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Phosphotungstic acid (H₃PW₁₂O₄₀)-loaded onto titanium porous montmorillonite heterostructure for the effective enhanced kinetics and thermodynamic conversion of citronellal

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Case Studies in Chemical and Environmental engineering 2025年 11卷

作者： Fatimah, Is Yahya, Amri Rubiyanto, Dwiarso Sagadevan, Suresh Oh, Won-Chun Doong, Ruey-an Department of Chemistry Faculty of Mathematics and Natural Sciences Universitas Islam Indonesia Kampus Terpadu UII Jl. Kaliurang Km 14 Sleman Yogyakarta Indonesia Nanomaterials and Sustainable Chemistry Research Centre Chemistry Laboratory Universitas Islam Indonesia Kampus Terpadu UII Jl. Kaliurang Km 14 Sleman Yogyakarta Indonesia Chemistry Study Program Nusa Bangsa University JL. KH Sholeh Iskandar KM.4 Tanah Sareal Bogor 16166 Indonesia Nanotechnology & Catalysis Research Centre University of Malaya Kuala Lumpur 50603 Malaysia Department of Advanced Materials Science and Engineering Hanseo University Seosan-si 356-706 South Korea Institute of Analytical and Environmental Sciences National Tsing Hua University 101 Sec 2 Kuang Fu Road Hsinchu 30013 Taiwan

In present work, nanocomposite of phosphotungstic acid (H3PW12O40)-loaded onto titanium-porous clay heterostructure (PTA/Ti–PCH) was prepared using natural montmorillonite as parent material (Mnt). Characterization o... 详细信息

In present work, nanocomposite of phosphotungstic acid (H₃PW₁₂O₄₀)-loaded onto titanium-porous clay heterostructure (PTA/Ti–PCH) was prepared using natural montmorillonite as parent material (Mnt). Characterization of the material was performed using X-ray diffraction, X-ray photoelectron spectroscopy, scanning electron microscopy-energy dispersive X-ray fluorescence, transmission electron microscopy, Fourier-Transform Infra-Red spectroscopy, and solid acidity measurement. The material was examined as superacid catalyst in citronellal conversion into isopulegol by varied reaction conditions. Kinetics and thermodynamic studies of catalyzed reaction revealed the role of increased total surface acidity and the Lewis to Brønsted to enhance the reaction conversion and selectivity. Thermodynamic study demonstrated a lower activation energy of the reaction over PTA/Ti–PCH compared to Ti–PCH. A 100 % conversion was exhibited by the sample during 120 min of the reaction at 90°C, and the sample also demonstrated activity at room temperature. Reusability of the sample was expressed by a maintained conversion until 5th cycle. Conclusively, the prepared material showed a potency to be developed for heterogeneously acid-catalyzed organic reactions. © 2025 The Authors

关键词： Acid Citronellal Clay-based nanocomposite Heterogeneous catalysis Porous clay heterostructure

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Nonreciprocal transport in a bilayer of MnBi2Te4 and Pt

arXiv

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arXiv 2022年

作者： Ye, Chen Xie, Xiangnan Lv, Wenxing Huang, Ke Yang, Allen Jian Jiang, Sicong Liu, Xue Zhu, Dapeng Qiu, Xuepeng Tong, Mingyu Zhou, Tong Hsu, Chuang-Han Chang, Guoqing Lin, Hsin Li, Peisen Yang, Kesong Wang, Zhenyu Jiang, Tian Wang, Xiao Renshaw Division of Physics and Applied Physics School of Physical and Mathematical Sciences Nanyang Technological University 21 Nanyang Link 637371 Singapore State Key Laboratory of High Performance Computing College of Computer Science and Technology National University of Defense Technology Changsha410073 China Physics Laboratory Industrial Training Center Shenzhen Polytechnic Guangdong Shenzhen518055 China Department of NanoEngineering Program of Chemical Engineering University of California La Jolla San DiegoCA92093-0448 United States Program of Materials Science and Engineering University of California La Jolla San DiegoCA92093-0418 United States Institutes of Physical Science and Information Technology Anhui University Hefei230601 China Fert Beijing Institute MIIT Key Laboratory of Spintronics School of Integrated Circuit Science and Engineering Beihang University Beijing100191 China Beihang-Goertek Joint Microelectronics Institute Qingdao Research Institute Beihang University Qingdao266000 China Shanghai Key Laboratory of Special Artificial Microstructure Materials and Technology School of Physics Science and Engineering Tongji University Shanghai200092 China College of Advanced Interdisciplinary Studies National University of Defense Technology Changsha410073 China Insitute of Physics Academia Sinica Taipei115229 Taiwan College of Intelligence Science and Technology National University of Defense Technology Changsha410073 China National Innovation Institute of Defense Technology Academy of Military Sciences PLA China Beijing100010 China Beijing Academy of Quantum Information Sciences Beijing100084 China Beijing Institute for Advanced Study National University of Defense Technology Changsha410073 China School of Electrical and Electronic Engineering Nanyang Technological University 50 Nanyang Ave 639798 Singapore

MnBi2Te4 (MBT) is the first intrinsic magnetic topological insulator with the interaction of spin-momentum locked surface electrons and intrinsic magnetism, and it exhibits novel magnetic and topological phenomena. Recent studies suggested that the interaction of electrons and magnetism can be affected by the Mn-doped Bi2Te3 phase at the surface due to inevitable structural defects. Here we report an observation of nonreciprocal transport, i.e. current-direction-dependent resistance, in a bilayer composed of antiferromagnetic MBT and nonmagnetic Pt. The emergence of the nonreciprocal response below the Néel temperature confirms a correlation between nonreciprocity and intrinsic magnetism in the surface state of MBT. The angular dependence of the nonreciprocal transport indicates that nonreciprocal response originates from the asymmetry scattering of electrons at the surface of MBT mediated by magnon. Our work provides an insight into nonreciprocity arising from the correlation between magnetism and Dirac surface electrons in intrinsic magnetic topological insulators. © 2022, CC BY.

关键词： Magnetism

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Numerical Simulation on Effects of TCO Work Function on Performance of a-Si:H Solar Cells 4th

Numerical Simulation on Effects of TCO Work Function on Perf...

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4th International Conference on Functional materials science, ICFMS 2018

作者： Sholih, Ahmad Hamdani, Dadan Wicaksono, Sigit Tri Hidayat, Mas Irfan Purbawanto Cahyono, Yoyok Darminto Advanced Materials Research Group Department of Physics Institut Teknologi Sepuluh Nopember Kampus ITS Sukolilo Surabaya60111 Indonesia Department of Materials and Metallurgical Engineering Institut Teknologi Sepuluh Nopember Kampus ITS Sukolilo Surabaya60111 Indonesia Physics Study Program Faculty of Mathematics and Natural Science Universitas Mulawarman Samarinda Indonesia

ISBN: (纸本)9783035714968

In this paper, we have investigated the effect of the work function of transparent conducting oxides (TCO) on the performance of a-Si:H p-i-n solar cells, including open circuit voltage (VOC), short circuit current (JSC), fill factor (FF) and conversion efficiency, using AFORS-HET software. The simulation has focused on two layers: front contact work function (ΦTCO-front) and back contact work function (ΦTCO-back) with various band energy gap from 4.7 eV to 5.3 eV and 4.2 eV to 4.9 eV respectively. From the simulation results, we know that the work function of TCO greatly affects the performance of solar cells such as Voc, Jsc, FF and conversion efficiency. By optimization, we arrive at results of Voc, Jsc, FF and conversion efficiencies of 0.88 V, 8.95 mA / cm2, 65% and 5.1% respectively, by using ΦTCO-front of 5.2 eV. When ΦTCO-front > 5.2 eV, the values of VOC, FF and conversion efficiency have been saturated, while the value of the J sc actually begins to decrease. Furthermore, when the ΦTCO-back is 4.3 eV, we get the best results for VOC, Jsc, FF and conversion Efficiency of 0.9 V, 8.96 mA / cm2, 73 % and 5.9 % respectively. When ΦTCO-back > 4.3 eV, the values of VOC, FF and conversion efficiency begin to decrease, while the value of the Jsc does not change significantly. These optimizations may help for producing low cost high efficiency p-i-n solar cells experimentally. © 2019 Trans Tech Publications Ltd, Switzerland.

关键词： Work function

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Photoluminescence of oxygen vacancy-rich nano-TiO2 photocatalyst for methylene blue color degradation

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materials science and engineering: B 2025年 320卷

作者： Simanjuntak, Mayer Made Joni, I. Faizal, Ferry Gultom, Noto Susanto Kuo, Dong-Hau Panatarani, Camellia Department of Physics Faculty of Mathematic and Natural Sciences Universitas Padjadjaran Jl. Raya Bandung-Sumedang KM 21 Jatinangor Sumedang45363 Indonesia Study Program of Biotechnology Faculty of Graduate School Universitas Padjadjaran Jl. Dipati Ukur No.35 Coblong Bandung40132 Indonesia Functional Nano Powder University Center of Excellence Universitas Padjadjaran Jl. Raya Bandung-Sumedang KM 21 Jatinangor Sumedang45363 Indonesia Department of Materials Science and Engineering National Taiwan University of Science and Technology No.43 Sec. 4 Keelung Road Taipei10607 Taiwan

Wastewater containing synthetic dyes poses a critical environmental hazard, necessitating the development of effective treatment techniques. Despite its promise as a photocatalyst, TiO2′s inability to efficiently absorb visible light limits its practical use. To overcome this limitation, oxygen vacancy (OV) engineering was carried out in TiO2 through solvothermal at temperatures of 150°C, 180°C, and 210°C. Comprehensive analyses confirmed a temperature-induced increase in crystallinity and OV concentration. Furthermore, photoluminescence analysis revealed mid-gap states that improve visible light absorption. Notably, the T150 sample achieved 93.43% degradation of methylene blue within 3 h under sunlight, outperforming commercial TiO2. The superior performance was attributed to a reduced bandgap energy, enhanced charge carrier separation, and increased generation of reactive oxygen species, all facilitated by an optimal concentration of OV. This study clarifies the interaction between photoluminescence and photocatalytic activity, highlighting OV engineering as a highly effective strategy for developing advanced TiO2-based materials for wastewater treatment. © 2025 Elsevier B.V.

关键词： Photocatalytic activity

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The Japanese Vision for the Black Hole Explorer Mission

arXiv

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arXiv 2024年

作者： Akiyama, Kazunori Niinuma, Kotaro Hada, Kazuhiro Doi, Akihiro Hagiwara, Yoshiaki Higuchi, Aya E. Honma, Mareki Kawashima, Tomohisa Kolev, Dimitar Koyama, Shoko Masui, Sho Ohsuga, Ken Sano, Hidetoshi Takami, Hideki Tsunetoe, Yuh Uzawa, Yoshinori Akahori, Takuya Akiyama, Yuto Galison, Peter Hayashi, Takayuki J. Hirota, Tomoya Inoue, Makoto Iwata, Yuhei Johnson, Michael D. Kino, Motoki Kofuji, Yutaro Mizuno, Yosuke Moriyama, Kotaro Nagai, Hiroshi Nakamura, Kenta Notsu, Shota Ono, Fumie Oya, Yoko Oyama, Tomoaki Rana, Hannah Saida, Hiromi Saito, Ryo Saito, Yoshihiko Sasada, Mahito Sawada-Satoh, Satoko Takahashi, Mikiya M. Takamura, Mieko Tong, Edward Tsuji, Hiroyuki Yoshioka, Shogo Watanabe, Yoshimasa Massachusetts Institute of Technology Haystack Observatory WestfordMA01886 United States Mizusawa VLBI Observatory National Astronomical Observatory of Japan Iwate023-0861 Japan Black Hole Initiative Harvard University CambridgeMA02138 United States Graduate School of Sciences and Technology for Innovation Yamaguchi University Yamaguchi753-8512 Japan The Graduate School of Science Nagoya City University Aichi467-0001 Japan Institute of Space and Astronautical Science Japan Aerospace Exploration Agency Kanagawa252-5210 Japan Department of Space and Astronautical Science The Graduate University for Advanced Studies SOKENDAI Kanagawa229-8510 Japan Natural Science Laboratory Toyo University Tokyo112-8606 Japan Division of Science School of Science and Engineering Tokyo Denki University Saitama350-0394 Japan Department of Astronomy Graduate School of Science The University of Tokyo Tokyo113-0033 Japan Institute for Cosmic Ray Research The University of Tokyo Chiba277-8582 Japan Space Communication Systems Laboratory Wireless Networks Research Center National Institute of Information and Communications Technology Tokyo184-8795 Japan Graduate School of Science and Technology Niigata University Niigata950-2181 Japan Advanced Technology Center National Astronomical Observatory of Japan Tokyo181-8588 Japan Center for Computational Sciences University of Tsukuba Ibaraki305-8577 Japan Faculty of Engineering Gifu University Gifu501-1193 Japan Harvard University CambridgeMA02138 United States Azabu Junior and Senior High School Tokyo106-0046 Japan Astronomical Science Program The Graduate University for Advanced Studies SOKENDAI Tokyo181-8588 Japan Institute of Astronomy and Astrophysics Academia Sinica Taipei10617 Taiwan Center for Astrophysics Harvard & Smithsonian CambridgeMA02138 United States Kogakuin University of Technology & Engineering Academic Support Center 2665-1 Nakano Hachioji Tokyo192-0015 Japan Tsung-Dao Lee Institut

The Black Hole Explorer (BHEX) is a next-generation space very long baseline interferometry (VLBI) mission concept that will extend the ground-based millimeter/submillimeter arrays into space. The mission, closely aligned with the science priorities of the Japanese VLBI community, involves an active engagement of this community in the development of the mission, resulting in the formation of the Black Hole Explorer Japan Consortium. Here we present the current Japanese vision for the mission, ranging from scientific objectives to instrumentation. The Consortium anticipates a wide range of scientific investigations, from diverse black hole physics and astrophysics studied through the primary VLBI mode, to the molecular universe explored via a potential single-dish observation mode in the previously unexplored 50-70 GHz band that would make BHEX the highest-sensitivity explorer ever of molecular oxygen. A potential major contribution for the onboard instrument involves supplying essential elements for its high-sensitivity dual-band receiving system, which includes a broadband 300 GHz SIS mixer and a space-certified multi-stage 4.5K cryocooler akin to those used in the Hitomi and XRISM satellites by the Japan Aerospace Exploration Agency. Additionally, the Consortium explores enhancing and supporting BHEX operations through the use of millimeter/submillimeter facilities developed by the National Astronomical Observatory of Japan, coupled with a network of laser communication stations operated by the National Institute of Information and Communication Technology. Copyright © 2024, The Authors. All rights reserved.

关键词： Radio astronomy

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Front Cover: Pyromellitic-Diimide-Based Liquid Material Forming an Exciplex with Naphthalene (ChemPhotoChem 6/2023)

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ChemPhotoChem 2023年第6期7卷

作者： Yuya Tanabe Hiroki Tsutsui Dr. Shinya Matsuda Dr. So Shikita Prof. Takuma Yasuda Dr. Kyosuke Isoda Program in Advanced Materials Science Faculty of Engineering and Design Kagawa University 2217-20 Hayashi-cho Takamatsu Kagawa 761-0396 Japan Department of Applied Chemistry Graduate School of Engineering Kyushu University 744 Motooka Nishi-ku Fukuoka 819-0395 Japan Institute for Advanced Study Kyushu University 744 Motooka Nishi-ku Fukuoka 819-0395 Japan Health Research Institute National Institute of Advanced Industrial Science and Technology (AIST) 2217-14 Hayashi-cho Takamatsu Kagawa 761-0395 Japan Organic Materials Chemistry Group Sagami Chemical Research Institute 2743-1 Hayakawa Ayase Kanagawa 252-1193 Japan

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Critical pore radius and transport properties of disordered hard- And overlapping-sphere models

arXiv

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arXiv 2021年

作者： Klatt, Michael A. Ziff, Robert M. Torquato, Salvatore Department of Physics Princeton University PrincetonNJ08544 United States Institut für Theoretische Physik FAU Erlangen-Nürnberg Staudtstr. 7 Erlangen91058 Germany Center for the Study of Complex Systems Department of Chemical Engineering University of Michigan Ann ArborMI48109 United States Department of Physics Princeton University PrincetonNJ08544 United States Department of Chemistry Princeton Institute for the Science and Technology of Materials Program in Applied and Computational Mathematics Princeton University PrincetonNJ08544 United States

Transport properties of porous media are intimately linked to their pore-space microstructures. We quantify geometrical and topological descriptors of the pore space of certain disordered and ordered distributions of spheres, including pore-size functions and the critical pore radius δc. We focus on models of porous media derived from maximally random jammed sphere packings, overlapping spheres, equilibrium hard spheres, "quantizer" sphere packings, and crystalline sphere packings. For precise estimates of the percolation thresholds, we use a strict relation of the void percolation around sphere configurations to weighted bond percolation on the corresponding Voronoi networks. We use the Newman-Ziff algorithm to determine the percolation threshold using universal properties of the cluster size distribution. The critical pore radius δc is often used as the key characteristic length scale that determines the fluid permeability k. A recent study [Torquato. Adv. Wat. Resour. 140,103565 (2020)] suggested for porous media with a well-connected pore space an alternative estimate of k based on the second moment of the pore size hδ2i, which is easier to determine than δc. Here, we compare δc to the second moment of the pore size hδ2i, and indeed confirm that, for all porosities and all models considered, δc2 is to a good approximation proportional to hδ2i. However, unlike hδ2i, the permeability estimate based on δc2 does not predict the correct ranking of k for our models. Thus, we confirm hδ2i to be a promising candidate for convenient and reliable estimates of the fluid permeability for porous media with a well-connected pore space. Moreover, we compare the fluid permeability of our models with varying degrees of order, as measured by the τ order metric. We find that (effectively) hyperuniform models tend to have lower values of k than their nonhyperuniform counterparts. Our findings could facilitate the design of porous media with desirable transport properties via target

关键词： Porous materials

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Roadmap on Nonlocality in Photonic materials and Metamaterials

arXiv

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arXiv 2025年

作者： Monticone, Francesco Mortensen, N. Asger Fernández-Domínguez, Antonio I. Luo, Yu Tserkezis, Christos Khurgin, Jacob B. Shahbazyan, Tigran V. Chaves, André J. Peres, Nuno M.R. Wegner, Gino Busch, Kurt Hu, Huatian della Sala, Fabio Zhang, Pu Ciracì, Cristian Aizpurua, Javier Babaze, Antton Borisov, Andrei G. Chen, Xue-Wen Christensen, Thomas Yan, Wei Yang, Yi Hohenester, Ulrich Huber, Lorenz Wubs, Martijn de Liberato, Simone Gonçalves, P.A.D. de Abajo, F. Javier García Hess, Ortwin Tarasenko, Illya Cox, Joel D. Jelver, Line Dias, Eduardo J.C. Sánchez, Miguel Sánchez Margetis, Dionisios Gómez-Santos, Guillermo Stauber, Tobias Tretyakov, Sergei Simovski, Constantin Pakniyat, Samaneh Gómez-Díaz, J. Sebastián Bondarev, Igor V. Biehs, Svend-Age Boltasseva, Alexandra Shalaev, Vladimir M. Krasavin, Alexey V. Zayats, Anatoly V. Alù, Andrea Song, Jung-Hwan Brongersma, Mark L. Levy, Uriel Long, Olivia Y. Guo, Cheng Fan, Shanhui Bozhevolnyi, Sergey I. Overvig, Adam Prudêncio, Filipa R. Silveirinha, Mário G. Gangaraj, S. Ali Hassani Argyropoulos, Christos Huidobro, Paloma A. Galiffi, Emanuele Yang, Fan Pendry, John B. Miller, David A.B. School of Electrical and Computer Engineering Cornell University IthacaNY14853 United States POLIMA Center for Polariton-driven Light–Matter Interactions University of Southern Denmark Campusvej 55 Odense MDK-5230 Denmark D-IAS—Danish Institute for Advanced Study University of Southern Denmark Campusvej 55 Odense MDK-5230 Denmark Departamento de Física Teórica de la Materia Condensada Universidad Autónoma de Madrid MadridE-28049 Spain Universidad Autónoma de Madrid MadridE-28049 Spain School of Electrical and Electronic Engineering Nanyang Technological University Singapore639798 Singapore Key Laboratory of Radar Imaging and Microwave Photonics Ministry of Education College of Electronic and Information Engineering Nanjing University of Aeronautics and Astronautics Nanjing211106 China Department of Electrical and Computer Engineering Johns Hopkins University BaltimoreMD21218 United States Department of Physics Jackson State University JacksonMS39217 United States Department of Physics Aeronautics Institute of Technology SP So Jos dos Campos12228-900 Brazil Departamento de Física Universidade do Minho BragaP-4710-057 Portugal Av Mestre José Veiga Braga4715-330 Portugal Max-Born-Institut Berlin12489 Germany Humboldt-Universität zu Berlin Institut für Physik AG Theoretische Optik and Photonik Berlin12489 Germany Center for Biomolecular Nanotechnologies Istituto Italiano di Tecnologia Via Barsanti 14 Arnesano73010 Italy Via Monteroni Campus Unisalento Lecce73100 Italy School of physics Huazhong University of Science and Technology Luoyu Road 1037 Wuhan430074 China Donostia International Physics Center DIPC Donostia-San Sebastián20018 Spain Ikerbasque Basque Foundation for Science Bilbao48009 Spain Department of Electricity and Electronics University of the Basque Country Leioa48940 Spain Department of Applied Physics University of the Basque Country Donostia20018 Spain Université Paris-Saclay CNRS Institut des Scienc

Photonic technologies continue to drive the quest for new optical materials with unprecedented responses. A major frontier in this field is the exploration of nonlocal (spatially dispersive) materials, going beyond the local, wavevector-independent assumption traditionally made in optical material modeling. On one end, the growing interest in plasmonic, polaritonic and quantum materials has revealed naturally occurring nonlocalities, emphasizing the need for more accurate models to predict and design their optical responses. This has major implications also for topological, nonreciprocal, and time-varying systems based on these material platforms. Beyond natural materials, artificially structured materials—metamaterials and metasurfaces–can provide even stronger and engineered nonlocal effects, emerging from long-range interactions or multipolar effects. This is a rapidly expanding area in the field of photonic metamaterials, with open frontiers yet to be explored. In the case of metasurfaces, in particular, nonlocality engineering has become a powerful tool for designing strongly wavevector-dependent responses, enabling enhanced wavefront control, spatial compression, multifunctional devices, and wave-based computing. Furthermore, nonlocality and related concepts play a critical role in defining the ultimate limits of what is possible in optics, photonics, and wave physics. This Roadmap aims to survey the most exciting developments in nonlocal photonic materials, highlight new opportunities and open challenges, and chart new pathways that will drive this emerging field forward–toward new scientific discoveries and technological advancements. Copyright © 2025, The Authors. All rights reserved.

关键词： Nanocrystals

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Parameter processes and their impact on Tinospora cordifolia stem extracts for antibacterial and antioxidant materials

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materials Today: Proceedings 2023年

作者： Ahmad Royani Muhammad Hanafi Puspa Dewi N. Lotulung Muhammad Eka Prastya Chandrabhan Verma Akram Alfantazi Azwar Manaf Postgraduate Program of Materials Science Study Department of Physics Faculty of Mathematics and Natural Sciences Universitas Indonesia Depok 16424 Indonesia Research Center for Metallurgy National Research and Innovation Agency (BRIN) Tangerang Selatan Banten 15314 Indonesia Research Center for Pharmaceutical Ingredients and Traditional Medicine National Research and Innovation Agency (BRIN) Tangerang Selatan Banten 15314 Indonesia Research Center for Chemistry National Research and Innovation Agency (BRIN) Tangerang Selatan Banten 15314 Indonesia Department of Chemical Engineering Khalifa University of Science and Technology P. O. Box 127788 Abu Dhabi United Arab Emirates

This work extracted the Tinospora cordifolia stem for antibacterial and antioxidant materials. The stems of T. cordifolia were extracted by using a simple maceration method. The effect of three independent variables (solvent ratios, temperature, and extraction time) was investigated to obtain optimal conditions. Ten grams of T. cordifolia were extracted using a mixture of methanol–water ratios 00:100, 15:85, 30:70, and 45:55 (% v/v) at 50–95 °C for 0.5 to 3 h. The total phenolic and flavonoid content in the T. cordifolia extracts was analyzed by Folin-Ciocalteu and Colorimetric-AlCl 3 methods. The antibacterial activities against Pseudomonas aeruginosa were assessed by serial dilution methods, and antioxidant properties were performed by DPPH methods. The optimum condition was achieved at methanol–water ratios of 00:100 % (v/v) at 95 °C for 2 h. The yield extraction for this condition is around 13.97%. The total phenolic and flavonoid contents for these conditions are about 6.85% and 7.07%, respectively. The minimum inhibitory concentration value against P. aeruginosa is 1024 µg/mL, and the minimum bacterial concentration is above 2048 µg/mL. Meanwhile, the antioxidant obtained is 217.55 µg/mL at a ratio of 00:100 methanol–water. The extraction process parameters significantly influenced the phytochemical (TPC and TFC), antibacterial activity, and antioxidant properties of T. cordifolia stem extracts. This work clearly shows the antibacterial potential of T. cordifolia stem extracts, suggesting that more investigation is required to isolate the bioactive compounds in this extract.

关键词： Antibacterial Antioxidant Maceration Parameter effect P. aeruginosa T. cordifolia

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Calcium release and physical properties of modified carbonate apatite cement as pulp capping agent in dental application

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Biomaterials Research 2018年第1期22卷 346-351页

作者： Zakaria, Myrna Nurlatifah Cahyanto, Arief El-Ghannam, Ahmed Department of Endodontology and Operative Dentistry Program Study of Dentistry Faculty of Medicine Universitas Jenderal Achmad Yani Cimahi Indonesia Department of Dental Materials Science and Technology Faculty of Dentistry Universitas Padjadjaran Sumedang-Jatinangor Indonesia Department of Mechanical Engineering and Engineering Science The University of North Carolina at Charlotte Charlotte NC United States

Background: Carbonate apatite (CO3Ap) and silica-calcium phosphate composite (SCPC) are bone substitutes with good prospect for dental application. SCPC creates a hydroxyapatite surface layer and stimulate bone cell f... 详细信息

Background: Carbonate apatite (CO₃Ap) and silica-calcium phosphate composite (SCPC) are bone substitutes with good prospect for dental application. SCPC creates a hydroxyapatite surface layer and stimulate bone cell function while, CO₃Ap induce apatite crystal formation with good adaptation providing good seal between cement and the bone. Together, these materials will add favorable properties as a pulp capping material to stimulate mineral barrier and maintain pulp vitality. The aim of this study is to investigate modification of CO₃Ap cement combined with SCPC, later term as CO₃Ap-SCPC cement (CAS) in means of its chemical (Calcium release) and physical properties (setting time, DTS and pH value). Methods: The study consist of three groups;group 1 (100% calcium hydroxide, group 2 CO₃Ap (60% DCPA: 40% vaterite, and group 3 CAS (60% DCPA: 20% vaterite: 20% SCPC. Distilled water was employed as a solution for group 1, and 0.2 mol/L Na₃PO₄ used for group 2 and group 3. Samples were evaluated with respect to important properties for pulp capping application such as pH, setting time, mechanical strength and calcium release evaluation. Results: The fastest setting time was in CO₃Ap cement group without SCPC, while the addition of 20% SCPC slightly increase the pH value but did not improved the cement mechanical strength, however, the mechanical strength of both CO₃Ap groups were significantly higher than calcium hydroxide. All three groups released calcium ions and had alkaline pH. Highest pH level, as well as calcium released level, was in the control group. Conclusion: The CAS cement had good mechanical and acceptable chemical properties for pulp capping application compared to calcium hydroxide as a gold standard. However, improvements and in vivo studies are to be carried out with the further development of this material. © The Author(s).

关键词： Carbonate apatite CO3Ap-SCPC cement Pulp capping Silica-calcium phosphate composite

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