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EFFECTS OF SAMPLE ISOLATION AND HANDLING ON THE RECOVERY OF PURGEABLE ORGANIC-COMPOUNDS

GROUND WATER MONITORING AND REMEDIATION 1994年第2期14卷 142-152页

作者： GIBS, J IMBRIGIOTTA, TE FICKEN, JH PANKOW, JF ROSEN, ME Jacob Gibs is a water quality specialist with the USGS Water Resources Division (810 Bear Tavern Rd. Ste. 206 West Trenton NJ 08628). He received his B.S. in mechanical engineering in 1968 his M.S. in environmental engineering in 1975 and his Ph.D. in environmental engineering in 1983 all from Drexel University in Philadelphia. His research interests include evaluating representative ground water and surface water sampling techniques for trace levels of organic and inorganic compounds and designing new sampling devices. Thomas E. Imbrigiotta received a B.S. in chemistry with a concentration in environmental studies from Oakland University Rochester Michigan in 1975. He then attended the University of Wisconsin Madison and received an M.S. in water chemistry in 1982. He has been a hydrologist with the USGS Water Resources Division (810 Bear Tavern Rd. Ste. 206 West Trenton NJ 08628) since 1977. He worked in the Indiana District from 1977 to 1984 prior to coming to the New Jersey District. Currently he is project coordinator for the Picatinny Research project a study of the fate and transport of chlorinated solvents in ground water at Picatinny Arsenal New Jersey. Previously he was chief of a project evaluating sampling techniques for organics in ground water. James H. Ficken worked for the USGS Water Resources Division as a chemical engineer from 1964 to 1992. He received his B.S. in chemical engineering in 1962 from Washington University in St. Louis Missouri. His research interests were water quality instrumentation and sensors that measure real-time environmental data. He contributed as a team member to the design and development of the USGS water quality flow-through and mini-monitor system. Ficken passed away in 1992. James F. Pankow is a professor in the Department of Environmental Science and Engineering at the Oregon Graduate Institute (Oregon Graduate Institute of Science and Technology Department of Environmental Science and Engineering P.O. Box 1900 Portland OR 97291–1000). He

This report compares the recovery of purgeable organic compounds (POCs) obtained by using a downhole isobaric sampler developed by the U.S. Geological Survey, a helical-rotor submersible pump, and a point source bailer to collect and isolate samples of ground water from three wells in New York and New Jersey, the samples contained a total of 13 POCs detectable at concentrations ranging from 0.5 mug/L to about 400 mug/L. This report also compares the effects of sample handling, specifically the differences in POC concentration recovery when an isobaric sample container is filled at land surface vs. when it is filled downhole, and when samples are taken using a bailer with and without a bottom-emptying device. These case studies are used to quantify the possible effects of different sample-isolation and sample-handling techniques on POC recovery. The relative effectiveness of the three devices varied by site and by compound. Overall, the POC recoveries achieved by using the helical-rotor submersible pump and the downhole isobaric sampler were not significantly different at the 95 percent confidence level. POC recovery obtained by using the point source bailer was 11 percent lower overall. The downhole isobaric sampler results exhibited smaller coefficients of variation than did the helical-rotor submersible pump or the point-source bailer results. However, the differences between the coefficients of variation of the downhole isobaric sampler and those of the helical-rotor submersible pump were not significant the 95 percent confidence level. The nonsignificant smaller coefficient of variation of the downhole isobaric sampler apparently resulted from two fewer sample handling steps that exposed the sample water to ambient air. An independent experiment performed with a different downhole sampler at one of the wells used in this investigation produced a similar statistical result. Also, the POC recovery obtained by pouring sample water out the top Of a point source bail

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MPSA abstracts

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Journal of Protein Chemistry 1994年第5期13卷 515-543页

作者： Aminlari, Mahmoud Asquith, Thomas Sarlo, Katherine Bailey, Jerome M. Tu, Oanh Issai, Gilbert Ha, Alice Shively, John E. Bell, Alexander W. Baur, Nicole C. Bergeron, John J. M. Ou, Wei -Jia Thomas, David Y. Cianflone, Katherine Baldo, Allain Hincke, Maxwell T. Momparler, Richard L. Laliberté, Josée Thomson, David M. P. Sutherland, M. Besada, Vladimir Gonzalez, Javier Padron, Gabriel Garay, Hilda Reyes, Osvaldo Takao, Toshifumi Shimonishi, Yasutsugu Bischoff, Rainer Roecklin, Dominique Bouchon, Bernadette Klarskov, Klaus Van Dorsselaer, Alain Brake, Patricia G. Pacitti, Anne Higgins, Terry Stevis, Panos Malinowski, John McElhiney, Sue Huang, Janes Vestal, Christine Buckel, Scott D. Stevenson, Tracy Loo, Joseph A. Caffrey, Martin Wang, Jin Wallace, Carmichael J. A. Clark-Lewis, Ian Carraway, C. A. Carothers Huang, J. Li, Y. Juang, S. -H. Gallo, A. Mayer, B. J. Carraway, K. L. Coleman, Patrick L. Sarpong, Daniel Deerfield, David W. Holland-Minkley, Amanda Hempel, John D. Nicholas, Hugh B. Denslow, Nancy D. Folmar, Leroy C. Sullivan, Craig V. Dixon, James D. Mark, Jonathan P. Elicone, Christopher P. Maleknia, Simin D. McGuinness, Brian F. Regnier, Fred E. Afeyan, Noubar B. Dolence, Julia M. Poulter, C. Dale Egorov, Tsezi Musolyamov, Alexander Popineau, Yves Andersen, Jens Roepstorff, Peter Falkenstein, Roberto J. Biscoglio de Jiménez Bonino, Mirtha J. Peña, Clara Gauggel, D. L. Asquith, T. N. Isfort, R. J. Miller, N. S. Cody, D. B. Giblin, Michael F. Wong, Tuck C. Quinn, Thomas P. Grant, Gregory A. Crankshaw, Mark W. Griffith, Scott Schroeder, Steve Quinn, Thomas Guinet, F. Petillot, Y. Chapsal, J. M. Dubayle, J. Greco, F. Barge, O. Forest, E. Valentin, C. Hahn, Frederick M Baker, Jonathan A. Haniu, Mitsuru Kenney, William C. Rohde, Michael F. Harman, James G. Lee, Eun Ju Glasgow, Joel Lew, Sew Fen Belduz, Ali O. Harris, Reed J. Molony, Michael S. Keyt, Lene H. Wu, Shiaw -Lin Hawke, David H. Tso, Jaqueline Early, Sherrell Miller, Chad G. Hayman, G. Thomas Miernyk, Jan A. Hellman, Ulf Wernstedt, Christer Góñez, Jorge H Department of Biochemistry School of Veterinary Medicine Shiraz University Shiraz Iran Corporate Professional & Regulatory Services/Human Safety Dept. The Procter & Gamble Co. Cincinnati Division of Immunology Beckman Research Institute of the City of Hope Duarte Protein Analytic Facility Sheldon Biotechnology Centre USA McGill University Montreal Department of Anatomy USA Biotechnology Research Institute NRC Canada Division of Cardiology Royal Victoria Hospital USA Department of Anatomy University of Ottawa Faculty of Health Science Ottawa Centre de Recherche Pediatrique Hôpital Ste-Justine Université de Montréal Montreal Department of Immunology Montreal General Hospital USA Center for Genetic Engineering & Biotechnology Cuba Institute for Protein Research Osaka University Osaka Japan Protein Analytical Group TRANSGENE S.A. Strasbourg Cedex France Vakgroep Biochemie Fysiologie en Microbiologie Gent Belgium Laborat. de Spectrométrie de Masse Bioorganique URA 31 CNRS Université Louis Pasteur Strasbourg Cedex France Sterling winthrop Inc. Collegeville Lexin Pharmaceutical Corporation Horsham PerSeptive Biosystems Houston Parke-Davis Pharmaceutical Research Division of Warner Lambert Company Ann Arbor Dept. of Chemistry The Ohio State University Columbus USA Dept. of Biochemistry Dalhousie University Halifax Canada Biomedical Research Center University of British Columbia Vancouver Canada Dept. of Biochem. & Molec. Biol. Univ. of Miami Sch. of Medicine Miami The Rockefeller Institute New York Dept. of Cell Biol. & Anat. Univ. of Miami Sch. of Medicine Miami Biosciences Laboratory 3M Co. St. Paul Pittsburgh Supercomputing Center Pittsburgh Department of Molecular Genetics/Biochemistry University of Pittsburgh Pittsburgh Dept. Biochem. and Mol. Biol. University of Florida Gainesville U.S. Environmental Protection Agency Gulf Breeze Dept. Zoology North Carolina State University Raleigh PerSeptive Biosystems Inc. Cambridge Department of Chemistry Univ

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COMPARISON OF DOWNHOLE AND SURFACE SAMPLING FOR THE DETERMINATION OF VOLATILE ORGANIC-COMPOUNDS (VOCS) IN GROUND-WATER

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GROUND WATER MONITORING AND REMEDIATION 1992年第1期12卷 126-133页

作者： ROSEN, ME PANKOW, JF GIBS, J IMBRIGIOTTA, TE Michael E. Rosen received his B.A. in chemistry from the State University of New York at Binghamton in 1981 and a Ph.D. in environmental science and engineering from the Oregon Graduate Institute in 1988. His research interests include trace environmental analysis of organic compounds. He is now manager of the Voluntary Cleanup Section of the Oregon Department of Environmental Quality (Environmental Cleanup Division 811 S.W. 6th Ave. Portland OR 97204) where he is working to develop streamlined procedures and processes for the investigation and cleanup of hazardous substance sites. James F. Pankow is professor and chairman of the Department of Environmental Science and Engineering at the Oregon Graduate Institute (Oregon Graduate Institute of Science and Technology Department of Environmental Science and Engineering 19600 N.W. von Neumann Dr. Beaverton OR 97006–1999). He received his B.A. in chemistry in 1973 from the State University of New York in Binghamton and his Ph.D. in environmental engineering science from the California Institute of Technology in Pasadena California in 1979. His group is involved in the study of the physical and chemical processes affecting the behavior of organic and inorganic chemicals in the environment. This work includes the development and application of sensitive analytical methods for the determination of trace organic contaminants in ground water systems. Jacob Gibs is an environmental engineer with the U.S. Geological Survey Water Resources Division (810 Bear Tavern Rd. Ste. 207 West Trenton NJ 08628). He received a B.S. in mechanical engineering in 1968 an M.S. in environmental engineering in 1975 and a Ph.D. in environmental engineering in 1983 all from Drexel University Philadelphia Pennsylvania. He is currently project chief of a study on representative sampling of ground water for trace levels of organic compounds. His research interests include evaluating ground water sampling techniques and devices for purgeable organic compounds design of sampling

The relative precision and accuracy of sampling and analysis methods for the determination of trace concentrations of volatile organic compounds (VOCs) in ground water were compared. Samples were collected from a well containing nanogram-per-liter (ng/L) to microgram-per-liter (mu-g/L) levels of VOCs. A Keck helical rotor submersible pump was used to collect samples at the surface for analysis by purge and trap (P&T) and for analysis by adsorption/thermal desorption (ATD). Downhole samples were collected by passing water through an ATD cartridge. Although slight spontaneous bubble outgassing occurred when the water was brought to the surface, the relative precisions and comparabilities of the surface and downhole methods were generally found to be equivalent from a statistical point of view. A main conclusion of this study is that bringing sample water to the surface for placement in VOC vials (and subsequent analysis by P&T) can be done reliably under many circumstances. However, care must still be taken to prevent adsorption losses and cross contamination. Samples subject to strong bubble outgassing will need to be handled in a special fashion (e.g., by downhole ATD) to minimize volatilization losses. Additionally, the higher sensitivity of the ATD method allows lower detection limits than are possible with P&T. For example, several compounds present at the ng/L level could be determined with confidence by ATD, but not by P&T.

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USING THE PROPERTIES OF ORGANIC-COMPOUNDS TO HELP design A TREATMENT SYSTEM

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GROUND WATER MONITORING AND REMEDIATION 1991年第4期11卷 81-86页

作者： NYER, E BOETTCHER, G MORELLO, B Evan K. Nyer is an expert in the research and application of technology to ground water cleanups. As vice president with Geraghty & Miller Inc. he is responsible for engineering services including hazardous and solid waste management environmental and natural resource management remediation activities and designing treatment systems for contaminated sites throughout the United States and in foreign countries. He has designed more than 100 ground water treatment systems. Nyer travels throughout the country teaching treatment techniques at seminars and universities. He has written numerous papers on ground water decontamination and other water and waste water cleanup techniques. He is responsible for bringing to the field many innovative techniques for biological treatment of water soils and in situ treatment and the application of existing technologies to ground water contamination. He is a member of the Water Pollution Control Federation The National Water Well Association The American Institute of Chemical Engineers and The American Society of Civil Engineers. Bridget Morello received a B.S. Che from the University of South Florida in 1987 and is currently working for Geraghty & Miller's Process Group in Tampa Florida. She is mainly involved in treatability evaluation and design of ground water treatment systems. Gary Boettcher is a project scientists with Geraghty & Miller Inc. in Tampa Florida. He received his B.S. degree in microbiology from the University of South Florida and is currently pursuing a Master of Public Health (MPH) degree. He is involved in investigation treatability and design of biological remediation systems.

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Static hazards of drum filling. II. Electrostatic models: Theory and experiment

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process Safety Progress 1988年第1期7卷 63-78页

作者： Laurence G. Britton Jack A. Smith Larry Britton earned BS and PhD degrees in Fuel and Combustion Science at Leeds University England. After four years as Research Fellow in Applied Electrostatics at Southampton University he joined Union Carbide's Safety Research Laboratory in 1981 and is currently a Project Scientist. He is a Fellow of the Institute of Energy a Member of AIChE and the Combustion Institute and is a Chartered Engineer in the UK. He was cowinner of the AIChE “Bill Doyle” Award in 1987. Larry serves on the “Classification and Properties of Flammable Liquids” and “Properties of Hazardous Chemicals” committees of the NFPA. Jack Smith is a staff engineer for the Applied Mathematics and Process Simulation group of Central Research and Engineering at Union Carbide specializing in software development for engineering workstations and computational chemistry. He holds M.S. and Ph.D. degrees from the University of Florida in chemical physics and a B.S. from Purdue University in chemistry and mathematics.

For drum filling, a demarcation of 50 pS/m (below which a liquid may accumulate hazardous static in a grounded drum) is conservative and takes account of the effects of temperature and/or charge density on relaxation rate. The worst-case conductivity as regards static accumulation rate is about 0.5 pS/m, but in practice this should not correspond to the worst-case charge generation rate. Published forms of the Schon equation are not conservative for smooth-bore pipes and hoses; a new equation is proposed. Certain rough-bore hoses containing an inner grounding spiral can generate almost as much charge as a microfilter. Theory and experiment are discussed with reference to published Codes and Guidelines; attention is given to filter placement and drum linings.

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MICROBIAL CATABOLITES AS chemical SYNTHESIS INTERMEDIATES - A COST-BENEFIT-ANALYSIS

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BIOTECHNOLOGY PROGRESS 1987年第3期3卷 127-130页

作者： JOHNSTON, JB WINICOV, H CUNNINGHAM, VL Chemical Engineering Department Smith Kline and French Laboratories Swedeland PA 19479 James B. Johnston is Senior Investigator in Chemical Engineering at Smith Kline and French Laboratories where he conducts research on biocatalytic transformations of organic compounds. Herbert Winicov recently retired from his position as Senior Investigator in Chemical Engineering at Smith Kline and French Laboratories. He specialized in cost estimation and costing of chemical processes under development. Virginia L. Cunningham is Assistant Director Chemical Engineering Smith Kline and French Laboratories. She heads a group responsible for process engineering and related environmental process analytical and costing issues. Dr. Cunningham is the author of ECAS—Environmental Cost Analysis System an expert system for estimating the costs of waste treatment in chemical processes.

Cost projections have been developed for a biologically mediated synthesis. Significant cost advantages can be realized using the biochemical approach.

关键词： BIOSYNTHESIS

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INTERCOMPARTMENTAL FLUID SHIFTS IN HEMODIALYSIS-PATIENTS

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BIOTECHNOLOGY PROGRESS 1987年第2期3卷 69-73页

作者： HEINEKEN, FG EVANS, MC KEEN, ML GOTCH, FA COBE Laboratories Inc. Lakewood Colorado Fred G. Heineken is currently Program Director for Biotechnology within the Emerging Engineering Technologies Division of the Engineering Directorate of the National Science Foundation. He received his B.Sc. degree in Chemical Engineering from Northwestern University and his Ph.D. degree in the same discipline from the University of Minnesota. His work experience includes fermentation research at Monsanto teaching and research in respiration physiology at the University of Colorado and hemodialysis product design and evaluation at COBE Laboratories. Hemodialysis Treatment and Research Center Franklin Hospital Ralph K. Davis Medical Center San Francisco California Mary C. Evans has a BS degree in Chemistry from the University of Florida. She has held positions in the artificial kidney development group at Dow Chemical Company and the new product development group of Cordis-Dow Corporation. She is currently working in clinical research in the Hemodialysis Treatment & Research Center at Franklin Hospital in San Francisco. Marcia Keen is currently a doctoral student at the University of California San Francisco and serves as Clinical Research Supervisor at the Hemodialysis Treatment & Research Center at Franklin Hospital in San Francisco. She received her MS at the University of California San Francisco. Her thesis research developed a non-invasive Doppler technique to quantitate vascular access graft flow in hemodialysis patients. Her research interests include physiologic responses to dialysis therapy manipulations. Frank Gotch is an Associate Clinical Professor of Medicine at the University of California San Francisco. He received his BA and MD from the University of California and is currently Medical Director of the Hemodialysis Treatment & Research Center at Franklin Hospital in San Francisco. His research has addressed such issues as adequacy of dialysis and mathematical modeling of hemodialysis and associated therapies. He is a past president of the American

Hemodialysis is a therapeutic procedure for replacing some functions of the natural kidney. As such, it is capable of allowing people with little or no residual kidney function to survive and in some cases to lead productive lives. There are, unfortunately, a number of side effects associated with this procedure (shock, muscle cramps, fatigue, etc.). In order to minimize these side effects, we have undertaken to model shifts of fluid between the intracellular and extracellular fluid spaces in hemodialysis patients. Fluid shifts are primarily a function of osmolality differences between these fluid spaces. Changes in osmolality are caused mainly by changes in urea and salt concentrations. Least squares analysis of patient data has been used to estimate the appropriate ultrafiltration and urea mass transfer coefficients for each patient. The model has then been used to find a dialysate sodium concentration profile that will minimize fluid shifts into and out of the intracellular fluid space.

关键词： BIOMEDICAL EQUIPMENT

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MPCS - THE MANUFACTURING process-CONTROL SYSTEM

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AT&T TECHNICAL JOURNAL 1986年第4期65卷 35-45页

作者： DUNIETZ, IS HSU, JLC MCEACHERN, MT STOCKING, JH SWARTZ, MA TROMBLY, RM The authors Irwin S. Dunietz John L.C. Hsu Michael T. McEachern James H. Stocking Mark A. Swartz andRodney M. Tromblyare responsible for design and development of the Manufacturing Process Control System. Mr. Dunietz joined AT&T in 1980. He is a member of the technical staff in the Manufacturing Information Automation department at AT&T Engineering Research Center Princeton New Jersey. He received an A.B. in mathematics from Cornell University and an M.S.E. in computer science from Princeton University. Mr. Hsu who joined AT&T in 1970 is a department head in the Manufacturing Information Automation department at the Engineering Research Center. He received an M.S. in electrical engineering from the University of Missouri. Mr. McEachern joined AT&T in 1962 and is a supervisor in the 5ESS™ Line Unit Manufacturing department at AT&T Technologies in Oklahoma City Oklahoma. He is responsible for the manufacturing process control center in Oklahoma City which provides computerized support for all circuit pack manufacturing. Mr. Stocking who joined AT&T in 1975 is a supervisor in the Manufacturing Information Automation department at the Engineering Research Center. He received a B.S. in chemical engineering from Rensselaer Polytechnic Institute and a Ph.D. in chemical engineering from the University of California Berkeley. Mr. Swartz joined AT&T in 1980 and is a member of the technical staff in the Manufacturing Information Automation department at the Engineering Research Center. He received an A.B. in computer science from Cornell University and an M.S. in computer science from Rutgers—The State University. Mr. Trombly who joined AT&T in 19 78 is an assistant manager at the AT&T Merrimack Valley Works in Massachusetts. Previously he was a supervisor at the Engineering Research Center. He holds a B.S. in computers and systems engineering and an M.S.E.E. from Rensselaer Polytechnic Institute.

The central challenge of all manufacturing is making products to the right standards and delivering them at the right time. AT&T is upgrading its corporate and factory resource planning systems to improve control of day-to-day manufacturing. The Manufacturing process Control System (MPCS), developed at the AT&T engineering research Center (ERC), provides this support. MPCS connects the shop floor with production scheduling, accounting, product data archive, and engineering support systems.

关键词： PRODUCTION CONTROL

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A FEDERAL STRATEGY FOR INTERNATIONAL INDUSTRIAL COMPETITIVENESS

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BIO-TECHNOLOGY 1986年第6期4卷 522-525页

作者： PERPICH, JG Joseph G. Perpich M.D. J.D. vice president of planning and development Meloy Laboratories Inc. Rorer Group Inc. 6708 Industrial Drive Springfield VA 22151. He is editor of Biotechnology in Society: Private Initiatives and Public Oversight Pergamon Press New York 1986.REFERENCES Global CompetitionThe New Reality (Vol. I). Report of the President's Commission on Industrial Competitiveness. U.S. Government Printing Office Washington D.C. January 1985.Federal Financial Support for High Technology Industries. The Congress of the United States Congressional Budget Office. Washington D.C. June 1985.Commercial BiotechnologyAn International Analysis. The Congress of the United States Office of Technology Assessment. Washington D.C. January 1984.Report of the Research Briefing Panel on Chemical and Process Engineering for Biotechnology in Research Briefings 1984. National Academy Press Washington D.C.Guidelines for Engineering Research Centers: A Report for the National Science Foundation. Report of the National Academy of Engineering. Washington D.C. February 1984.Wyngaarden J.B. 1985. NIH's Role in Fostering Biotechnology. Bio/Technology 3:1040.|ISI|Press F. 1985. Back to the Future. Bio/Technology 3:1120.|ISI|

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MODELING THE STABILITY OF CEPHAMYCIN-C - PRODUCING N-LACTAMDURANS DURING CONTINUOUS CULTURE

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BIOTECHNOLOGY PROGRESS 1985年第4期1卷 231-236页

作者： KIRPEKAR, AC KIRWAN, DJ STIEBER, RW Department of Chemical Engineering University of Virginia Charlottesville VA 22901 Abhay C. Kirpekar received a Ph.D. degree in Chemical Engineering from the University of Virginia in May 1985. This paper is a part of his dissertation for which experiments were carried out at Merck Chemical Manufacturing Division of Merck & Co. Inc. where he is currently employed. His interests include gas-liquid mass transfer scale-up and design of fermentors Merck Chemical Manufacturing Division Elkton VA 22827 Robert W. Stieber received a Ph.D. degree from the Department of Microbiology and Public Health at Michigan State University in 1979. He then joined the Merck Chemical Manufacturing Division of Merck & Co. Inc. His main interests are in fermentation research process development and production

The reversion of a cephamycin C-producing strain of Nocardia lactamdurans to a non-producing variant under continuous culture conditions was examined at dilution rates between 0.025 and 0.045 hr-1. A model incorporating the influence of revertants, when present in the culture in significant numbers, was necessary to adequately describe the dynamics of the reversion process.

关键词： BIOTECHNOLOGY

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