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Gel-derived NiO–MoS 2 for the scalable fabrication of bifunctional screen-printed electrodes for overall water splitting

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International Journal of Hydrogen Energy 2025年 139卷 247-256页

作者： Zhoveta Yhobu Muralikrishna Sreeramareddygari Chatuporn Phanthong Srinivasa Budagumpi Doddahalli H. Nagaraju Wachira Chaiworn Mithran Somasundrum Patsamon Rijiravanich Surawut Chuangchote Werasak Surareungchai Sensor Technology Laboratory Pilot Plant Development and Training Institute King Mongkut's University of Technology Thonburi Bangkhuntien-chaitalay Road Thakam Bangkok 10150 Thailand Centre for Nano and Material Sciences JAIN (Deemed–to–be University) Jain Global Campus Kanakapura Bangalore 562 112 Karnataka India Industrial Sensor Technology Research Team Biochemical Engineering and System Biology Research Group National Center for Genetic Engineering and Biotechnology National Science and Technology Development Agency at KMUTT (Bangkhuntien Campus) Bangkok 10150 Thailand Department of Chemistry School of Applied Sciences REVA University Kattigenahalli Yelahanka Bangalore 560 064 Karnataka India Department of Tool and Materials Engineering Faculty of Engineering King Mongkut's University of Technology Thonburi (KMUTT) 126 Prachauthit Rd. Bangmod Thungkru Bangkok 10140 Thailand Research Center for Advanced Materials for Energy and Environmental Technology (MEET) King Mongkut's University of Technology Thonburi (KMUTT) 126 Prachauthit Rd. Bangmod Thungkru Bangkok 10140 Thailand Nanoscience & Nanotechnology Graduate Programme Faculty of Science King Mongkut's University of Technology Thonburi Bangkhuntien-chaitalay Road Thakam Bangkok 10150 Thailand

The fabrication of flexible, free-standing electrodes is crucial for advancing renewable energy technologies, particularly in energy conversion and storage. Traditional electrode fabrication methods often involve complex procedures, high material wastage, and limited scalability, whereas screen printing offers a cost-effective, reproducible, and scalable approach for producing high-performance electrodes with uniform coatings. This study introduces a versatile screen-printing strategy for fabricating flexible carbon cloth (CC) electrodes using NiO–MoS 2 ink derived from a solvothermal method. The resulting screen-printed CC electrodes function as efficient bifunctional catalysts for the hydrogen evolution reaction (HER), oxygen evolution reaction (OER), and overall water splitting in alkaline media. The NiO–MoS 2 screen-printed CC electrode exhibits excellent electrocatalytic performance, achieving an OER overpotential ( η 10 ) of 382 mV vs RHE with a Tafel slope of 75 mV/dec and HER overpotential ( η 10 ) of −159 mV vs RHE and Tafel slope of 116 mV/dec. To further demonstrate its bifunctionality, the NiO–MoS 2 screen-printed CC electrode was assembled into a water-splitting electrolyzer, requiring a cell voltage of 1.79 V to reach a current density of 10 mA/cm 2 and exhibiting outstanding operational durability. The robustness and structural integrity of the developed electrode is confirmed by the post-stability analysis, highlighting the potential of the methodology reported in this work for the scalable fabrication of high-performance electrodes for water splitting applications.

关键词： Screen printing

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ATLAS multlspectral sensor calibration and right test results

ATLAS multlspectral sensor calibration and right test result...

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Recent Advances in sensors, Radiometric Calibration, and Processing of Remotely Sensed Data 1993

作者： DaMommio, T. Kuo, S. Advanced Sensor Development Laboratory Sverdrup Technology Inc. Stennis Space Center MS39529 United States

The ATLAS (Airborne Terrestrial Applications sensor) is a 15-channel multispectral scanning imager, currently under development for NASA's Commercial Remote Sensing Program (CRSP) Office. The sensor package utilizes a rotating linescan mirror, and a modified Dall-Kirkham telescope with a 7.5-inch clear aperture and 2.0 mrad ifov. Scan rates are adjustable from 6-50 rev/sec, with a total field of view of ∼ 73°. Three spectrometers with grating dispersive elements are used to provide wide spectral coverage, shown below: o VIS/NIR, 6 channels: 0.45-0.90 μm o SW/MWIR, 3 channels: 1.55-4.20 μm o TIR, 6 channels: 8.2-12.2 μm. Blackbody sources (hi/o) and a modified integrating sphere source, built into the scanhead, are employed to provide in-flight radiometric calibration data for quantitative inference of ground scene temperatures and radiance values. In this paper, the overall design of the ATLAS scanner system is reviewed. Results of spectral response, NETD, NER and MTF calibration measurements are presented for each channel. Additionally, some initial ATLAS flight test data and analysis are described, including SNR, uniformity of TIR data over water, overall image quality and other results. © 1993 SPIE. All rights reserved.

关键词： NASA

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Commercial applications multispectral sensor system design 3

Commercial applications multispectral Sensor system design

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Infrared Imaging Systems: Design, Analysis, Modeling, and Testing III 1992

作者： Birk, R. Damommio, T. Kuo, S. Advanced Sensor Development Laboratory Lockheed Engineering and Sciences Co. Stennis Space CenterMS39529 United States

Funded by NASA's Office of Commercial Programs, the ATLAS (Airborne Terrestrial Applications sensor) is a 15-channel multispectral imager for remote sensing applications under development at the Stennis Space Center (MS). This paper describes the overall ATLAS system design, functional sub-systems, and projected sensor performance characteristics (SNR, NETD, etc). In order to satisfy a variety of applications, both wide spectral coverage (0.45-12.2μm), as well as variable spatial resolution (2-25 m), are provided. The optics train includes a linescan mirror, Dall-Kirkham telescope, and three spectrometers. The ATLAS sensor package has a 7.5-inch entrance aperture, 2.0 mrad ifov, total field of view of 73°, and scan rates of 6-50 rev/sec. The spectrometer channels are divided as follows: VIS/NIR, 6 channels: 0.45-0.90 μm;SWIR/MWIR, 3 channels: 1.55-4.20 μm;and TIR, 6 channels: 8.2-12.2 μm. The ATLAS system combines the functionality of the TIMS (Thermal Infrared Multispectral Scanner) and the CAMS (Calibrated Airborne Multispectral Scanner), currently deployed, calibrated, and maintained by the advanced sensor development laboratory at Stennis Space Center. The major optical sub-systems, radiometric calibration sources, signal conditioning electronics, and other other functions, will be described. ATLAS system specifications will also be presented. © 1992 SPIE. All rights reserved.

关键词： Spectrometers

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Evaluation of immune responses and protection in Asian seabass (Lates calcarifer Bloch, 1790) against Vibrio vulnificus using immersion and oral nanoemulsion vaccines

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Fish and Shellfish Immunology 2025年 162卷 110354页

作者： Rodwihok, Chatchai Thompson, Kim D. Srisapoome, Prapansak Thangsunan, Patcharapong Thangsunan, Pattanapong Buncharoen, Wararut Saenphet, Kanokporn Saenphet, Supap Meachasompop, Pakapon Kumwan, Benchawan Tangal, Jasper Kit Wiratama, Nugroho Mai, Thao Thu Uchuwittayakul, Anurak Special Research Incubator Unit for Development and Application of Vaccine Delivery Systems for Aquatic Animals Department of Aquaculture Faculty of Fisheries Kasetsart University Bangkok 10900 Thailand Laboratory of Aquatic Animal Health Management Department of Aquaculture Faculty of Fisheries Kasetsart University Bangkok 10900 Thailand Center of Excellence in Aquatic Animal Health Management Faculty of Fisheries Kasetsart University Bangkok 10900 Thailand Moredun Research Institute Pentlands Science Park Penicuik EH26 0PZ United Kingdom Division of Biochemistry and Biochemical Innovation Department of Chemistry Faculty of Science Chiang Mai University Chiang Mai 50200 Thailand Office of Research Administration Chiang Mai University Chiang Mai 50200 Thailand Center of Excellence for Innovation in Chemistry and Research Laboratory on Advanced Materials for Sensor and Biosensor Innovation Material Science Research Center Faculty of Science Chiang Mai University Chiang Mai 50200 Thailand Department of Biology Faculty of Science Chiang Mai University Chiang Mai 50200 Thailand

Vaccination is an important strategy in aquaculture for enhancing disease resistance and ensuring the health and productivity of cultured fish. This study investigated the distinct systemic and mucosal immune responses elicited by immersion (ImV) and oral (OrV) nanoemulsion vaccines encapsulating Vibrio vulnificus in Asian seabass (Lates calcarifer). Two vaccination methods, ImV and OrV, were administered to separate groups of Asian seabass, followed by challenges with V. vulnificus via immersion and intraperitoneal (i.p.) injection administration. Immune responses were assessed by measuring specific IgM antibodies, lysozyme activity, bactericidal activity, and immune-related gene expression across multiple organs, including serum, head kidney, liver, gills, skin, and intestine. The results demonstrate that the OrV group had a significantly increased level of specific IgM antibody in their serum, head kidney and liver compared to the immersion vaccine group and control, with the OrV group maintaining higher antibody levels post-immersion and injection challenge. In mucosal tissues, the ImV group elicited stronger IgM responses in the gills and skin, whereas the OrV group enhanced antibody responses in the liver and intestine. Lysozyme and bactericidal activities varied by organ and vaccination route, indicating differential activation of innate immune defenses. Additionally, immune-related gene expression was upregulated in a tissue-specific manner, reflecting the targeted activation of adaptive and innate immune mechanisms by each vaccine type. Both vaccination strategies significantly improved survival and relative percent survival (RPS), with ImV offering stronger protection against immersion challenges, while OrV provided strong protection in systemic (injection) challenges. These findings suggest that ImV and OrV groups induced distinct immune responses in Asian seabass, with immersion vaccination primarily enhancing mucosal immunity at barrier surfaces and ora

关键词： Aquaculture Asian seabass Immersion vaccine Immune response Mucosal immunity Oral nanoemulsion vaccine Systemic immunity Vibrio vulnificus

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Intestinal mucosal transcriptomic responses of Asian seabass (Lates calcarifer) vaccinated with an oral hydrogel-encapsulated multivalent Vibrio antigen following Vibrio spp. infection

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Comparative Biochemistry and Physiology - Part D: Genomics and Proteomics 2025年 55卷 101512页

作者： Kumwan, Benchawan Meachasompop, Pakapon Thompson, Kim D. Thangsunan, Pattanapong Buncharoen, Wararut Thangsunan, Patcharapong Srisapoome, Prapansak Uchuwittayakul, Anurak Special Research Incubator Unit for Development and Application of Vaccine Delivery Systems for Aquatic Animals Department of Aquaculture Faculty of Fisheries Kasetsart University Bangkok 10900 Thailand Laboratory of Aquatic Animal Health Management Department of Aquaculture Faculty of Fisheries Kasetsart University Bangkok 10900 Thailand Center of Excellence in Aquatic Animal Health Management Faculty of Fisheries Kasetsart University Bangkok 10900 Thailand Moredun Research Institute Pentlands Science Park Penicuik EH26 0PZ United Kingdom Division of Biochemistry and Biochemical Innovation Department of Chemistry Faculty of Science Chiang Mai University Chiang Mai 50200 Thailand Center of Excellence for Innovation in Chemistry and Research Laboratory on Advanced Materials for Sensor and Biosensor Innovation Material Science Research Center Faculty of Science Chiang Mai University Chiang Mai 50200 Thailand Department of Biology Faculty of Science Chiang Mai University Chiang Mai 50200 Thailand Office of Research Administration Chiang Mai University Chiang Mai 50200 Thailand

This study examined the intestinal mucosal immune responses elicited by an oral hydrogel-encapsulated multivalent Vibrio vaccine in Asian seabass (Lates calcarifer) to protect against vibriosis caused by Vibrio harveyi, V. vulnificus, and Photobacterium damselae (formerly Vibrio damsela). Both 7-day and 14-day oral vaccination regimens effectively enhanced innate and adaptive immune responses while supporting gut recovery post-infection. Transcriptomic analyses of intestines from fish that received consecutive 7- and 14-day vaccination regimens, followed by co-infection with multistrain Vibrio spp., revealed significant upregulation of innate and specific immune markers at week 8 post-vaccination. These responses were further bolstered by a strong adaptive immune activation, characterized by T-cell and B-cell receptor signaling as well as antibody production. In addition, the vaccine also demonstrated cross-protective immunomodulatory effects, evidenced by elevated interferon-related pathways (e.g., IFNAR2 and IFN-induced proteins), suggesting its potential to protect against co-infecting pathogens, a critical advantage in aquaculture systems facing diverse pathogen pressures. Beyond immune activation, the involvement proteins of TGF-β family members, including BMP3 and BMP4, highlights the vaccine's role in tissue repair and remodeling. These responses likely mitigate epithelial damage and preserve gut barrier integrity post-infection, showcasing the dual benefits of immunoprotection and post-infection recovery. The findings highlight the oral hydrogel-encapsulated multivalent Vibrio vaccine's ability to enhance immunity against specific bacterial pathogens while offering broader immunomodulatory and tissue-repair benefits. Its cross-protective and recovery-supporting properties make it a promising solution for sustainable aquaculture practices, effectively addressing pathogen control and boosting host resilience. © 2025 Elsevier Inc.

关键词： Hydrogel Intestinal mucosal immunity Lates calcarifer Oral vaccine P. damselae Transcriptome V. harveyi V. vulnificus Vibriosis

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Sustainable uric acid sensor based on a lab-fabricated electrode modified with rice straw-derived carbon materials

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Scientific reports 2025年第1期15卷 18380页

作者： Pakin Noppawan Jaroon Jakmunee Andrew J Hunt Nontipa Supanchaiyamat Suwiwat Sangon Jamras Lerdsri Thidarat Kruatian Jantima Upan Department of Chemistry Faculty of Science Mahasarakham University Maha Sarakham 44150 Thailand. Research Laboratory for Analytical Instrument and Electrochemistry Innovation Department of Chemistry Faculty of Science Chiang Mai University Chiang Mai 50200 Thailand. Research Laboratory on Advanced Materials for Sensor and Biosensor Innovation Materials Science Research Center Center of Excellence for Innovation in Chemistry Faculty of Science Chiang Mai University Chiang Mai 50200 Thailand. Materials Chemistry Research Center Department of Chemistry Center of Excellence for Innovation in Chemistry Faculty of Science Khon Kaen University Khon Kaen 40002 Thailand. Department of Livestock Development Veterinary Research and Development Center (Upper Northern Region) Lampang 52190 Thailand. Institute of Community Science Technology Department of Science Service Ministry of Higher Education Science Research and Innovation Bangkok 10400 Thailand. Department of Chemistry Faculty of Science Mahasarakham University Maha Sarakham 44150 Thailand. jantima.u@msu.ac.th.

A novel and facile electrochemical sensor for the quantification of uric acid has been fabricated through the strategic modification of a screen-printed carbon electrode (SPCE) using mesoporous carbon-zinc oxide (MC-ZnO) synthesized from rice straw waste. The MC-ZnO materials, generated via a controlled pyrolysis process, exhibit homogeneous dispersion and a substantial electroactive surface area of 0.1286 cm. The electrochemical oxidation of uric acid exhibits a distinct peak at 0.18 V in differential pulse voltammetry (DPV), indicative of efficient charge transfer kinetics. A linear range spanning 20 to 225 µM was obtained with a limit of detection (LOD) of 3.76 µM, signifying exceptional analytical sensitivity. Furthermore, the sensor demonstrates robust selectivity toward uric acid in the presence of typical interferents, underscoring its applicability for precise uric acid determination in complex biological matrices. The sensor's analytical performance was validated by quantifying uric acid in spiked urine samples, yielding recovery rates between 97.9% and 114.8% and relative standard deviations (RSD) below 4.92%, affirming its accuracy and precision. This platform heralds a promising avenue for clinical diagnostics, leveraging sustainable materials for uric acid detection.

关键词： Agricultural waste Biomass Eco-friendly sensor Modified electrode Voltammetry

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A Hybrid Biofuel and Triboelectric Nanogenerator for Bioenergy Harvesting

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Nano-Micro Letters 2020年第4期12卷 53-64页

作者： Hu Li Xiao Zhang Luming Zhao Dongjie Jiang Lingling Xu Zhuo Liu Yuxiang Wu Kuan Hu Ming‑Rong Zhang Jiangxue Wang Yubo Fan Zhou Li Beijing Advanced Innovation Centre for Biomedical Engineering Key Laboratory for Biomechanics and Mechanobiology of Chinese Education MinistrySchool of Biological Science and Medical EngineeringBeihang UniversityBeijing 100083People’s Republic of China CAS Center for Excellence in Nanoscience Beijing Key Laboratory of Micro‑Nano Energy and SensorBeijing Institute of Nanoenergy and NanosystemsChinese Academy of SciencesBeijing 100083People’s Republic of China School of Nanoscience and Technology University of Chinese Academy of SciencesBeijing 100049People’s Republic of China School of Physical Education Jianghan UniversityWuhan 430056People’s Republic of China Center on Nanoenergy Research School of Physical Science and TechnologyGuangxi UniversityNanning 530004People’s Republic of China Department of Radiopharmaceuticals Development National Institute of Radiological SciencesNational Institutes for Quantum and Radiological Science and TechnologyChiba 263‑8555Japan

Various types of energy exist everywhere around us,and these energies can be harvested from multiple sources to power micro-/nanoelectronic system and even personal electronic *** this work,we proposed a hybrid energy-harvesting system(HEHS)for potential in vivo *** HEHS consisted of a triboelectric nanogenerator and a glucose fuel cell for simultaneously harvesting biomechanical energy and biochemical energy in simulated body *** two energy-harvesting units can work individually as a single power source or work simultaneously as an integrated *** design strengthened the flexibility of harvesting multiple energies and enhanced corresponding electric *** with any individual device,the integrated HEHS outputs a superimposed current and has a faster charging *** the harvested energy,HEHS can power a calculator or a green light-emitting diode *** the widely existed biomechanical energy and glucose molecules in the body,the developed HEHS can be a promising candidate for building in vivo self-powered healthcare monitoring system.

关键词： Self-powered Triboelectric nanogenerator Glucose fuel cell Hybrid energy harvester Bioenergy

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An Improved Non-Geometrical Stochastic Model for Non-WSSUS Vehicle-to-Vehicle Channels

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ZTE Communications 2019年第4期17卷 62-71页

作者： HUANG Ziwei CHENG Xiang ZHANG Nan State Key Laboratory of Advanced Optical Communication Systems and Networks School of Electronics Engineering and Computer SciencePeking UniversityBeijing 100871China Key Laboratory of Wireless Sensor Network&Communication Shanghai Institute of Microsystem and Information TechnologyChinese Academy of SciencesShanghai 200050China Wireless Algorithm Department Product Research and Development SystemZTE CorporationShanghai 201203China

A novel non-geometrical stochastic model(NGSM)for non-wide sense station ary uncorrelated scattering(non-WSSUS)vehicle-to-vehicle(V2V)channels is *** model is based on a conventional NGSM and employs a more accurate method to reproduce the realistic characteristics of V2V channels,which successfully extends the existing NGSM to include the line-of-sight(LoS)***,the statistical properties of the proposed model in different scenarios,including Doppler power spectral density(PSD),power delay profile(PDP),and the tap correlation coefficient matrix are simulated and compared with those of the existing ***,the simulation results dem onstrate not only the utility of the proposed model,but also the correctness of our theoreti cal derivations.

关键词： vehicle-to-vehicle non-WSSUS channels non-geometrical stochastic model LoS component statistical properties

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Local structural study of α-MoO3 micro-strips using synchrotron X-ray diffraction and X-ray Absorption Spectroscopy at Mo K-edge

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EUROPEAN PHYSICAL JOURNAL-APPLIED PHYSICS 2022年 97卷 65-65页

作者： Gawai, Umesh Kamble, Shilpa Kamble, Charudipa Waghmare, Yogita Kulkari, Suvarna Singh, Manvendra Yadav, Ashok Jha, Shambhu Dole, Babasaheb Department of Physics DDSP Arts Commerce and Science College Erandol Jalgaon 425109 (M.S.) India Department of Physics Shri Madhavrao Patil Mahavidyalaya Murum Osmanabad 413606 India Department of Physics and RUSA Centre for Advanced Sensor Technology Dr. Babasaheb Ambedkar Marathwada University Aurangabad 431004 (M.S.) India Department of Electronics K.R.T. Arts B.H. Commerce and A.M. Science College Nashik 422002 India Synchrotrons Utilization Section Raja Ramanna Centre for Advanced Technology Indore 452013 India Atomic & Molecular Physics Division Bhabha Atomic Research Centre Mumbai 400094 India Beamline Development & Application Section Bhabha Atomic Research Centre Mumbai 400094 India Advanced Materials Research Laboratory Department of Physics Dr. Babasaheb Ambedkar Marathwada University Aurangabad 431004 India

The orthorhombic MoO3 micro-strips sample was synthesized using microwave assisted chemical co-precipitation technique. Synchrotron X-ray Diffraction (SXRD) pattern and Rietveld Refinement was used to estimate structural parameter, crystallite size of sample. It reveals that the synthesized sample MoO3 crystallized as an orthorhombic phase. X-ray Absorption Spectroscopy (XAS) measurement, which comprises both X-ray Absorption Near Edge Structure (XANES) and Extended X-ray Absorption Fine Structure (EXAFS) techniques, have been carried out on Mo K-edge to probe the local structure of samples. Local structure is also confirmed from the SXRD and Raman spectra of sample. XAS measurement reveals that the first bond length of Mo-O and Mo-Mo is 1.69 and 3.42 angstrom in orthorhombic MoO3 respectively. Transmission electron microscopy and SAED patterns showed stripe-like structure and single-crystal formation of MoO3 respectively.

关键词： Crystal structure

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High-Performance Stretchable Piezo-Electrically Enhanced Hybrid Triboelectric Nanogenerator Generated Maxwell's Displacement Current Towards Underwater Wireless Communication Assisted Self-Powered Biomechanical Signal Monitoring

SSRN

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SSRN 2024年

作者： Mahanty, Biswajit Ghosh, Sujoy Kumar Lee, Dong-Weon MEMS and Nanotechnology Laboratory School of Mechanical Engineering Chonnam National University Gwangju61186 Korea Republic of Department of Condensed Matter Physics and Material Sciences S.N. Bose National Centre for Basic Sciences Block JD Sector III Salt Lake Kolkata7000106 India Center for Next-Generation Sensor Research and Development Chonnam National University Gwangju61186 Korea Republic of Advanced Medical Device Research Center for Cardiovascular Disease Chonnam National University 77 Yongbong-ro Buk-gu Gwangju61186 Korea Republic of

This study proposes an underwater wireless communication approach for transmission of biomechanical signals that relies on Maxwell's displacement current generated by a stretchable piezoelectric-enhanced triboelectric hybrid nanogenerator (PET-HNG). A high performing nano-/micro-composite film was prepared by embedding MXene nanosheets and ferro-/piezo-electric LiNbO3 microparticles into Ecoflex polymer matrix. The MXene sheets function as a micro capacitor network while LiNbO3 microparticles play a crucial role in the resulting dipole orientation and electrical polarization enhancing surface charge density to improve the triboelectric energy harvesting performance. The realized PET-HNG using this composite film shows greatly enhanced output performance in comparison to piezoelectric and triboelectric nanogenerators individually, with open circuit output voltage of 455 V, short circuit current of 140 µA, instantaneous power density (P) of 15.6 W m-2 and energy conversion efficiency of 78.5%. Indeed, the PET-HNG shows superior output performance stability even after releasing the stretching strain (30% for 20 times), which makes it a promising self-powered wearable sensor for real-time monitoring of biomechanical signals from human body movement. The proposed stretchable PET-HNG can promote the development of self-powered intelligent wearable sensors and flexible electronics. © 2024, The Authors. All rights reserved.

关键词： Nanogenerators

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