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Phosphotungstic acid (H₃PW₁₂O₄₀)-loaded onto titanium porous montmorillonite heterostructure for the effective enhanced kinetics and thermodynamic conversion of citronellal

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Case Studies in Chemical and Environmental engineering 2025年 11卷

作者： Fatimah, Is Yahya, Amri Rubiyanto, Dwiarso Sagadevan, Suresh Oh, Won-Chun Doong, Ruey-an Department of Chemistry Faculty of Mathematics and Natural Sciences Universitas Islam Indonesia Kampus Terpadu UII Jl. Kaliurang Km 14 Sleman Yogyakarta Indonesia Nanomaterials and Sustainable Chemistry Research Centre Chemistry Laboratory Universitas Islam Indonesia Kampus Terpadu UII Jl. Kaliurang Km 14 Sleman Yogyakarta Indonesia Chemistry Study Program Nusa Bangsa University JL. KH Sholeh Iskandar KM.4 Tanah Sareal Bogor 16166 Indonesia Nanotechnology & Catalysis Research Centre University of Malaya Kuala Lumpur 50603 Malaysia Department of Advanced Materials Science and Engineering Hanseo University Seosan-si 356-706 South Korea Institute of Analytical and Environmental Sciences National Tsing Hua University 101 Sec 2 Kuang Fu Road Hsinchu 30013 Taiwan

In present work, nanocomposite of phosphotungstic acid (H3PW12O40)-loaded onto titanium-porous clay heterostructure (PTA/Ti–PCH) was prepared using natural montmorillonite as parent material (Mnt). Characterization o... 详细信息

In present work, nanocomposite of phosphotungstic acid (H₃PW₁₂O₄₀)-loaded onto titanium-porous clay heterostructure (PTA/Ti–PCH) was prepared using natural montmorillonite as parent material (Mnt). Characterization of the material was performed using X-ray diffraction, X-ray photoelectron spectroscopy, scanning electron microscopy-energy dispersive X-ray fluorescence, transmission electron microscopy, Fourier-Transform Infra-Red spectroscopy, and solid acidity measurement. The material was examined as superacid catalyst in citronellal conversion into isopulegol by varied reaction conditions. Kinetics and thermodynamic studies of catalyzed reaction revealed the role of increased total surface acidity and the Lewis to Brønsted to enhance the reaction conversion and selectivity. Thermodynamic study demonstrated a lower activation energy of the reaction over PTA/Ti–PCH compared to Ti–PCH. A 100 % conversion was exhibited by the sample during 120 min of the reaction at 90°C, and the sample also demonstrated activity at room temperature. Reusability of the sample was expressed by a maintained conversion until 5th cycle. Conclusively, the prepared material showed a potency to be developed for heterogeneously acid-catalyzed organic reactions. © 2025 The Authors

关键词： Acid Citronellal Clay-based nanocomposite Heterogeneous catalysis Porous clay heterostructure

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Developing critical and creative thinking skills through STEAM integration in chemistry learning 1

Developing critical and creative thinking skills through STE...

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1st International Conference of chemistry 2018, ICCHEM 2018

作者： Rahmawati, Y. Ridwan, A. Hadinugrahaningsih, T. Soeprijanto Chemistry Education Study Program Universitas Negeri Jakarta Rawamangun Muka Street Jakarta Indonesia Electrical Engineering Vocational Education Study Program Universitas Negeri Jakarta Rawamangun Muka Street Jakarta Indonesia

This paper describes a second year of two-year of longitudinal study of the integration of Science, Technology, engineering, Art, and Mathematics (STEAM) in chemistry learning in secondary schools in which the importance of critical and creative thinking skills were explored. The study involved 76 students of Year 11 from two secondary schools in Indonesia. The STEAM integration was implemented in the teaching of acid and base through a project-based learning model. The research employed a qualitative approach to explore the integration of STEAM in chemistry, students' critical and creative thinking skills development. Data were collected through observations, interviews, reflective journals, critical and creative thinking skills assessment. The students develop their STEAM projects by integrating chemistry concepts with STEAM principles. The study results were analyzed based on the pattern themes found in different data sources. It showed that students developed creativity and critical thinking skills. The study faced challenges of STEAM integration with chemistry concepts, empowering teachers, engaging students, and managing time and resources. The integration of STEAM provided the opportunities for students in chemistry learning engagement and several areas of thinking skills development in relation to the current curricula objectives. © Published under licence by IOP Publishing Ltd.

关键词： Integration

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Fabrication a sustainable adsorbent nanocellulose-mesoporous hectorite bead for methylene blue adsorption

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Case Studies in Chemical and Environmental engineering 2024年 10卷

作者： Holilah Asranudin El Messaoudi, Noureddine Ulfa, Maria Hamzah, Amir Hamid, Zuratul Ain Abdul Ramadhani, Dini Viandi Suryanegara, Lisman Mahardika, Melbi Melenia, Alvina Tata Pratama, Agus Wedi Prasetyoko, Didik Research Center for Biomass and Bioproducts National Research and Innovation Agency of Indonesia (BRIN) Research Collaboration Center for Nanocellulose BRIN-Andalas University Research Collaboration Center for Biomass and Biorefinery Between BRIN and Universitas Padjadjaran Laboratory of Applied Chemistry and Environment Faculty of Sciences Ibn Zohr University Chemistry Education Study Program Faculty of Teacher Training and Education Sebelas Maret University Deputy for Infrastructure Research and Innovation National Research and Innovation Agency of Indonesia (BRIN) School of Materials & Mineral Resources Engineering Universiti Sains Malaysia Department of Biology Faculty of Science and Data Analytics Institut Teknologi Sepuluh Nopember Department of Chemistry Faculty of Science and Data Analytics Institut Teknologi Sepuluh Nopember (ITS) Kampus ITS Sukolilo

In this study, fabrication of mesoporous nanocellulose-hectorite-alginate bead (B-NcH) composites and their application for adsorption of MB from water was carried out. The synthesis of nanocellulose (NC) was conducted from mangosteen waste peel (Garcinia mangostana L.). Garcinia mangostana L. peel had 58.9 ± 0,41 % content of cellulose. NCs was successfully isolated using the acid hydrolysis method. NC from Garcinia mangostana L. peel had a diameter of 24.5 ± 0.2 nm and a length of 381.2 ± 10.4 nm. The superabsorbent was composed of nanocrystalline cellulose, mesoporous hectorite, and alginate. The functional group, phase, and morphology of composite was investigated. The composite with 5 % NC had excellent mechanical strength. The B-NcH5 showed a high adsorption capacity of methylene blue (MB), reaching 98.64 % at an adsorbent dose of 30 mg for 90 min. The presence of hectorite can increase the adsorption ability compared to NCs-alginate. The equilibrium adsorption data followed the Freundlich isotherm;however, the kinetics of adsorption showed the usefulness of adopting the PSO kinetic model. The highest adsorption capacity of B-NcH5 for MB was determined to be 57.59 mg/g. For thermodynamic studies, it was revealed that the adsorption of MB on BNcH-5 is a spontaneous and endothermic process. The removal efficiency was observed in six consecutive cycles, indicating at the favorable reusability of this adsorbent. These results validate the potential use of this B-NcH5 adsorbent for water treatment applications. © 2024

关键词： Adsorption Bead Hectorite Methylene blue Nanocellulose Water treatment

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Empowering Biomedical Discovery with AI Agents

arXiv

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arXiv 2024年

作者： Gao, Shanghua Fang, Ada Huang, Yepeng Giunchiglia, Valentina Noori, Ayush Schwarz, Jonathan Richard Ektefaie, Yasha Kondic, Jovana Zitnik, Marinka Department of Biomedical Informatics Harvard Medical School BostonMA United States Department of Chemistry and Chemical Biology Harvard University CambridgeMA United States Program in Biological and Biomedical Sciences Harvard Medical School BostonMA United States Department of Brain Sciences Imperial College London London United Kingdom Harvard College CambridgeMA United States Program in Biomedical Informatics Harvard Medical School BostonMA United States Department of Electrical Engineering and Computer Science MIT CambridgeMA United States Kempner Institute for the Study of Natural and Artificial Intelligence Harvard University MA United States Broad Institute of MIT and Harvard CambridgeMA United States Harvard Data Science Initiative CambridgeMA United States

We envision "AI scientists" as systems capable of skeptical learning and reasoning that empower biomedical research through collaborative agents that integrate AI models and biomedical tools with experimental platforms. Rather than taking humans out of the discovery process, biomedical AI agents combine human creativity and expertise with AI’s ability to analyze large datasets, navigate hypothesis spaces, and execute repetitive tasks. AI agents are poised to be proficient in various tasks, planning discovery workflows and performing self-assessment to identify and mitigate gaps in their knowledge. These agents use large language models and generative models to feature structured memory for continual learning and use machine learning tools to incorporate scientific knowledge, biological principles, and theories. AI agents can impact areas ranging from virtual cell simulation, programmable control of phenotypes, and the design of cellular circuits to developing new therapies. © 2024, CC BY.

关键词： Adversarial machine learning

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Characterization of crystal structure and mechanical properties of polycaprolactone-hydroxyapatite-collagen nanofiber for scaffold anterior cruciate ligament (ACL) applications

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AIP Conference Proceedings 2022年第1期2663卷

作者： Faika Hanum Salsabilah Djony Izak Rudyardjo Sofijan Hadi Tahta Amrillah Aminatun Aminatun 1Program Study of Biomedical Engineering Department of Physics Faculty of Science and Technology Universitas Airlangga Surabaya 60115 Indonesia 2Program Study of Physics Department of Physics Faculty of Science and Technology Universitas Airlangga Surabaya 60115 Indonesia 3Program Study of Chemistry Department of Chemistry Faculty of Science and Technology Universitas Airlangga Surabaya 60115 Indonesia 4Program Study of Nanotechnology Faculty of Advance technology and Multidiscipline-Universitas Airlangga Surabaya 60115 Indonesia

Recently, it was found that the case of knee injuries could reach a prevalence of 48 per 1000 peoples in one year, with 9% being categorized as Anterior Cruciate Ligament (ACL) injuries. The most common cause of ACL injuries is sports activities. Several strategies were used to heal this injury, such as a treatment, up to autographs bone graft surgery. Current research developments lead to the use of artificial ligaments to heal the ACL injuries which have many advantages over autografts. Thus, this present study aims to fabricate the artificial ligament using hydroxyapatite (HA)/collagen/polycaprolactone (PCL) nanofiber composites. Here, we try to determine the effect of variations of HA, collagen, and PCL compositions in the nanofiber composites by studying their crystal structure and mechanical properties (tensile strength). We use variations of PCL: HA: collagen compositions about of 50:45:5, 50:40:10, 50:35:15, 50:30:20, and 50:25:25 wt%, respectively, in the 10% w/v of solution concentrations. In this present research, the nanofiber was fabricated by using electrospinning method with a voltage of 23 kV, while, the distance between the needle and the collector of about of 15 cm. The XRD and tensile strength tests were used to study the effects of PCL: HA: collagen compositions. In the XRD test, we found that the PCL peaks were detected at 2θ = 21° and 23° and HA was found at 2θ = 31°. The PCL crystal size is found to be 47.82-86.87 nm and the degree of crystallinity is 24.31-36.87%. In the mechanical test, the Ultimate Tensile Strength (UTS) value was obtained in the range of 0.942 MPa-2.864 MPa. It was found that the PCL could increase the tensile strength. However, the obtained UTS value is still far from the UTS of the original human ACL value.

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Synthesis activated carbon from shell of Elaeis guineensis Jacq and modified with magnetite (AC-Fe3O4) as adsorbent for waste metal ion Pb(II) in waters

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AIP Conference Proceedings 2024年第1期2970卷

作者： A. S. Zulaicha Buhani A. R. Nuralita A. Setiajaya Cosmetic Engineering Study Program Faculty of Sciences Sumatera Institute of Technology Jl. Terusan Ryacudu Way Huwi Jati Agung South Lampung 35365 Indonesia Department of Chemistry Faculty of Mathematics and Natural Sciences University of Lampung Jl. Sumantri Brojonegoro No 1 Bandar Lampung Lampung 34154 Indonesia Environmental Engineering Study Program Faculty of Sciences Sumatera Institute of Technology Jl. Terusan Ryacudu Way Huwi Jati Agung South Lampung 35365 Indonesia

In this study, the manufacture of palm shell activated carbon was obtained from PT Inti Sentosa Alam Bahtera (ISAB) Lampung. The content of cellulose is quite large, namely 45% and hemicellulose 26%, which causes this oil palm shell to be used as a basic material for making activated carbon. This study proposes to modify activated carbon using magnetite (AC-Fe3O4). Modified physical-chemical activated carbon is exhausted as an adsorbent which has the advantage of facilitating the filtration or separation process with the adsorbate. The adsorbent test used an adsorbate in the form of heavy metal ions Pb(II). The XRD characterization of AC-Fe3O4 has intensity peaks at 2θ at 30, 35, 43, and 56° which are consistent with the XRD pattern of magnetite. SEM-EDX characterization was also carried out to see differences in morphology and elemental composition between unmodified activated carbon and AC-Fe3O4. Then the external range analysis was carried out using the BET (surface area) method. As well as identification of the amount of metal ions Pb(II) adsorbed using Atomic Absorption Spectrophotometry (AAS). The test results on the adsorbent (AC-Fe3O4) were carried out at the optimum variation, namely the adsorbent dose of 0.1 grams, contact time of 120 minutes, and at a dilution of 300 mg/L. Based on the zeta potential, the pH of PZC was obtained, namely 6 as the pH of the adsorbate solution with a Q value (number of Pb(II) ions adsorbed) of 6.175 mg/g. Adsorption isotherms tend to follow the pattern of Freundlich adsorption isotherms.

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Tailoring acid-base properties on metal-free zeolite from Indonesia kaolin to enhance the CO₂ hydrogenation to CH₄

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Case Studies in Chemical and Environmental engineering 2024年 10卷

作者： Sholeha, Novia Amalia Dewanto, Bintang Jovita, Stella Nugraha, Reva Edra Taufiq-Yap, Yun Hin Ulfa, Maria Fauzi, Anees Ameera Jalil, Aishah Abdul Bahruji, Hasliza Prasetyoko, Didik College of Vocational Studies Bogor Agricultural University (IPB University) Jalan Kumbang No. 14 Bogor 16151 Indonesia Department of Chemistry Faculty of Science Institut Teknologi Sepuluh Nopember Keputih Sukolilo Surabaya 60111 Indonesia Department of Chemical Engineering Faculty of Engineering Universitas Pembangunan Nasional “Veteran” Jawa Timur Surabaya 60294 Indonesia Department of Chemistry Faculty of Science Universiti Putra Malaysia Serdang Selangor Malaysia Chemistry Education Study Program Faculty of Teacher Training and Education Sebelas Maret University Jl. Ir. Sutami 36A Surakarta 57126 Indonesia Research Center for Biomass and Bioproduct National Research and Innovation Agency (BRIN) Indonesia Department of Chemical Engineering Faculty of Chemical and Energy Engineering Universiti Teknologi Malaysia UTM Skudai Johor Johor Bahru 81310 Malaysia Centre of Hydrogen Energy Institute of Future Energy Universiti Teknologi Malaysia UTM Skudai Johor Johor Bahru 81310 Malaysia Centre of Advanced Material and Energy Science Universiti Brunei Darussalam Jalan Tungku Link BE 1410 Brunei Darussalam

The catalytic thermal conversion of carbon dioxide is essential for carbon capture, storage, and utilization, helping to reduce CO2 emissions and potentially stimulating future economic activities. Zeolite Y, ZSM-5, B... 详细信息

The catalytic thermal conversion of carbon dioxide is essential for carbon capture, storage, and utilization, helping to reduce CO₂ emissions and potentially stimulating future economic activities. Zeolite Y, ZSM-5, BEA, and A were synthesized using the hydrothermal technique from Indonesian kaolin to examine the potential use of zeolite as a catalyst without metal nanoparticles. In the absence of metal, catalytic activity for CO₂ methanation relies solely on textural properties and basicity-acidity. Zeolite Y exhibits the highest CO₂ conversion at 36.64 % and attained 100 % of CH₄ selectivity at 400 °C. The exceptional CO₂ conversion of zeolite Y relies on a high basicity level of 1.02 mmol/g, as shown by CO₂-TPD analysis, and a relatively low acid site concentration of 1.48 mmol/g, as determined by NH₃-TPD analysis. ZSM-5, BEA, and zeolite A, demonstrated CO₂ conversion of 29.85 %, 23.86 %, and 12.15 %, respectively. Stability studies revealed ZSM-5 maintains methane (CH₄) selectivity of 94 %, which is only slightly lowered by 6 % for 30 hours, while zeolite Y achieved 90 % selectivity for 26 hours. The presence of mesopores in zeolite ZSM-5 reduced coke or carbon production, maintaining crystalline framework. © 2024 The Authors

关键词： Basicity Greenhouse carbon dioxide Metal free catalyst Methane Zeolite

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The potency of hydrothermally prepared sulfated silica (SO4/SiO2) as a heterogeneous acid catalyst for ethanol dehydration into diethyl ether

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Chemosphere 2023年第1期341卷

作者： Pratika, Remi Ayu Wijaya, Karna Utami, Maisari Mulijani, Sri Patah, Aep Alarifi, Saud Ram Mani, Ravishankar Kumar Yadav, Krishna Ravindran, Balasubramani Chung, Woo Jin Chang, Soon Woong Munusamy-Ramanujam, Ganesh Study Program of Chemistry Faculty of Mathematics and Natural Sciences Universitas Palangka Raya Palangka Raya Indonesia Department of Chemistry Faculty of Mathematics and Natural Sciences Universitas Gadjah Mada Yogyakarta55281 Indonesia Department of Chemistry Faculty of Mathematics and Natural Sciences Universitas Islam Indonesia Yogyakarta55584 Indonesia Department of Chemistry Faculty of Mathematics and Natural Sciences Institut Pertanian Bogor Bogor Indonesia Department of Chemistry Faculty of Mathematics and Natural Sciences Institut Teknologi Bandung Bandung Indonesia Department of Zoology College of Science King Saud University P.O. Box 2455 Riyadh11451 Saudi Arabia Department of Pharmaceutical Biology Faculty of Pharmaceutical Sciences UCSI University Cheras Taman Connaught Kuala Lumpur56000 Malaysia Faculty of Science and Technology Madhyanchal Professional University Ratibad Bhopal462044 India Environmental and Atmospheric Sciences Research Group Scientific Research Center Al-Ayen University Thi-Qar Nasiriyah 64001 Iraq Department of Environmental Energy and Engineering Kyonggi University Yeongtong-Gu Gyeonggi-Do Suwon16227 Korea Republic of Department of Medical Biotechnology and Integrative Physiology Institute of Biotechnology Saveetha School of Engineering Saveetha Institute of Medical and Technical Sciences Thandalam Tamil Nadu Chennai602105 India Molecular Biology and Immunobiology Division Interdisciplinary Institute of Indian System of Medicine SRM-IST Tamil Nadu Kattankulathur603203 India

The dehydration of ethanol into diethyl ether over a SO4/SiO2 catalyst was investigated. The SO4/SiO2 catalysts were prepared by the sulfation method using 1, 2, and 3 M of sulfuric acid (SS1, SS2, and SS3) via hydrothermal treatment. This study is focused on the synthesis of a SO4/SiO2 catalyst with high total acidity that can be subsequently utilized to convert ethanol into diethyl ether. The total acidity test revealed that the sulfation process increased the total acidity of SiO2. The SS2 catalyst (with 2 M sulfuric acid) displayed the highest total acidity of 7.77 mmol/g, whereas the SiO2 total acidity was only 0.11 mmol/g. Meanwhile, the SS3 catalyst (with 3 M sulfuric acid) has a lower total acidity of 7.09 mmol/g due to the distribution of sulfate groups on the surface having reached its optimum condition. The crystallinity and structure of the SS2 catalyst were not affected by the hydrothermal treatment or the sulfate process on silica. Furthermore, The SS2 catalyst characteristics in the presence of sulfate lead to a flaky surface in the morphology and non-uniform particle size. In addition, the surface area and pore volume of the SS2 catalyst decreased (482.56–172.26 m2/g) and (0.297–0.253 cc/g), respectively, because of the presence of sulfate on the silica surface. The SS2 catalyst's pore shape information explains the formation of non-uniform pore sizes and shapes. Finally, the activity and selectivity of SO4/SiO2 catalysts in the conversion of ethanol to diethyl ether yielded the highest ethanol conversion of 70.01% and diethyl ether product of 9.05% from the SS2 catalyst (the catalyst with the highest total acidity). Variations in temperature reaction conditions (175–225 °C) show an optimum reaction temperature to produce diethyl ether at 200 °C (11.36%). © 2023 Elsevier Ltd

关键词： Silica

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chemistry in context: The development of hydrocarbon chemistry and petroleum module based on vehicle case 1

Chemistry in context: The development of hydrocarbon chemist...

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1st International Conference of chemistry 2018, ICCHEM 2018

作者： Febrianto Wiyarsi, A. Partana, C.F. Sulistyo, B. Study Program of Chemistry Education Faculty of Mathematics and Natural Sciences Universitas Negeri Yogyakarta Indonesia Department of Chemistry Education Faculty of Mathematics and Natural Science Universitas Negeri Yogyakarta Indonesia Automotive Engineering Education Department Faculty of Engineering Universitas Negeri Yogyakarta Indonesia

This study aims to analyze the characteristic, feasibility, teachers' and students' responses of Hydrocarbon chemistry and Petroleum (HCP) module based on the context of vehicle case on automotive engineering. Exploratory mixed method has been employed in this research. The research procedures used four steps including qualitative, development, quantitative, and interpretation step. The instruments used to collect the data consisting the three questionnaires, one open questionnaire to obtain the validation and two close questionnaires to collect the teachers and students' responses toward the HCP module. HCP module based on the context of vehicle case on automotive engineering program was yielded as a result of this reseach. The characteristic of research product was integrating between chemistry and automotive subject based on basic competence of curriculum and integrated by vehicle context in first chapter, concept map, activities, examples, and exercise. A group of experts consisting two lectures were confirmed that the HCP module has a correct chemistry content. A very good category was given as the response of the teacher. Moreover, the students response were very interest toward the HCP module. The students and the tachers could be utilize the HCP module as learning sources reference to gain a succesfull chemistry learning. © Published under licence by IOP Publishing Ltd.

关键词： Vehicles

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Automotive engineering chemistry module: Exploring acid base and electrochemistry topic in vehicle context 1

Automotive engineering chemistry module: Exploring acid base...

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1st International Conference of chemistry 2018, ICCHEM 2018

作者： Febiana, H. Partana, C.F. Wiyarsi, A. Sulistyo, B. Study Program of Chemistry Education Faculty of Mathematics and Natural Sciences Universitas Negeri Yogyakarta Indonesia Chemistry Education Department Faculty of Mathematics and Natural Science Universitas Negeri Yogyakarta Indonesia Automotive Engineering Education Department Faculty of Engineering Universitas Negeri Yogyakarta Indonesia

The research purposed to analyze the characteristics of chemistry module on acid-base and electrochemistry topic based on vehicle context, to analyze the feasibility of module according to chemistry learning experts and to analyze the response of chemistry teachers and students of Automotive engineering program (AEP) about this module. This research using mixed methods and exploratory model design. The data collected from expert validation sheets also teachers and students response questionnaire. Technique of data analysis begins by converting qualitative data into quantitative data using Likert scales. Furthermore, the total and average score of each component can be determined from the quantitative data. The result of the average scores were converted into qualitative feasibility criteria according to the rating category. The product of the development was a chemistry module on acid-base and electrochemistry topic based on vehicle context for students in AEP. The experts considered feasibility of the module. This module had assessed by 5 teachers and 10 students. The module assessed by teachers showed a very good response while the module assessed by students showed a good response. Therefore, this module is feasible and can be used as a learning resource for students of AEP to enhance quality of chemistry learning. © Published under licence by IOP Publishing Ltd.

关键词： Students

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