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8th International Conference on Nanostructures, Nanomaterials and Nanoengineering, ICNNN 2019 and 4th International Conference on Materials Technology and Applications, ICMTA 2019

作者： Ngamthanacom, Nutchaporn Kaewtrakulchai, Napat Chaiwat, Weerawut Chuenchom, Laemthong Fuji, Masayoshi Eiad-Ua, Apiluck College of Nanotechnology King Mongkut’s Institute of Technology Bangkok10520 Thailand Environmental Engineering and Disaster Management Program Mahidol University Kanchanaburi Campus Sai yok Kanchanaburi71150 Thailand Department of Chemistry Faculty of Science Prince of Songkhla University Songkhla90112 Thailand Advanced Ceramic Research Center Nagoya Institute of Technology Gifu Tajimi507-0033 Japan

ISBN: (纸本)9783035715873

Waste lignin (WL) from the pulp mill and paper was studied for its potential application to prepare the nanoporous carbon with high porosity via carbonization assisted acid activation. The effect of acid activation such as HNO3, HCl, H2SO4, and H3PO4 on lignin transformation to nanoporous carbon investigated. The physicochemical properties of nanoporous carbon were comprehensively characterized through N2 sorption, Scanning electron microscope (SEM), X-ray diffraction (XRD), and Fourier transform infrared (FTIR), respectively. N2 sorption revealed that the condition using 5% vol of phosphoric acid activation at carbonization temperature of 700°C for 2 h exhibited the highly porous structure of carbon nanoparticles with a total pore volume of 0.035 cm3 /g. With the properly selecting process variables of waste lignin development could be producing high porosity nanoporous carbon. © 2020 Trans Tech Publications Ltd, Switzerland.

关键词： Carbonization

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Influence of acid-treatment on waste lignin for synthesis of carbon nanoparticles 13th

Influence of acid-treatment on waste lignin for synthesis of...

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13th Pure and Applied Chemistry International Conference, PACCON 2019

ISBN: (纸本)9783035715521

Waste lignin (WL) obtained from paper mills, was studied for its potential application in preparing carbon nanoparticles (CNPs) with high porosity. This was done by impregnation of 0, 5, 10 and 20% concentrations of phosphoric acid under various carbonization temperatures (600, 700, 800 and 900°C). The physicochemical properties of CNPs were characterized through nitrogen sorption, X-ray diffraction (XRD), Scanning electron microscopy (SEM), and Fourier transforms infrared spectroscopy (FTIR). Nitrogen sorption revealed that the condition using 10% concentration of phosphoric acid treatment at a carbonization temperature of 700°C formed carbon nanoparticles with a highly porous structure (Surface area 27.65 m2 /g and pore volume 0.07 cm3 /g). Additionally, in order to high surface area, porosity and concentrated carbon nanoparticle. © 2019 Trans Tech Publications Ltd, Switzerland.

关键词： Carbonization

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Influence of chemical activation on synthesis of carbon nanoparticles via carbonization from lignin

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AIP Conference Proceedings 2020年第1期2279卷

作者： N. Ngamthanacom N. Kaewtrakulchai W. Chaiwat L. Chuenchom M. Fuji A. Eiad-ua 1College of Nanotechnology King Mongkut’s Institute of Technology Bangkok 10520 Thailand 2Environmental Engineering and Disaster Management Program Mahidol University Kanchanaburi Campus Sai yok Kanchanaburi 71150 Thailand 3Department of Chemistry Faculty of Science Prince of Songkhla University Songkhla 90112 Thailand 4Advanced Ceramic Research Center Nagoya Institute of Technology Tajimi Gifu 507-0033 Japan

Carbon nanoparticles (CNPs) have been successfully synthesized from waste lignin via carbonization and base activation. The effect of base activation on lignin transformation to carbon nanoparticles was investigated. The physicochemical properties of CNPs were comprehensively characterized through a Scanning electron microscope (SEM), Surface area and pore analysis, X-ray diffraction (XRD), and Raman spectroscopy. The results revealed that the condition using 5 wt% of sodium hydroxide (NaOH) and carbonization at 700°C on the N2 atmosphere exhibited the highly porous structure of carbon nanoparticles. In conclusion, the NaOH-treated CNPs led to the production of high specific surface areas and high micropore volumes.

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LZS/Al2O3 glass-ceramic composites sintered by fast firing

LZS/Al2O3 glass-ceramic composites sintered by fast firing

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作者： Arcaro, Sabrina Nieto, Maria Isabel Moreno, Rodrigo Salvador, Maria Dolores Borrell, Amparo Moreno, Berta Chinarro, Eva De Oliveira, Antonio Pedro Novaes Laboratory of Glass-Ceramic Materials VITROCER Federal University of Santa Catarina - UFSC Florianópolis SC88040-900 Brazil Graduate Program in Materials Science and Engineering - PGMAT Federal University of Santa Catarina - UFSC Florianópolis SC88040-900 Brazil Institute of Ceramics and Glass - CSIC Madrid Spain Institute of Materials Technology Polytechnic University of Valencia Spain

In this work, nanometric Al2O3 (1-5 vol.%) particles (13 nm, 100 m2/g) were added to a 19.58Li2O•11.10ZrO2•69.32SiO2 (mol%) (3.5 µm, 2.5 m2/g) parent glass-ceramic matrix to prepare composites with the purpose of studying the influence of Al2O3 on their structure, microstructure, mechanical, thermal and electrical properties when sintered by fast firing. The parent glass-ceramic was prepared by melting and fast cooling (in water) to obtain a glass frit. The resulting glass frit was milled according to a two-step procedure consisting on a dry milling stage followed by a long wet milling step down. Each composition was wet homogenized and then dried at 110 ºC for 48 h for disaggregation. The obtained powders were uniaxially pressed (100 MPa) and compacts sintered by fast firing (175 ºC/min) between 800 and 900 ºC for 30 min. The composites, with relative densities ranging from 89% to 93%, showed zircon and β-spodumene as main crystalline phases. The hardness and Young's modulus varied from 4.5 to 6.5 GPa, and from 65 to 102 GPa, respectively. The formation of β-spodumene in the obtained composites leads to reduce the CTEs, whose values ranged from 13 to 7 x 10-6 ºC-1 © 2017 Universidade Federal de Sao Carlos. All rights reserved.

关键词： Sintering

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Search for Continuous Gravitational Waves from Known Pulsars in the First Part of the Fourth LIGO-Virgo-KAGRA Observing Run

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Astrophysical Journal 2025年第2期983卷 99-99页

作者： Abac, A.G. Abbott, R. Abouelfettouh, I. Acernese, F. Ackley, K. Adhicary, S. Adhikari, N. Adhikari, R.X. Adkins, V.K. Agarwal, D. Agathos, M. Aghaei Abchouyeh, M. Aguiar, O.D. Aguilar, I. Aiello, L. Ain, A. Ajith, P. Akutsu, T. Albanesi, S. Alfaidi, R.A. Al-Jodah, A. Alléné, C. Allocca, A. Al-Shammari, S. Altin, P.A. Alvarez-Lopez, S. Amato, A. Amez-Droz, L. Amorosi, A. Amra, C. Ananyeva, A. Anderson, S.B. Anderson, W.G. Andia, M. Ando, M. Andrade, T. Andres, N. Andrés-Carcasona, M. Andrić, T. Anglin, J. Ansoldi, S. Antelis, J.M. Antier, S. Aoumi, M. Appavuravther, E.Z. Appert, S. Apple, S.K. Arai, K. Araya, A. Araya, M.C. Areeda, J.S. Argianas, L. Aritomi, N. Armato, F. Arnaud, N. Arogeti, M. Aronson, S.M. Ashton, G. Aso, Y. Assiduo, M. Assis de Souza Melo, S. Aston, S.M. Astone, P. Attadio, F. Aubin, F. AultONeal, K. Avallone, G. Babak, S. Badaracco, F. Badger, C. Bae, S. Bagnasco, S. Bagui, E. Baier, J.G. Baiotti, L. Bajpai, R. Baka, T. Ball, M. Ballardin, G. Ballmer, S.W. Banagiri, S. Banerjee, B. Bankar, D. Baral, P. Barayoga, J.C. Barish, B.C. Barker, D. Barneo, P. Barone, F. Barr, B. Barsotti, L. Barsuglia, M. Barta, D. Bartoletti, A.M. Barton, M.A. Bartos, I. Basak, S. Basalaev, A. Bassiri, R. Basti, A. Bates, D.E. Bawaj, M. Baxi, P. Bayley, J.C. Baylor, A.C. Baynard, P.A. Bazzan, M. Bedakihale, V.M. Beirnaert, F. Bejger, M. Belardinelli, D. Bell, A.S. Benedetto, V. Benoit, W. Bentley, J.D. Ben Yaala, M. Bera, S. Berbel, M. Bergamin, F. Berger, B.K. Bernuzzi, S. Beroiz, M. Bersanetti, D. Bertolini, A. Betzwieser, J. Beveridge, D. Bevins, N. Bhandare, R. Bhardwaj, U. Bhatt, R. Bhattacharjee, D. Bhaumik, S. Bhowmick, S. Bianchi, A. Bilenko, I.A. Billingsley, G. Binetti, A. Bini, S. Birnholtz, O. Biscoveanu, S. Bisht, A. Bitossi, M. Bizouard, M.-A. Blackburn, J.K. Blagg, L.A. Blair, C.D. Blair, D.G. Bobba, F. Bode, N. Boileau, G. Boldrini, M. Bolingbroke, G.N. Bolliand, A. Bonavena, L.D. Bondarescu, R. Bondu, F. Bonilla, E. Bonilla, M.S. Bonino, A. Bonnand, R. Booker, P. Borchers, A. Boschi, V. Bose, S. Boss Max Planck Institute for Gravitational Physics (Albert Einstein Institute) Potsdam D-14476 Germany LIGO Laboratory California Institute of Technology Pasadena 91125 CA United States LIGO Hanford Observatory Richland 99352 WA United States Dipartimento di Farmacia Università di Salerno Fisciano Salerno I-84084 Italy INFN Sezione di Napoli Napoli I-80126 Italy University of Warwick Coventry CV 47AL United Kingdom The Pennsylvania State University University Park 16802 PA United States University of Wisconsin-Milwaukee Milwaukee 53201 WI United States Louisiana State University Baton Rouge 70803 LA United States Université Catholique de Louvain Louvain-la-Neuve B-1348 Belgium Inter-University Centre for Astronomy and Astrophysics Pune 411007 India Queen Mary University of London London E1 4NS United Kingdom Department of Physics and Astronomy Sejong University 209 Neungdong-ro Gwangjin-gu Seoul 143-747 South Korea Instituto Nacional de Pesquisas Espaciais São José dos Campos São Paulo 12227-010 Brazil Stanford University Stanford 94305 CA United States Università di Roma Tor Vergata Roma I-00133 Italy INFN Sezione di Roma Tor Vergata Roma I-00133 Italy Cardiff University Cardiff CF24 3AA United Kingdom Universiteit Antwerpen Antwerpen 2000 Belgium International Centre for Theoretical Sciences Tata Institute of Fundamental Research Bengaluru 560089 India Gravitational Wave Science Project National Astronomical Observatory of Japan 2-21-1 Osawa Mitaka City Tokyo 181-8588 Japan Advanced Technology Center National Astronomical Observatory of Japan 2-21-1 Osawa Mitaka City Tokyo 181-8588 Japan INFN Sezione di Torino Torino I-10125 Italy Theoretisch-Physikalisches Institut Friedrich-Schiller-Universität Jena Jena D-07743 Germany Dipartimento di Fisica Università degli Studi di Torino Torino I-10125 Italy SUPA University of Glasgow Glasgow G12 8QQ United Kingdom OzGrav University of Western Australia Crawley 6009 WA

Continuous gravitational waves (CWs) emission from neutron stars carries information about their internal structure and equation of state, and it can provide tests of general relativity. We present a search for CWs from a set of 45 known pulsars in the first part of the fourth LIGO-Virgo-KAGRA observing run, known as O4a. We conducted a targeted search for each pulsar using three independent analysis methods considering single-harmonic and dual-harmonic emission models. We find no evidence of a CW signal in O4a data for both models and set upper limits on the signal amplitude and on the ellipticity, which quantifies the asymmetry in the neutron star mass distribution. For the single-harmonic emission model, 29 targets have the upper limit on the amplitude below the theoretical spin-down limit. The lowest upper limit on the amplitude is 6.4 × 10^-27 for the young energetic pulsar J0537-6910, while the lowest constraint on the ellipticity is 8.8 × 10^-9 for the bright nearby millisecond pulsar J0437-4715. Additionally, for a subset of 16 targets, we performed a narrowband search that is more robust regarding the emission model, with no evidence of a signal. We also found no evidence of nonstandard polarizations as predicted by the Brans-Dicke theory. © 2025. The Author(s). Published by the American Astronomical Society.

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Search for Gravitational Waves Emitted from SN 2023ixf

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The Astrophysical Journal 2025年第2期985卷 183-183页

作者： A. G. Abac R. Abbott I. Abouelfettouh F. Acernese K. Ackley S. Adhicary N. Adhikari R. X. Adhikari V. K. Adkins D. Agarwal M. Agathos M. Aghaei Abchouyeh O. D. Aguiar I. Aguilar L. Aiello A. Ain T. Akutsu S. Albanesi R. A. Alfaidi A. Al-Jodah C. Alléné A. Allocca S. Al-Shammari P. A. Altin S. Alvarez-Lopez A. Amato L. Amez-Droz A. Amorosi C. Amra A. Ananyeva S. B. Anderson W. G. Anderson M. Andia M. Ando T. Andrade N. Andres M. Andrés-Carcasona T. Andrić J. Anglin S. Ansoldi J. M. Antelis S. Antier M. Aoumi E. Z. Appavuravther S. Appert S. K. Apple K. Arai A. Araya M. C. Araya J. S. Areeda L. Argianas N. Aritomi F. Armato N. Arnaud M. Arogeti S. M. Aronson G. Ashton Y. Aso M. Assiduo S. Assis de Souza Melo S. M. Aston P. Astone F. Attadio F. Aubin K. AultONeal G. Avallone S. Babak F. Badaracco C. Badger S. Bae S. Bagnasco E. Bagui J. G. Baier L. Baiotti R. Bajpai T. Baka M. Ball G. Ballardin S. W. Ballmer S. Banagiri B. Banerjee D. Bankar P. Baral J. C. Barayoga B. C. Barish D. Barker P. Barneo F. Barone B. Barr L. Barsotti M. Barsuglia D. Barta A. M. Bartoletti M. A. Barton I. Bartos S. Basak A. Basalaev R. Bassiri A. Basti D. E. Bates M. Bawaj P. Baxi J. C. Bayley A. C. Baylor P. A. Baynard II M. Bazzan V. M. Bedakihale F. Beirnaert M. Bejger D. Belardinelli A. S. Bell V. Benedetto W. Benoit J. D. Bentley M. Ben Yaala S. Bera M. Berbel F. Bergamin B. K. Berger S. Bernuzzi M. Beroiz D. Bersanetti A. Bertolini J. Betzwieser D. Beveridge N. Bevins R. Bhandare U. Bhardwaj R. Bhatt D. Bhattacharjee S. Bhaumik S. Bhowmick A. Bianchi I. A. Bilenko G. Billingsley A. Binetti S. Bini O. Birnholtz S. Biscoveanu A. Bisht M. Bitossi M.-A. Bizouard J. K. Blackburn L. A. Blagg C. D. Blair D. G. Blair F. Bobba N. Bode G. Boileau M. Boldrini G. N. Bolingbroke A. Bolliand L. D. Bonavena R. Bondarescu F. Bondu E. Bonilla M. S. Bonilla A. Bonino R. Bonnand P. Booker A. Borchers V. Boschi S. Bose V. Bossilkov V. Boudart A. Boudon A. Bozzi C. Bradaschia P. R. Brady M. Braglia A. Branch M. Branchesi J. Brandt I. Braun M. Breschi T. B Max Planck Institute for Gravitational Physics (Albert Einstein Institute) D-14476 Potsdam Germany LIGO Laboratory California Institute of Technology Pasadena CA 91125 USA LIGO Hanford Observatory Richland WA 99352 USA Dipartimento di Farmacia Università di Salerno I-84084 Fisciano Salerno Italy INFN Sezione di Napoli I-80126 Napoli Italy University of Warwick Coventry CV4 7AL UK The Pennsylvania State University University Park PA 16802 USA University of Wisconsin-Milwaukee Milwaukee WI 53201 USA Louisiana State University Baton Rouge LA 70803 USA Université catholique de Louvain B-1348 Louvain-la-Neuve Belgium Inter-University Centre for Astronomy and Astrophysics Pune 411007 India Queen Mary University of London London E1 4NS UK Department of Physics and Astronomy Sejong University 209 Neungdong-ro Gwangjin-gu Seoul 143-747 Republic of Korea Instituto Nacional de Pesquisas Espaciais 12227-010 São José dos Campos São Paulo Brazil Stanford University Stanford CA 94305 USA Università di Roma Tor Vergata I-00133 Roma Italy INFN Sezione di Roma Tor Vergata I-00133 Roma Italy Cardiff University Cardiff CF24 3AA UK Universiteit Antwerpen 2000 Antwerpen Belgium Gravitational Wave Science Project National Astronomical Observatory of Japan 2-21-1 Osawa Mitaka City Tokyo 181-8588 Japan Advanced Technology Center National Astronomical Observatory of Japan 2-21-1 Osawa Mitaka City Tokyo 181-8588 Japan INFN Sezione di Torino I-10125 Torino Italy Theoretisch-Physikalisches Institut Friedrich-Schiller-Universität Jena D-07743 Jena Germany Dipartimento di Fisica Università degli Studi di Torino I-10125 Torino Italy SUPA University of Glasgow Glasgow G12 8QQ UK OzGrav University of Western Australia Crawley Western Australia 6009 Australia University Savoie Mont Blanc CNRS Laboratoire d’Annecy de Physique des Particules - IN2P3 F-74000 Annecy France Università di Napoli “Federico II ” I-80126 Napoli Italy OzGrav Australian National University C

We present the results of a search for gravitational-wave transients associated with core-collapse supernova SN 2023ixf, which was observed in the galaxy Messier 101 via optical emission on 2023 May 19, during the LIGO–Virgo–KAGRA 15th engineering Run. We define a five-day on-source window during which an accompanying gravitational-wave signal may have occurred. No gravitational waves have been identified in data when at least two gravitational-wave observatories were operating, which covered ∼14% of this five-day window. We report the search detection efficiency for various possible gravitational-wave emission models. Considering the distance to M101 (6.7 Mpc), we derive constraints on the gravitational-wave emission mechanism of core-collapse supernovae across a broad frequency spectrum, ranging from 50 Hz to 2 kHz, where we assume the gravitational-wave emission occurred when coincident data are available in the on-source window. Considering an ellipsoid model for a rotating proto-neutron star, our search is sensitive to gravitational-wave energy 1 × 10⁻⁴ M_⊙c² and luminosity 2.6 × 10⁻⁴ M_⊙c² s⁻¹ for a source emitting at 82 Hz. These constraints are around an order of magnitude more stringent than those obtained so far with gravitational-wave data. The constraint on the ellipticity of the proto-neutron star that is formed is as low as 1.08, at frequencies above 1200 Hz, surpassing past results.

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MgAl2O4 foams obtained by combustion synthesis

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Chemical engineering Transactions 2015年 43卷 1801-1806页

作者： Moraes, Graziela G. Pozzobom, Ida E.F. Fernandes, Celso P. Novaes De Oliveira, Antonio P. Graduate Program in Materials Science and Engineering - PGMAT Laboratory of Glass-Ceramic Materials - VITROCER Federal University of Santa Catarina - UFSC Florianópolis - SC88040 900 Brazil

ISBN: (纸本)9788895608341

This work aims to study magnesium aluminate (MgAl2O4) ceramic foams obtained by combustion synthesis in solution without the need of surfactants to stabilize *** ceramic suspension containing acetone (75 wt%), calcined powder (25 wt%) and a mixture of glycerine (80 % blonde glycerine and 20 % crude glycerine) in the fraction of 100 % with respect to solids was prepared in an alumina ball mill, for 60 min. Subsequently, the suspension was heated at 40 °C, for 30 min, until it became rigid. In order to promote foaming, the suspension was heated to 70 °C and then the following substances were added to it: 2.5 wt% distilled water, 25 wt% Al(NO3)3.9H2O), 12.5 wt% (Mg(NO3)2.6H2O) and 0.625 wt% of a glycerine mixture (80 % blonde glycerine and 20% crude glycerine). After additions the suspension was stirred for 5 min at 950 rpm in a mixer. The resulting foams were dried at 40 °C, for 24 h, in a muffle and fired in two steps, i.e., heating at 0.5 °C/min up to 600 °C/120 min and at 5 °C/min up to 1600 °C/120 *** obtained materials were characterized by SEM,TEM and from tomographic images. The results showed that the obtained magnesium aluminate foams have a high porosity (97 %), a high connectivity and pore sizes (diameters) between 30 and 1200 μm. Copyright © 2015, AIDIC ServiziS.r.l.

关键词： Pore size

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Production and characterisation of ceramic foams from industrial solid waste

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Chemical engineering Transactions 2015年 43卷 1783-1788页

作者： Zilli, Marina Arcaro, Sabrina Cesconeto, Francielly R. De Oliveira Maia, Bianca G. Pereira, Fabiano R. Novaes De Oliveira, Antonio P. Graduate Program in Materials Science and Engineering - PGMAT Laboratory of Glass-Ceramic Materials - VITROCER Federal University of Santa Catarina - UFSC Florianópolis-SC88040-900 Brazil

ISBN: (纸本)9788895608341

This work has as objective to produce and to characterize ceramic foams from glass bottles, sludge from sewage treatment station and graphite (0 - 10 wt%) as a foaming agent. Different compositions were formulated and prepared to obtain materials with controlled porosity for applications where thermal insulation is the main requirement. The raw materials of the prepared compositions were mixed and uniaxially pressed at 40 MPa. Subsequently, the prepared samples were dried and fired at different temperatures (800 - 950 °C) for 30 minutes, respectively. The raw materials and obtained ceramic foams were characterized in terms of their chemical, morphological, thermal and mechanical properties. The results showed that it is possible to produce ceramic foams for thermal insulation with optimized compositions containing 90 vol% glass and 10 vol% sludge with addition of 10 wt% graphite. The ceramic foams showed porosities between 40 and 70 %, thermal conductivity from 0.101 to 0.175 W/mK and compressive strength between 6.4 and 12.5 MPa. Copyright © 2015, AIDIC Servizi S.r.l.

关键词： Thermal insulation

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Production and characterisation of glass foams for thermal insulation

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Chemical engineering Transactions 2015年 43卷 1777-1782页

作者： Dias, Gabriella M.V. Arcaro, Sabrina Cesconeto, Francielly R. De Oliveira Maia, Bianca G. Pereira, Fabiano R. Novaes De Oliveira, Antonio P. Graduate Program in Materials Science and Engineering - PGMAT Laboratory of Glass-Ceramic Materials - VITROCER Federal University of Santa Catarina - UFSC Florianópolis-SC88040-900 Brazil

ISBN: (纸本)9788895608341

In this work, glass compositions from glass bottles with different colours and graphite (2 - 12 vol%) as the pore-forming agent were prepared for the production of materials with controlled porosity for applications where thermal and acoustic insulations are main technical requirements. The formulated compositions were, in a later stage, uniaxially pressed (40 MPa) and fired at different temperatures (800 - 950 °C) and cycles with holding times between 15 and 120 minutes. The results showed that it is possible to produce glass foams for thermal insulation from optimized compositions containing 90 vol% glass and 10 vol% graphite, fired between 800 and 950 °C for 30 minutes, which showed porosities between 53 and 76 %, with thermal conductivities between 0.16 and 0.08 W/mK and compressive strength between 20 and 4.6 MPa. The obtained glass foams are strong candidates for applications requiring thermal insulation with suitable combination of thermal conductivity, porosity and mechanical strength. Copyright © 2015, AIDIC Servizi S.r.l.

关键词： Thermal insulation

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Microstructure and Thermal Conductivity of Porous Al2 O3-ZrO2 ceramics 58th

Microstructure and Thermal Conductivity of Porous Al2 O3-ZrO...

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58th Brazilian ceramic Conference, CBC 2014

作者： Delbrücke, Tiago Gouvêa, Rogério A. Raubach, Cristiane W. Longo, Elson Sousa, Vânia C. M.tebcheranic, Sergio Kubaski, Evaldo T. Moreira, Mário L. Jurado, Jose R. Cava, Sergio Graduate Program in Science and Materials Engineering Technology Development Center Federal University of Pelotas RS Pelotas96010-900 Brazil Laboratory of Biomaterials & Advanced Ceramics Federal University of Rio Grande do Sul RS Porto Alegre91509-900 Brazil Interdisciplinary Laboratory of Ceramic Materials Ponta Grossa State University PR Ponta Grossa84030-900 Brazil National Institute of Science and Technology of Materials in Nanotechnology Paulista State University SP Araraquara14801-907 Brazil Glass Department Institute of Glass and Ceramic Madrid28049 Spain Institute of Physics and Mathematics Federal University of Pelotas RS Pelotas96010-900 Brazil

The improvement on the development of porous ceramic materials has leaded to new technologies in thermal insulation, for example, composite materials for better performance of pressure vessels in rocket engines. Within this context, the present work aims to evaluate the ability of a refractory ceramic base alumina/zirconia through the processes of co-precipitation and replica method in an organic fiber template. The green body was burnt-out and sintered at 1200-1600°C to obtain the continuous porous ceramic fibers. In the FEG-SEM analysis, an interconnected porous structure with small grains was observed. The crystalline phases were determined by X-ray diffraction and compared to micro-Raman results regarding the crystalline structure confirms that there present in the material zirconia is composed of more than one phase. Porosity was calculated through a mercury porosimeter as 77.9%, and the Laser Flash method gave a thermal conductivity value of 1.61 K W.m−1 .K−1 for the Al2 O3-ZrO2 fibers. © 2015 Trans Tech Publications Ltd, Switzerland.

关键词： Porosity

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