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A high-entropy rare-earth phosphate and its principle single component REPO_(4)for environmental barrier coatings

Journal of Advanced Ceramics 2025年第3期14卷 103-119页

作者： Bishnu Pada Majee Keith Bryce Liping Huang Jie Lian Department of Materials Science and Engineering Rensselaer Polytechnic InstituteNY 12180USA Department of Mechanical Aerospace and Nuclear EngineeringRensselaer Polytechnic InstituteNY 12180USA

Xenotime rare-earth(RE)phosphates are emerging as promising materials for environmental barrier coatings(EBCs)for SiC-based ceramic-matrix composites(CMCs)because of their close coefficients of thermal expansion(CTEs)and resistance to calcium-magnesium-alumina-silicate(CMAS)*** this work,high-entropy(HE)(Sc_(0.2)Lu_(0.2)Yb_(0.2)Er_(0.2)Y_(0.2))PO_(4) and five single-component REPO4(RE=Sc,Lu,Yb,Er,and Y)compounds were synthesized,and their stability,thermal properties,and CMAS corrosion resistance were *** CTE values of four REPO_(4) compounds(RE=Lu,Yb,Er,and Y;~(5.6-6)×10^(−6)℃^(−1))are close to those of SiC-CMC((4.5-5.5)×10^(−6)℃^(−1)),whereas ScPO_(4)(6.98×10^(−6)℃^(−1))and HE(5RE_(0.2))PO_(4)(6.39×10^(−6)℃^(−1))have slightly higher values in the temperature range of 200-1300℃.HE phosphate has the lowest thermal conductivity due to its size and mass *** CMAS corrosion tests at 1300℃ for 5,45,and 96 h revealed that all RE phosphates formed a continuous and dense reaction layer predominantly composed of Ca_(8)MgRE(PO_(4))_(7),effectively impeding CMAS ***,REPO_(4) with smaller RE³−cations displays a slower reaction rate and reduced corrosion kinetics,as evidenced by the smaller thickness of the reaction layer.A larger negative difference in the optical basicity(OB)value between REPO_(4) and CMAS signifies greater corrosion resistance.A mechanistic understanding of CMAS corrosion and elucidation of the effects of critical parameters such as the ionic mass and ionic radius of RE elements on their thermal properties and CMAS corrosion kinetics are useful for the development of novel xenotime-type phosphates as EBCs for SiC-CMCs.

关键词： environmental barrier coatings(EBCs) rare-earth(RE)phosphate coefficients of thermal expansion(CTEs) thermal conductivity calcium-magnesium-alumina-silicate(CMAS)corrosion

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Deformation Behavior of Commercially Pure Titanium Subjected to Blast Assisted Deformation: New Insights on f112̅1g Extension Twinning

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materials Transactions 2025年第5期66卷 521-531页

作者： Bisht, Anuj Subburaj, Janardhanraj Jagadeesh, Gopalan Suwas, Satyam Department of Mechanical and Industrial Engineering Indian Institute of Technology Roorkee Roorkee India Department of Aerospace Engineering Indian Institute of Science Bangalore India Department of Materials Engineering Indian Institute of Science Bangalore India

In the present work, the microstructure and texture evolution in commercially pure titanium subjected to blast assisted deformation has been investigated by means of electron backscattered diffraction and transmission electron microscopy. The evolved texture in the deformed material is primarily attributed to the dominant h1¯010i 64.4° contraction twinning. Other deformation twins were also observed in a low fraction. A uniform dislocation background with other microstructural features observed suggested the formation of a superimposed microstructure in the material. f112¯1g extension twins (ET2) with a thick uniform pile-up of dislocation along its boundary have formed in the material. Parts of ET2 have detwinned leaving gaps along the twin length, revealing the unstable nature of ET2 twins. The in-depth microstructural analysis reveals the ET2 twin formation mechanism, where the instability developed in the material due to progressive lattice rotation via accumulative slip is relieved by ET2 twin formation by atomic shuffling. The gaps (local detwinning) observed in the present case is attributed to the transient oscillatory response of the material under impulsive loading, which has been previously reported in the literature. ©2025 The Japan Institute of Metals and materials.

关键词： High resolution transmission electron microscopy

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Texture development and surface reconstruction of BiVO_(4)photoanode via one-pot hydrothermal reaction for enhanced photoelectrochemical water splitting

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Journal of Advanced Ceramics 2025年第3期14卷 133-141页

作者： Sung Won Hwang Yoo Jae Jeong Runfa Tan Indhujasri Saravanan Hyun Soo Han Dong Hoe Kim In Sun Cho Department of Energy Systems Research Ajou UniversitySuwon 16499Republic of Korea Department of Material Science&Engineering Ajou UniversitySuwon 16499Republic of Korea Department of Mechanical Engineering Stanford UniversityStanford 94305USA Department of Material Science&Engineering Korea UniversitySeoul 02841Republic of Korea Materials Science and Engineering Program University of Colorado BoulderBoulder 80303USA

The simultaneous optimization of the bulk and surface characteristics of photoelectrodes is essential to maximize their photoelectrochemical(PEC)*** report a novel one-pot hydrothermal synthesis of textured and surface-reconstructed BiVO_(4)photoanodes(ts-BVO),achieving significant improvements in PEC water *** controlling precursor molarity and ethylene glycol(EG)addition,we developed a stepwise dual reaction(SDR)mechanism,which enables simultaneous bulk texture development and surface *** optimized CoBi/ts-BVO photoanode exhibited a photocurrent density of 4.3 mA∙cm^(−2)at 1.23 V *** hydrogen electrode(RHE)with a high Faradaic efficiency of 98%under one sun *** with nontextured BiVO_(4),the charge transport efficiency increased from 8%to 70%,whereas the surface charge transfer efficiency improved from 9%to 85%.These results underscore the critical role of both bulk and surface engineering in enhancing PEC *** findings offer a streamlined approach for improving the intrinsic properties of photoanodes in solar water splitting.

关键词： BiVO_(4) hydrothermal texture surface reconstruction ethylene glycol(EG) photoelectrochemical water splitting

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Impact of annealing on structural and corrosion resistance properties of Ti_(20)Zr_(20)Hf_(20)Be_(20)Ni_(20)high-entropy metallic glass

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Rare Metals 2025年第1期44卷 565-580页

作者： Ke-Ran Li Pan Gong Dong-Liang Wang Cheng Zhang Hu Huang Muhammad Yasir Mao Zhang Xin-Yun Wang State Key Laboratory of Materials Processing and Die&Mould Technology School of Materials Science and EngineeringHuazhong University of Science and TechnologyWuhan 430074China Research Institute of Huazhong University of Science and Technology in Shenzhen Shenzhen 518057China Key Laboratory of CNC Equipment Reliability Ministry of EducationSchool of Mechanical and Aerospace EngineeringJilin UniversityChangchun 130022China Department of Materials Science&Engineering Institute of Space TechnologyIslamabad 44000Pakistan

This study comprehensively investigates the effects of annealing on the structural,electrochemical properties and passivation film characteristics of Ti_(20)Zr_(20)Hf_(20)Be_(20)Ni_(20)(at%)high-entropy metallic glass(HE-MG).Subjected to various annealing temperatures,the samples were analyzed in a 3.5 wt%NaCl solution to evaluate changes in their microstructure and assess their corrosion *** reveal that the HE-MG undergoes multistage crystallization,displaying an amorphous matrix integrated with face centered cubic(FCC)and Ni_(7)Zr_(2)phases between 420 and 500℃,indicating robust thermal *** assessments identify a critical temperature threshold:Below the glass transition temperature(Tg),the HE-MG maintains excellent corrosion resistance,promoting stable passivation *** Tg,enhanced long-range atomic rearrangement during relaxation increases passivation layer defects and significantly diminishes corrosion resistance.X-ray photoelectron spectroscopy(XPS)analyses show that the primary components of the passivation layer are TiO_(2),ZrO_(2),HfO_(2)and *** annealing temperatures lead to enhanced Be and Ni content and decreased Ti,Zr and ***,high mixing entropy and significant atomic size mismatch suppress long-range atomic rearrangement and *** crystallization begins above Tg by_(20)℃,with crystalline phases evenly distributed within the matrix without drastically affecting corrosion *** investigation highlights the impact of thermal treatment on the properties of HE-MG,contributing valuable insights into optimizing their performance and applications.

关键词： High-entropy metallic glass Annealing Corrosion resistance Glass transition temperature Cluster

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Low-cost chemical surface smoothing of CO2 laser-etched acrylic using WELD ON 4 acrylic solvent cement

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International Journal of Advanced Manufacturing Technology 2025年第5期138卷 2245-2255页

作者： Moncada, Luis H. Safaripour, Samira Hutter, Tanya Walker Department of Mechanical Engineering The University of Texas at Austin AustinTX78712 United States Materials Science and Engineering Program and Texas Materials Institute The University of Texas at Austin AustinTX78712 United States

With the increasing use of micro-manufactured devices and the demand for low-cost fabrication techniques, this study presents a simple and scalable surface polishing method for laser etched acrylic using WELD-ON 4 acrylic solvent cement, a solvent typically used for bonding thermoplastics. The method’s effectiveness was evaluated by treating acrylic samples up to three times and analyzing changes in transparency, surface roughness average (Ra), luminescence, and wettability. Results show that even a single treatment significantly improved surface smoothness, reduced light scattering, and brought contact angle and optical clarity closer to those of unetched acrylic. After three treatments, the surface became isotropic, with laser-etched lines disappearing. Specifically, a 60% reduction in Ra was observed in the direction perpendicular to the etched lines, while the parallel direction initially showed a similar trend, followed by a slight increase attributed to the formation of surface irregularities caused by the re-solidification of dissolved acrylic. Contact angle measurements indicated that the surface remained hydrophilic, with controllable wettability based on the number of treatments. Overall, this method provides a low-cost, cleanroom-free solution for improving the surface finish of laser-fabricated acrylic components. Its compatibility with complex or recessed geometries makes it particularly suitable for microfluidic devices and other precision applications requiring both optical clarity and controlled surface properties. © The Author(s), under exclusive licence to Springer-Verlag London Ltd., part of Springer Nature 2025.

关键词： Carbon dioxide lasers

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Combined anisotropic and cyclic constitutive model for laser powder bed fusion fabricated aluminum alloy

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Chinese Journal of Aeronautics 2025年第1期38卷 165-184页

作者： Fei-Fan LI Jihong ZHU Weihong ZHANG Shifeng WEN Jingwen SONG Jun MA Gang FANG State IJR Center of Aerospace Design and Additive Manufacturing School of Mechanical EngineeringNorthwestern Polytechnical UniversityXi’an 710072China Research&Development Institute of Northwestern Polytechnical University in Shenzhen Shenzhen 518063China School of Materials Science and Engineering Northwestern Polytechnical UniversityXi'an 710072China Department of Mechanical and Industrial Engineering Norwegian University of Science and TechnologyTrondheim 7491Norway State Key Laboratory of Tribology in Advanced Equipment Department of Mechanical EngineeringTsinghua UniversityBeijing 100084China

This study presents new methods to effectively model the anisotropic yielding and hardening behavior of laser powder bed fusion fabricated aluminum alloy under both monotonic and cyclic loading *** proposed model combines the yield surface-interpolation method to accurately describe the anisotropic hardening rates in various directions,with the Chaboche kinematic hardening rule to precisely reflect the cyclic *** numerical implementation of the combined anisotropic and cyclic constitutive model,a fully implicit stress integration algorithm based on return mapping method is ***,the multiple parameters associated with the model are categorized and identified in an uncoupled *** isotropic and cyclic hardening parameters are determined by an inverse method,and the stability of the optimization outcomes is validated by applying different starting points for the ***,the back-stress effect on the identification of anisotropic parameters associated with the stress invariant-based Hill48 yield function is considered for the first *** consideration leads to an improved prediction accuracy compared to the identification of anisotropic parameters without considering back-stress *** combined anisotropic and cyclic constitutive model,along with the calibrated parameters,are proven capable of accurately reproducing the intricate deformation behavior of laser powder bed fusion fabricated AlSi10Mg.

关键词： Constitutive models Anisotropy Kinematic hardening Laser powder bed fusion Aluminum alloys

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Microstructural evolution and its influence on the wear resistance of a laser directed energy deposited Ni-based single crystal superalloy

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材料科学技术（英文版） 2025年第2期205卷 127-138页

作者： Chenyu Ren Kai Chen Jingjing Liang R.Lakshmi Narayan Upadrasta Ramamurty Jinguo Li Center for Advancing Materials Performance from the Nanoscale(CAMP-Nano) State Key Laboratory for Mechanical Behavior of MaterialsXi'an Jiaotong UniversityXi'an 710049China Superalloys Division Institute of Metal ResearchChinese Academy of SciencesShenyang 110016China Department of Materials Science and Engineering Indian Institute of TechnologyDelhiNew Delhi 110016India School of Mechanical and Aerospace Engineering Nanyang Technological UniversitySingapore 639798Singapore

The wear behavior of Ni-based single crystal(NBSC)superalloy SRR99 fabricated by laser-directed energy deposition(LDED)is investigated and compared with that of its cast *** γ'precipitate size in the latter is＞400 nm,that in the former is an order of magnitude *** sliding wear tests reveal that the wear rate and coefficient of friction of the LDED alloy are 75％and 20％lower than that of its cast counterpart,*** transmission electron microscopy investigation of the wear-tested cast alloy indicates that there is orientation change and formation of nanoscale grains only at the top layer of the worn surface,whereas regions below undergo moderate plastic deformation via dislocation *** contrast,the sub-surface of the worn LDED alloy has a graded microstructure,with a composite of NiO/γ-Ni on the top,γ'free nano-grains in the middle,and a highly deformed nanoscale layer at the *** improved wear behavior of the LDED alloy is attributed to its higher dislocation density,finer γ'precipitates,and the formation of this graded ***,a detailed description of mechanisms that lead to the formation of this unique graded microstructure is provided.

关键词： In-situ formed gradient nanostructure Enhanced wear resistance Laser-directed energy deposition additive manufacturing Ni-based single crystal superalloys Plastic deformation

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The Influence of Silicon Dioxide as a Fuel Additive in a Diesel Engine Fuelled by Pure Palm Oil 4

The Influence of Silicon Dioxide as a Fuel Additive in a Die...

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4th International Symposium on Advances and Innovation in mechanical engineering, ISAIME 2023

作者： Prahmana, Rico Aditia Darmanto, Prihadi Setyo Reksowardojo, Iman Kartolaksono Prakoso, Tirto Juangsa, Firman Bagja Doctoral Program of Mechanical Engineering Faculty of Mechanical and Aerospace Engineering Institut Teknologi Bandung Bandung40132 Indonesia Program Study of Mechanical Engineering Faculty of Industrial Technology Institut Teknologi Sumatera South Lampung35365 Indonesia Thermal Science and Engineering Research Group Faculty of Mechanical and Aerospace Engineering Institut Teknologi Bandung Bandung Indonesia Department of Chemical Engineering Faculty of Industrial Technology Institut Teknologi Bandung Bandung40132 Indonesia Program Study of Mechanical Engineering Faculty of Industrial Technology Universitas Pertamina Jakarta12220 Indonesia

In the last decade, the Indonesian government has implemented a program to use biodiesel as a substitute for fossil diesel to reduce dependence on fossil fuels. On the other hand, the development of biodiesel as an alternative fuel to replace fossil diesel has several challenges, one of which is the production of biodiesel, which is more complicated and requires a long process. However, the direct use of crude palm oil (CPO) in diesel engines is not recommended because it has many drawbacks. Research recently shows that fuel additives in diesel engines have promising prospects. Therefore, to solve the problem, this study used pure palm oil (PPaO) as the primary fuel, with the addition of silicon oxide (SiO2) as a fuel additive in diesel engines. The results showed that using SiO2 additive in PPaO can increase thermal efficiency by 18.8% at 60% load compared to diesel fuel (DF). Nevertheless, using this fuel increased specific fuel consumption (SFC) by 3.9% on average and increased the opacity by 153% compared to diesel fuel. These results indicate that SiO2 has the potential to be developed as an effective additive to PPaO fuel that can improve the efficiency and performance of diesel engines. © 2025 Institute of Physics Publishing. All rights reserved.

关键词： Biodiesel

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La-substituted W-type barium-nickel ferrites for tunable and high-performance electromagnetic wave absorption

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International Journal of Minerals,Metallurgy and materials 2025年第3期32卷 645-656页

作者： Long Wang Jiurong Liu Shenghui Xie Yanli Deng Zhou Wang Shanyue Hou Shengying Yue Gang Wang Na Wu Zhihui Zeng Key Laboratory for Liquid-Solid Structural Evolution and Processing of Materials(Ministry of Education) School of Materials Science and EngineeringShandong UniversityJinan 250061China Electronic Materials Research Laboratory Key Laboratory of the Ministry of Education and International Center for Dielectric ResearchSchool of Electronic Science and EngineeringXi’an Jiaotong UniversityXi’an 710049China Army Engineering University of PLA College of Field Engineering Nanjing 210007China Laboratory for Multiscale Mechanics and Medical Science State Key Laboratory for Strength and Vibration of Mechanical StructuresSchool of AerospaceXi’an Jiaotong UniversityXi’an 710049China Department of Electrical and Computer Engineering Beckman Institute for Advanced Science and TechnologyUniversity of Illinois at Urbana-ChampaignUrbana 61801USA School of Chemistry and Chemical Engineering Shandong UniversityJinan 250100China

W-type barium-nickel ferrite(BaNi_(2)Fe_(16)O_(27))is a highly promising material for electromagnetic wave(EMW)absorption be-cause of its magnetic loss capability for EMW,low cost,large-scale production potential,high-temperature resistance,and excellent chemical ***,the poor dielectric loss of magnetic ferrites hampers their utilization,hindering enhancement in their EMW-absorption *** efficient strategies that improve the EMW-absorption performance of ferrite is highly desired but re-mains ***,an efficient strategy substituting Ba^(2+)with rare earth La^(3+)in W-type ferrite was proposed for the preparation of novel La-substituted ferrites(Ba_(1-x)LaxNi_(2)Fe_(15.4)O_(27)).The influences of La^(3+)substitution on ferrites’EMW-absorption performance and the dissipative mechanism toward EMW were systematically explored and ***^(3+)efficiently induced lattice defects,enhanced defect-induced polarization,and slightly reduced the ferrites’bandgap,enhancing the dielectric properties of the ***^(3+)also enhanced the ferromagnetic resonance loss and strengthened magnetic *** effects considerably improved the EMW-absorption perform-ance of Ba_(1-x)LaxNi_(2)Fe_(15.4)O_(27)compared with pure W-type *** x=0.2,the best EMW-absorption performance was achieved with a minimum reflection loss of-55.6 dB and effective absorption bandwidth(EAB)of 3.44 GHz.

关键词： electromagnetic wave absorption W-type barium ferrite rare earth dielectric

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Metal-organic frameworks (MOFs) in aqueous batteries (ABs):unlocking potential through innovative materials design

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science China Chemistry 2025年

作者： Bo Han Erhai Hu Bei-Er Jia Ziyang Liu Shuen Tso Afriyanti Sumboja Ivandini T.Anggraningrum Anne Zulfia Syahrial Qingyu Yan SCARCE Laboratory Energy Research Institute NTU (ERIN) Nanyang Technological University School of Materials Science and Engineering Nanyang Technological University Material Science and Engineering Research Group Faculty of Mechanical and Aerospace Engineering Institut Teknologi Bandung Department of Chemistry University of Indonesia Metallurgical & Materials Engineering Department Fakultas Teknik Universitas Indonesia

Metal-organic frameworks (MOFs) represent a revolutionary class of materials in the field of energy storage,particularly for aqueous batteries (ABs).Distinguished by their large surface area,tuneable porosity,and adaptable chemical activity,MOFs offer significant advantages over conventional materials in battery *** article provides a thorough analysis of the crucial role that MOFs play in improving the efficiency of *** includes a concise review of the current research progress,emphasizing the fundamental processes by which MOFs enhance electrochemical ***,the review examines the synthesis and design strategies for the structure of MOFs to maximize ion transport,improve conductivity,and enhance *** structural advantages,chemical versatility,stability,durability and functionalization potential of MOFs are comprehensively ***,we explore the distinct advantages of MOFs in overcoming common challenges encountered in ABs,such as declining capacity,inadequate cycling stability,and limited energy *** paper also highlights the future research directions needed to fully harness their *** goal is to develop a fundamental understanding and stimulate further progress in the use of MOFs for advanced energy storage solutions.

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