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Fine grains with high-density annealing twins and precipitates inducing favorable strength and excellent plasticity in laser powder b e d fusion-fabricate d Inconel 718 via deep cryogenic and heat treatments

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Journal of materials Science & technology 2024年第20期187卷 28-48页

作者： Bo Liu Jiayu Xu Yubi Gao Yong Hu Xiaokang Yang Yutian Ding Dong Zhang Sujun Lu State Key Laboratory of Advanced Processing and Recycling of Non-ferrous Metals Lanzhou University of TechnologyLanzhou 730050China School of Material Science and Engineering Lanzhou University of TechnologyLanzhou 730050China School of Electromechanics and Automobile Engineering Tianshui Normal UniversityTianshui 741001China Jinchuan Nickel Cobalt Research and Design Institute Jinchuan Group Co.LtdJinchang 737100China

Tailoring high-density annealing twins in laser powder bed fusion(LPBF)-fabricated alloys based on their intrinsic residual stress requires high annealing temperatures and/or long-term annealing,result-ing in the abnormal growth of large recrystallized grains,which is detrimental to mechanical *** work proposes a new strategy for achieving a favorable strength-plasticity synergy of the LPBF-fabricated Inconel 718 superalloy by performing a deep cryogenic treatment(DCT)with the subsequent heat treatment(including annealing and double aging)to tailor fine grains with“high-density annealing twins+precipitates”architectures and compares the obtained material with an alloy subjected to a direct heat treatment without a prior *** obtained results reveal that the additional internal stress gen-erated during DCT increases the stored energy and dislocation density,which provide a sufficient driving force for activating high-density annealing twin boundaries(63.2%)with fine grains(31.6μm)within a short annealing *** more homogeneous tailored microstructure with the“finer grains+high-density twins+precipitates”architectures decreases the mean free path of slipping dislocations,pro-moting intensive interactions with dislocations and inducing a strong strain hardening *** mul-tiple deformation modes of stacking faults coupled with Lomer-Cottrell locks,thin primary deformation twins,and secondary twins activated during tensile loading,sustaining a strong work hardening ability and delaying the plastic instability,which exhibits a high strength(yield strength of 1088 MPa and tensile strength of 1369 MPa)and excellent plasticity(elongation of 30%).This work not only describes a fea-sible method for simultaneously enhancing the strength and plasticity in additively manufactured(AM)alloys but also provides new insights into increasing the fraction of twins at a small grain size to improve the grain boundary-related properties without destroying the AM allo

关键词： Laser powder bed fusion Deep cryogenic treatment Stored energy High-density annealing twins Work hardening

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Investigation of wide-angle thin metamaterial absorber at infrared region

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Optoelectronics Letters 2021年第11期17卷 669-672页

作者： HUANG Xiutao ZHANG Chunbo CONG Lin FAN Jun YUAN Hang Aerospace Institute of Advanced Materials&Processing Technology Beijing 100074China

In the practical application,a wide-angle absorption with simple structure is still crucial property of metamaterial absorbers(MAs).A single-band infrared MA is introduced to analyze the angle insensitive *** simulation reveals that a perfect absorption peak with 99.9%(7.55μm)is achieved at normal incidence,as well as the absorptivity is respectively 69.7%(7.46μm)and 93.5%(7.46μm)for transverse electric(TE)and transverse magnetic(TM)modes at 70°*** changing substrate thickness,the absorption ratio at 70°is increased to 91%(7.46μm)for TE *** design can also keep the good absorption stability for the geometric *** E z-field distributions for different incident angles are given to investigate the physical *** designed MA can realize good wide-angle *** MA owns great applications,including infrared spectroscopy,solar harvester and plasmonic sensors.

关键词： Investigation of wide-angle thin metamaterial absorber at infrared region

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High-entropy spinel ferrites MFe_(2)O_(4)(M=Mg,Mn,Fe,Co,Ni,Cu,Zn)with tunable electromagnetic properties and strong microwave absorption

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Journal of advanced Ceramics 2022年第5期11卷 754-768页

作者： Jiabin MA Biao ZHAO Huimin XIANG Fu-Zhi DAI Yi LIU Rui ZHANG Yanchun ZHOU Henan Key Laboratory of Aeronautical Materials and Application Technology School of Materials Science and EngineeringZhengzhou University of AeronauticsZhengzhou 450046China Science and Technology on Advanced Functional Composite Laboratory Aerospace Research Institute of Materials&Processing TechnologyBeijing 100076China School of Material Science and Engineering Shaanxi University of Science and TechnologyXi'an 710021China School of Materials Science and Engineering Luoyang Institute of Science and TechnologyLuoyang 471023China

Ferrites are the most widely used microwave absorbing materials to deal with the threat of electromagnetic(EM)***,the lack of sufficient dielectric loss capacity is the main challenge that limits their *** cope with this challenge,three high-entropy(HE)spineltype ferrite ceramics including(Mg_(0.2)Mn_(0.2)Fe_(0.2)Co_(0.2)Ni_(0.2))Fe_(2)O_(4),(Mg_(0.2)Fe_(0.2)Co_(0.2)Ni_(0.2)Cu_(0.2))Fe_(2)O_(4),and(Mg_(0.2)Fe_(0.2)Co_(0.2)Ni_(0.2)Zn_(0.2))Fe_(2)O_(4)were designed and successfully prepared through solid state *** results show that all three HE MFe_(2)O_(4) samples exhibit synergetic dielectric loss and magnetic *** good magnetic loss ability is due to the presence of magnetic components;while the enhanced dielectric properties are attributed to nano-domain,hopping mechanism of resonance effect and HE *** three HE spinels,(Mg_(0.2)Mn_(0.2)Fe_(0.2)Co_(0.2)Ni_(0.2))Fe_(2)O_(4)shows the best EM wave absorption performance,e.g.,its minimum reflection loss(RL_(min))reaches-35.10 dB at 6.78 GHz with a thickness of 3.5 mm,and the optimized effective absorption bandwidth(EAB)is 7.48 GHz from 8.48 to 15.96 GHz at the thickness of 2.4 *** to the easy preparation and strong EM dissipation ability,HE MFe_(2)O_(4) are promising as a new type of EM absorption materials.

关键词： high-entropy ceramics(HECs) spinel-type ferrite electromagnetic(EM)wave absorption dielectric loss magnetic loss

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Recent progress in C-N coupling for electrochemical CO_(2) reduction with inorganic nitrogenous species in aqueous solution

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materials Reports(Energy) 2023年第1期3卷 65-77,I0003页

作者： Shuxia Liu Tanyuan Wang Lior Elbaz Qing Li State Key Laboratory of Material Processing and Die&Mould Technology School of Materials Science and EngineeringHuazhong University of Science and TechnologyWuhanHubei430074China Department of Chemistry and the Institute of Nanotechnology and Advanced Materials Bar-Ilan UniversityRamat-Gan5290002Israel

The electrocatalytic CO_(2) reduction in aqueous solution mainly involves bond cleavage and formation between C,H and O,and it is highly desirable to expand the bond formation reaction of C with other atoms to obtain novel and valuable *** electrochemical synthesis of N-containing organic chemicals in electrocatalytic CO_(2) reduction via introducing N sources is an effective strategy to expand the product scope,since chemicals con-taining C–N bonds(*** and amines)are important reactants/products for medicine,agriculture and *** article focuses on the research progress of C–N coupling from CO_(2) and inorganic nitrogenous species in aqueous ***,the reaction pathways related to the reaction intermediates for urea,formamide,acetamide,methylamine and ethylamine are ***,the electrocatalytic performance of different catalysts for these several N-containing products are summarized and ***,the challenges and op-portunities are analyzed,aiming to provide general insights into future research directions for electrocatalytic C–N coupling.

关键词： CO_(2) reduction C-N coupling Heterogeneous electrocatalysis Amide Amine

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Tunnel-structured willemite Zn_(2)SiO_(4):Electronic structure,elastic,and thermal properties

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Journal of advanced Ceramics 2022年第8期11卷 1249-1262页

作者： Ruqiao DAI Renfei CHENG Jiemin WANG Chao ZHANG Cuiyu LI Hailong WANG Xiaohui WANG Yanchun ZHOU Shenyang National Laboratory for Materials Science Institute of Metal ResearchChinese Academy of SciencesShenyang 110016China School of Materials Science and Engineering University of Science and Technology of ChinaShenyang 110016China Advanced Computing East China Sub-center Suma Technology Company LimitedKunshan 215300China School of Material Science and Engineering Zhengzhou UniversityZhengzhou 450001China Science and Technology on Advanced Functional Composite Laboratory Aerospace Research Institute of Materials&Processing TechnologyBeijing 100076China

Willemite Zn_(2)SiO_(4)crystallizes in such a way that Zn and Si are tetrahedrally coordinated with O in an ionic–covalent manner to form ZnO_(4)and SiO_(4)tetrahedra as the building *** tetrahedra are corner-sharing,of which one SiO_(4)tetrahedron connects eight ZnO_(4)tetrahedra,and one ZnO_(4)tetrahedron links four ZnO_(4)tetrahedra and four SiO_(4)*** unique crystallographic configuration gives rise to parallel tunnels with a diameter of 5.7Åalong the c-axis *** tunnel structure of Zn_(2)SiO_(4)definitely correlates with its interesting elastic and thermal *** the one hand,the elastic modulus,coefficient of thermal expansion(CTE),and thermal conductivity are ***_(2)SiO_(4)has low Vickers hardness of 6.6 GPa at 10 N and low thermal conductivity of 2.34 W/(m·K)at 1073 *** the other hand,the elastic modulus and CTE along the c-axis are significantly larger than those along the a-and b-axes,showing obvious elastic and thermal expansion ***,the Young’s modulus along the z direction(Ez=179 GPa)is almost twice those in the x and y directions(Ex=Ey=93 GPa).The high thermal expansion anisotropy is ascribed to the empty tunnels along the c-axis,which are capable of more accommodating the thermal expansion along the a-and *** striking properties of Zn_(2)SiO_(4)in elastic modulus,hardness,CTE,and thermal conductivity make it much useful in various fields of ceramics,such as low thermal expansion,thermal insulation,and machining tools.

关键词： Zn_(2)SiO_(4) electronic structure elastic properties thermal expansion thermal conductivity

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Oil-soluble polymer brushes-functionalized nanoMOFs for highly efficient friction and wear reduction

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Friction 2024年第7期12卷 1499-1511页

作者： Jianxi LIU Yong QIAN Dongsheng LI Wei WU Mengchen ZHANG Jie YAN Bin LI Feng ZHOU State Key Laboratory of Solidification Processing Center of Advanced Lubrication and Seal MaterialsSchool of Materials Science and EngineeringNorthwestern Polytechnical UniversityXi'an 710072China Shaanxi Engineering Research Center of Special Sealing Technology Xi'an Aerospace Propulsion InstituteXi'an 710100China State Key Laboratory of Solid Lubrication Lanzhou Institute of Chemical PhysicsChinese Academy of SciencesLanzhou 730000China

Nanomaterials as lubricating oil additives have attracted significant attention because of their designable composition and structure,suitable mechanical property,and tunable surface ***,the poor compatibility between nanomaterials and base oil limits their further *** this work,we demonstrated oil-soluble poly(lauryl methacrylate)(PLMA)brushes-grafted metal-organic frameworks nanoparticles(nanoMOFs)as lubricating oil additives that can achieve efficient friction reduction and anti-wear *** were synthesized by free-radical polymerization,which was coordinatively grafted onto the surface of the UiO-67 ***,PLMA brushes were grown on the macroinitiator-modified UiO-67 by surface-initiated atom transfer radical polymerization,which greatly improved the lipophilic property of the UiO-67 nanoparticles and significantly enhanced the colloidal stability and long-term dispersity in both non-polar solvent and base *** adding UiO-67@PLMA nanoparticles into the 500 SN base oil,coefficient of friction and wear volume reductions of 45.3%and 75.5%were achieved due to their excellent mechanical properties and oil ***,the load-carrying capacity of 500 SN was greatly increased from 100 to 500 N by the UiO-67@PLMA additives,and their excellent tribological performance was demonstrated even at a high friction frequency of 65 Hz and high temperature of 120℃.Our work highlights oil-soluble polymer brushes-functionalized nanoMOFs for highly efficient lubricating additives.

关键词： MOFs polymer brushes surface modification tribological properties friction reduction anti-wear

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Influence of different rolling processes on microstructure and strength of the Al–Cu–Li alloy AA2195

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Progress in Natural Science:materials International 2022年第1期32卷 87-95页

作者： Fan Ye Ling Mao Jian Rong Baoshuai Zhang Lijun Wei Sihan Wen Haojun Jiao Sujun Wu International Research Center for Advanced Structural and Biomaterials School of Materials Science and Engineering Beihang University School of Materials Science and Engineering Beihang University Aerospace Research Institute of Materials & Processing Technology

The influence of different rolling processes on precipitation behaviour, crystallography texture, grain morphology,and their consequent effects on tensile properties for Al–Cu–Li alloy AA2195 was investigated in the present *** H-T8 samples(hot rolled + T8) presented better tensile strength and ductility(with serious strength anisotropy) than the HC-T8 samples(hot rolled + cold rolled + T8), due to their different microstructures and textures. The higher dislocation density was found in the H-T8 samples, which promoted the nucleation of main strengthening phase T1in the matrix and suppressed the grain boundary precipitation, resulted in better strength and ductility. The increase of the dynamic recovery(DRV) during hot rolling enhanced the generation of Brass texture, and brought serious strength anisotropy. The cold rolling was performed after the hot-rolling process for the HC-T8 samples which increased deformation energy and resulted in full recrystallization of the deformed microstructure during the following solution treatment. The formation of recrystallized microstructure reduced the dislocation density and the heterogeneous precipitate nucleation positions which limited the strengthening phase precipitation in matrix and accelerated the precipitation along grain boundaries, resulted in fewer T1precipitates, coarse grain-boundary precipitates(GBPs), and wider precipitate-free zones(PFZs). The localized strain may be concentrated on the grain boundary to induce the dislocation pile-up, breaking of the GBPs, and intergranular fracture during stretching.

关键词： Al-Cu-Li alloys Rolling Mechanical properties Microstructure evolution Fracture

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Air plasma-sprayed high-entropy (Y_(0.2)Yb_(0.2)Lu_(0.2)Eu_(0.2)Er_(0.2))_(3)Al_(5)O_(12) coating with high thermal protection performance

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Journal of advanced Ceramics 2022年第10期11卷 1571-1582页

作者： Kailun WANG Jinpeng ZHU Hailong WANG Kaijun YANG Yameng ZHU Yubin QING Zhuang MA Lihong GAO Yanbo LIU Sihao WEI Yongchun SHU Yanchun ZHOU Jilin HE School of Material Science and Engineering Zhengzhou UniversityZhengzhou 450001China National Key Laboratory of Science and Technology on Materials under Shock and Impact School of Materials Science and EngineeringBeijing Institute of TechnologyBeijing 100081China Beijing Institute of Technology Chongqing Innovation Center Chongqing 401120China Aerospace Research Institute of Materials&Processing Technology Beijing 100076China

High-entropy rare-earth aluminate(Y_(0.2)Yb_(0.2)Lu_(0.2)Eu_(0.2)Er_(0.2))_(3)Al_(5)O_(12)(HE-RE_(3)Al_(5)O_(12))has been considered as a promising thermal protection coating(TPC)material based on its low thermal conductivity and close thermal expansion coefficient to that of ***,such a coating has not been experimentally prepared,and its thermal protection performance has not been *** prove the feasibility of utilizing HE-RE_(3)Al_(5)O_(12) as a TPC,HE-RE_(3)Al_(5)O_(12) coating was deposited on a nickelbased superalloy for the first time using the atmospheric plasma spraying *** stability,surface,and cross-sectional morphologies,as well as the fracture surface of the HE-RE_(3)Al_(5)O_(12) coating were investigated,and the thermal shock resistance was evaluated using the oxyacetylene flame *** results show that the HE-RE_(3)Al_(5)O_(12) coating can remain intact after 50 cycles at 1200℃ for 200 s,while the edge peeling phenomenon occurs after 10 cycles at 1400℃ for 200 *** study clearly demonstrates that HE-RE_(3)Al_(5)O_(12) coating is effective for protecting the nickel-based superalloy,and the atmospheric plasma spraying is a suitable method for preparing this kind of coatings.

关键词： high-entropy ceramics thermal protection coating(TPC) (Y_(0.2)Yb_(0.2)Lu_(0.2)Eu_(0.2)Er_(0.2))_(3)Al_(5)O_(12)(HE-RE_(3)Al_(5)O_(12)) air plasma spraying thermal protection performance

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Effect of densification process on mechanical enhancement of graphene laminates

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Nano materials Science 2025年第2期 240-248页

作者： Yue Zhu Yalong Liao Meng Wang Jingxin Dai Chaoshuai Lei Xiaobo Liu Pengyu Mu Wenjing Li Hao Zhang Aerospace Institute of Advanced Material & Processing Technology Academy of Deep Earth Sciences China Coal Research Institute

Graphene nanosheets have attracted great attention in the field of nanotechnology applications due to their extraordinary mechanical properties. While the structural defects such as gaps will occur during the preparation of graphene laminates, which will greatly damage the performance of the macroscopic material. Hence, a simple and promising mechanical compression method is used to improve the mechanical properties of graphene laminates. However, the roles of the densification process in the mechanical enhancement mechanism of graphene laminates are not clear. In our work, the mechanical enhancement of the compressed graphene (PG) laminates was investigated by the coarse-grained molecular dynamics simulation method. The tensile strength of PG model could be increased by increasing the graphene nanosheet size and the degree of compression in the system. And the model has the stronger van der Waals effect between graphene sheets due to the larger graphene size as well as the higher overlap ratio. Furthermore, two kinds of PG laminates were prepared by densification method, and the tensile strength was consistent with the upward trend of the PG model. This work provides an in-depth understanding on the mechanical enhancement of the densification process and lays a foundation for the future practical application of graphene laminates.

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Medium-entropy(Me,Ti)_(0.1)(Zr,Hf,Ce)_(0.9)O_(2)(Me=Y and Ta):Promising thermal barrier materials for high-temperature thermal radiation shielding and CMAS blocking

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Journal of materials Science & technology 2022年第28期123卷 144-153页

作者： Shuaihang Qiu Huimin Xiang Fu-Zhi Dai Hailong Wang Muzhang Huang Chunlei Wan Qing Meng Jiangtao Li Xiaohui Wang Yanchun Zhou Science and Technology on Advanced Functional Composite Laboratory Aerospace Research Institute of Materials and Processing TechnologyBeijing 100076China State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of TechnologyWuhan 430070China School of Materials Science and Engineering Zhengzhou UniversityZhengzhou 450001China State Key Lab of New Ceramics and Fine Processing School of Materials Science and EngineeringTsinghua UniversityBeijing 100084China Technical Institute of Physics and Chemistry Chinese Academy of SciencesBeijing 100190China Institute of Metal Research Chinese Academy of SciencesShenyang 110016China

With continuous enhancement of gas-turbine inlet temperature and rapid increase of radiant heat transfer,thermal barrier coating(TBC)materials with a combination of low thermal conductivity and good high-temperature thermal radiation shielding performance play vital roles in ensuring the durability of metallic ***,yttria-stabilized zirconia(YSZ),as the state-of-the-art TBC and current industry standard,is unable to meet such demands since it is almost translucent to high-temperature thermal ***,poor corrosion resistance of YSZ to molten calcia-magnesia-alumina-silicates(CMAS)also impedes its application in sand,dust,or volcanic ash laden *** order to improve the hightemperature thermal radiation shielding performance and CMAS resistance of YSZ and further reduce its thermal conductivity,two medium-entropy(ME)oxide ceramics,ME(Y,Ti)_(0.1)(Zr,Hf,Ce)_(0.9)O_(2)and ME(Ta,Ti)_(0.1)(Zr,Hf,Ce)_(0.9)O_(2),were designed and prepared by pressureless sintering of binary powder compacts in this ***(Y,Ti)_(0.1)(Zr,Hf,Ce)_(0.9)O_(2)presents cubic structure but a trace amount of secondary phase,while ME(Ta,Ti)_(0.1)(Zr,Hf,Ce)_(0.9)O_(2)displays a combination of tetragonal phase(81.6 wt.%)and cubic phase(18.4 wt.%).Both ME(Y,Ti)_(0.1)(Zr,Hf,Ce)_(0.9)O_(2)and ME(Ta,Ti)_(0.1)(Zr,Hf,Ce)_(0.9)O_(2)possess better high-temperature thermal radiation shielding performance than ***,the high-temperature thermal radiation shielding performance of ME(Ta,Ti)_(0.1)(Zr,Hf,Ce)_(0.9)O_(2)is superior to that of ME(Y,Ti)_(0.1)(Zr,Hf,Ce)_(0.9)O_(2)due to its narrower band gap and correspondingly higher infrared absorbance(above 0.7)at the waveband of 1 to 5μ*** two ME oxides also display significantly lower thermal conductivity than YSZ and close thermal expansion coefficients(TECs)to YSZ and Ni-based *** addition,the two ME oxides possess excellent CMAS *** attack by molten CMAS at 1250℃for 4 h,merely~2μm thick penetration

关键词： Medium-entropy ceramics Thermal barrier coatings Thermal radiation shielding CMAS resistance Infrared absorbance

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