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Synthesis of amorphous silica from rice husk ash using the sol–gel method: Effect of alkaline and alkaline concentration

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Materials Today: Proceedings 2023年 87卷 225-229页

作者： Aprilia S. Rosnelly C.M. Zuhra Fitriani F. Haffiz Akbar E. Raqib M. Rahmah K. Amin A. Baity R.A. Department of Chemical Engineering Engineering Faculty Universitas Syiah Kuala Banda Aceh 23111 Indonesia Doctoral Program School of Engineering Post Graduate Program Universitas Syiah Kuala Banda Aceh 23111 Indonesia Mechanical Engineering Department Engineering Faculty University of Abulyatama Lampoh Keude-Aceh Besar Indonesia

In this study, silica extraction from RHA (rice husk ash) has been successfully performed by alkaline using KOH and NaOH with sol–gel precipitation. The silica gel was characterized for the functional group by FTIR, crystallinity with XRD, structure silica with SEM and particle size with PSA. The results show the higher concentration of solvent led to higher silica. The FTIR analysis revealed vibrations of Si[sbnd]O and Si[sbnd]O[sbnd]Si on the product. Additionally, observed to be amorphous and aggregated, the silica extracted from RHA also exhibited a decrease in all samples. © 2023

关键词： Alkaline extraction Concentration of solvent Potassium hydroxide Rice husk ash Silica Sodium hydroxide

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Supercritical CO2 mediated construction of aluminium waste recovered γ-Al2O3 impregnated Dracaena trifasciata biomass-derived carbon composite: A robust electrocatalyst for mutagenic pollutant detection

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Journal of Colloid and Interface Science 2024年 659卷 71-81页

作者： Pandiyarajan, Sabarison Manickaraj, Shobana Sebastin Mary Liao, Ai-Ho Baskaran, Gopinath Selvaraj, Manickam Assiri, Mohammed A. Zhou, Hong Chuang, Ho-Chiao Department of Chemical Engineering and Biotechnology National Taipei University of Technology Taipei106344 Taiwan Department of Mechanical Engineering National Taipei University of Technology Taipei106344 Taiwan Graduate Institute of Biomedical Engineering National Taiwan University of Science and Technology Taipei106335 Taiwan Department of Biomedical Engineering National Defense Medical Center Taipei114201 Taiwan Global Calcium Pvt. Ltd. Karnataka Banglore India Department of Chemistry Faculty of Science King Khalid University Abha61413 Saudi Arabia Department of Electronics Information and Communication Engineering Osaka Institute of Technology 5-16-1 Omiya Osaka Asahi-ku535-8585 Japan

Inspired by the waste-to-wealth concept, we have recovered the gamma phase aluminium oxide nanoparticles (γ-Al2O3 NPs) from waste aluminium (Al) foils and fabricated a composite with Dracaena trifasciata biomass-derived activated carbon matrix (DT-AC) using supercritical carbon-di-oxide (SC-CO2) pathway. The prepared samples are characterized altogether by various micro- and spectroscopic analyses. Based on the results, the recovered γ-Al2O3 NPs are well impregnated in the DT-AC surface by the action of the microbubble effect from the SC-CO2. The higher D-band and ID/IG value of 1.07 in the Al2O3/DT-AC nanocomposite indicate increased defects and the amorphous nature of the carbon materials. The effect of scan rate (ν) demonstrated greater linearity in ν1/2 vs peak current in the electrochemical detection study of the mutagenic pollutant 4-(methylamino) phenol hemi sulfate, showing a quasi-reversible electron transfer process undergoing diffusion-controlled kinetics. Furthermore, the limit of detection is determined to be 3.2 nM L–1 with an extensive linear range, spanning from 0.05 to 618.25 µM/L. The incredible sensitivity of 2.117 μA μM−1 cm−2, along with excellent selectivity, repeatability, and stability, is observed. Further, the respectable recovery percentage of 98.61 % in the environmental water sample is perceived. The observed outcomes suggest that the prepared Al2O3/DT-AC composite performs as an excellent electrocatalyst material, and the processing techniques used are thought to be sustainable in nature. © 2023 Elsevier Inc.

关键词： Aluminum oxide

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A Virtual Characterization of QUAD and DOUBLE-DOUBLE Laminates: Buckling Studies

A Virtual Characterization of QUAD and DOUBLE-DOUBLE Laminat...

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AIAA Science and Technology Forum and Exposition, AIAA SciTech Forum 2025

作者： Avila, Antonio F. Mapa, Lidianne P.P. Department of Mechanical Engineering Universidade Federal de Minas Gerais Belo Horizonte Minas Gerais31270-901 Brazil Mechanical Engineering Graduate Studies Program Universidade Federal de Minas Gerais Belo Horizonte Minas Gerais31270-901 Brazil

ISBN: (纸本)9781624107238

A new strategy for virtually designing and analyzing double-double laminates to resist buckling under uniaxial compression or in-plane shear conditions has been proposed. This approach combines the off-the-shelf method for carbon/epoxy prepregs with the master-ply concept. The off-the-shelf method utilizes unidirectional prepregs (0° and 90°) and non-crimped fabrics (±30°, ±45°, and 90°). The strength of this non-dimensional design strategy lies in its simplicity, requiring only two parameters: Tsai’s modulus and the number of repetitions. Results were compared with finite element analyses, showing good agreement in all cases. The double-double formulation not only provides higher buckling loads for both uniaxial compression and in-plane shear but also results in distinct buckling modes. © 2025, American Institute of Aeronautics and Astronautics Inc, AIAA. All rights reserved.

关键词： Buckling loads

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Fabrication of versatile poly(xylitol sebacate)-co-poly(ethylene glycol) hydrogels through multifunctional crosslinkers and dynamic bonds for wound healing

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Acta Biomaterialia 2023年 170卷 344-359页

作者： Yeh, Ying-Yu Lin, Yi-Yun Wang, Ting-Teng Yeh, Yu-Jia Chiu, Ting-Hsiang Wang, Reuben Bai, Meng-Yi Yeh, Yi-Cheun Institute of Polymer Science and Engineering National Taiwan University Taipei Taiwan Institute of Biomedical Engineering National Taiwan University Taipei Taiwan Biomedical Engineering Program Graduate Institute of Applied Science and Technology National Taiwan University of Science and Technology Taipei Taiwan Institute of Food Safety and Health National Taiwan University Taipei Taiwan Graduate Institute of Biomedical Engineering National Taiwan University of Science and Technology Taipei Taiwan Adjunct Appointment to the Department of Biomedical Engineering National Defense Medical Center Taipei Taiwan Program National Taiwan University Taipei Taiwan GIP-TRIAD Master's Degree in Agro-Biomedical Science National Taiwan University Taipei Taiwan

Poly(polyol sebacate) (PPS) polymer family has been recognized as promising biomaterials for biomedical applications with their characteristics of easy production, elasticity, biodegradation, and cytocompatibility. Poly(xylitol sebacate)-co-poly(ethylene glycol) (PXS-co-PEG) has been developed to fabricate PPS-based hydrogels;however, current PXS-co-PEG hydrogels presented limited properties and functions due to the limitations of the crosslinkers and crosslinking chemistry used in the hydrogel formation. Here, we fabricate a new type of PXS-co-PEG hydrogels through the use of multifunctional crosslinkers as well as dynamic bonds. In our design, polyethyleneimine-polydopamine (PEI-PDA) macromers are utilized to crosslink aldehyde-functionalized PXS-co-PEG (APP) through imine bonds and hydrogen bonds. PEI-PDA/APP hydrogels present multiple functional properties (e.g., fluorescent, elastomeric, biodegradable, self-healing, bioadhesive, antioxidant, and antibacterial behaviors). These properties of PEI-PDA/APP hydrogels can be fine-tuned by changing the PDA grafting degrees in the PEI-PDA crosslinkers. Most importantly, PEI-PDA/APP hydrogels are considered promising wound dressings to promote tissue remodeling and prevent bacterial infection in vivo. Taken together, PEI-PDA/APP hydrogels have been demonstrated as versatile biomaterials to provide multiple tailorable properties and desirable functions to expand the utility of PPS-based hydrogels for advanced biomedical applications. Statement of significance: Various strategies have been developed to fabricate poly(polyol sebacate) (PPS)-based hydrogels. However, current PPS-based hydrogels present limited properties and functions due to the limitations of the crosslinkers and crosslinking chemistry used in the hydrogel formation. This work describes that co-engineering crosslinkers and interfacial crosslinking is a promising approach to synthesizing a new type of poly(xylitol sebacate)-co-poly(ethylene glycol) (PXS-co-

关键词： Polyols

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Pose Synchronization for Semi-Autonomous Dynamic Robotic Swarms with a Passivity-Short Human Operator 49

Pose Synchronization for Semi-Autonomous Dynamic Robotic Swa...

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49th Annual Conference of the IEEE Industrial Electronics Society, IECON 2023

作者： Kanazawa, Reo Murao, Toshiyuki Kawai, Hiroyuki Kanazawa Institute of Technology Graduate Program in Mechanical Engineering Ishikawa Japan Kanazawa Institute of Technology Department of Robotics Ishikawa Japan

ISBN: (纸本)9798350331820

This paper presents a pose synchronization method for semi-autonomous dynamic robotic swarms with a passivityshort human operator. In the human-robot network, a human operator sends a command signal to and receives visual information from only a part of the robotic group. In this setting, the proposed dynamic control scheme achieves not only pose synchronization of all mobile robots but also convergence to the reference pose that the human operator specifies. The main advantage of the proposed method is to guarantee convergence of not only the position but also the orientation to the reference ones in the human-robot network. Finally, we provide human-in-the-loop simulation results through the human operation using a tablet PC to illustrate the performance of the proposed control method. © 2023 IEEE.

关键词： Synchronization

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Microwave dielectric and structural characteristics in Li2O-B2O3-SiO2 glass ceramics

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Ceramics International 2025年第16期51卷 22925-22931页

作者： Qiu, Jun-Yan Tu, Chi-Shun Huang, Szu-Ting Li, Yongxiang Chen, Pin-Yi Chen, Cheng-Sao Montecillo, Rhys Feng, Kuei-Chih International Ph.D. Program in Innovative Technology of Biomedical Engineering and Medical Devices Ming Chi University of Technology New Taipei City Taiwan Department of Physics Fu Jen Catholic University New Taipei City Taiwan Department of Mechanical Engineering Ming Chi University of Technology New Taipei City Taiwan School of Engineering RMIT University MelbourneVIC3000 Australia Research Center for Intelligent Medical Devices Ming Chi University of Technology New Taipei City Taiwan Department of Mechanical Engineering Hwa Hsia University of Technology New Taipei City Taiwan

Advancements in high-frequency communication devices have emphasized miniaturization and low energy consumption. This work focuses on developing microwave dielectric materials characterized by an ultra-low dielectric constant and low dielectric loss coefficient. In this study, B2O3 and Li2O were added into the SiO2 matrix to form the LBS glass-ceramics. The B2O3-added SiO2 shows a formation of α-cristobalite phase, and the Li2O additive in the B2O3-SiO2 glass-ceramics sintered at 900 °C reveal a primary quartz phase with a secondary phase Li2Si2O5, that partially transformed into Li2SiO3 in the specimen sintered at 950 °C. The LBS12 (x = 12 wt%) show stronger Raman peaks of Li2Si2O5 and Li2SiO3, indicating increase of highly-crystallized Si-O network. As the quartz phase diminishes, Li2Si2O5 and Li2SiO3 begin to develop in the glass-ceramic matrix. Dense microstructures and well-formed crystalline grains were observed in the LBS glass-ceramics. The quality factors were primarily affected by grain size and density. The Li2Si2O5 additive in the LBS glass-ceramics can reduce dielectric permittivity (Εr) and increase Q × f, particularly at higher frequencies. A low Εr of 4.7–5, a high Q × f of 2600 GHz, and a hardness of 249 MHV were achieved in the LBS12 sintered at 900 °C. These LBS glass-ceramics exhibit potential for use in low-temperature co-fired ceramic (LTCC) applications in high-frequency communication devices. © 2025

关键词： Sintering

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Optically-generated focused ultrasound for noninvasive brain stimulation with ultrahigh precision

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Light(Science & Applications) 2022年第11期11卷 2817-2831页

作者： Yueming Li Ying Jiang Lu Lan Xiaowei Ge Ran Cheng Yuewei Zhan Guo Chen Linli Shi Runyu Wang Nan Zheng Chen Yang Ji-Xin Cheng Department of Mechanical Engineering Boston UniversityBostonMA 02215USA Graduate Program for Neuroscience Boston UniversityBostonMA 02215USA Department of Electrical and Computer Engineering Boston UniversityBostonMA 02215USA Department of Chemistry Boston UniversitBostonMA 02215USA Department of Biomedical Engineering Boston UniversityBostonMA 02215USA Division of Materials Science and Engineering Boston UniversityBostonMA 02215USA Department of Biological Engineering Massachusetts Institute of TechnologyCambridgeMA 02142USA

High precision neuromodulation is a powerful tool to decipher neurocircuits and treat neurological *** non-invasive neuromodulation methods offer limited precision at the milimeter ***,we report opticallygenerated focused ultrasound(OFUS)for non-invasive brain stimulation with ultrahigh *** is generated by a soft optoacoustic pad(SOAP)fabricated through embedding candle soot nanoparticles in a curved polydimethylsiloxane *** generates a transcranial ultrasound focus at 15 MHz with an ultrahigh lateral resolution of 83μm,which is two orders of magnitude smaller than that of conventional transcranial-focused ultrasound(tFUS).Here,we show effective OFUS neurostimulation in vitro with a single ultrasound *** demonstrate submillimeter transcranial stimulation of the mouse motor cortex in *** acoustic energy of 0.6 mJ/cm?,four orders of magnitude less than that of tFUS,is suffcient for successful OFUS *** offers new capabilities for neuroscience studies and disease treatments by delivering a focus with ultrahigh precision noninvasively.

关键词： SOAP stimulation precision

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Development of a Gesture Analysis System for Human System Interaction 13

Development of a Gesture Analysis System for Human System In...

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Joint 13th International Conference on Soft Computing and Intelligent Systems and 25th International Symposium on Advanced Intelligent Systems, SCIS and ISIS 2024

作者： Matsumoto, Chifuyu Sone, Yuka Woo, Jinseok Ohyama, Yasuhiro Graduate School of Engineering Tokyo University of Technology Sustainable Engineering Program 1404-1 Katakuracho Hachioji Tokyo192-0982 Japan School of Engineering Tokyo University of Technology Department of Mechanical Engineering 1404-1 Katakuracho Hachioji Tokyo192-0982 Japan

ISBN: (纸本)9798350373332

Recently, Japan has been facing various social issues, and to solve these problems, it is necessary to create a society where diverse people can live comfortably. To build such a society, appropriate support tailored to individuals is required, necessitating the analysis of various types of information to understand the people's needs at any given moment. In particular, analyzing non-verbal elements such as posture, facial expressions, and gestures is crucial, as these naturally indicate a person's condition. Therefore, this study focuses on human gestures, one of the non-verbal elements, and proposes a gesture recognition method using Dynamic Time Warping (DTW) and K-Means. We demonstrated that symbolic gesture recognition is possible by recording arm trajectories from skeletal measurements with an RGB-D camera. © 2024 IEEE.

关键词： Gesture recognition

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Thermoeconomic and thermoenvironmental analysis of the chilled water system in a shopping mall

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INTERNATIONAL JOURNAL OF REFRIGERATION 2022年 134卷 304-311页

作者： Abreu, Renata Portela Correia, Victor Hugo Lobo Lourenco, Atilio Barbosa Marques, Adriano da Silva Carvalho, Monica [a]Graduate Program of Mechanical Engineering Federal University of Paraíba João Pessoa Brazil [b]Department of Mechanical Engineering Federal University of Espírito Santo Vitória Brazil [c]Department of Mechanical Engineering Federal Rural University of Pernambuco Cabo de Santo Agostinho Brazil [d]Department of Renewable Energy Engineering Federal University of Paraíba João Pessoa Brazil

This is the first study to apply a combination of two thermoeconomic approaches (UFS and H & S) with Life Cycle Assessment (LCA) to a chilled water system installed in a shopping mall. The objective is to obtain monetary and environmental costs for the thermal energy stored by developing both thermoeconomic and thermoenvir-onmental assessments. The thermoeconomic study determined internal flows, defined inputs and products, and described the productive structure to obtain exergy and monetary costs. The LCA methodology quantified the greenhouse gas emissions associated with equipment operation and energy flows. The results indicated efficient thermoeconomic behavior for the heat exchangers. The monetary and environmental costs of chilled water are, respectively, US$ 0.2267/MJ and 0.8186 kg CO2-eq/MJ.

关键词： UFS model H&S model Life Cycle Assessment Greenhouse gases Refrigeration Cooling

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Investigation of thermal conductivity and physical properties of oil palm trunks/ramie fiber reinforced biopolymer hybrid composites as building bio-insulation

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Materials Today: Proceedings 2022年 60卷 373-377页

作者： Mawardi, Indra Aprilia, Sri Faisal, Muhammad Rizal, Samsul Doctoral Program School of Engineering Post Graduate Program Universitas Syiah Kuala Banda Aceh23111 Indonesia Department of Mechanical Engineering Politeknik Negeri Lhokseumawe Lhokseumawe24301 Indonesia Department of Chemical Engineering Universitas Syiah Kuala Banda Aceh23111 Indonesia Department of Mechanical Engineering Universitas Syiah Kuala Banda Aceh23111 Indonesia

The current buildings insulating materials in the construction market, which mainly consist of synthetic materials, have a high performance in thermal resistivity. However, they negatively impact the human health and the environment, thereby finding bio-insulating materials is necessary. This research investigates the thermal conductivity and physical performance of oil palm trunks/ramie fibers reinforced biopolymer hybrid composites for thermal insulation of buildings. The hybrid composites were further prepared using oil palm trunk particles, ramie fiber as the reinforcement, and tapioca starch as a biopolymer binder. All the manufactured hybrid composites exhibited thermal conductivity in a range of 0.0723 W/mK to 0.1344 W/mK and density of 732 kg/m3 to 801 kg/m3, respectively. Sample C1, with a density of 732 kg/m3 had the lowest thermal conductivity of (0.0723 W/mK). Moreover, the minimum absorbed water (53.66%) and thickness swelling (21.36%) were found in the C1 sample hybrid composites after 24-hours immersion in water. Thermal conductivity performance was influenced positively by physical properties. Therefore, the results of this research show that waste oil palm trunks and ramie fiber could be used as a thermal insulating material for buildings. © 2022

关键词： Thermal conductivity

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