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Novel synthesis of nickel-based bimetallic compounds using ammonium tetrafluoroborate and ammonium bifluoride as structure directing agents for energy storage application

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Journal of Energy Storage 2024年 75卷

作者： Kuo, Tsung-Rong Yu, You Zher Lee, Pin-Yan Wu, Chung-Hsien Chen, Hung-Ming Husain, Sadang Kongvarhodom, Chutima Ho, Kuo-Chuan Lin, Lu-Yin International PhD Program in Biomedical Engineering College of Biomedical Engineering Taipei Medical University Taipei11031 Taiwan Graduate Institute of Nanomedicine and Medical Engineering College of Biomedical Engineering Taipei Medical University Taipei11031 Taiwan Department of Chemical Engineering and Biotechnology National Taipei University of Technology Taipei Taiwan Department of Chemical Engineering National Taiwan University Taipei Taiwan Gingen Technology Co. LTD. Rm. 7 10F. No.189 Sec. 2 Keelung Rd. Xinyi Dist. Taipei11054 Taiwan Department of Physics Faculty of Mathematics and Natural Science Lambung Mangkurat University Banjarmasin70124 Indonesia Department of Chemical Engineering King Mongkut's University of Technology Thonburi 126 Pracha-u-thit Toong-kru Bangkok10140 Thailand

Nickel-based compounds are widely applied as the active material for energy storage devices, owing to high theoretical capacity and easy-fabricated process. Bimetallic compounds having multiple redox states can provide abundant redox reactions for charge storage. Structure directing agent (SDA) can promote the preferable growth of active materials and to enhance energy storage abilities. In this work, NH4BF4 and NH4HF2 are firstly used as SDA to synthesize nickel-based compounds along with 2-methylmidozole in the one-step solution process for energy storage applications. The bimetallic compounds are synthesized by incorporating Al, Mn, Co, Cu and Zn salts in the precursor solution including the Ni salt. The system with Al, Cu or Zn possesses single metal compound and barely nickel compound. Mn and Co-incorporated systems present clear bimetallic components with nickel hydroxide. The highest specific capacitance (CF) of 1336.3 F/g (297.0 mAh/g) are achieved at 20 mV/s for the NiCo-based electrode, owing to the bimetallic feature and favorable two-dimensional sheet-like structures. An energy storage device is assembled using the NiCo-based compound and reduced graphene oxide electrodes. The maximum energy density of 10.5 Wh/kg at 0.3 kW/kg, and the CF retention of 78.5% and Coulombic efficiency of 85.2% are achieved after 10,000 times charge/discharge cycles. © 2023 Elsevier Ltd

关键词： Energy storage

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Methylcellulose-AgNPs-oat hydrogel as a wound dressing for burn wound

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AIP Conference Proceedings 2024年第1期3047卷

作者： Prihartini Widiyanti Firza Siswanto Biomedical Engineering Study Program Faculty of Science and Technology Universitas Airlangga Surabaya Indonesia Physics Study Program Faculty of Science and Technology Universitas Airlangga Surabaya Indonesia

Based on the RISKESDAS in 2018 the prevalence of burns reached 1,3% of the total population of Indonesia and basen on WHO there were 195,000 cases of deaths due to burns every year. One clinical treatment for burns is to use hydrogels as wound dressing. Hydrogel wound dressing functions to absorb wound exudates, by keeping the wound moist. This study was conducted to determine the effect of adding oat extrac to the hydrogel methylcellulose-AgNPs. Hydrogel methylcellulose-AgNPs are mixed with oat extract, with an oat extract concentration of 0 wt%, 0.5 wt%, 1 wt%, 1.5 wt%, and 2 wt%. The characterization carried out included XRD crystallinity test and SEM morphology test for the characterization of AgNPs, and it was found that 10.2% of AgNPs were formed and evenly distributed AgNPs. In addition, characterization of hydrogel wound dressing was carried out which included antibacterial test, cytotoxicity test, swelling test, and antioxidant test. From the results of the analysis it was found that the best variable methylcellulose-AgNPs-oat hydrogel was a sample with an oat concentration of 2 wt%, which had a clear zone diameter of 10.35 mm and was sensitive to bacteria, had a% viability of 2.206%, a swelling value of 71, 7%, and has an antioxidant value of 95%. It shows that the addition of oats can increase the cell viability because oats are antioxidants, so they can counteract the free radicals produced by AgNPs, but the addition of oats increases sensitivity to bacteria because oats also function as antibacterial. Samples with oats of 2 wt% have the best characterization even though they have not met the standard wound dressing.

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Biomass waste as an alternative source of carbon and silicon-based absorbents for CO2 capturing application

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Chemosphere 2023年 343卷

作者： Suresh, R. Gnanasekaran, Lalitha Rajendran, Saravanan Jalil, A.A. Soto-Moscoso, Matias Khoo, Kuan Shiong Ma, Zengling Halimatul Munawaroh, Heli Siti Show, Pau Loke Departamento de Ingeniería Mecánica Facultad de Ingeniería Universidad de Tarapacá Avda. General Velásquez 1775 Arica Chile University Centre for Research & Development Department of Mechanical Engineering Chandigarh University Punjab Mohali140413 India Department of Chemical Engineering Lebanese American University Byblos Lebanon Centre of Hydrogen Energy Institute of Future Energy Johor UTM Johor Bahru81310 Malaysia Faculty of Chemical and Energy Engineering Universiti Teknologi Malaysia Johor UTM Johor Bahru81310 Malaysia Universidad Autónoma de Chile Chile Department of Chemical Engineering and Materials Science Yuan Ze University Taoyuan Taiwan Centre for Herbal Pharmacology and Environmental Sustainability Chettinad Hospital and Research Institute Chettinad Academy of Research and Education Tamil Nadu Kelambakkam603103 India Zhejiang Provincial Key Laboratory for Subtropical Water Environment and Marine Biological Resources Protection Wenzhou University Wenzhou325035 China Study Program of Chemistry Faculty of Mathematics and Science Education Universitas Pendidikan Indonesia Jalan Dr. Setiabudhi 229 Bandung40154 Indonesia Department of Chemical Engineering Khalifa University P.O. Box 127788 Abu Dhabi United Arab Emirates Department of Chemical and Environmental Engineering Faculty of Science and Engineering University of Nottingham Malaysia Jalan Broga Selangor Darul Ehsan Semenyih Malaysia

The production of low-cost solid adsorbents for carbon dioxide (CO2) capture has gained massive consideration. Biomass wastes are preferred as precursors for synthesis of CO2 solid adsorbents, due to their high CO2 adsorption efficiency, and ease of scalable low-cost production. This review particularly focuses on waste biomass-derived adsorbents with their CO2 adsorption performances. Specifically, studies related to carbon (biochar and activated carbon) and silicon (silicates and geopolymers)-based adsorbents were summarized. The impact of experimental parameters including nature of biomass, synthesis route, carbonization temperature and type of activation methods on the CO2 adsorption capacities of biomass-derived pure carbon and silicon-based adsorbents were evaluated. The development of various enhancement strategies on biomass-derived adsorbents for CO2 capture and their responsible factors that impact adsorbent's CO2 capture proficiency were also reviewed. The possible CO2 adsorption mechanisms on the adsorbent's surface were highlighted. The challenges and research gaps identified in this research area have also been emphasized, which will help as further research prospects. © 2023 Elsevier Ltd

关键词： Carbon dioxide

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Multi-Stakeholder Collaboration for the Provision of Public Open Space (Case of Taman Indonesia Kaya, Semarang) 1

Multi-Stakeholder Collaboration for the Provision of Public ...

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1st International Conference on Urban Design and Planning, ICUDEP 2019

作者： Aswad, W.O.S.J. Damayanti, M. Urban and Regional Planning Study Program Faculty of Engineering Diponegoro University Semarang Indonesia Department Urban Dan Regional Planning Faculty of Engineering Diponegoro University Semarang Indonesia

Budget constraints are a common problem in Indonesian cities to provide attractive and attractive public open space. There is a need for cooperation between all parties, not only the government but also the private sector and society. These conditions encourage the Semarang City government to increase stakeholder collaboration in the provision of public green open space, one of which is in the development of Taman Indonesia Kaya. The purpose of this study is to examine the model of the collaboration process, the involvement and role of each stakeholder and the sustainability of collaboration. This study uses descriptive qualitative methods, data collection using observations and interviews on each stakeholder element, namely government, private and public. The results show that the collaboration process model starts from face to face dialogue, trust building, commitment to the process, shared understanding between stakeholders until the realization of attractive and attractive public green open space development. However, the sustainability of collaboration is a big challenge going forward. The structure of cooperation is not yet supported by clear institutional design, so that government courage and innovation are needed to determine the form of structural governance in collaborative management of public green open space. Collaboration should be carried out over the long term and use a networked administrative organization model so that the network that is built is in an administrative entity. The model is expected to create efficiency management and support the sustainability of collaboration. © Published under licence by IOP Publishing Ltd.

关键词： Sustainable development

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High fluorescent carbon dots/Ag as a sensitive sensor for tetracycline waste in aqueous solution 10

High fluorescent carbon dots/Ag as a sensitive sensor for te...

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10th International Seminar on New Paradigm and Innovation of Natural Sciences and itsApplication, ISNPINSA 2020

作者： Alkian, I. Sutanto, H. Hadiyanto, H. Hidayanto, E. Hapsari, H.P. Wibowo, A.A. Syahida, A.N. Irianti, F.D.D. Master Program of Environmental Science School of Postgraduate Studies Diponegoro University Semarang Indonesia Departemen of Physics Faculty of Science and Mathematics Diponegoro University Semarang Indonesia Departemen of Chemical Engineering Faculty of Engineering Diponegoro University Semarang Indonesia Smart Materials Research Center Laboratory Diponegoro University Semarang Indonesia

Currently, antibiotics waste produced by hospitals and pharmacies is increasing, increasing demand and public consumption. Tetracyclines are a popular type of antibiotic that can pollute the environment even in low concentrations. This study aimed to detect tetracyclines in an aqueous environment using C-dots/Ag. C-dots material was synthesized by microwave radiation method with the addition of Ag 0-4 %. C-dots/Ag is produced in the form of a brown-black powder that glows green. FTIR testing shows that C-dots/Ag contains various functional groups O-H, N-H, C-H, C=O, and C=C. The surface morphology of the C-dots based on SEM testing is round and rough. Ag's addition causes C-dots' surface morphology to agglomerate, shifting the C-dots' absorbance peaks towards a larger wavelength and decreasing the energy bandgap. C-dots/Ag 2% has the best optical properties based on the intensity of the resulting fluency. In general, C-dots/Ag has excellent potential to be a susceptible, selective, and effective tetracycline detection agent. © Published under licence by IOP Publishing Ltd.

关键词： Surface morphology

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Unlocking Green Potential: Enhancing Biomass Valorization Via Thermal Depolymerization With Spent Catalysts

SSRN

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SSRN 2023年

作者： Damayanti, Damayanti Wulandari, Yeni Ria Marpaung, David Septian Supriyadi, Didik Yohana, Dian Tessa Saputri, Desi Riana Sanjaya, Andri Fahni, Yunita Taharuddin, Taharuddin Wu, Ho Shing Department of Chemical Engineering Institut Teknologi Sumatera Jl. Terusan Ryacudu Way Huwi Kec. Jati Agung Lampung Selatan 35365 Indonesia Department of Chemical Engineering and Materials Science Yuan Ze University 135 Yuan Tung Road Chung Li Taoyuan320315 Taiwan Study Program of Industrial Chemical Engineering Technology Lampung State Polytechnic Indonesia Department of Biosystems Engineering Institut Teknologi Sumatera Jl. Terusan Ryacudu Way Huwi Kec. Jati Agung Lampung Selatan 35365 Indonesia Institut Teknologi Sumatera Indonesia

Biomass is globally recognized as an up-and-coming environmentally friendly carbon-based energy source, Suitable catalysts for managing thermal depolymerization of biomass present an alternative method for reducing overall energy usage while maintaining the *** spent catalyst could increase bio-organics production by up to 11%,31%,6%,and 21% in rice straw,brown solid,alkaline, and dealkaline lignin pyrolysis, respectively. The amount of biochar produced in the thermal depolymerization was reduced to 18%,27%,35%,and 32% in rice straw, brown solid, alkaline, and dealkaline pyrolysis, respectively, upon utilizing the spent catalyst. These findings indicate the potential of the spent catalyst for the biomass thermal depolymerization process. © 2023, The Authors. All rights reserved.

关键词： Lignin

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Biocompatibility evaluation of electrospun Poly-L lactic Acid-chitosan immobilized with heparin as scaffold for vascular tissue repair

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Journal of Science: Advanced Materials and Devices 2023年第3期8卷

作者： Suroto, Nur Setiawan Al Fauzi, Asra Widiyanti, Prihartini Bella, Fitria Renata Department of Neurosurgery Faculty of Medicine Universitas Airlangga – Dr. Soetomo General Academic Hospital Surabaya Indonesia Biomedical Engineering Study Program Department of Physics Faculty of Science and Technology Universitas Airlangga Jawa Timur 60115 Indonesia

Stroke is the second leading cause of death worldwide, disability, high morbidity, and mortality. One of the leading causes of infarct stroke is carotid stenosis. The postoperative narrowing of the carotid artery diameter is a common complication after primary arterial closure in carotid endarterectomy surgery. A biomaterial design that combines synthetic and natural polymers is a promising strategy for patching arterial closure. In this paper, the electrospinning process was employed and Poly-L Lactic Acid (PLLA) was used as a base material. Chitosan and heparin were added to increase the biocompatibility of the biomaterial. The electrospun PLLA-chitosan immobilized with heparin (C sample) had better characteristics than the pure electrospun PLLA. The fiber diameter decreased to a micrometer scale and the pore size fell and became narrower, resulting in a smoother surface. Fiber diameter results for each sample were 1312.66 nm, 486.29 nm and 387.87 nm. Thereby potentially reducing the activation of blood coagulation and inflammation. The ultimate tensile strength test result for each sample were 2.28 MPa, 3.61 MPa and 3.25 MPa, for elongation results were 12.05%, 17.39%, and 18.14%, aligned with those of the human carotid artery and indicating potential use in patch angioplasty applications. This scaffold nanofiber was declared non-haemolytic for the C sample was 1.13% and non-cytotoxic. Percent viability for each sample was 89.35%, 83.81% and 78.92%. The in vivo host tissue response was shown to decrease pro-inflammatory cytokine expressions. This research shows that the proposed PLLA-chitosan-heparin biomaterial has strong physical properties and can modify the inflammatory response. However, it requires additional biofunctional alterations to optimize its tissue engineering capabilities. © 2023 Vietnam National University, Hanoi

关键词： Chitosan Electrospinning Heparin Poly-L-lactic acid Vascular patch

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Carbonaceous and nitrogenous disinfection by-products potential formation and removal technologies from the water treatment process: A review

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AIP Conference Proceedings 2024年第1期3026卷

作者： Tazkiaturrizki Tazkiaturrizki Sandyanto Adityosulindro Djoko Mulyo Hartono Setyo Sarwanto Moersidik Environmental Engineering Study Program Department of Civil Engineering Faculty of Engineering Universitas Indonesia Depok Indonesia Environmental Engineering Department Faculty of Architecture Landscape and Environmental Engineering Universitas Trisakti Jakarta Indonesia

Not only at the water treatment process, disinfection is required for the inactivation of pathogen microorganisms in wastewater treatment before it is released to the waterbodies or for recycling purposes. During the disinfection process by chlorination, it found the formation of harmful disinfection by-products (DBPs). DBPs formed because of the reaction of inorganic and organic matter as precursors with chlorine/chloramine. The aim of this research is to analyze the potential formation of Carbonaceous Disinfection By-products (C-DBPs) as the most DBPs in the water and Nitrogenous Disinfection By-products (N-DBPs) as the most DBPs of the wastewater. Most DBPs have precursors from natural organic matter (NOM) and the effluent of sewage treatment contributes to increasing the DBPs precursor. The review method start with identifying DBPs precursor, potential formation of DBPs, factor affecting the formation DBPs, and finding the advanced technologies that are appropriate to remove DBPs and their precursors. It found that trihalomethanes (THMs) is the most widely found in water treatment such as chloroform, bromodichloromethane, and bromoform. N-nitrosodimethylamine (NDMA) is one of N-DBPs that most presence in polluted water and also haloacetonitriles (HANs), haloacetamides (HAcAms), Nitrosoamine (NAs), cyanogen halides (CNX), halonitromethanes (HNMs), N-nitrosomethylethylamine (NMEA). The result shows that disinfection plays a role of formation DBPs in water and wastewater treatment. DBPs have potential health risks for the human body because they are genotoxic and carcinogenic. Physicochemical treatment can remove the precursor of DBPs and advanced treatment enhances the removal of DBPs.

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Harnessing Liposomal Nanocellulose Hydrogel for Nir-Light Driven On-Demand Drug Delivery

SSRN

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SSRN 2025年

作者： Gangurde, Puja Gounani, Zahra Polez, Roberta Teixeira Österberg, Monika Lauren, Patrick Lajunen, Tatu Laaksonen, Timo Drug Research Program Division of Pharmaceutical Biosciences Faculty of Pharmacy University of Helsinki Viikinkaari 5 E HelsinkiFI-00790 Finland Department of Bioproducts and Biosystems School of Chemical Engineering Aalto University Espoo02150 Aalto Finland School of Pharmacy University of Eastern Finland P.O. Box 1627 KuopioFI-70211 Finland Faculty of Engineering and Natural Sciences Tampere University TampereFI-33101 Finland

Stimuli-responsive nanoparticles have gained attention for their ability to control drug release via external signals. However, challenges like biodegradation and toxicity hinder their applications. This study introduces a novel system by integrating light-activated liposomes with cellulose nanofiber (CNF) hydrogel, creating a controlled release system where liposomes act as drug reservoirs, protecting drug molecules and preventing unwanted cargo leakage, for on-demand localized drug delivery. Our surface interaction study between cationic liposomes and nanocellulose shows that the liposomes, while not uniformly distributed, are bound to the nanocellulose hydrogel due to strong electrostatic interactions and fiber networks, thus forming a depot-like drug reservoir *** evaluated hydrogel thickness and light dose to optimize the cargo release. Upon activation with near-infrared light (808 nm, 1 W/cm2), the photosensitizer inside the bilayer of thermosensitive liposome generates heat, which makes liposome leaky resulting in on-demand cargo release. We observed up to 50 % release at low dose (20 J/cm2) of light, which increased to 80 % after exposure to higher dose of light (80 J/cm2), highlighting the sensitivity of the system. This dual-platform combines the biocompatibility of nanocellulose with tunability of light-activated liposomes, presenting promising approach for on-demand drug delivery with significant potential for personalized medicine. © 2025, The Authors. All rights reserved.

关键词： Nanofibers

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History Woyla Arc of the Garba Complex: Implications for Tectonic Evolution of the South Sumatra Region, Indonesia

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Journal of Geoscience and Environment Protection 2021年第12期9卷 118-132页

作者： Idarwati Heru Sigit Purwanto Edy Sutriyono Carolus Prasetyadi Stevanus Nalendra Jati Geology Study Program Faculty of Engineering University of Sriwijaya Indralaya Indonesia Department of Geology Faculty of Mineral Technology University of Pembangunan Nasional “Veteran” Yogyakarta Indonesia

Studies on outcrop-scale structures have been conducted at the Garba complex. This study aims to add the high-resolution of the South Sumatra region to reconstruct the structural geology and implications of tectonics for the region. The study area is commonly referred to as crystalline basement highs forming the southwestern boundary of the Paleogene South Sumatra basin. The structures commonly show the NW-SE, NNW-SSE, and ENE-WSW trends. The methodology used includes field mapping, analysis of Digital Elevation Model (DEM), petrography, and X-ray fluorescence (XRF). The major fractures include wrench slip, reverse, and normal faults, while the observable microstructures comprise pull-apart calcite veins, shear joints, boudins, parasitic folds, and the augens. The earlier structuring episode was probably related to crustal extension, perhaps associated with the Paleogene rifting that occurred along the western margin of Sundaland. In the Late Neogene, tectonic compression took place in the entire region, allowing inversion of the Pre-Tertiary sequence. As compression waned in the Pleistocene, extension commenced, and a number of the ENE-WSW tensional block faulting developed and intersected the older NNW-SSE alignments. It is important to note that the latest tectonic event in conjunction with deep erosional denudation had likely exhumed the terrain and eventually shaped the present-day fractured and rough landforms in the study area.

关键词： Basement High Crystalline Sequence Structure Tectonics

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