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Tailoring precipitate distribution in 2024 aluminum alloy for improving strength and corrosion resistance

Journal of materials science & technology 2024年第27期194卷 16-27页

作者： Yong Zhang Lantian Zhang Xiang Gao Xulong An Le Zong Zhihong Jia Hao Zhou Yudong Sui Wenwen Sun Jiangsu Key Laboratory for Advanced Metallic Materials School of Materials Science and EngineeringSoutheast UniversityNanjing 211189China Department of Materials Science and Engineering Monash UniversityClaytonVICAustralia School of Materials Science and Engineering Changzhou UniversityChangzhou 213164China Key Laboratory for Light-weight Materials Nanjing Tech UniversityNanjing 210009China Nano and Heterogeneous Materials Center School of Materials Science and EngineeringNanjing University of Science and TechnologyNanjing 210094China School of Materials Science and Engineering Kunming University of Science and TechnologyKunming 650093China

For the traditional peak-aged (PA) AA2024 alloy, the formation of large S-phase precipitates within the grains, wide precipitate-free zones (PFZs) near the grain boundaries (GBs), and continuous distribution of grain boundary precipitates (GBPs) can be observed. As a result, the PA alloy exhibits relatively high strength but poor corrosion resistance. However, with the application of cyclic plasticity treatment, high-density 1–2 nm clusters form within the matrix, and no PFZs form near GBs. In this study, this treatment yields the optimal balance between strength–elongation characteristics and corrosion resistance. By combining cyclic plasticity and ageing heat treatment with different heating rates, the nanoscale clusters play a crucial role as heterogeneous nucleation sites, resulting in the formation of finer and higher number density of S precipitates within the matrix. Additionally, the presence of these clusters reduces the formation of GBPs and minimizes the width of PFZs. Consequently, compared to the traditional PA sample, this approach achieves a significantly higher yield strength (increased by 46 %) and ultimate tensile strength (increased by 18 %), along with superior corrosion resistance. Although the influence of ageing heat treatment with different rates on mechanical properties is not significant, it notably affects the formation of GBPs and corrosion resistance. Specifically, a slower heating rate leads to an increase in the spacing between adjacent GBPs, resulting in improved corrosion resistance. In summary, cyclic strengthening, as a novel method for alloy strengthening, when combined with ageing heat treatment, modulates the distribution of S precipitates within the matrix and GBs. This optimization maximizes the effects of precipitation strengthening and breaks the inverse relationship between strength and corrosion resistance.

关键词： Aluminum alloys Mechanical properties Intergranular corrosion Cyclic plasticity Precipitate-free zone Grain boundary precipitates

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Multi-Scale Time Series Segmentation Network Based on Eddy Current Testing for Detecting Surface Metal Defects

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IEEE/CAA Journal of Automatica Sinica 2025年第3期12卷 528-538页

作者： Xiaorui Li Xiaojuan Ban Haoran Qiao Zhaolin Yuan Hong-Ning Dai Chao Yao Yu Guo Mohammad S.Obaidat George Q.Huang the School of Intelligence Science and Technology University of Science and Technology Beijing the Beijing Advanced Innovation Center for Materials Genome Engineering the Key Laboratory of Intelligent Bionic Unmanned Systems and the Institute of Materials Intelligent Technology Liaoning Academy of Materials IEEE the Department of Computer Science Hong Kong Baptist University the School of Computer and Communication Engineering Key Laboratory of Advanced Materials and Devices for Post-Moore Chips Ministry of Education University of Science and Technology Beijing the Beijing Advanced Innovation Center for Materials Genome Engineering University of Science and Technology Beijing the School of Computer and Communication Engineering University of Science and Technology Beijing the King Abdullah Ⅱ School of Information Technology The University of Jordan the Department of Computational Intelligence the School of Computing SRM University the School of Engineering The Amity University The Hong Kong Polytechnic University

In high-risk industrial environments like nuclear power plants, precise defect identification and localization are essential for maintaining production stability and safety. However, the complexity of such a harsh environment leads to significant variations in the shape and size of the defects. To address this challenge, we propose the multivariate time series segmentation network(MSSN), which adopts a multiscale convolutional network with multi-stage and depth-separable convolutions for efficient feature extraction through variable-length templates. To tackle the classification difficulty caused by structural signal variance, MSSN employs logarithmic normalization to adjust instance distributions. Furthermore, it integrates classification with smoothing loss functions to accurately identify defect segments amid similar structural and defect signal subsequences. Our algorithm evaluated on both the Mackey-Glass dataset and industrial dataset achieves over 95% localization and demonstrates the capture capability on the synthetic dataset. In a nuclear plant's heat transfer tube dataset, it captures 90% of defect instances with75% middle localization F1 score.

关键词： Eddy current testing nondestructive testing semantic segmentation time series analysis

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ZIF-8 modified by isocyanate as a photocatalytic antibacterial agent

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Rare Metals 2024年第6期43卷 2708-2718页

作者： Yi-Ning Zhang Zhen Pei Zi-Hao Wang Chong-En Wang Fen-Fen Liang Li-Qiao Wei College of Architecture Taiyuan University of TechnologyTaiyuan 030024China Key Laboratory of Interface Science and Engineering in Advanced Materials of Taiyuan University of Technology Ministry of EducationTaiyuan 030024China Department of Materials Science and Engineering Shanxi Institute of TechnologyYangquan 045000China Shanxi-Zheda Institute of Advanced Materials and Chemical Engineering Taiyuan 030000China

Zeolite imidazole skeleton(ZIF-8)is a promising option for self-cleaning of building exterior walls due to its large specific surface area,high antibacterial activity and low ***,it suffers from low antibacterial efficiency and yield under visible light *** address the issues,we developed the photocatalytic materials T-ZIF-8-TDI(thermally treated-ZIF-8-toluene 2,4-diisocyanate)by modifying ZIF-8 with thermal oxygen sensitization and chemical *** results show that the yield of T-ZIF-8-TDI photocatalytic antibacterial agent is increased to 11.5 times of that of T-ZIF-8,while maintaining the crystal structure of T-ZIF-8 and thermal stability up to 60℃.Furthermore,T-ZIF-8-TDI exhibits extended optical response range to the nearinfrared region,significantly narrowed band gap,improved photogenerated elec tron-hole separation efficiency,reduced recombination rate,and excellent photocatalytic *** the concentration of antibacterial agent is 600 mg·L^(-1),the antibacterial rate of Escherichia coli(***)reaches 99.99%irradiated by visible light for30 min,and when the concentration of antibacterial agent is 200 mg·L^(-1),the antibacterial rate of Staphylococcus aureus(***)reaches 99.99%irradiated by visible light for 25 *** also analyzed the reasons in detail from the aspects of bacterial species and antibacterial mechanism,and proposed the antibacterial mechanism of·O_(2)^(-)and h^(+)as the main active *** findings suggest that T-ZIF-8-TDI photocatalytic antibacterial agent has potential for use in self-cleaning of building exterior walls.

关键词： ZIF-8 Hot oxygen sensitization Modified by isocyanate Antimicrobial performance Photocatalytic antibacterial mechanism

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MgO-attached graphene nanosheet(MgO@GNS)reinforced magnesium matrix nanocomposite with superior mechanical,corrosion and biological performance

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International Journal of Minerals,Metallurgy and materials 2024年第9期31卷 2062-2076页

作者： S.Abazari A.Shamsipur H.R.Bakhsheshi-Rad M.S.Soheilirad F.Khorashadizade S.S.Mirhosseini Department of Materials and Metallurgical Engineering Amirkabir University of TechnologyTehran ***Iran Iranian National Standards Organization of Hormozgan HormozganIran Advanced Materials Research Center Department of Materials EngineeringNajafabad BranchIslamic Azad UniversityNajafabadIran Department of Materials and Metallurgical Engineering Iran University of Science and TechnologyTehranIran

Magnesium(Mg)alloys are gaining great consideration as body implant materials due to their high biodegradability and ***,they suffer from low corrosion resistance and antibacterial *** this research,semi-powder metallurgy followed by hot extrusion was utilized to produce the magnesium oxide@graphene nanosheets/magnesium(MgO@GNS/Mg)composite to improve mechanical,corrosion and cytocompatibility *** have revealed that the incorporation of MgO@GNS nanohybrids into Mg-based composite enhanced microhardness and compressive *** vitro,osteoblast cell culture tests show that using MgO@GNS nanohybrid fillers enhances osteoblast adhesion and apatite *** presence of MgO@GNS nanoparticles in the composites decreased the opening defects,micro-cracks and micro-pores of the composites thus preventing the penetration of the corrosive solution into the *** demonstrated that the MgO@GNS/Mg composite possesses excellent antibacterial properties because of the combination of the release of MgO and physical damage to bacterium membranes caused by the sharp edges of graphene nanosheets that can effectively damage the cell wall thereby facilitating penetration into the bacterial lipid ***,the MgO@GNS/Mg composite with high mechanical strength,antibacterial activity and corrosion resistance is considered to be a promising material for load-bearing implant applications.

关键词： metal matrix composites MgO@GNS nanohybrid strengthening mechanisms antibacterial activity biocompatibility

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High-strength and thermally stable TiB_(2)-modified Al-Mn-Mg-Er-Zr alloy fabricated via selective laser melting

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International Journal of Minerals,Metallurgy and materials 2024年第10期31卷 2221-2232页

作者： Jiang Yu Yaoxiang Geng Yongkang Chen Xiao Wang Zhijie Zhang Hao Tang Junhua Xu Hongbo Ju Dongpeng Wang School of Materials Science and Engineering Jiangsu University of Science and TechnologyZhenjiang 212003China Beijing Advanced Innovation Center for Materials Genome Engineering Institute for Advanced Materials and TechnologyUniversity of Science and Technology BeijingBeijing 100083China National Engineering Research Center of Near-Net Shape Forming for Metallic Materials Guangdong Provincial Key Laboratory for Processing and Forming of Advanced Metallic MaterialsSouth China University of TechnologyGuangzhou 510640China CEMMPRE-Centre for Mechanical Engineering Materials and Processes Department of Mechanical EngineeringUniversity of CoimbraRua Luís Reis SantosCoimbra 3030-788Portugal

To increase the processability and plasticity of the selective laser melting(SLM)fabricated Al-Mn-Mg-Er-Zr alloys,a novel TiB_(2)-modified Al-Mn-Mg-Er-Zr alloy with a mixture of Al-Mn-Mg-Er-Zr and nano-TiB_(2) powders was fabricated by *** pro-cessability,microstructure,and mechanical properties of the alloy were systematically investigated by density measurement,microstruc-ture characterization,and mechanical properties *** alloys fabricated at 250 W displayed higher relative densities due to a uni-formly smooth top surface and appropriate laser energy *** maximum relative density value of the alloy reached(99.7±0.1)%,demonstrating good *** alloy exhibited a duplex grain microstructure consisting of columnar regions primarily and equiaxed regions with TiB_(2),Al6Mn,and Al3Er phases distributed along the grain *** directly aging treatment at a high tem-perature of 400℃,the strength of the SLM-fabricated TiB_(2)/Al-Mn-Mg-Er-Zr alloy increased due to the precipitation of the secondary Al6Mn *** maximum yield strength and ultimate tensile strength of the aging alloy were measured to be(374±1)and(512±13)MPa,*** SLM-fabricated TiB_(2)/Al-Mn-Mg-Er-Zr alloy demonstrates exceptional strength and thermal stability due to the synergistic effects of the inhibition of grain growth,the incorporation of TiB_(2) nanoparticles,and the precipitation of secondary Al6Mn nanoparticles.

关键词： selective laser melting aluminum alloy processability mechanical properties thermal stability

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Role of solute elements in Mg-Mg_(2)Ni hydrogen storage alloys:A first-principles calculation study

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Journal of Magnesium and Alloys 2024年第11期12卷 4574-4593页

作者： Min-Seok Yoon Jae Hur Seo-Hui Park Ui-Jong Lee Guanglong Xu Hyung-Ki Park Byeong-Chan Suh Young Min Kim Won-Seok Ko Department of Materials Science and Engineering Inha UniversityIncheon 22212Republic of Korea College of Materials Science and Engineering Nanjing Tech UniversityNanjing 211816China Functional Materials and Components R&D Group Korea Institute of Industrial TechnologyGangneung 25440Republic of Korea Advanced Metals Division Korea Institute of Materials ScienceChangwon 51508Republic of Korea Advanced Materials Engineering University of Science and TechnologyDaejeon 34113Republic of Korea

The effects of various alloying elements on the performance of Mg-Mg_(2)Ni hydrogen storage alloys were investigated by performing firstprinciples density functional theory *** examined the important characteristics of hydrogen storage alloys by considering both Mg-based solid solution and Mg_(2)Ni-based intermetallic compound phases,where the hydride forms are Mg H2and Mg_(2)NiH4,*** particular,qualitatively valid information for predicting changes in plateau pressures in the pressure-composition-temperature(PCT)curve was provided by calculating changes in the energy of related hydrogenation *** effects of alloying elements on volume changes due to hydrogenation reactions were also obtained to provide additional criteria for the practical use of hydrogen storage *** the Mg_(2)Ni-based intermetallic compound,we examined the site preference of each alloying element,considering the designated stoichiometry of the base *** on the revealed site preferences,the effects of various possible alloying elements on the properties of Mg_(2)Ni-based hydrides were also *** structure analyses were further conducted to elucidate the detailed mechanisms underlying the role of the additional solute elements.

关键词： Mg-Mg_(2)Ni alloys Density functional theory Hydrogen storage alloys Metal hydrides

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Application of high-temperature confocal scanning laser microscopy to investigate non-metallic inclusions in steel:a review

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Journal of Iron and Steel Research International 2025年第2期32卷 334-352页

作者： N.Preisser Y.Wang J.Cejka I.Gruber W.Mu S.K.Michelic Christian Doppler Laboratory for Inclusion Metallurgy in Advanced Steelmaking Montanuniversitaet LeobenLeoben8700Austria Engineering Materials Department of Engineering Science and MathematicsLuleåUniversity of TechnologyLuleå97187Sweden Department of Materials Science and Engineering KTH Royal Institute of TechnologyStockholm10044Sweden

High-temperature confocal scanning laser microscopy(HT-CSLM)is a potent methodology for investigating various phenomena in the field of *** applied to the observation of solid phase transformations and solidification,this method has gained traction in the field of non-metallic inclusion in steels in recent *** overview of the experimental capabilities of HT-CSLM and the most important results of recent investigations regarding the topics of clean steel production are *** includes the formation of intragranular acicular ferrite(IAF)from the surface of non-metallic inclusions during the continuous cooling and heat treatment,which can be especially beneficial in the toughness of heat-affected zones of welded ***,the investigation of agglomeration mechanisms of non-metallic inclusions(NMIs)in liquid steel is discussed to improve the insight into attraction forces between particles and clogging phenomena during continuous ***,the dissolution of NMIs in various steelmaking slags can be observed by HT-CSLM to compare dissolution rates and mechanisms of NMI,where significant influences of temperature and chemical composition of the slag were *** but not least,the experimental work regarding the interface between steel and slag is discussed,where novel techniques are currently being developed.A comprehensive summary of experimental techniques using HT-CSLM equipment to investigate different interactions of NMIs with steel and slag phases is compiled.

关键词： Non-metallic inclusion Steel High-temperature confocal scanning laser microscopy Interfacial phenomenon Kinetics

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Segregation behaviors in{101^(-)1}compressive twin boundaries of Mg-RE alloy under deformation at room temperature

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Journal of Magnesium and Alloys 2025年第1期13卷 330-337页

作者： Yujie Cui Lili Guo Yunwei Gui Kenta Aoyagi Haotian Tong Qinqin Wei Fangzhou Liu Yuichiro Hayasaka Akihiko Chiba Beijing Advanced Innovation Center for Materials Genome Engineering University of Science and Technology BeijingBeijing 100083China Key Laboratory for Advanced Materials Processing(MOE) University of Science and Technology BeijingBeijing 100083China Beijing Laboratory of Metallic Materials and Processing for Modern Transportation Institute for Advanced Materials and TechnologyUniversity of Science and Technology BeijingBeijing 100083China School of Materials Science and Engineering University of Science and Technology BeijingBeijing 100083China Institute for Materials Research Tohoku University2-1-1 KatahiraAoba-kuSendaiMiyagi 980-8577Japan Department of Materials Science and Engineering Jilin University5988 Renmin StreetChangchunJilin 130025China School of Materials Science and Engineering Wuhan University of TechnologyWuhan 430070China The Electron Microscopy Center Tohoku UniversitySendai 980-8577Japan

Solute atoms and precipitates significantly influence the mechanical properties of Mg *** studies have mainly focused on the segregation behaviors of Mg alloys after *** this study,we investigated the segregation behaviors of an Mg-RE alloy under *** found that the enrichment of solute atoms occurred in{101^(-)1}compressive twin boundaries under compression at 298 K without any annealing in an Mg-RE alloy by scanning transmission electron microscopy and energy-dispersive X-ray *** segregated solutes and precipitates impeded the twin growth,partially contributing to the formation of small-sized{101^(-)1}compressive *** research indicates the twin boundaries can be strengthened by segregated solutes and precipitates formed under deformation at room temperature.

关键词： Magnesium alloys Compression test Scanning/transmission electron microscopy(STEM) Segregation Twin boundaries

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Structural Difference in the Core-forming Block Reshapes RAFT-mediated Polymerization-induced Self-assembly

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Chinese Journal of Polymer science 2025年第3期43卷 429-438页

作者： Yue-Xi Zhan Li Zhang Chun Feng Jian-Bo Tan Department of Polymeric Materials and Engineering School of Materials and EnergyGuangdong University of TechnologyGuangzhou 510006China Guangdong Provincial Key Laboratory of Functional Soft Condensed Matter Guangzhou 510006China Shanghai Key Laboratory of Advanced Polymeric Materials School of Materials Science and EngineeringEast China University of Science and TechnologyShanghai 200237China

Polymerization-induced self-assembly(PISA)has become one of the most versatile approaches for scalable preparation of linear block copolymer nanoparticles with various ***,the controlled introduction of branching into the core-forming block and the effect on the morphologies of block copolymer nanoparticles under PISA conditions have rarely been ***,a series of multifunctional macromolecular chain transfer agents(macro-CTAs)were first synthesized by a two-step green light-activated photoiniferter polymerization using two types of chain transfer monomers(CTMs).These macro-CTAs were then used to mediate reversible addition-fragmentation chain transfer(RAFT)dispersion polymerization of styrene(St)to prepare block copolymers with different core-forming block structures and the *** effect of the core-forming block structure on the morphology of block copolymer nanoparticles was investigated in *** electron microscopy(TEM)analysis indicated that the brush-like core-forming block structure facilitated the formation of higher-order morphologies,while the branched core-forming block structure favored the formation of lower-order ***,it was found that using macroCTAs with a shorter length also promoted the formation of higher-order ***,structures of block copolymers and the assemblies were further controlled by changing the structure of macro-CTA or using a binary mixture of two different *** expect that this work not only sheds light on the synthesis of block copolymer nanoparticles but also provide important mechanistic insights into PISA of nonlinear block copolymers.

关键词： Polymerization-induced self-assembly RAFT polymerization Block copolymer nanoparticles Branched structure

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Ultra-high-temperature application of MXene: Stabilization of 2D Ti_(3)C_(2)T_(x) for cross-scale strengthening and toughening of 3D TiC

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Journal of advanced Ceramics 2024年第1期13卷 1-10页

作者： Lu Liu Guobing Ying Quanguo Jiang Dong Wen Peng Wang Meng Wu Ziying Ji Yongting Zheng Xiang Wang Department of Materials Science and Engineering College of Mechanics and MaterialsHohai UniversityNanjing 211100China Key Laboratory of Superlight Materials&Surface Technology Ministry of EducationHarbin Engineering UniversityHarbin 150001China Shenzhen Key Laboratory for Advanced Materials School of Materials Science and EngineeringHarbin Institute of Technology(Shenzhen)Shenzhen 518055China Center for Composite Materials and Structures Harbin Institute of TechnologyHarbin 150001China

Transition metal carbide/nitride cores within MXenes make them considerably useful for ultra-high-temperature ***,extensive research on Ti_(3)C_(2)T_(x) MXene has revealed its tendency to undergo a phase transition to TiCy at temperatures above 800℃due to high activity of a superficial Ti atomic ***,spark plasma sintering of Ti_(3)C_(2)T_(x) and TiC is performed to prevent the Ti_(3)C_(2)T_(x) phase transition at temperatures up to 1900℃through the fabrication of composites at a pressure of 50 *** a focused ion beam scanning electron microscope to separate layered substances in the composites and examining selected area diffraction spots in a transmission electron microscope enabled identification of non-phase-transitioned ***-principles calculations based on density functional theory indicated the formation of strong chemical bonding interfaces between Ti_(3)C_(2)T_(x) and TiC,which imposed a stability constraint on the Ti atomic layer at the Ti_(3)C_(2)T_(x) *** performance tests,such as three-point bending and fracture toughness analysis,demonstrated that the addition of Ti_(3)C_(2)T_(x) can effectively improve the cross-scale strengthening and toughening of the TiC matrix,providing a new path for designing and developing two-dimensional(2D)carbides cross-scale-enhanced three-dimensional(3D)carbides with the same elements relying on a wide variety of MXenes.

关键词： MXene ultra-high-temperature phase stability interface bonding cross-scale strengthening and toughening structural ceramic composites

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