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Effect of Sn addition on electrochemical activity of ribbons of Mg-Al-Ca anode material for rechargeable magnesium batteries fabricated by rapid solidification

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Keikinzoku/Journal of Japan Institute of Light Metals 2025年第1期75卷 9-13页

作者： Fukuta, Yoshitaka Kikura, Kensei Tsukeda, Tadayoshi Aida, Tetsuo Tabata, Hironobu Kurihara, Hideki Suzuki, Mayumi Program of Materials Science and Engineering Studies in Science and Engineering Graduate School of Science and Engineering University of Toyama 3190 Gofuku Toyama-shi Toyama930-8555 Japan Graduate School of Science and Engineering University of Toyama Toyama-shi Toyama Japan Faculty of Sustainable Design Academic Assembly University of Toyama Toyama-shi Toyama Japan CHUETSU METAL WORKS CO. LTD. Nakaniikawagun Toyama Japan Saitama Industrial technology Center Kawaguchi-shi Saitama Japan Department of Mechanical Systems Engineering Faculty of Engineering Toyama Prefectural University Imizu-shi Toyama Japan

Magnesium-based batteries are potential candidates for next-generation rechargeable batteries due to the divalent nature of magnesium cations and the natural abundance of magnesium resources. In this study, the electrochemical activity of Mg-6mass%Al-3mass%Ca anodes combined with Sn was investigated. Thin ribbons of the anode specimens were prepared by a single-roll rapid solidification method. The results showed that the electrochemical activity increased upon adding 1 mass% Sn, while it decreased for 3 mass% Sn. Based on the results of an X-ray diffraction analysis, the addition of Sn led to the formation of Mg2Sn and Ca2Sn phases, which increased the lattice distortion. Scanning electron microscopy observations indicated that these secondary phases were homogeneously distributed for 1 mass% Sn addition, while they were coarsely distributed for 3 mass% Sn. © 2025 The Japan Institute of Light Metals.

关键词： X ray diffraction analysis

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Synthesis, characterization, and interfacial adhesion of titania iodine-doped nanotubes architectures on additively manufactured Ti-6Al-4 V implant

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Materialwissenschaft und Werkstofftechnik 2025年第3期56卷 438-454页

作者： Taweekitikul, P. Aliyu, A.A. Decha-Umphai, D. Tantavisut, S. Khamwannah, J. Puncreobutr, C. Lohwongwatana, B. Biomedical Engineering Program Faculty of Engineering Chulalongkorn University Bangkok10330 Thailand Trauma Unit Department of Orthopaedic Queen Savang Vadhana Memorial Hospital Chonburi20110 Thailand Biomedical Engineering Research Center Chulalongkorn University Bangkok10330 Thailand M3D Laboratory Advanced Materials Analysis Research Unit Department of Metallurgical Engineering Faculty of Engineering Chulalongkorn University Phayathai Road Wangmai Pathumwan District Bangkok10330 Thailand Biomechanics Research Center Meticuly Co. Ltd. Chulalongkorn University Bangkok10330 Thailand Hip Fracture Research Unit Department of Orthopaedic Faculty of Medicine Chulalongkorn University Bangkok10330 Thailand Department of Metallurgical Engineering Faculty of Engineering Chulalongkorn University Bangkok10330 Thailand CambridgeMA02139 United States

This study aimed to synthesize, characterize, and evaluate the adhesion strength of titania nanotubes (titania nanotubes) and iodine-doped titania nanotubes (I-titania nanotubes) architectures on the additively manufactured Ti-6Al-4 V (Ti64) implant surface. The titania nanotubes and I-titania nanotubes were synthesized through two stages of electrochemical anodization, whereby titania nanotubes are anodically fabricated through a conventional approach and then modified by replacing the ethylene glycol electrolyte with potassium iodide solution. The characterization results revealed the formation of α-Ti, β-Ti, and titanium iodide (TiI2) phases on the titania nanotubes and I-titania nanotubes surfaces. The morphology of titania nanotubes exhibits a consistent diameter, evenly distributed, well-ordered array, and densely packed nanotubular structures. Formation of a water-soluble fluoride-rich [TiF6]2 complexes in the inner titania nanotubes surface and incessant nanotube′s sidewall etching resulted in poor interfacial titania nanotubes adhesion to the titanium-substrate surface. Iodine doping on the titania nanotubes is believed to reduce the [TiF6]2 complexes accumulation and the titania nanotubes sidewall etching. This facilitates the adhesion and interfacial mechanical anchorage between the titania nanotubes and the surface of the Ti64 implant. The hardness and adhesion strength of the titania nanotubes increased by more than 50 %, due to the formation of a hard titanium iodide film at the titania nanotubes/I-titania nanotubes surfaces and interfaces. © 2025 The Author(s). Materialwissenschaft und Werkstofftechnik published by Wiley-VCH GmbH.

关键词： Potassium iodide

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A bioactive glass functional hydrogel enhances bone augmentation via synergistic angiogenesis,self-swelling and osteogenesis

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Bioactive materials 2023年第4期22卷 201-210页

作者： Fujian Zhao Zhen Yang Huacui Xiong Yang Yan Xiaofeng Chen Longquan Shao Stomatological Hospital Southern Medical UniversityGuangzhou510280China Department of Biomedical Engineering School of Materials Science and EngineeringSouth China University of TechnologyGuangzhou510641China National Engineering Research Center for Tissue Restoration and Reconstruction South China University of TechnologyGuangzhou510006China Guangdong Provincial Key Laboratory of Construction and Detection in Tissue Engineering Guangzhou510515China

Bone augmentation materials usually cannot provide enough new bone for dental implants due to the material degradation and mucosal *** use of hydrogels with self-swelling properties may provide a higher bone augmentation,although swelling is generally considered to be a disadvantage in tissue ***,a double-crosslinked gelatin-hyaluronic acid hydrogels(GH)with self-swelling properties were ***,niobium doped bioactive glasses(NbBG)was dispersed in the hydrogel network to prepare the GH-NbBG *** composite hydrogel exhibited excellent biocompatibility and the addition of NbBG significantly improved the mechanical properties of the *** vivo results found that GH-NbBG synergistically promoted angiogenesis and increased bone augmentation by self-swelling at the early stage of *** addition,at the late stage after implantation,GH-NbBG significantly promoted new bone formation by activating RUNX2/Bglap signaling ***,this study reverses the self-swelling disadvantage of hydrogels into advantage and provides novel ideas for the application of hydrogels in bone augmentation.

关键词： Bioactive glass Bone formation Osteogenesis Angiogenesis

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Supertough spontaneously self-healing polymer based on septuple dynamic bonds integrated in one chemical group

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science China Chemistry 2022年第2期65卷 363-372页

作者： Luzhi Zhang Qingbao Guan Ao Shen Rasoul Esmaeely Neisiany Zhengwei You Meifang Zhu State Key Laboratory for Modification of Chemical Fibers and Polymer Materials Shanghai Belt and Road Joint Laboratory of Advanced Fiber and Low-dimension Materials(Donghua University)College of Materials Science and EngineeringShanghai Engineering Research Center of Nano-Biomaterials and Regenerative MedicineInstitute of Functional MaterialsDonghua UniversityResearch Base of Textile Materials for Flexible Electronics and Biomedical ApplicationsChina Textile Engineering SocietyShanghai 201620China Department of Materials and Polymer Engineering Hakim Sabzevari UniversitySabzevar ***Iran

The development of spontaneously self-healing materials with excellent mechanical properties remains a formidable challenge despite the extensive interest in such *** is because the self-healing and mechanical properties of a material are usually optimized via contradictory *** present study demonstrated a supertough spontaneously self-healing polymer,Fe-(2,6-diacetylpyridine dioxime)-urethane-based polyurethane(Fe-PPOU)based on septuple dynamic bonds integrated in one chemical group.A synergistic effect was induced by the presence of multiple dynamic crosslinking points,which comprised the integrated dynamic interactions,and the hidden lengths of the folded polymeric chains in ***,the mechanical and self-healing properties of the polymer were simultaneously ***-PPOU demonstrated the highest reported toughness(139.8 MJ m^(-3))among all the room-temperature spontaneously self-healing polymers with a nearly 100%healing ***-PPOU exhibited instant(30 s)self-healing to reach a strength of 1.6 MPa that was higher than the original strength of numerous recently reported self-healing polymers.

关键词： oxime-urethane bonds hydrogen bonds metal-coordination bonds 2 6-diacetylpyridine dioxime self-healing

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Novel GaN-Based Substrates with Gold Nanostructures for Ultra-Sensitive SERS Analysis: Micro-Nano Pit Morphology for Enhanced Molecular Detection

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Journal of Medical and Biological engineering 2024年第4期44卷 522-530页

作者： Ko, Tsung-Shine Deng, Chen-An Shieh, Jiann Huang, Hung Ji Lin, Yung-Sheng Lin, Yang-Wei Du, Yi-Chun Department of Electronic Engineering National Changhua University of Education Changhua Taiwan Department of Materials Science and Engineering National United University Miaoli Taiwan Department of Electro-Optical Engineering National Formosa University Taiwan Department of Chemical Engineering National United University Miaoli Taiwan Department of Chemistry National Changhua University of Education Changhua Taiwan Department of Biomedical Engineering National Cheng Kung University Tainan Taiwan Medial Device Innovation Center National Cheng Kung University Tainan Taiwan

Purpose: Surface-enhanced Raman scattering (SERS) is a technique for trace analysis detection based on the interaction of light with matter and between materials. In the past development of SERS, precious metals were primarily chosen as substrates due to their high electromagnetic effect, which leads to significantly enhanced SERS signals. However, the effect of using only precious metals is limited. Therefore, this study utilizes the characteristic micro-nano V-shaped pits that appear on the surface of c-plane GaN after wet etching. By depositing a gold film of various thicknesses, we aim to increase the contact area with the target molecule Rhodamine 6G (R6G), thereby further enhancing the sensitivity of SERS detection. Methods: After fabricating pitted c-plane GaN using chemical etching techniques, we analyzed the sample surface with a scanning electron microscope and assessed the impact of different gold film thicknesses on the SERS intensity of R6G using Raman spectroscopy. The comprehensive biomedical detection effectiveness was also evaluated using contact angle measurement, and fluorescence microscopy. Results: For the target molecule R6G, after depositing a 25 nm gold film, the enhancement factor of the substrate for detection reached 2.21×108, and the limit of detection was achieved at a concentration of 10− 10 M. Conclusion: This study confirms the feasibility of using wet etching techniques on hexagonal materials like GaN for SERS applications. The GaN substrate with V-shaped pits provides an increased surface area, effectively enhancing SERS signal strength. This offers different choices and perspectives for SERS substrate selection in the detection of various target molecules. © Taiwanese Society of biomedical engineering 2024.

关键词： Nanostructures

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Plasma-Enabled Graphene Quantum Dot Hydrogel-Magnesium Composites as Bioactive Scaffolds for In Vivo Bone Defect Repair

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ACS Applied materials and Interfaces 2023年第38期15卷 44607-44620页

作者： Wong, Pei-Chun Kurniawan, Darwin Wu, Jia-Lin Wang, Wei-Ru Chen, Kuan-Hao Chen, Chieh-Ying Chen, Ying-Chun Veeramuthu, Loganathan Kuo, Chi-Ching Ostrikov, Kostya Ken Chiang, Wei-Hung Graduate Institute of Biomedical Optomechatronics College of Biomedical Engineering Taipei Medical University Taipei110 Taiwan Orthopedics Research Center Taipei Medical University Hospital Taipei110 Taiwan Department of Chemical Engineering National Taiwan University of Science and Technology Taipei10607 Taiwan Department of Orthopedics School of Medicine College of Medicine Taipei Medical University Taipei110 Taiwan Department of Orthopedics Taipei Medical University Hospital Taipei110 Taiwan Centers for Regional Anesthesia and Pain Medicine Wan Fang Hospital Taipei Medical University Taipei110 Taiwan School of Biomedical Engineering College of Biomedical Engineering Taipei Medical University Taipei110 Taiwan Graduate Institute of Biomedical Materials and Tissue Engineering College of Biomedical Engineering Taipei Medical University Taipei110 Taiwan Department of Orthopedics Shuang Ho Hospital Taipei Medical University New Taipei235 Taiwan Department of Mechanical Engineering National Taiwan University of Science and Technology Taipei10607 Taiwan Department of Molecular Science and Engineering Institute of Organic and Polymeric Materials National Taipei University of Technology Taipei106 Taiwan BrisbaneQLD4000 Australia

Bioactive and mechanically stable metal-based scaffolds are commonly used for bone defect repair. However, conventional metal-based scaffolds induce nonuniform cell growth, limiting damaged tissue restoration. Here, we develop a plasma nanotechnology-enhanced graphene quantum dot (GQD) hydrogel-magnesium (Mg) composite scaffold for functional bone defect repair by integrating a bioresource-derived nitrogen-doped GQD (NGQD) hydrogel into the Mg ZK60 alloy. Each scaffold component brings major synergistic advantages over the current alloy-based state of the art, including (1) mechanical support of the cortical bone and calcium deposition by the released Mg2+ during degradation;(2) enhanced uptake, migration, and distribution of osteoblasts by the porous hydrogel;and (3) improved osteoblast adhesion and proliferation, osteogenesis, and mineralization by the NGQDs in the hydrogel. Through an in vivo study, the hybrid scaffold with the much enhanced osteogenic ability induced by the above synergy promotes a more rapid, uniform, and directional bone growth across the hydrogel channel, compared with the control Mg-based scaffold. This work provides insights into the design of multifunctional hybrid scaffolds, which can be applied in other areas well beyond the demonstrated bone defect repair. © 2023 American Chemical Society.

关键词： Semiconductor quantum dots

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Tin-induced microstructural changes and associated corrosion resistance of biodegradable Mg–Zn alloy

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Rare Metals 2022年第3期41卷 883-888页

作者： Yun Gao Ping Zhao Xiang-Qian Cao R.Devesh K.Misra Wei Wang Ke-Zheng Chen Laboratory of Functional and Biomedical Nanomaterials College of Materials Science and EngineeringQingdao University of Science and TechnologyQingdao 266042China Shandong Provincial University Laboratory for Protected Horticulture&Architecture and Art College Weifang University of Science and TechnologyWeifang 262700China Department of Metallurgical Materials and Biomedical EngineeringUniversity of TexasEl PasoTX 79968USA

As a new degradable medical metal material, Mg–Zn alloy has been widely used in clinical application. However, its popularization and application are seriously restricted by poor corrosion performance in the biological liquid environment. For this reason, we added a relatively non-toxic element to the human body (Sn) to Mg–Zn alloy, and we prepared Mg–2Zn–3Sn ternary system alloy.

关键词： alloy corrosion alloy.

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Downsizing and soft X-ray tomography for cellular uptake of interpenetrated metal-organic frameworks

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Journal of materials Chemistry B 2024年第25期12卷 6079-6090页

作者： Yu, Yu-Sheng Liang, Yung-Yi Hsieh, Chia-Chun Lin, Zi-Jing Cheng, Po-Hsiu Cheng, Chih-Chan Chen, Shu-Ping Lai, Lee-Jene Wu, Kevin C.-W. National Taiwan University Department of Chemical Engineering Taipei Taiwan National Health Research Institute Institute of Biomedical Engineering and Nanomedicine Miaoli Taiwan Hsinchu Taiwan International Graduate Program of Molecular Science and Technology Taiwan International Graduate Program Academia Sinica Taipei Taiwan National Taiwan University Taipei Taiwan

Metal-organic frameworks (MOFs) are porous materials with potential in biomedical applications such as sensing, drug delivery, and radiosensitization. However, how to tune the properties of the MOFs for such applications remains challenging. Herein, we synthesized two MOFs, Zr-PEB and Hf-PEB. Zr-PEB can be classified as porous interpenetrated zirconium frameworks (PIZOFs) and Hf-PEB is its analogue. We controlled their sizes while maintaining their crystal structure by employing a coordination modulation strategy. They were designed to serve as sensitizer for X-ray therapy and as potential drug carriers. Comprehensive characterizations of the MOFs' properties have been conducted, and the in vitro biological impacts have been studied. Since viability assay showed that Hf-PEB was more biocompatible compared to Zr-PEB, the cellular uptake of Hf-PEB by cells was evaluated using both fluorescence microscopy and soft X-ray tomography (SXT), and the three-dimensional structure of Hf-PEB in cells was observed. The results revealed the potential of Zr-PEB and Hf-PEB as nanomaterials for biomedical applications and demonstrated that SXT is an effective tool to assist the development of such materials. © 2024 The Royal Society of Chemistry.

关键词： Organometallics

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Enhanced Responsivity of Solar Blind Ultraviolet Photodetector by PEALD Deposited Zn-Doped Ga2O3Thin Films

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IEEE Transactions on Electron Devices 2024年第1期71卷 664-669页

作者： Fan, Hui-Chen Wang, Chen Ruan, Yu-Jiao Shen, Kun-Ching Wu, Wan-Yu Wuu, Dong-Sing Lai, Feng-Min Lien, Shui-Yang Zhu, Wen-Zhang Xiamen Institute of Measurement and Testing National Measurement and Testing Center for Flat Panel Display Industry Xiamen361024 China Fuzhou University College of Physics and Information Engineering Fuzhou350108 China National United University Department of Materials Science and Engineering Miaoli36063 Taiwan National Chi Nan University Department of Applied Materials and Optoelectronic Engineering Nantou54561 Taiwan Xiamen University of Technology Xiamen Key Laboratory of Development and Application for Advanced Semiconductor Coating Technology School of Opto-Electronic and Communication Engineering Xiamen361026 China Da-Yeh University Department of Biomedical Engineering Changhua51591 Taiwan

In this article, the tunable Zn-doped Ga2O3 films were obtained by introducing ZnO intercalation during the film deposition using plasma-enhanced atomic layer deposition (PEALD). The effect of the ZnO cycle ratio on the performance of solar-blind photodetectors (PDs) was first analyzed. Compared to the pure Ga2O3, an obviously enhanced performance of Zn-doped Ga2O3 films PDs was observed by the introduction of Zn dopants, especially photocurrent or responsivity, even if the light intensity is low. A high sensitivity of Zn-doped Ga2O3 PD has been achieved with superior photoelectric characteristics for an extremely low dark current of 2.22 × 10-13 A, an ultrahigh light ON/ OFF current ratio of 2.89 × 106, and a satisfactory responsivity of 104 mA/W when the ZnO cycle ratio is 5%. The above excellent results imply that the Zn-doped Ga2O3 PD can be greatly beneficial to the application in deep-ultraviolet (DUV) detection. © 1963-2012 IEEE.

关键词： II-VI semiconductors

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Smart bioadhesives for wound healing and closure

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Bioactive materials 2023年第1期19卷 360-375页

作者： Jia Zhu Honglei Zhou Ethan Michael Gerhard Senhao Zhang Flor Itzel Parra Rodríguez Taisong Pan Hongbo Yang Yuan Lin Jian Yang Huanyu Cheng Department of Engineering Science and Mechanics The Pennsylvania State UniversityUniversity ParkPA16802USA AML Department of Engineering MechanicsTsinghua UniversityBeijing100084China Institute of Flexible Electronics Technology of THU ZhejiangJiaxing314000China Department of Biomedical Engineering The Pennsylvania State UniversityUniversity ParkPA16802USA Suzhou Institute of Biomedical Engineering and Technology Chinese Academy of ScienceSuzhou215011PR China School of Materials and Energy State Key Laboratory of Electronic Thin Films and Integrated DevicesUniversity of Electronic Science and Technology of ChinaChengdu610054PR China Materials Research Institute The Pennsylvania State UniversityUniversity ParkPA16802USA

The high demand for rapid wound healing has spurred the development of multifunctional and smart bioadhesives with strong bioadhesion,antibacterial effect,real-time sensing,wireless communication,and on-demand treatment *** with bio-inspired structures and chemicals have shown unprecedented adhesion strengths,as well as tunable optical,electrical,and bio-dissolvable *** wound healing has been achieved via directly released antibacterial and growth factors,material or drug-induced host immune responses,and delivery of curative *** recently,the integration of biosensing and treatment modules with wireless units in a closed-loop system yielded smart bioadhesives,allowing real-time sensing of the physiological conditions(e.g.,pH,temperature,uric acid,glucose,and cytokine)with iterative feedback for drastically enhanced,stage-specific wound healing by triggering drug delivery and treatment to avoid infection or prolonged *** rapid advances in the burgeoning field,challenges still exist in the design and fabrication of integrated systems,particularly for chronic wounds,presenting significant opportunities for the future development of next-generation smart materials and systems.

关键词： Smart bioadhesives Immunomodulatory bioadhesives Mechanically/electrically active bioadhesives Closed-loop system On-demand treatments Wound healing and closure

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