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Amination of biochar surface from watermelon peel for toxic chromium removal enhancement

Chinese Journal of Chemical engineering 2021年第8期34卷 199-222页

作者： Mohamed A.El-Nemr Ibrahim M.A.Ismail Nabil M.Abdelmonem Ahmed El Nemr Safaa Ragab Department of Chemical Engineering Faculty of EngineeringCairo UniversityGizaEgypt Renewable Energy Program Zewail City of Science and TechnologyEgypt Environmental Division National Institute of Oceanography and FisheriesKayet BeyEl-AnfoushyAlexandriaEgypt

Watermelon peel residues were used to produce a new biochar by dehydration *** new biochar has undergone two methods of chemical modification and the effect of this chemical modification on its ability to adsorb Cr(VI)ions from aqueous solution has been *** biochars,Melon-B,Melon-BO-NH_(2) and Melon-BO-TETA,were made from watermelon peel via dehydration with 50%sulfuric acid to give Melon-B followed by oxidation with ozone and amination using ammonium hydroxide to give Melon-BO-NH_(2) or Triethylenetetramine(TETA)to give *** prepared biochars were characterized by BET,BJH,SEM,FT-IR,TGA,DSC and EDAX *** highest removal percentage of Cr(VI)ions was 69%for Melon-B,98%for Melon-BO-NH_(2) and 99%for Melon-BO-TETA biochars of 100 mg·L^(−1) Cr(VI)ions initial concentration and 1.0 g·L^(−1) adsorbents *** unmodified biochar(Melon-B)and modified biochars(Melon-BO-NH_(2) and Melon-BO-TETA)had maximum adsorption capacities(Q_(m))of 72.46,123.46,and 333.33 mg·g^(−1),*** amination of biochar reduced the pore size of modified biochar,whereas the surface area was *** obtained data of isotherm models were tested using different error function *** Freundlich,Tempkin and Langmuir isotherm models were best fitted to the experimental data of Melon-B,Melon-BO-NH_(2) and Melon-BO-TETA,*** adsorption rate was primarily controlled by pseudo-second–order rate ***,the functional groups interactions are important for adsorption mechanisms and expected to control the adsorption *** adsorption for the Melon-B,Melon-BO-NH_(2) and Melon-BO-TETA could be explained for acid–base interaction and hydrogen bonding interaction.

关键词： Waste treatment Powder technology Citrullus lanatus Hexavalent chromium Biochar amination Adsorption

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Fish weight prediction using empirical and data-driven models in aquaculture systems

Fish weight prediction using empirical and data-driven model...

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Control Technology and Applications (CCTA),

作者： Xiao Chen Ibrahima N’Doye Fahad Aljehani Taous-Meriem Laleg-Kirati Computer Electrical and Mathematical Science and Engineering Division (CEMSE) King Abdullah University of Science and Technology (KAUST) Saudi Arabia Environmental Science and Engineering Program Biological and Environmental Science and Engineering Division King Abdullah University of Science and Technology (KAUST) Saudi Arabia National Institute for Research in Digital Science and Technology (INRIA) Paris-Saclay France

ISBN: (数字)9798350370942

ISBN: (纸本)9798350370959

Predicting fish growth trajectory is crucial in achieving better control for the growing phase of the fish in aquaculture systems. However, fish biomass sensors that directly measure the fish’s weight are currently unavailable. Additionally, the fish growth model that relies on the fish weight is affected by environmental and feeding management factors, raising the difficulty of predicting the weight. This paper proposes comparative empirical and data-driven models for fish weight prediction. The empirical fish growth model relies directly on the growth ratio, an essential component for optimizing fish growth, while the data-driven model is based on long short-term memory (LSTM). Since the exact daily food ratio, proportional to the body weight of a growing fish, cannot be prescribed, we optimize the growth ratio of the empirical model in a sliding window framework based on the previous growth periods and then predict the fish weights a few days ahead through a nonlinear exponential regression approach. The LSTM method uses a normal distribution to generate multiple datasets over the experimental fish weight range and interpolate these data to provide a good prediction. To this end, we propose a weighted sum optimization method that combines the individual cost of the LSTM and empirical methods to achieve better short-term prediction performance. The simulation results demonstrate the effectiveness of the proposed models in predicting the fish weight and show that the combined weighted sum approach reduces the testing errors by 61.3% and 70.9% compared to the empirical and LSTM methods, respectively. Furthermore, an increasing specific growth rate (SGR) for both LSTM and combined models was observed in the short-term predictions.

关键词： Weight measurement Costs Biological system modeling Simulation Predictive models Fish Trajectory

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Properties of the mixing layer height retrieved from ceilometer measurements in Slovakia and its relationship to the air pollutant concentrations

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environmental science and Pollution Research 2023年第54期30卷 115666-115682页

作者： Nguyen, Duy-Hieu Štefánik, Dušan Šedivá, Tereza Lin, Chitsan Ph.D. Program in Maritime Science and Technology College of Maritime National Kaohsiung University of Science and Technology Kaohsiung811213 Taiwan Slovak Hydrometeorological Institute Jeséniova 17 Bratislava833 15 Slovakia Faculty of Mathematics Physics and Informatics Comenius University in Bratislava Mlynská Dolina F1 Bratislava842 48 Slovakia Department of Marine Environmental Engineering National Kaohsiung University of Science and Technology Kaohsiung811213 Taiwan

Mixing layer height (MLH) is an important meteorological parameter for air quality since it significantly affects ground-level pollution in the atmosphere. This study examined the properties of the MLH on diurnal and seasonal timescales over a 3-year period (2020–2022) using high temporal resolution measurements from eight Vaisala CL31 ceilometers situated around Slovakia. Hourly averaged MLH data was retrieved from the BL-View software using merged method. The highest daily maxima for the MLH occurred mostly in summer and spring, while the lowest values occurred predominantly during winter and autumn. The average MLH daily maximum in summer was 2229 m, and just 859 m in winter. During summer, the spatial distribution of the MLH daily maxima was more uniform compared to winter, when the air masses within the individual valleys did not mix well. Correlations between ground-level pollutant concentrations and hourly mean/daily mean MLH were analyzed. The highest correlation, R≈0.6, was found for O3. For PM10, PM2.5, and NOx, the anticorrelations with MLH were found with maximum in winter (R ≈ − 0.3 for hourly data and R ≈ − 0.5 for daily mean data) but no relation in summer. Lastly, the ceilometer MLH was compared to the radiosonde retrieved MLH for various cloud covers. Our analysis is based on an extensive set of empirical data, which can improve the accuracy and effectiveness of meteorological and atmospheric chemistry models. The findings can support air pollution forecasting and warning systems, providing valuable insights for policymakers and researchers. © 2023, The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature.

关键词： Air quality

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Microwave processing of carbon doped Nickel-Cobalt composites for high-performance supercapacitors

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Materials Today: Proceedings 2022年 67卷 1005-1009页

作者： Kumar, Niraj Bhusan Sahoo, Bibhuti Kumar Sahoo, Naresh Soam, Ankur Kumar, Rahul Dash, Barada P. Kumar Sahoo, Prasanta Maharashtra Pune 411025 India Department of Mechanical Engineering Siksha ‘O’ Anusandhan Deemed to be University Odisha Bhubaneswar 751030 India Department of Chemistry Environmental Science and Technology Program Siksha ‘O’ Anusandhan Deemed to be University Odisha Bhubaneswar 751030 India Department of Energy Science and Engineering IIT Delhi New Delhi 110016 India

A facile and rapid microwave synthesis method was used to make Co/Ni-carbon black (CB) nanocomposites. Several sophisticated techniques confirm the formation and the effects of carbon nanoparticles incorporated into Co/Ni-CB composites. Carbon engrafted Co/Ni composite demonstrates excellent morphology, more significant area, and higher conductive region, thus improving electrode/electrolyte accessibility to enhance electrochemical kinetics. The interaction and combination of CB with Co/Ni composite shows excellent capacitive behavior, assessed by galvanostatic discharge method, cyclic voltage voltammetry, and electrochemical impedance spectroscopy. CB plays a crucial role in stimulating the formation of robust structures, surface activity, and specific capacitance through enhancing electron transport and catalytic properties. This electrode material (NX3) has the highest specific capacitance of 748 Fg−1 at scan rates of 5 mVs−1 and was found to have excellent cycle stability (92.8%) over 5000 cycles. Solid-state supercapacitors fabricated from developed electrodes are highly effective for brightening LEDs. In this study, we demonstrated for the first time a single-step technique that is both quick and efficient for the synthesis of Co/Ni-carbon black heterostructure by using microwave irradiation. The present work suggests that low-cost electrodes can be used in a wide range of future energy storage systems as a potential hybrid material. © 2022

关键词： Nickel

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High-performance solid-solution potassium-ion intercalation mechanism of multilayered turbostratic graphene nanosheets

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Journal of Energy Chemistry 2022年第4期31卷 814-823页

作者： Jiae Um Seung Uk Yoon Hoseong Kim Beom Sik Youn Hyoung-Joon Jin Hyung-Kyu Lim Young Soo Yun Program in Environmental and Polymer Engineering Inha Universityncheon 22212 South Korea Department of Polymer Science and Engineering Inha UniversityIncheon 22212South Korea Division of Chemical Engineering and Bioengineering Kangwon National University Chuncheon Gangwon-do 24341 South Korea KU-KIST Graduate School of Converging Science and Technologyea University 145 Anam-roSeongbuk-guSoul02841 South Korea Department of Integrative Energy Engineering 145 Anam-roSongbuk-guKorea UniversitySeoul 02841 South Korea

The solid-solution reaction between an alkali cation and an active host material is known as a singlephase redox mechanism,and it is typically accompanied by a continuous voltage *** is distinct from the typical alkali cation intercalation reaction at an equivalent site of the active host material,which exhibits a voltage ***,we report an unusual solid-solution potassium-ion intercalation mechanism with a low-voltage plateau capacity on multilayered turbostratic graphene nanosheets(T-GNSs).Despite the disordered graphitic structure with a broad range of d-spacings(3.65–4.18À),the T-GNSs showed a reversible plateau capacity of~200 m A h g^(-1),which is higher than that of a well-ordered graphite nanoplate(~120 m A h g^(-1)).In addition,a sloping capacity of~220 m A h g^(-1)was delivered with the plateau capacity,and higher rate capabilities,better reversibility,and a more stable cycling performance were confirmed on the turbostratic ***-principles calculations suggest that the multitudinous lattice domains of the T-GNSs contain diverse intercalation sites with strong binding energies,which could be the origin of the high-performance solid-solution potassium-ion intercalation behavior when the turbostratic graphene stacks have a d-spacing smaller than that of equilibrium potassium–graphite intercalation compounds(5.35À).

关键词： Turbostratic graphite Graphene nanosheet Defective carbon Anode Potassium-ion batteries

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Impacts of ship emissions and sea-land breeze on urban air quality using chemical characterization, source contribution and dispersion model simulation of PM2.5 at Asian seaport

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environmental Pollution 2024年 347卷

作者： Tseng, Yu-Lun Cheng, Wen-Hsi Yuan, Chung-Shin Lo, Kuo-Cheng Lin, Chitsan Lee, Chia-Wei Bagtasa, Gerry Institute of Environmental Engineering National Sun Yat-sen University ROC Kaohsiung City Taiwan Ph.D. Program in Maritime Science and Technology College of Maritime National Kaohsiung University of Science and Technology ROC Kaohsiung City Taiwan Department of Marine Environmental Engineering National Kaohsiung University of Science and Technology ROC Kaohsiung City Taiwan Department of Safety Health and Environmental Engineering National Kaohsiung University of Science and Technology ROC Kaohsiung City Taiwan Institute of Environmental Science and Meteorology University of the Philippines at Diliman Quezon City Philippines

Fine particulate matter (PM2.5) emitted from marine transportation, bulk materials handling at the docks, and dust dispersion has garnered increased attention, particularly in the interface between port and urban areas. This study explored the inter-transport of PM2.5 between Kaohsiung Harbor and neighboring Metro Kaohsiung. Chemical analyses of PM2.5 samples from four sites include water-soluble ions, metallic elements, carbons, anhydrosugars, and organic acids to establish PM2.5's chemical fingerprints. The CALPUFF air dispersion model is employed to simulate the spatiotemporal distribution of PM2.5 in Kaohsiung Harbor and adjacent urban areas. A clear seasonal and diurnal variation of PM2.5 concentrations and chemical composition was observed in both harbor and urban areas. The high correlation of nighttime PM2.5 levels between the port and urban areas suggests inter-transport phenomena. Sea salt spray, ship emissions, secondary aerosols, and heavy fuel-oil boilers exhibit higher levels in the port area than in the urban area. In Metro Kaohsiung, mobile sources, fugitive dust, and waste incinerators emerge as major PM2.5 contributors. Furthermore, sea breeze significantly influences PM2.5 dispersion from Kaohsiung Harbor to Metro Kaohsiung, particularly in the afternoon. The average contribution of PM2.5 from ships' main engines in Kaohsiung Harbor ranges from 2.9% to 5.3%, while auxiliary engines contribute 3.8%–8.3% of PM2.5 in Metro Kaohsiung. © 2024 Elsevier Ltd

关键词： Ships

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environmentally-friendly alkaline ionized water pretreatment and hydrolysis of macroalga via microwave-assisted heating to improve monosaccharide yield for bioethanol production

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Process Safety and environmental Protection 2024年 189卷 702-713页

作者： Chen, Wei-Hsin Liu, Li-Xuan Khoo, Kuan Shiong Sheen, Herng-Kuang Kwon, Eilhann E. Saravanakumar, Ayyadurai Chang, Jo-Shu Department of Aeronautics and Astronautics National Cheng Kung University Tainan701 Taiwan Research Center for Smart Sustainable Circular Economy Tunghai University Taichung407 Taiwan Department of Mechanical Engineering National Chin-Yi University of Technology Taichung411 Taiwan International Master Degree Program on Energy National Cheng Kung University Tainan701 Taiwan Department of Chemical Engineering and Materials Science Yuan Ze University Taoyuan Taiwan Sugar Business Division Taiwan Sugar Corporation Taiwan701 Taiwan Department of Earth Resources and Environmental Engineering Hanyang University Seoul04763 Korea Republic of Directorate of Research SRM Institute of Science and Technology Chengalpattu District Tamil Nadu Kattankulathur603203 India Department of Chemical Engineering and Materials Science College of Engineering Tunghai University Taichung Taiwan Department of Chemical Engineering National Cheng Kung University Tainan Taiwan

This study synthesizes three sequential steps: pretreatment, acid hydrolysis, and enzyme hydrolysis for bioethanol and hydrochar production from macroalga Gracilaria. The Taguchi method is employed separately in each step to optimize relevant operating factors, aiming to maximize the monosaccharide yield. During pretreatment, environmentally friendly alkaline ionized water is utilized as it does not contain chemical additives. Afterward, microwave-assisted hydrolysis is adopted to enhance the monosaccharide yield of the macroalga for bioenergy production. The results show that the total sugar of Gracilaria undergoing acid hydrolysis alone is 28.72 g‧L−1. The total sugar content after alkaline pretreatment followed by acid hydrolysis is 32.64 g‧L−1, and it increases to 34.76 g‧L−1 after adding enzymes. Meanwhile, the higher heating value of Gracilaria increases from 10.884 MJ‧kg−1 to 12.620 MJ‧kg−1 after undergoing alkaline pretreatment. After the acid and enzyme hydrolysis processes, it increases to 15.164 MJ‧kg−1. The solid biofuel's calorific value increases by 39 % from the three-stage processes. The liquid product combined with Saccharomyces cerevisiae can produce bioethanol, while the produced hydrochar can be used as a solid fuel. This research promotes the development of macroalgal biomass for energy and environmental applications, thereby advancing the circular bioeconomy. © 2024 The Institution of Chemical Engineers

关键词： Ethanol

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Zero Thermal Expansion Metamaterial Designs for Space Structures

Zero Thermal Expansion Metamaterial Designs for Space Struct...

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AIAA science and Technology Forum and Exposition, AIAA SciTech Forum 2025

作者： Lu, Wei-Chun Oudghiri-Idrissi, Othman Poli, Andrea Arruda, Ellen M. Tol, Serife Department of Mechanical Engineering University of Michigan 2350 Hayward St Ann ArborMI48109 United States Fariborz Maseeh Department of Civil Architectural and Environmental Engineering The University of Texas at Austin 301 E. Dean Keeton St AustinTX78712 United States Department of Mechanical Engineering Macromolecular Science and Engineering Program University of Michigan 2350 Hayward St Ann ArborMI48109 United States

ISBN: (数字)9781624107238

ISBN: (纸本)9781624107238

The precision of space structures is sensitive to high-temperature variation during on-orbit operations. This work develops zero thermal expansion (ZTE) metamaterials that can be integrated into space structures to restrict large thermal deformation under precision requirements. The proposed bi-material ZTE metamaterial beams show extremely low coefficients of thermal expansion (CTE) for a wide temperature variation. Static and dynamic analyses are conducted on the designed metamaterials for performance evaluation. The proposed ZTE beam elements are integrated into a 48-meter rib of a space RF antenna to enhance its thermal precision over a wide temperature range. Further, experimental validation of the ZTE truss beam design is conducted in a thermal chamber to demonstrate its low thermal deformation compared to a reference aluminum truss beam. © 2025, American Institute of Aeronautics and Astronautics Inc, AIAA. All rights reserved.

关键词： Trusses

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Response to Comment on"Mechanistic Understanding ofSuperoxide Radical-Mediated Degradation of PerfluorocarboxylicAcids"

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environmental science & TECHNOLOGY 2022年第8期56卷 5289-5291页

作者： Bai, Lu Jiang, Ying Xia, Deming Wei, Zongsu Spinney, Richard Dionysiou, Dionysios D. Minakata, Daisuke Xiao, Ruiyang Xie, Hong-Bin Chai, Liyuan Institute of Environmental Engineering School of Metallurgy and Environment Central South University Changsha 410083 China. Chinese National Engineering Research Center for Control & Treatment of Heavy Metal Pollution Changsha 410083 China. Key Laboratory of Industrial Ecology and Environmental Engineering (Ministry of Education) School of Environmental Science and Technology Dalian University of Technology Dalian 116024 China. Centre for Water Technology (WATEC) & Department of Engineering Aarhus University Hangøvej 2 Aarhus N DK-8200 Denmark. Department of Chemistry and Biochemistry The Ohio State University Columbus Ohio 43210 United States. Environmental Engineering and Science Program University of Cincinnati Cincinnati Ohio 45221 United States. Department of Civil and Environmental Engineering Michigan Technological University Houghton Michigan 49931 United States.

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Biosorption of chromium by live and dead cells of Bacillus nitratireducens isolated from textile effluent

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Chemosphere 2024年 359卷 142389页

作者： Imron, Muhammad Fauzul Setiawan, Wahyu Putranto, Trisnadi Widyaleksono Catur Abdullah, Siti Rozaimah Sheikh Kurniawan, Setyo Budi Study Program of Environmental Engineering Department of Biology Faculty of Science and Technology Universitas Airlangga Campus C UNAIR Jalan Mulyorejo Surabaya60115 Indonesia Department of Water Management Faculty of Civil Engineering and Geosciences Delft University of Technology Stevinweg 1 CN Delft2628 Netherlands Study Program of Environmental Science Postgraduate Program Sriwijaya University Palembang30139 Indonesia Department of Chemical and Process Engineering Faculty of Engineering and Built Environment Universiti Kebangsaan Malaysia UKM Bangi Selangor 43600 Malaysia

Bacillus nitratireducens was isolated from textile effluent and showed high tolerance to chromium (Cr), reaching up to a 1000 mg/L MIC value. This research was aimed at utilizing biosorbents from live and dead cells of B. nitratireducens to remove Cr from an aqueous solution. A batch biosorption test was performed, and mechanisms analysis was approached by an adsorption-desorption test, SEM-EDS, and FTIR analysis. Cr removal by dead cells in 25, 50, and 100 mg/L of Cr were 58.99 ± 0.7%, 69.8 ± 0.2%, and 82.87 ± 0.11%, respectively, while that by live cells was 73.08 ± 1.9%, 80.27 ± 6.33%, and 86.17 ± 1.93%, respectively. Live cells showed significantly higher Cr removal and adsorption capacities as compared to dead cells. In all concentrations, absorption contributed more than adsorption to the Cr removal by both live and dead cells. Absorption of Cr was subjected to occur due to passive mechanisms in dead cells while involving some active mechanisms in live cells. SEM-EDS confirmed the detection of Cr on the cell surface, while FTIR revealed the shifting of some peaks after the biosorption test, suggesting interactions between Cr and functional groups. Further TEM analysis is suggested to be conducted as a future approach to reveal the inner structure of cells and confirm the involvement of absorption mechanisms. © 2024 Elsevier Ltd

关键词： Heavy metals

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