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作者： Sekido, Kaoru Ohmura, Takahito Hara, Toru Tsuzaki, Kaneaki Doctoral Program in Materials Science and Engineering University of Tsukuba Tsukuba 305-0047 Japan National Institute for Materials Science Tsukuba 305-0047 Japan

The effect of pre-existing dislocations and interstitial carbon on the initiation of plastic deformation in interstitial free (IF) steel and ultra low carbon (ULC) steel were investigated by the nanoindentation technique. The critical load, Pc, of the pop-in phenomenon, which corresponds to plasticity initiation, appeared clearly on the loading curve. The Pc in high dislocation density materials was smaller than that in low dislocation density materials with no difference between IF and ULC while the Pc in low dislocation density materials was remarkably higher in ULC than in IF. These results indicate that the interstitial carbon in the matrix does not affect the pop-in phenomenon when there are pre-existing dislocations or dislocation sources, and we discuss the reason for their occurrence occurs in high dislocation density materials. © 2012 The Japan Institute of Metals.

关键词： Nanoindentation

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Role of delamination fracture for enhanced impact toughness in 0.05 %P doped high strength steel with ultrafine elongated grain structure

Role of delamination fracture for enhanced impact toughness ...

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7th International Conference on Processing and Manufacturing of Advanced materials, THERMEC'2011

作者： Jafari, Meysam Kimura, Yuuji Tsuzaki, Kaneaki Doctoral Program in Materials Science and Engineering Graduate School of Pure and Applied Science University of Tsukuba 1-2-1 Sengen Tsukuba Ibaraki 305-0047 Japan Structural Metals Center National Institute for Materials Science 1-2-1 Sengen Tsukuba Ibaraki 305-0047 Japan

ISBN: (纸本)9783037853047

Ultrafine elongated grain (UFEG) structures with strong 〈110〉// rolling direction (RD) fiber deformation texture were produced by warm caliber-rolling at 773 K, namely tempforming in the 1200 MPa-class medium-carbon low-alloy steel with phosphorous (P) contents of 0.001 and 0.053 mass%. Charpy impact tests were performed at temperature range of -196 to 150 °C on the UFEG structure. Regardless of P content, high upper shelf energy about 145 J and a very low ductile to brittle transition temperature (DBTT) of around -175 °C were obtained. P segregation embrittlement completely disappeared in the 0.053 %P steel and both steels showed ductile fracture on the planes normal to RD at temperature range of -150 to 150 °C. The main reason for the high upper shelf energy and very low DBTT in the 0.053 %P steel would be delamination fracture along RD when both 0.001 and 0.053 %P steels showed quite similar microstructures including texture. Since the occurrence of delamination requires relatively weak interfaces or planes, P segregated to the ferrite grain boundaries and interfaces of cementite particles-ferrite matrix and made them feasible paths for crack branching and consequently delamination occurred. We showed in this work the advantage of delamination (crack arrester-type) on the high absorbed energy obtained by 0.053 %P steel in comparison with 0.001 %P steel. © (2012) Trans Tech Publications, Switzerland.

关键词： Fracture toughness

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Crystal Structure of ζ 2 ′ Martensite in Au-49.5at%Cd Alloy

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MRS Online Proceedings Library 1991年第1期246卷 73-78页

作者： Yutaka Emura Takuya Ohba Kazuhiro Otsuka Doctoral Program in Engineering University of Tsukuba Tsukuba Ibaraki Japan Department of Materials Science and Engineering School of Science and Engineering Teikyo University Utsunomiya Japan Institute of Materials Science University of Tsukuba Tsukuba Ibaraki Japan

Crystal structure of the ζ2′ martensite in a Au-49.5at%Cd ally has been analyzed by the single crystal x-ray diffraction method. The crystal lattice was trigonal and the lattice constants were a=0.8095(3) and c=0.57940(6) nm. There were 18 atoms in a unit cell. The space group was P3, which was different from that previously determined by Vatanayon and Hehemann. The structure was refined by the full matrix least squares method to a final R factor of 7.8% and a weighted R factor of 4.1%.

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Nano-Flower MnO 2 Coated Graphene Composite Electrodes for Energy Storage Devices

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MRS Online Proceedings Library 2011年第1期1303卷 157-162页

作者： Qian Cheng Jie Tang Jun Ma Han Zhang Norio Shinya Lu-Chang Qin National Institute for Materials Science Sengen Japan Doctoral Program in Materials Science and Engineering University of Tsukuba Tennodai Japan Department of Physics and Astronomy University of North Carolina at Chapel Hill Chapel Hill USA

Graphene, two-dimensional layers of sp2-bonded carbon, has many unique properties. In this paper, graphene is decorated with flower-like MnO2 nanostructures for the application in energy storage devices. The as-prepared graphene and MnO2 nano-flowers, which were characterized by scanning electron microscopy (SEM) and transmission electron microscopy (TEM), were assembled into an asymmetric supercapacitor. The specific capacitance of the graphene electrode reached 245 F/g at a charging current of 1 mA. The MnO2 nano-flowers which consisted of tiny rods with a diameter of less than 10 nm were coated onto the graphene electrodes by electrodeposition. The specific capacitance after the MnO2 deposition is 328 F/g at the charging current of 1 mA with an energy density of 11.4Wh/kg and power density of 25.8 kW/kg. This work suggests that our graphene-based electrodes can be a promising candidate for high-performance energy storage devices.

关键词： electrodeposition energy storage C

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Nano-flower MnO2 coated graphene composite electrodes for energy storage devices

Nano-flower MnO2 coated graphene composite electrodes for en...

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2010 MRS Fall Meeting

作者： Cheng, Qian Tang, Jie Ma, Jun Zhang, Han Shinya, Norio Qin, Lu-Chang National Institute for Materials Science 1-2-1 Sengen Tsukuba 305-0047 Japan Doctoral Program in Materials Science and Engineering University of Tsukuba 1-1-1 Tennodai Tsukuba 305-8577 Japan Department of Physics and Astronomy University of North Carolina at Chapel Hill Chapel Hill NC 27599-3255 United States

ISBN: (纸本)9781605112800

Graphene, two-dimensional layers of sp2-bonded carbon, has many unique properties. In this paper, graphene is decorated with flower-like MnO2 nanostructures for the application in energy storage devices. The as-prepared graphene and MnO2 nano-flowers, which were characterized by scanning electron microscopy (SEM) and transmission electron microscopy (TEM), were assembled into an asymmetric supercapacitor. The specific capacitance of the graphene electrode reached 245 F/g at a charging current of 1 mA. The MnO2 nano-flowers which consisted of tiny rods with a diameter of less than 10 nm were coated onto the graphene electrodes by electrodeposition. The specific capacitance after the MnO2 deposition is 328 F/g at the charging current of 1 mA with an energy density of 11.4 Wh/kg and power density of 25.8 kW/kg. This work suggests that our graphene-based electrodes can be a promising candidate for high-performance energy storage devices. © 2011 materials Research Society.

关键词： Graphene

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Hierarchical electrospun nanofibers treated by solvent vapor annealing as air filtration mat for high-efficiency PM2.5 capture

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science China materials 2019年第3期62卷 423-436页

作者： Xinxin Huang Tifeng Jiao Qingqing Liu Lexin Zhang Jingxin Zhou Bingbing Li Qiuming Peng State Key Laboratory of Metastable Materials Science and Technology Yanshan UniversityQinhuangdao 066004China Hebei Key Laboratory of Applied Chemistry School of Environmental and Chemical EngineeringYanshan UniversityQinhuangdao 066004China Department of Chemistry Science of Advanced Materials Doctoral ProgramCentral Michigan UniversityMount PleasantMI 48859USA

Recently, air pollution has become more serious and started to have a dramatic effect on the health of humans in many large cities. Generally, outdoor personal protection,such as commercial masks, cannot effectively prevent the inhalation of many pollutants. Particulate matter(PM) pollutants are a particularly serious threat to human health. Here we introduce a new efficient air filtration mat that can be used for outdoor protection. The new efficient air filter’s nanocomposite materials were successfully fabricated from poly(ε-caprolactone)/polyethylene oxide(PCL/PEO) using an electrospinning technique and solvent vapor annealing(SVA).SVA treatment endows the wrinkled fiber surface and enhances the PM2.5 capture capacity of protective masks. This nanowrinkled air filtration mat can effectively filter PM2.5 with a removal efficiency of 80.01% under seriously polluted conditions(PM2.5 particle concentration above 225 mg m-3).Our field test in Qinhuangdao indicated that the air filtration mat had a high PM2.5 removal efficiency under thick *** to commercial masks, the fabricated SVA-treated PCL/PEO air filter mat demonstrated a simpler and ecofriendly preparation process with excellent degradation characteristics, showing wide potential applications with a high filtration efficiency.

关键词： electrospinning nanofiber mat solvent vapor annealing air filtration PM2.5 removal

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Topological band gaps and edge modes materialized by symmetric silicon-on-insulator photonic crystal slabs in the mid-IR range

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Physical Review A 2023年第4期107卷 043507-043507页

作者： Afshan Begum Yuanzhao Yao Takashi Kuroda Yoshihiko Takeda Naoki Ikeda Yoshimasa Sugimoto Takaaki Mano Kazuaki Sakoda Center for Green Research on Energy and Environmental Materials National Institute for Materials Science Tsukuba 305-0003 Japan Doctoral Program in Materials Science and Engineering University of Tsukuba Tsukuba 305-8577 Japan Research Center for Functional Materials National Institute for Materials Science Tsukuba 305-0044 Japan Research Network and Facility Service Division National Institute for Materials Science Tsukuba 305-0047 Japan

We successfully fabricated silicon-on-insulator (SOI) photonic crystal (PhC) slabs in which electromagnetic topological band gaps and edge modes were materialized for symmetric transverse-electric-like modes. Because the structure of our specimens can be regarded as symmetric about the horizontal middle plane of the PhC slab, their symmetric and antisymmetric eigenmodes were rigorously separated, so we could achieve genuine photonic band gaps for the former. We fabricated those specimens by electron beam lithography of the top Si layer of SOI wafers and successive plasma-enhanced chemical vapor deposition of a SiO2 capping layer. We confirmed the complete common band gap of topologically trivial and nontrivial PhCs and the topological edge modes on the boundary between them by angle-resolved reflection spectroscopy in the mid-infrared range. This is an observation of the common band gap and edge modes that materialized in symmetric PhC slabs without a membrane structure, that is, without the etching of a sacrificial layer under the PhC to increase the refractive-index contrast and the width of the common band gap.

关键词： Nanophotonics Photonic crystals Photonics Topological effects in photonic systems

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Polystyrene nanoplastics cause developmental abnormalities, oxidative damage and immune toxicity in early zebrafish development

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Comparative biochemistry and physiology. Toxicology & pharmacology : CBP 2025年 295卷 110216页

作者： Febriyansyah Saputra Azzah Dyah Pramata Agoes Soegianto Shao-Yang Hu Department of Biology Faculty Sciences and Technology Universitas Airlangga Campus C Surabaya 60115 Indonesia Mathematics and Natural Sciences Doctoral Program Faculty of Science and Technology Universitas Airlangga Surabaya 60115 Indonesia. Department of Materials and Metallurgical Engineering Faculty of Industrial Technology and Systems Engineering Institut Teknologi Sepuluh Nopember Surabaya 60116 Indonesia. Electronic address: azzah@its.ac.id. Department of Biology Faculty Sciences and Technology Universitas Airlangga Campus C Surabaya 60115 Indonesia. Electronic address: agoes_soegianto@fst.unair.ac.id. Department of Biological Science and Technology National Pingtung University of Science and Technology Pingtung 912301 Taiwan. Electronic address: syhu@mail.npust.edu.tw.

Aquatic organisms are increasingly affected by polystyrene nanoplastics (PSNPs), which have the potential to disrupt development, induce oxidative stress, and impair immune function. This study examined the effects of PSNPs on zebrafish (Danio rerio) embryos exposed to 0.01, 0.1, 1, and 10 μg/mL from 2 to 120 h post-fertilization (hpf). The findings indicated that developmental abnormalities occurred in a dose-dependent manner, including delayed hatching, decreased survival rates, reduced body length, smaller eye diameter, and enlarged yolk sac area. PSNPs accumulated in the chorion and yolk sac as early as 6 hpf and were detected in vital tissues, such as the eyes, heart, yolk sac, liver, pancreas, intestine, neuromasts, and tail, immediately after hatching. By 120 hpf, PSNPs significantly reduced swimming distance and velocity. Exposure to PSNPs induced oxidative damage evidenced by altered expression of antioxidant-related genes (CAT1, GPX1A, SOD1, NRF2, KEAP1, HSP70, MT), disrupting cellular homeostasis and causing structural and organ defects. Immune toxicity was marked by dysregulated expression of immune-related genes (IL-1β, IL-6, NF-κB, TNF-α, C3B, TLR-1, TLR-3, TLR-4), indicating inflammation and innate immune activation triggered by oxidative damage. This study highlights the interconnected impacts of developmental abnormalities, oxidative damage, and immune toxicity caused by PSNPs exposure, highlighting the systemic impacts of nanoplastics contamination in aquatic environments.

关键词： Developmental abnormalities Immune toxicity Oxidative damage Polystyrene nanoplastics Zebrafish embryos

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Novel spent bleaching earth industrial waste as low-cost ceramic membranes material: elaboration and characterization

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materials Today: Proceedings 2023年 87卷 136-140页

作者： Rahma A. Elma M. Roil Bilad M. Isnasyauqiah Rahman Wahid A. Sirajul Huda M. Resa Lamandau D. Doctoral Program of Environemntal Science Postgraduate Program Lambung Mangkurat University Jl Brigjen H. Hasan Basri Kayutangi South Kalimantan Banjarmasin 70123 Indonesia Materials and Membranes Research Group (M2ReG) Lambung Mangkurat University Jl A. Yani Km 36 South Kalimantan Banajrbaru 70714 Indonesia Chemical Engineering Department Engineering Faculty Lambung Mangkurat University Jl A. Yani Km 36 South Kalimantan Banajrbaru 70714 Indonesia Faculty of Integrated Technologies Universiti Brunei Darussalam Gedung BE1410 Brunei Darussalam

Ceramic membrane support derived from spent bleaching earth (SBE) become a novel study due to their low-cost, sustainable features, abundance material, and there is not yet applicated as membrane. In this study, flat disk ceramic membrane configuration was fabricated and characterized from solid waste of crude palm oil bleaching process by pressing method in different SBE loading mass (38–42 %wt.). The SBE as raw material was deoiled using n-hexane and acetone solvent, followed by fabricated it become flat disk SBE membranes. Afterward, the SBE flat disk membranes was characterized through fourier-transform infrared spectroscopy (FTIR) and X-ray fluorescence (XRF) analyzer. The result exhibits the flat disk SBE ceramic membrane has dimension of 41 and 6 mm for diameter and thickness, respectively. SBE membranes indicating have montmorillonite structure due to presence of silica as main component materials of SBE. Besides that, the existence of siloxane vibration band in SBE membranes for the sample after regeneration with n-hexane and acetone were dominated over using raw SBE. It concludes the oil residue was removed and produced SBE membrane properties become robust with less organic contaminant. © 2023

关键词： Ceramic membrane CPO Pressing method SBE Support

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Carbon nitride- and graphene-based materials for the photocatalytic degradation of emerging water pollutants

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materials Advances 2024年第7期5卷 2668-2688页

作者： Indra Jaya Budiarso Valentinus Alphano Dabur Riska Rachmantyo Hermawan Judawisastra Chechia Hu Arie Wibowo Master Program in Materials Science and Engineering Faculty of Mechanical and Aerospace Engineering Institut Teknologi Bandung Ganesha 10 Bandung 40132 West Java Indonesia Doctoral Program in Materials Science and Engineering Faculty of Mechanical and Aerospace Engineering Institut Teknologi Bandung Ganesha 10 Bandung 40132 West Java Indonesia Materials Science and Engineering Faculty of Mechanical and Aerospace Engineering Institut Teknologi Bandung Ganesha 10 Bandung 40132 West Java Indonesia ariewibowo@itb.ac.id Department of Chemical Engineering National Taiwan University of Science and Technology Taipei 106 Taiwan R&D Center for Membrane Technology Chung Yuan Christian University Taoyuan 320 Taiwan Research Center for Nanoscience and Nanotechnology Institut Teknolgi Bandung Ganesha 10 Bandung 40132 West Java Indonesia

Photocatalytic degradation is a promising way to treat emerging pollutants in wastewater. Recently, metal-free photocatalysts such as carbon nitride- and graphene-based materials have attracted much interest in the photocatalytic degradation of emerging water pollutants owing to their visible light activity and unique electrical properties, respectively. Graphitic carbon nitride (GCN) is considered a superior visible light–active photocatalyst because of its suitable bandgap (2.7 eV). Moreover, the facile synthesis process and the high chemical and thermal stability of GCN make it one of the research hotspots in photocatalytic wastewater treatment. Besides GCN, graphene and its derivatives are utilized to support main photocatalysts by enhancing their light absorption, pollutant adsorption, and photogenerated charge separation. Furthermore, the vast modification of these materials has promoted various outstanding performances in carbon nitride- and graphene-based photocatalysts in the application of pollutant degradation. In this review, we highlight recent developments in carbon nitride- and graphene-based photocatalysts (2018–2023), focusing on the strategies to improve the activity of GCN as a visible light–active photocatalyst and the role of graphene and its derivatives as supporting materials in wastewater pollutant remediation applications.

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