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A high-entropy rare-earth phosphate and its principle single component REPO_(4)for environmental barrier coatings

Journal of Advanced Ceramics 2025年第3期14卷 103-119页

作者： Bishnu Pada Majee Keith Bryce Liping Huang Jie Lian Department of Materials Science and Engineering Rensselaer Polytechnic InstituteNY 12180USA Department of Mechanical Aerospace and Nuclear EngineeringRensselaer Polytechnic InstituteNY 12180USA

Xenotime rare-earth(RE)phosphates are emerging as promising materials for environmental barrier coatings(EBCs)for SiC-based ceramic-matrix composites(CMCs)because of their close coefficients of thermal expansion(CTEs)and resistance to calcium-magnesium-alumina-silicate(CMAS)*** this work,high-entropy(HE)(Sc_(0.2)Lu_(0.2)Yb_(0.2)Er_(0.2)Y_(0.2))PO_(4) and five single-component REPO4(RE=Sc,Lu,Yb,Er,and Y)compounds were synthesized,and their stability,thermal properties,and CMAS corrosion resistance were *** CTE values of four REPO_(4) compounds(RE=Lu,Yb,Er,and Y;~(5.6-6)×10^(−6)℃^(−1))are close to those of SiC-CMC((4.5-5.5)×10^(−6)℃^(−1)),whereas ScPO_(4)(6.98×10^(−6)℃^(−1))and HE(5RE_(0.2))PO_(4)(6.39×10^(−6)℃^(−1))have slightly higher values in the temperature range of 200-1300℃.HE phosphate has the lowest thermal conductivity due to its size and mass *** CMAS corrosion tests at 1300℃ for 5,45,and 96 h revealed that all RE phosphates formed a continuous and dense reaction layer predominantly composed of Ca_(8)MgRE(PO_(4))_(7),effectively impeding CMAS ***,REPO_(4) with smaller RE³−cations displays a slower reaction rate and reduced corrosion kinetics,as evidenced by the smaller thickness of the reaction layer.A larger negative difference in the optical basicity(OB)value between REPO_(4) and CMAS signifies greater corrosion resistance.A mechanistic understanding of CMAS corrosion and elucidation of the effects of critical parameters such as the ionic mass and ionic radius of RE elements on their thermal properties and CMAS corrosion kinetics are useful for the development of novel xenotime-type phosphates as EBCs for SiC-CMCs.

关键词： environmental barrier coatings(EBCs) rare-earth(RE)phosphate coefficients of thermal expansion(CTEs) thermal conductivity calcium-magnesium-alumina-silicate(CMAS)corrosion

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A systematic study of thermomechanical properties and calcium–magnesium–aluminosilicate(CMAS)corrosion of multicomponent rare-earth phosphates

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Journal of Advanced Ceramics 2024年第11期13卷 1807-1822页

作者： Keith Bryce Bishnu Pada Majee Liping Huang Jie Lian Department of Mechanical Aerospace and Nuclear EngineeringRensselaer Polytechnic InstituteNY 12180USA Department of Materials Science&Engineering Rensselaer Polytechnic InstituteNY 12180USA

Multicomponent rare earth phosphates hold immense potential as next-generation environmental barrier coatings(EBCs),offering enormous possibilities and flexibility by controlling and varying their components and fractions to tailor their *** this work,the key material parameters(e.g.,ionic size and ionic size disorder)and the elements governing their thermal‒mechanical properties and resistance against calcium‒magnesium‒aluminosilicate(CMAS)corrosion were *** thermal conductivities of multicomponent rare-earth phosphates correlate well with cation size disorder,but no clear trend is identified for the coefficient of thermal expansion(CTE).Er-containing compositions display low CTEs and high fracture *** formation of a dense interfacial layer occurs for most CAMS corrosion-resistant compositions when tested at 1300°C,e.g.,(Lu_(0.2)Yb_(0.2)Er_(0.2)Y_(0.2)Gd_(0.2))PO_(4) and(Lu_(0.2)Yb_(0.2)Er_(0.2)Dy_(0.2)Gd_(0.2))PO_(4).These multicomponent phosphates also display the least recession upon molten CMAS attack at 1400°C without significant volumetric swelling,which is superior to their single-component counterparts and state-of-the-art EBCs based on rare-earth *** contrast,Sc-containing multicomponent phosphates display inferior performance against CMAS corrosion and penetration.A mechanistic understanding and understanding of the kinetics of the interfacial interaction at higher temperatures,as well as the key parameters governing their thermomechanical properties and CMAS corrosion,are valuable for designing data-driven materials of multicomponent phosphates for EBC applications.

关键词： environmental barrier coating(EBC) high-entropy ceramics(HECs) rare earth phosphates

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Dual-compressed photoacoustic single-pixel imaging

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National science Review 2023年第1期10卷 187-195页

作者： Yuning Guo Baowen Li Xiaobo Yin Department of Mechanical Engineering University of Colorado Department of Material Science and Engineering Department of Physics Shenzhen Institute for Quantum Science and Engineering Southern University of Science and Technology Materials Science and Engineering Program University of Colorado

Photoacoustic imaging,an acoustic imaging modality with potentially optical resolution in an optical turbid medium,has attracted great ***,the convergence of wavefront optimization and raster scanning in computational photoacoustic imaging leads to the challenge of fast mapping,especially for a spatial resolution approaching the acoustic deep-subwavelength *** a sparse sampling paradigm,compressive sensing has been applied in numerous fields to accelerate data acquisition without significant quality *** this work,we propose a dual-compressed approach for photoacoustic surface tomography that enables high-efficiency imaging with 3D spatial resolution unlimited by the acoustics in a turbid *** dual-compressed photoacoustic imaging with single-pixel detection,enabled by spatially optical modulation with synchronized temporally photoacoustic coding,allows decoding of the fine optical information from the modulated acoustic signal even when the variance of original photoacoustic signals is *** perform a proof-of-principle numerical demonstration of dual-compressed photoacoustic imaging, that resolves acoustic sub-acoustic-wavelength details with a significantly reduced number of measurements,revealing the potential for dynamic *** dual-compressed concept,which transforms unobtrusive spatial difference into spatio-temporal detectable information,can be generalized to other imaging modalities to re alize efficient,high-spatial-resolution imaging.

关键词： photoacoustic imaging compressive sensing single-pixel imaging surface tomography

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Harnessing the flatbandλ-Ti_(3)O_(5):A breakthrough in solar steam generation

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science China materials 2023年第11期66卷 4515-4516页

作者： Chuxin Lei Guihua Yu Materials Science and Engineering Program and Walker Department of Mechanical Engineering The University of Texas at AustinAustinTX 78712USA

As global population rises,accompanied by escalating environmental pollution and climate change,numerous countries find themselves grappling with an acute scarcity of natural freshwater resources^([1]).Seawater desalination presents a compelling solution to this looming crisis,especially considering the oceans are Earth’s largest water reservoir^([2]).

关键词： reservoir Earth breakthrough

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Deformation Behavior of Commercially Pure Titanium Subjected to Blast Assisted Deformation: New Insights on f112̅1g Extension Twinning

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materials Transactions 2025年第5期66卷 521-531页

作者： Bisht, Anuj Subburaj, Janardhanraj Jagadeesh, Gopalan Suwas, Satyam Department of Mechanical and Industrial Engineering Indian Institute of Technology Roorkee Roorkee India Department of Aerospace Engineering Indian Institute of Science Bangalore India Department of Materials Engineering Indian Institute of Science Bangalore India

In the present work, the microstructure and texture evolution in commercially pure titanium subjected to blast assisted deformation has been investigated by means of electron backscattered diffraction and transmission electron microscopy. The evolved texture in the deformed material is primarily attributed to the dominant h1¯010i 64.4° contraction twinning. Other deformation twins were also observed in a low fraction. A uniform dislocation background with other microstructural features observed suggested the formation of a superimposed microstructure in the material. f112¯1g extension twins (ET2) with a thick uniform pile-up of dislocation along its boundary have formed in the material. Parts of ET2 have detwinned leaving gaps along the twin length, revealing the unstable nature of ET2 twins. The in-depth microstructural analysis reveals the ET2 twin formation mechanism, where the instability developed in the material due to progressive lattice rotation via accumulative slip is relieved by ET2 twin formation by atomic shuffling. The gaps (local detwinning) observed in the present case is attributed to the transient oscillatory response of the material under impulsive loading, which has been previously reported in the literature. ©2025 The Japan Institute of Metals and materials.

关键词： High resolution transmission electron microscopy

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Fibrillar adhesives with unprecedented adhesion strength,switchability and scalability

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National science Review 2024年第10期11卷 20-33页

作者： Changhong Linghu Yangchengyi Liu Xudong Yang Dong Li Yee Yuan Tan Mohamed Haziq Bin Mohamed Hafiz Mohammad Fadhli Bin Rohani Zihao Du Jiangtao Su Yan Li Yucheng Huo Hanyan Xu Xiufeng Wang Yifan Wang Jing Yu Huajian Gao K.Jimmy Hsia School of Mechanical and Aerospace Engineering Nanyang Technological University School of Materials Science and Engineering Xiangtan University Department of Engineering Mechanics Zhejiang University School of Materials Science and Engineering Nanyang Technological University Institute of High-Performance Computing A*STAR Mechano-X Institute Applied Mechanics Laboratory Department of Engineering Mechanics Tsinghua University School of Chemistry Chemical Engineering and BiotechnologyNanyang Technological University

Bio-inspired fibrillar adhesives have received worldwide attention but their potentials have been limited by a trade-off between adhesion strength and adhesion switchability, and a size scale effect that restricts the fibrils to micro/nanoscales. Here, we report a class of adhesive fibrils that achieve unprecedented adhesion strength（～2 MPa）, switchability（～2000）, and scalability（up to millimeter-scale at the single fibril level）,by leveraging the rubber-to-glass（R2G） transition in shape memory polymers（SMPs）. Moreover, R2G SMP fibrillar adhesive arrays exhibit a switchability of >1000（with the aid of controlled buckling） and an adhesion efficiency of 57.8%, with apparent contact area scalable to 1000 mm2, outperforming existing fibrillar adhesives. We further demonstrate that the SMP fibrillar adhesives can be used as soft grippers and reusable superglue devices that are capable of holding and releasing heavy objects >2000 times of their own weight. These findings represent significant advances in smart fibrillar adhesives for numerous applications,especially those involving high-payload scenarios.

关键词： JKR-DMT transition rubber-to-glass (R2G) transition R2G fibrillar adhesives shape memory polymers adhesion switchability and scalability

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A review of control strategies used for morphing aircraft applications

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Chinese Journal of Aeronautics 2024年第4期37卷 436-463页

作者： Muhammed S.PARANCHEERIVILAKKATHIL Jafar S.PILAKKADAN Rafic M.AJAJ Mohammadreza AMOOZGAR Davood ASADI Yahya ZWEIRI Michael I.FRISWELL Department of Aerospace Engineering Khalifa University of Science and TechnologyAbu DhabiUnited Arab Emirates Department of Aerospace Engineering Advanced Research and Innovation Center(ARIC)Khalifa University of Science and TechnologyAbu DhabiUnited Arab Emirates Department of Mechanical Materials&Manufacturing EngineeringUniversity of NottinghamNottingham NG72RDUK Department of Aerospace Engineering Adana Alparslan Turkes Science and Technology UniversityTurkey College of Engineering Swansea UniversitySwansea SA18ENUK

This paper reviews the various control algorithms and strategies used for fixed-wing morphing aircraft applications. It is evident from the literature that the development of control algorithms for morphing aircraft technologies focused on three main areas. The first area is related to precise control of the shape of morphing concepts for various flight conditions. The second area is mainly related to the flight dynamics, stability, and control aspects of morphing aircraft. The third area deals mainly with aeroelastic control using morphing concepts either for load alleviation purposes and/or to control the instability boundaries. The design of controllers for morphing aircraft/wings is very challenging due to the large changes that can occur in the structural, aerodynamic, and inertial characteristics. In addition, the type of actuation system and actuation rate/speed can have a significant effect on the design of such controllers. The aerospace community is in strong need of such a critical review especially as morphing aircraft technologies move from fundamental research at a low Technology Readiness Level(TRL) to real-life applications. This critical review aims to identify research gaps and propose future directions. In this paper, research activities/papers are categorized according to the control strategy used. This ranges from simple Proportional Integral Derivative(PID) controllers at one end to complex robust adaptive controllers and deep learning algorithms at the other end. This includes analytical, computational, and experimental studies. In addition, the various dynamic models used and their fidelities are highlighted and discussed.

关键词： Control strategies Morphing aircraft Shape morphing Flight dynamics Aeroelasticity

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Enhancing the thermal conductivity of semiconductor thin films via phonon funneling

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npj Computational materials 2024年第1期10卷 1414-1422页

作者： C.Jaymes Dionne Sandip Thakur Nick Scholz Patrick Hopkins Ashutosh Giri Department of Mechanical Industrialand Systems EngineeringUniversity of Rhode IslandKingston02881 RIUSA Department of Mechanical and Aerospace Engineering University of VirginiaCharlottesville22904 VAUSA Department of Materials Science and Engineering University of VirginiaCharlottesville22904 VAUSA Department of Physics University of VirginiaCharlottesville22904 VAUSA

The second law of thermodynamics asserts that energy diffuses from hot to *** resulting temperature gradients drive the efficiencies and failures in a plethora of ***,as the dimensionalities of materials shrink to the nanoscale regime,proper heat dissipation strategies becomemore challenging since the mean free paths of phonons become larger than the characteristic length *** leads to temperature gradients that are dependent on interfaces and boundaries,which ultimately can lead to severe thermal ***,we uncover a phenomenon which we refer to as‘phonon funneling’,that allows the control of phonon transport to preferentially direct phonon energy away from geometrically confined interfacial thermal bottlenecks and into localized colder *** phenomenon supersedes heat diffusion based on the macroscale temperature gradients,thus introducing a nanoscale regime in which boundary scattering increases the phonon thermal conductivity of thin films,an opposite effect than what is traditionally *** work advances the fundamental understanding of phonon transport at the nanoscale and the role of efficient scattering methods for enhancing thermal transport.

关键词： thermal conductivity films

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Texture development and surface reconstruction of BiVO_(4)photoanode via one-pot hydrothermal reaction for enhanced photoelectrochemical water splitting

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Journal of Advanced Ceramics 2025年第3期14卷 133-141页

作者： Sung Won Hwang Yoo Jae Jeong Runfa Tan Indhujasri Saravanan Hyun Soo Han Dong Hoe Kim In Sun Cho Department of Energy Systems Research Ajou UniversitySuwon 16499Republic of Korea Department of Material Science&Engineering Ajou UniversitySuwon 16499Republic of Korea Department of Mechanical Engineering Stanford UniversityStanford 94305USA Department of Material Science&Engineering Korea UniversitySeoul 02841Republic of Korea Materials Science and Engineering Program University of Colorado BoulderBoulder 80303USA

The simultaneous optimization of the bulk and surface characteristics of photoelectrodes is essential to maximize their photoelectrochemical(PEC)*** report a novel one-pot hydrothermal synthesis of textured and surface-reconstructed BiVO_(4)photoanodes(ts-BVO),achieving significant improvements in PEC water *** controlling precursor molarity and ethylene glycol(EG)addition,we developed a stepwise dual reaction(SDR)mechanism,which enables simultaneous bulk texture development and surface *** optimized CoBi/ts-BVO photoanode exhibited a photocurrent density of 4.3 mA∙cm^(−2)at 1.23 V *** hydrogen electrode(RHE)with a high Faradaic efficiency of 98%under one sun *** with nontextured BiVO_(4),the charge transport efficiency increased from 8%to 70%,whereas the surface charge transfer efficiency improved from 9%to 85%.These results underscore the critical role of both bulk and surface engineering in enhancing PEC *** findings offer a streamlined approach for improving the intrinsic properties of photoanodes in solar water splitting.

关键词： BiVO_(4) hydrothermal texture surface reconstruction ethylene glycol(EG) photoelectrochemical water splitting

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Temperature dependence of pressure sensitive flow in bulk metallic glass composites

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Journal of materials science & Technology 2024年第14期181卷 165-175页

作者： Priyanka Saini Yakai Zhao Biao Li Long Zhang U.Ramamurty R.L.Narayan Department of Materials Science and Engineering Indian Institute of TechnologyDelhi 110016India School of Mechanical and Aerospace Engineering Nanyang Technological UniversitySingapore 639798Republic of Singapore Institute of Materials Research and Engineering Agency for ScienceTechnology and Research138634Republic of Singapore Shi-changxu Innovation Center for Advanced Materials Institute of Metal ResearchChinese Academy of SciencesShenyang 110016China

The constraint factor,C,defined as hardness,H,to the yield strength,σ_(y),ratio,is an indirect measure of the pressure sensitivity in *** investigations determined that while C is less than 3 for crystalline materials,and remains invariant with change in temperature,it is greater than 3 for bulk metallic glasses(BMGs)and increases with increasing temperature,below their glass transition temper-ature,T_(g).In this study,the variations in C for two BMG composites(BMGCs),which have an amorphous matrix and in situ precipitated crystallineβ-Ti dendrites,which in one case transforms under stress toα”-Ti and deforms by slip in the other,as a function of temperature are examined and compared with that of a *** this purpose,instrumented indentation tests,with a Berkovich tip,and uniaxial com-pression tests were performed to measure the H andσ_(y),respectively,on all alloys and their constituents at temperatures in the range of 0.48 T_(g) and 0.75 T_(g).σ_(y) and H of the BMGC with transforming dendrites(BMGC-T)increase and remain invariant with increasing temperature,***,in BMG and the BMGC with non-transforming dendrites(BMGC–NT),the same properties decrease with increas-ing ***-T has the highest C of∼4.93 whereas that of BMGC–NT and BMG are∼3.72 and∼3.28,respectively,at 0.48 T_(g).With increasing temperature,C of the BMG and BMGC–NT increases with temperature,but that of the BMGC-T *** values of C and their variations as a function of temperature were explained by studying the variation of pressure sensitivity of the amorphous phase and concluding that the plastic flow in BMGCs under constrained conditions,such as indentation,is con-trolled by the flow resistance of the amorphous matrix whereas that in uniaxial compression,which is only partially constrained,is controlled by plasticity in both the dendrites and matrix.

关键词： Bulk metallic glass composites Hardness Pressure sensitivity Martensitic transformation

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