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2023 China Semiconductor technology International Conference, CSTIC 2023

作者： Wei, Yanzhao Yao, Jiaxin Xu, Renren Zhang, Qingzhu Yin, Huaxiang Chinese Academy of Sciences Integrated Circuit Advanced Process R&d Center Institute of Microelectronics Beijing100029 China Institute of Microelectronics Chinese Academy of Sciences Key Laboratory of Microelectronic Devices and Integrated Technology Beijing100029 China University of Chinese Academy of Sciences School of Integrated Circuits Beijing100049 China

ISBN: (纸本)9798350311006

In this paper, a La2O3/HfO2 bi-layer dipole-first (DF) process is proposed and investigated by ultra-low temperature PVD dielectric laminates to achieve lower gate effective work function (EWF) for monolithic 3D-IC (M3D) application. The impacts of ultra-low temperature La-dipole on EWF modulation and interfacial properties are comprehensively investigated. It is found that the flat-band voltage (VFB) negatively shifts 60 mV with sub-1nm La2O3 thickness, which provides an effective way to meet the require of Si conduction band-edge EWF modulation. Furthermore, the electron trap/detrap densities (Not) and interfacial trap densities (Dit) are suppressed by La2O3/HfO2 bi-layer DF process to improve device performance. These results exhibit a promising bi-layer DF process in low thermal integration for advanced IC technology. © 2023 IEEE.

关键词： Timing circuits

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Significantly Reduce Emissions Using Ammonia Enriched Fuel Gas for Gas Turbines

Significantly Reduce Emissions Using Ammonia Enriched Fuel G...

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2024 SPE Europe Energy Conference and Exhibition, EURO 2024

作者： Téllez-Schmill, R. Owodunni, T. KBC Advanced Technologies KBC Process Technology

ISBN: (纸本)9781959025399

The urgent need to address environmental challenges has prompted refiners and petrochemical operators worldwide to find cleaner and more sustainable energy sources, particularly in their gas turbine equipment (GT). Carbon dioxide (CO2), the primary constituent of greenhouse gases, mainly originates from fossil fuel combustion (Ji et al. 2021). In response, many countries have implemented strict legislation, exemplified by the Paris (COP21) and Glasgow (COP26) Climate Agreements to reduce carbon emissions. Within this dynamic shift toward sustainable energy, gas turbines (GT) stand at the pinnacle of turbomachinery excellence for power generation. In fact, industry leaders tout them as being unparalleled in this field. GTs are set to maintain a pivotal role as energy conversion equipment, characterized by high thermal efficiency, further affirming their importance in the ever-changing realm of energy infrastructure. Natural gas, compared to liquid fuels, emerges as a key player in the pursuit of sustainable power solutions. It not only cuts CO2 emissions by 20% but also produces lower levels of NOx. As part of global decarbonization efforts, major gas turbine manufacturers such as Mitsubishi, GE, Siemens, and others are modifying their commercial GT models to burn natural gas with either hydrogen or ammonia. This strategic modification significantly decreases CO2 emissions. Depending on the turbine model, most GT manufacturers can achieve a hydrogen content of up to 100 vol% in the fuel gas for very specific models, as advertised on their websites (GE Vernova 2024;Mitsubishi Power 2021;Siemens Energy 2024). Copyright 2024, Society of Petroleum Engineers.

关键词： Carbon dioxide

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Properties Evaluation of Copper-Titanium Composites by a Spark Plasma Sintering process

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Funtai Oyobi Fummatsu Yakin/Journal of the Japan Society of Powder and Powder Metallurgy 2025年 72卷 S931-S937页

作者： Yang, Min-Hyeok Park, Bum-Soon Oh, Ik-Hyun Moon, Hyoung-Seok Park, Hyun-Kuk Purpose Built Mobility Group Korea Institute of Industrial Technology Gwangju61012 Korea Republic of Extreme Process Control Group Korea Institute of Industrial Technology Busan46938 Korea Republic of Division of Advanced Materials Engineering Chonnam National University Gwangju61186 Korea Republic of

The Copper (Cu) - Titanium (Ti) powders with varying of Ti content(0.3, 0.5, 1, 2, 4, 6, 8 wt.%) were mixed using a horizontal ball milling. The milling process was performed for 6 hrs at 300 rpm. The Cu-Ti composites were fabricated by a spark plasma sintering process at a sintering temperature of 850℃ and heating rate of 30 ℃/min under a pressure of 40 MPa. The relative density of the composites was all densified to more than 99%. The Cu and Ti in the Cu matrix are unstable to exist in a single phase at temperature range of 800-875°C and a Ti content of 4-8 at.% (3.04-6.15 wt.%). Thus, each element is stabilized by forming a secondary phase. The phase of Cu3Ti was detected upon the Ti content was 4 wt.% or higher, which affected the thermal properties. The thermal conductivity decreased from 262.74 to 46.10 W/m·K according to increase the Ti contents. The Ti present in the heat transfer path in Cu matrix acted as an obstacle to heat diffusion. Furthermore, as the Ti contents increased, the Vickers hardness of Cu-Ti composite increased from 60.19 to 205.20 kg/mm2. In contrast, the crystallite size decreased from 66.63 to 22.43 nm. The Ti particles suppressed the grain growth of the Cu matrix, resulting in a decrease in crystallite size, which contributed to the improvement of the mechanical properties. ©2025 Japan Society of Powder and Powder Metallurgy.

关键词： Thermal conductivity

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Construction of Ni single-atom coordinated with doped N and S elements for mild hydrogenation of methyl acrylate to methyl propionate

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Nano Research 2025年第1期18卷 217-224页

作者： Taolue Sun Chen Jian Gang Wang Hui Zhao Guoliang Zhang Zengxi Li Chunshan Li State Key Laboratory of Mesoscience and Engineering CAS Key Laboratory of Green Process and EngineeringBeijing Key Laboratory of Ionic Liquids Clean ProcessInstitute of Process EngineeringChinese Academy of SciencesBeijing 100190China School of Chemical Engineering University of Chinese Academy of SciencesBeijing 100049China Huizhou Institute of Green Energy and Advanced Materials Huizhou 516081China Advanced Energy Science and Technology Guangdong Laboratory Huizhou 516081China

Although the nickel-based catalyst is able toexhibit comparative catalytic activity to noble metal formethyl acrylate hydrogenation,it requires strict reactioncondition,which can be improved by regulation ofcoordination *** this study,we constructed akind of Ni single-atom coordinated with N and S(Ni-NSC)through the pyrolysis of organic Ni-based precursors at600℃.The existence and fine structure of Ni single-atom were confirmed by the spherical electron microscopicobservation in combination with the X-ray absorption spectroscopy(XAS)*** addition,the catalytichydrogenation assessment suggested that the as-prepared Ni-NSC catalyst exhibited higher activity and stability than theNi/NSC supported catalyst prepared by incipient wetness impregnation *** remarkable catalytic activity was dueto the high dispersion and density of Ni single-atom and weak adsorption energy of intermediates on these Ni sites.

关键词： methyl acrylate mild hydrogenation Ni single-atom coordination environment adsorption energy

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Decentralized Federated Learning Algorithm Under Adversary Eavesdropping

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IEEE/CAA Journal of Automatica Sinica 2025年第2期12卷 448-456页

作者： Lei Xu Danya Xu Xinlei Yi Chao Deng Tianyou Chai Tao Yang the State Key Laboratory of Synthetical Automation for Process Industries Northeastern University the Department of Mechanical Engineering University of Victoria Shanghai Institute of Intelligent Science and Technology Tongji University IEEE the Institute of Advanced Technology Nanjing University of Posts and Telecommunications

In this paper, we study the decentralized federated learning problem, which involves the collaborative training of a global model among multiple devices while ensuring data *** classical federated learning, the communication channel between the devices poses a potential risk of compromising private information. To reduce the risk of adversary eavesdropping in the communication channel, we propose TRADE(transmit difference weight) concept. This concept replaces the decentralized federated learning algorithm's transmitted weight parameters with differential weight parameters, enhancing the privacy data against eavesdropping. Subsequently, by integrating the TRADE concept with the primal-dual stochastic gradient descent(SGD)algorithm, we propose a decentralized TRADE primal-dual SGD algorithm. We demonstrate that our proposed algorithm's convergence properties are the same as those of the primal-dual SGD algorithm while providing enhanced privacy protection. We validate the algorithm's performance on fault diagnosis task using the Case Western Reserve University dataset, and image classification tasks using the CIFAR-10 and CIFAR-100 datasets,revealing model accuracy comparable to centralized federated learning. Additionally, the experiments confirm the algorithm's privacy protection capability.

关键词： Adversary eavesdropping decentralized federated learning privacy protection stochastic gradient descent

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Adsorption removal of mercury from flue gas by metal selenide:A review

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Journal of Environmental Sciences 2025年第2期148卷 420-436页

作者： Yang Zheng Guoliang Li Yi Xing Wenqing Xu Tao Yue School of Energy and Environmental Engineering University of Science and Technology BeijingBeijing 100083China State Key Laboratory of Advanced Metallurgy University of Science and Technology BeijingBeijing 100083China CAS Key Laboratory of Green Process and Engineering Institute of Process EngineeringInnovation Academy for Green ManufactureChinese Academy of SciencesBeijing 100190China

Mercury(Hg)pollution has been a global concern in recent decades,posing a significant threat to entire ecosystems and human health due to its cumulative toxicity,persistence,and transport in the *** intense interaction between mercury and selenium has opened up a new field for studying mercury removal from industrial flue gas *** the advantages of good Hg^(0) capture performance and lowsecondary pollution of the mineral selenium compounds,the most noteworthy is the relatively low regeneration temperature,allowing adsorbent regeneration with low energy consumption,thus reducing the utilization cost and enabling recovery of mercury *** paper reviews the recent progress of mineral selenium compounds in flue gas mercury removal,introduces in detail the different types ofmineral selenium compounds studied in the field ofmercury removal,reviews the adsorption performance of various mineral selenium compounds adsorbents on mercury and the influence of flue gas components,such as reaction temperature,air velocity,and other factors,and summarizes the adsorption mechanism of different fugitive forms of selenium *** on the current research progress,future studies should focus on the economic performance and the performance of different carriers and sizes of adsorbents for the removal of Hg^(0) and the correlation between the gas-particle flow characteristics and gas phase mass transfer with the performance of Hg^(0) removal in practical industrial *** addition,it remains a challenge to distinguish the oxidation and adsorption of Hg^(0) quantitatively.

关键词： Non-conventional pollutants Adsorbents Metal selenides Flue gas Mercury removal

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Selective cyclohexane oxidation enhancement by electronic structures regulation of metal-poly(ionic liquid)s

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Green Chemical Engineering 2024年第2期5卷 213-221页

作者： Ying Jin Shengxin Chen Ruirui Wang Yumei Liu Xinxin Li Yingwei Li Ruirui Zhang Ruixia Liu Henan Institute of Advanced Technology Zhengzhou UniversityZhengzhou450001China Beijing Key Laboratory of Ionic Liquids Clean Process CAS Key Laboratory of Green Process and EngineeringState Key Laboratory of Multiphase Complex SystemsInstitute of Process EngineeringInnovation Academy for Green ManufactureCASBeijing100190China

Poly(ionic liquids)(PILs)combined with the macromolecular structure and unique properties of ionic liquids show unlimited potential in *** this work,a series of metal-based PIL with different ionic ratios were prepared for the selective oxidation of *** analysis reveals that different degrees of ionization could adjust the Co-N sites of the catalysts efficiently,leading to significant changes in their electronic structure,which strongly relate to catalytic performance in oxidation.20.07%cyclohexane conversion and 13.06%cyclohexanone and cyclohexanol(KA oil)yield can be achieved by metal-based PILs that are better than other commercial *** with CoCl_(2),metal-based PILs perform well,with superior conversion and KA oil *** interestingly,the catalyst created in this study features a malleable Co-N site,which may potentially have an impact on how oxygen species adsorb and desorb from the ***,the catalyst studied in this work is used as molecular oxygen for the selective oxidation of cyclohexane to produce KA oil,and its application prospect is promising.

关键词： Metal-PILs Cyclohexane oxidation C-H activation Co-N sites

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Effects of Environmental Factors on Corrosion Behavior of E690 Steel in Simulated Marine Environment

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Acta Metallurgica Sinica(English Letters) 2024年第4期37卷 678-694页

作者： Jingjing Peng Jing Liu Shen Zhang Zhihui Wang Xian Zhang Kaiming Wu Collaborative Innovation Center for Advanced Steels Hubei Province Key Laboratory of Systems Science in Metallurgical ProcessThe State Key Laboratory of Refractories and MetallurgyWuhan University of Science and TechnologyWuhan430081China

The effects of hydrostatic pressure, dissolved oxygen, temperature and flow velocity, and their interaction on the corrosion rates of E690 high-strength steel (HSS) in simulated marine environments were studied using response surface methodology. The results show that the flow velocity exerts the most significant influence on the corrosion rate of E690 HSS. Consequently, the corrosion behavior of E690 HSS under varying flow velocities were analyzed profoundly from initial pitting corrosion to long-term corrosion properties. The results indicate that the flow state facilitates the mass transfer and enhances the adsorption tendency of Cl− by enhancing the electrochemical activity of the steel surface. These factors accelerate the electrochemical reactions, resulting in increased pitting density, depth and the long-term corrosion rates in dynamic seawater environments.

关键词： E690 steel Simulated marine environment Corrosion behavior Flow velocity Response surface methodology(RSM)

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3D Foam-Based MXene Architectures:Structural and Electrolytic Engineering for advanced Potassium-Ion Storage

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Energy & Environmental Materials 2024年第4期7卷 64-73页

作者： Peng Zhang Yanmeng Peng Qizhen Zhu Razium Ali Soomro Ning Sun Bin Xu State Key Laboratory of Organic-Inorganic Composites Beijing Key Laboratory of Electrochemical Process and Technology for MaterialsBeijing University of Chemical TechnologyBeijing 100029China Beijing Advanced Innovation Centre for Soft Matter Science and Engineering Beijing University of Chemical TechnologyBeijing 100029China

MXenes are emerging rapidly as promising electrode materials for energy storage due to their high electronic conductivity and rich surface chemistry,but their potassium storage performance is unsatisfactory because of the large size of K^(+)and irreversible interfacial ***,a developed 3D foam-like MXene scaffold(3D-FMS)is constructed via an electrostatic neutralization of Ti_(3)C_(2)T_(x)with positive-charged melamine followed with calcination,which offers massive surface-active sites and facilitates fast K^(+)transfer for boosting the potassium-ion storage capacity and *** addition,using KFSI-based electrolyte,the formation of a robust solid electrolyte interface layer with more inorganic components on MXene anode is revealed for enhancing the Coulombic ***,the 3DFMS with KFSI-based electrolyte delivers enhanced potassium-ion storage performance in terms of capacity(161.4 mAh g^(-1)at 30 mA g^(-1)),rate capability(70 mAh g^(-1)at 2 A g^(-1)),and cycling stability(80.5 mAh g^(-1)at 1 A g^(-1)after 2000 cycles).Moreover,the assembled 3D-FMS//activated carbon potassium-ion hybrid supercapacitor delivers a high energy density of 57 Wh kg^(-1)at a power density of 290 W kg^(-1).These excellent performances demonstrate the great superiority of 3D-FMS in KFSI-based electrolyte and may accelerate the development of MXene-based materials for potassium storage systems.

关键词： 3D foam-like scaffold electrolyte chemistry electrostatic neutralization MXene potassium-ion batteries

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Experimental Investigation of Ultra-Low Temperature LA2O3/HFO2 Bi-Layer Dipole-First process Using PVD Method for advanced IC technology

Experimental Investigation of Ultra-Low Temperature LA2O3/HF...

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China Semiconductor technology International Conference (CSTIC)

作者： Yanzhao Wei Jiaxin Yao Renren Xu Qingzhu Zhang Huaxiang Yin Integrated Circuit Advanced Process R&D Center Institute of Microelectronics Chinese Academy of Sciences Beijing China School of Integrated Circuits University of Chinese Academy of Sciences Beijing China Key Laboratory of Microelectronic Devices and Integrated Technology Institute of Microelectronics Chinese Academy of Sciences Beijing China

In this paper, a La 2 O 3 /HfO 2 bi-layer dipole-first (DF) process is proposed and investigated by ultra-low temperature PVD dielectric laminates to achieve lower gate effective work function (EWF) for monolithic 3D-IC (M3D) application. The impacts of ultra-low temperature La-dipole on EWF modulation and interfacial properties are comprehensively investigated. It is found that the flat-band voltage (V FB ) negatively shifts 60 mV with sub-1nm La 2 O 3 thickness, which provides an effective way to meet the require of Si conduction band-edge EWF modulation. Furthermore, the electron trap/detrap densities (Not) and interfacial trap densities (Dit) are suppressed by La 2 O 3 /HfO 2 bi-layer DF process to improve device performance. These results exhibit a promising bi-layer DF process in low thermal integration for advanced IC technology.

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