was successfully demonstrated. After considering equipment size and operational personnel requirements, vat polymerization (VP) technology was found to be the most promising route to TFO manufacture. © 2022 Edi

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An infrared photothermoelectric detector enabled by MXene and PEDOT:PSS composite for noncontact fingertip tracking

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Microsystems & Nanoengineering 2023年第1期9卷 229-239页

作者： Jiaqi Wang Zhemiao Xie Guanxuan Lu Jiayu Alexander Liu John T.W.Yeow Advanced Micro-/Nano-Devices Lab Department of Systems Design EngineeringUniversity of Waterloo200 University Ave WestWaterlooONN2L 3G1Canada

Photothermoelectric(PTE)detectors functioning on the infrared spectrum show much potential for use in many fields,such as energy harvesting,nondestructive monitoring,and imaging *** advances in low-dimensional and semiconductor materials research have facilitated new opportunities for PTE detectors to be applied in material and structural ***,these materials applied in PTE detectors face some challenges,such as unstable properties,high infrared reflection,and miniaturization ***,we report our fabrication of scalable bias-free PTE detectors based on Ti3C2 and poly(3,4-ethylenedioxythiophene):polystyrene sulfonate(PEDOT:PSS)composites and characterization of their composite morphology and broadband *** also discuss various PTE engineering strategies,including substrate choices,electrode types,deposition methods,and vacuum ***,we simulate metamaterials using different materials and hole sizes and fabricated a gold metamaterial with a bottom-up configuration by simultaneously combining MXene and polymer,which achieved an infrared photoresponse ***,we demonstrate a fingertip gesture response using the metamaterial-integrated PTE *** research proposes numerous implications of MXene and its related composites for wearable devices and Internet of Things(IoT)applications,such as the continuous biomedical tracking of human health conditions.

关键词： unstable composite sizes

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Vibration Isolator of Quasi-Zero Stiffness Metamaterials with High Load-Carrying Capacity and Self-Sensing 23

Vibration Isolator of Quasi-Zero Stiffness Metamaterials wit...

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23rd International Conference on Composite Materials, ICCM 2023

作者： Hong, H. Jeong, K.I. Kim, W.K. Raja, M.A. Kim, S.S. Korea Advanced Institute of Science and Technology Department of Mechanical Engineering Mechanical Design Lab Korea Republic of

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Nanodiamond/Ti_(3)C_(2) MXene-coated quartz crystal microbalance humidity sensor with high sensitivity and high quality factor

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Rare Metals 2024年第6期43卷 2719-2729页

作者： Yao Yao Qiao Chen Yan-Qi Li Xian-He Huang Wei-Wei Ling Zhe-MiaoXie Jia-QiWang Chang-Ming Chen College of Communication Engineering Chengdu University of Information TechnologyChengdu 610225China School of Automation Chongqing University of Posts and TelecommunicationsChongqing 400065China School of Automation Engineering University of Electronic Science and Technology of ChinaChengdu 611731China Advanced Micro-/Nano-Devices Lab Department of Systems Design EngineeringUniversity of WaterlooWaterlooON N2L 3GlCanada

To address the challenge of achieving both high sensitivity and a high quality factor in quartz crystal microbalance(QCM)humidity sensors,a nanodiamond(ND)/Ti_(3)C_(2)MXene composite-coated QCM humidity sensor was *** material characteristics of ND,Ti_(3)C_(2)MXene,and ND/Ti_(3)C_(2)MXene composite were analyzed by transmission electron microscopy(TEM)and Fourier transform infrared(FTIR)*** experimental results demonstrated that the hydrophilic ND nanoparticles coated on Ti_(3)C_(2) MXene nanosheet prevented the self-stacking of Ti_(3)C_(2)MXene and enhanced the sensitivity of Ti_(3)C_(2) MXene-based QCM humidity ***,the high mechanical modulus of Ti_(3)C_(2) MXene material helped ND/Ti_(3)C_(2)MXene composite-coated QCM humidity sensor to achieve a high quality factor(>20,000).ND/Ti_(3)C_(2)MXene compositecoated QCM humidity sensor exhibited a sensitivity of 82.45 Hz/%RH,a humidity hysteresis of 1.1%RH,fast response/recovery times,acceptable repeatability,and good stability from 11.3%RH to 97.3%*** response mechanism of ND/Ti_(3)C_(2) MXene composite-coated QCM humidity sensor was analyzed in combination with a bi-exponential kinetic adsorption ***,the potential application of ND/Ti_(3)C_(2)MXene composite-coated QCM humidity sensor was demonstrated through its frequency response to wooden blocks with different moisture contents.

关键词： Humidity sensor Quartz crystal microbalance Nanodiamond Ti_(3)C_(2)MXene High quality factor

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High‑Defect‑Density Graphite for Superior‑Performance Aluminum‑Ion Batteries with Ultra‑Fast Charging and Stable Long Life

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Nano-Micro Letters 2021年第11期13卷 168-189页

作者： Jisu Kim Michael Ruby Raj Gibaek Lee Advanced Energy Materials Design Lab School of Chemical EngineeringYeungnam UniversityGyeongsan 38541Republic of Korea

Rechargeable aluminum-ion batteries(AIBs)are a new generation of low-cost and large-scale electrical energy storage ***,AIBs suffer from a lack of reliable cathode materials with insufficient intercalation sites,poor ion-conducting channels,and poor diffusion dynamics of large chloroaluminate anions(AlCl4−and Al2Cl7−).To address these issues,surfacemodified graphitic carbon materials[i.e.,acidtreated expanded graphite(AEG)and base-etched graphite(BEG)]are developed as novel cathode materials for ultra-fast chargeable *** has more turbostratically ordered structure covered with abundant micro-to nano-sized pores on the surface structure and expanded interlayer distance(d002=0.3371 nm)realized by surface treatment of pristine graphite with acidic media,which can be accelerated the diffusion dynamics and efficient AlCl4−ions(de)-intercalation *** AIB system employing AEG exhibits a specific capacity of 88.6 mAh g^(−1)(4 A g^(−1))and~80 mAh g^(−1) at an ultra-high current rate of 10 A g^(−1)(~99.1%over 10,000 cycles).BEG treated with KOH solution possesses the turbostratically disordered structure with high density of defective sites and largely expanded d-spacing(d002=0.3384 nm)for attracting and uptaking more AlCl4−ions with relatively shorter penetration ***,the AIB system based on the BEG cathode delivers a high specific capacity of 110 mAh g^(−1)(4 A g^(−1))and~91 mAh g^(−1)(~99.9%over 10,000 cycles at 10 A g^(−1)).Moreover,the BEG cell has high energy and power densities of 247 Wh kg^(−1) and 44.5 kW kg^(−1).This performance is one of the best among the AIB graphitic carbon materials reported for chloroaluminate anions storage *** finding provides great significance for the further development of rechargeable AIBs with high energy,high power density,and exceptionally long life.

关键词： Surface modification Etched graphite Cathode materials Energy storage Aluminum-ion batteries

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Deformation Evolution and Perceptual Prediction for Additive Manufacturing of Lightweight Composite Driven by Hybrid Digital Twins

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Chinese Journal of Mechanical engineering 2024年第5期37卷 94-112页

作者： Jinghua Xu Linxuan Wang Mingyu Gao Chen Jia Qianyong Chen Kang Wang Shuyou Zhang Jianrong Tan Shaomei Fei State Key Lab of Fluid Power and Mechatronic Systems Zhejiang UniversityHangzhou 310058China Zhejiang Key Lab of Advanced Manufacturing Technology School of Mechanical EngineeringZhejiang UniversityHangzhou 310058China State Key Laboratory of Materials Processing and Die and Mould Technology Huazhong University of Science and TechnologyWuhan 430074China Institute of Design Engineering Zhejiang UniversityHangzhou 310058China School of Mechanical and Aerospace Engineering Nanyang Technological UniversitySingapore City 639798Singapore

This paper proposes a deformation evolution and perceptual prediction methodology for additive manufacturing of lightweight composite driven by hybrid digital twins(HDT).In order to improve manufacturing quality of irregular lightweight composite through boosting conceptual design in aeronautic and aerospace engineering,the HDT meaning hybridization of physical and digital domains,including deformation and energy efficiency can be built,where the essential parameters can be perceptually predicted in advance,by virtue of the fusion of physical sensors and digital *** long short term memory(LSTM)can be employed to void vanishing gradient problem and improve predicting precision via Recurrent Neural Networks,thereby laying a foundation for the *** diverse manufacturing requirements of different regions are integrated into the parameters designing phase by attaching region weights confirmed via empiricism and in-service *** effects of slicing strategy and external support structures on manufacturing quality are considered from the perspective of improving dimensional *** manufacturing efficiency and comprehensive costs are accounted as consideration factors,which are perceptually predicted via *** designed manufacturing parameters through HDT were virtually examined by evaluating the deformation and equivalent stress distributions of fabricated lightweight component with composite material through AM process *** physical experiments were conducted to verify the HDT-based pre-designing and optimization method of manufacturing parameters via fused deposition modeling(FDM).The energy consumption of actual manufacturing process was measured via digital power meter and applied to evaluate accuracy of perceptual prediction *** dimensional accuracy and distortion distribution of the manufactured lightweight prototype made with composite material were measured through the coordinate measuring machine(CMM)and 3D optica

关键词： Deformation evolution Perceptual prediction Lightweight composite Hybrid digital twins(HDT) Long short term memory(LSTM)

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Effect of ball milling time on the microstructure and compressive properties of the Fe–Mn–Al porous steel

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International Journal of Minerals,Metallurgy and Materials 2023年第5期30卷 917-929页

作者： Lingzhi Xie Zhigang Xu Yunzhe Qi Jinrong Liang Peng He Qiang Shen Chuanbin Wang Hubei Key Laboratory of Advanced Technology for Automotive Components Wuhan University of TechnologyWuhan 430070China School of Materials Science and Engineering Wuhan University of TechnologyWuhan 430070China State Key Lab of Advanced Technology for Materials Synthesis and Processing Wuhan University of TechnologyWuhan 430070China Wuhan Second Ship Design and Research Institute Wuhan 430205China

In the present work,Fe–Mn–Al–C powder mixtures were manufactured by elemental powders with different ball milling time,and the porous high-Mn and high-Al steel was fabricated by powder *** results indicated that the powder size significantly decreased,and the morphology of the Fe powder tended to be increasingly flat as the milling time ***,the prolonged milling duration had limited impact on the phase transition of the powder *** main phases of all the samples sintered at 640℃ were α-Fe,α-Mn and Al,and a small amount of Fe2Al5 and *** the sintering temperature increased to 1200℃,the phase composition was mainly comprised of γ-Fe and α-*** weight loss fraction of the sintered sample decreased with milling time,i.e.,8.3wt% after 20 h milling compared to15.3wt% for 10 *** Mn depletion region(MDR) for the 10,15,and 20 h milled samples was about 780,600,and 370 μm,*** total porosity of samples sintered at 640℃ decreased from ~46.6vol% for the 10 h milled powder to ~44.2vol% for 20 h milled *** sintering at 1200℃,the total porosity of sintered samples prepared by 10 and 20 h milled powder was ~58.3vol% and ~51.3vol%,*** compressive strength and ductility of the 1200℃ sintered porous steel increased as the milling time increased.

关键词： powder metallurgy porous steel ball milling time microstructure evolution compressive properties

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Predictive defect detection for prototype additive manufacturing based on multi-layer susceptibility discrimination

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Advances in Manufacturing 2023年第3期11卷 407-427页

作者： Jing-Hua Xu Lin-Xuan Wang Shu-You Zhang Jian-Rong Tan State Key Lab of Fluid Power and Mechatronic Systems Zhejiang UniversityHangzhou 310058People's Republic of China Zhejiang Key Lab of Advanced Manufacturing Technology Zhejiang UniversityHangzhou 310058People's Republic of China Engineering Research Centre for Design Engineering and Digital Twin of Zhejiang Province Hangzhou 310058People's Republic of China Zhejiang-Singapore Innovation and AI Joint Research Lab Hangzhou 310027People's Republic of China

This paper presents a predictive defect detection method for prototype additive manufacturing(AM)based on multilayer susceptibility discrimination(MSD).Most current methods are significantly limited by merely captured images,disregarding the differences between layer-by-layer manufacturing approaches,without combining transcendental *** visible parts,originating from the prototype of conceptual design,are determined based on spherical flipping and convex hull theory,on the basis of which theoretical template image(TTI)is rendered according to photorealistic *** addition,to jointly consider the differences in AM processes,the finite element method(FEM)of transient thermal-structure coupled analysis was conducted to probe susceptible regions where defects appeared with a higher *** by prior knowledge acquired from the FEM analysis,the MSD with an adaptive threshold,which discriminated the sensitivity and susceptibility of each layer,was implemented to determine *** anomalous regions were detected and refined by superimposing multiple-layer anomalous regions and comparing the structural features extracted using the Chan-Vese(CV)model.A physical experiment was performed via digital light processing(DLP)with photosensitive resin of a non-faceted scaled V-shaped engine block prototype with cylindrical holes using a non-contact *** MSD method is practical for detecting defects and is valuable for a deeper exploration of barely visible impact damage(BVID),thereby reducing the defect of prototypical mechanical parts in engineering machinery or process equipment via intellectualized machinevision.

关键词： Predictive defects detection Additive manufacturing(AM) Convex hull theory Finite element method(FEM) Multi-layer susceptibility discrimination(MSD)

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Synthesis of a novel Al foam with a periodic architecture by introducing hollow Al tubes and Al/Mg powders

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Journal of Materials Science & Technology 2023年第17期148卷 105-115页

作者： Zhigang Xu Dayong Shen Kai Wang Peng He Jian Zhang Hao Zhang Peng Cao Shangyu Huang Jian Peng Qiang Shen Chuanbin Wang Lianmeng Zhang Hubei Key Laboratory of Advanced Technology for Automotive Components Wuhan University of TechnologyWuhan 430070China State Key Lab of Advanced Technology for Materials Synthesis and Processing Wuhan University of TechnologyWuhan 430070China School of Materials Science and Engineering Wuhan University of TechnologyWuhan 430070China Wuhan Second Ship Design and Research Institute Wuhan 430205China Department of Chemical and Materials Engineering University of AucklandPrivate Bag 92019Auckland 1142New Zealand

In this work,we synthesized a brand-new Al foam with a periodic structure via a simple powder metallurgical *** periodic architecture consists of both hierarchical porous and bi-directional composition-graded *** results show that the hierarchical porous material includes large pores on millimeter scale inheriting from the hollow structure of the Al tubes,and small pores on mi-crometer scale produced by the sintering of Al/Mg *** bi-directional Mg concentration-graded structure is formed in the tube walls due to the condensation of Mg vapor in the inner tube *** addition of Mg powders achieves excellent metallurgical bonding between the Al powders and the hollow tubes at 550℃.The plateau stress and energy absorption capacity of the Al foam in y-axis compression are significantly higher than that in the x-axis due to their anisotropic *** general,the Al foam with Mg addition presents the most superior compression performance,and we believe that our find-ings could open up a unique strategy for developing high-performance metallic foams with the periodic architecture involving both hierarchical porous and bi-directional graded structure.

关键词： Al foam Hollow Al tube Mg evaporation Bi-directional composition-graded structure Compression properties Energy absorbing performance

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