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Patchouli oil analysis of chemical components using FT-IR and GCMS method

AIP Conference Proceedings 2023年第1期2738卷

作者： Hermin Pancasakti Kusumaningrum Rizqi Sa’adatun Ni’mah Yunita Nurlindasari Annisa Imrani Sadam Arrois Eko Purnomo Fa’ireza Rafli Arfiansyah Erni Setyowati Bambang Dwi Loka Biotechnology Study Program Biology Department Faculty of Science and Mathematics Diponegoro University Jl. Prof. Soedharto SH. Tembalang Semarang 50275 Indonesia Department of Chemical Engineering Faculty of Engineering Diponegoro University Jl. Prof. Soedharto SH. Tembalang Semarang 50275 Indonesia Architecture Department Faculty of Engineering Diponegoro University Jl. Prof. Soedharto SH. Tembalang Semarang 50275 Indonesia Food Technology Department Faculty of Animal and Agricultural Sciences Diponegoro University Jl. Prof. Soedharto SH. Tembalang Semarang 50275 Indonesia

Patchouli (Pogostemon cablin Benth.) is a plant that produces essential oils to be used for cosmetics, soap, antiseptic, perfume, pharmaceutical, insecticide and aromatherapy industries. One of the products produced from the patchouli plant is patchouli oil. This study aims to determine the content of chemical compounds contained in the essential oil of patchouli using the GC-MS analysis method to determine the molecular structure of the compound and separate the fractions in patchouli oil. Another method is the FT-IR analysis method to identify the functional groups contained in patchouli oil. The chemical properties of patchouli oil from the Blado area, Batang Indonesia, are traditionally distilled from fresh patchouli leaves and stems. The results of the GCMS analysis showed that there were 10 compounds with 4 peaks of dominant components which were the constituents of patchouli essential oil, namely Patchouli Alcohol (39.46 %), Delta-Guaiene (21.51%), Alpha Guaiene (20.13%), Alpha-patchoulena (9.01%). In the FTIR results carried out in the range of 4000-450 cm-1, various functional groups such as C=C, –CH2, C-H, C=O, O-H, C-O, =C-H, and N-H. This shows that patchouli oil is rich in alcohol, aromatics, and aldehydes.

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The effect of organic acid hydrolysis on the properties of nanocellulose from edamame husk (Glycine max (L.) merill)

Case Studies in Chemical and Environmental Engineering

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Case Studies in Chemical and Environmental engineering 2025年 11卷

作者： Wahyudi, Muhammad Sapto Holilah Bahruji, Hasliza Prasetyoko, Didik Asranudin Pratama, Agus Wedi Indriani, Dina Wahyu Suryanegara, Lisman Faradilla, RH Fitri Mahardika, Melbi Wardani, Ratih Kusuma Piluharto, Bambang Knight, Victor Feizal Norrrahim, Mohd Nor Faiz Research Center for Biomass and Bioproducts National Research and Innovation Agency of Indonesia (BRIN) Cibinong Indonesia Research Collaboration Center for Nanocellulose BRIN-Andalas University Padang Indonesia Study Program of Chemistry Faculty of Science and Technology UIN Sunan Kalijaga Yogyakarta Indonesia Centre of Advanced Material and Energy Sciences Universiti Brunei Darussalam Jl. Tungku Link BE 1410 Brunei Darussalam Department of Chemistry Faculty of Science and Data Analytics Institut Teknologi Sepuluh Nopember Surabaya Indonesia Research Center for Applied Microbiology National Research and Innovation Agency (BRIN) Cibinong Indonesia Department of Biosystem Engineering Faculty of Agricultural Technology Universitas Brawijaya Jalan Veteran Malang Indonesia Department of Food Science and Technology Faculty of Agriculture Universitas Halu Oleo Kendari Indonesia Academy Pharmacy of Surabaya Ketintang Gayungan Surabaya 60231 Indonesia Department of Chemistry Faculty of Mathematics and Natural Sciences University of Jember Jember Indonesia Research Center for Chemical Defence Defence Research Institute Universiti Pertahanan Nasional Malaysia Kem Sungai Besi Kuala Lumpur 57000 Malaysia

The increasing demand for sustainable materials has highlighted nanocellulose as a promising candidate due to its exceptional mechanical strength, thermal stability, and superior barrier properties. These attributes enable its application in diverse fields, including packaging, biomedical devices, and nanocomposites. This study investigates the valorization of edamame bean husks, a byproduct of the globally consumed legume snack, as a sustainable feedstock for nanocellulose production. Cellulose was extracted from the husks via delignification and bleaching, followed by a green and facile acid hydrolysis method employing organic acids (maleic acid, lactic acid, citric acid, and formic acid) to produce nanocellulose. The resulting nanocellulose exhibited a fibrillar morphology with particle sizes ranging from 7.59 to 17.51 nm, depending on the acid used. X-ray diffraction analysis revealed a crystallinity index ranging from 63.49 % to 67.24 %. Notably, acid hydrolysis significantly enhanced the thermal stability of the nanocellulose compared to both the raw husk and isolated cellulose. These findings demonstrate the potential of edamame agricultural waste as a valuable resource for sustainable and eco-friendly nanocellulose production, contributing to a circular bioeconomy. © 2025 The Authors

关键词： Characterization Edamame husk waste Green synthesis Nanocellulose Organic acids

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Chemical compounds in essential oil of nutmeg leaves (Myristica fragrans) from Batang Indonesia

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Journal of Physics: Conference Series 2021年第1期1943卷

作者： H P Kusumaningrum M Zainuri H Endrawati B D Loka I N Widiasa E Sulistyowati Laboratory of Biotechnology Study Program of Biotechnology Faculty of Science and Mathematics Universitas Diponegoro Semarang Indonesia Laboratory of Oceanography Department of Oceanography Food Technology Department Faculty of Animal and Agricultural Sciences Diponegoro University Indonesia Chemical Engineering Department Faculty of Engineering Universitas Diponegoro Semarang Indonesia. Architecture Department Faculty of Engineering Universitas Diponegoro Semarang Indonesia.

Nutmeg oil has an important function as natural tropical biomedicine activity which commonly found in Batang region. This essential oil is one of the dominant traditional export product from Batang instead of patchouli oil, Clove oil, and lemongrass oil. The objective of the research was to analyze chemical compound of essential oil of nutmeg leaves from Batang region produced by traditional destillation. Research methods was conducted by GCMS method. The biomedical activity against some tropical diseases was analysed in-silico. The results showed that essential oil from nutmeg leaves showed potential antimicroabial activities in silico againts several tropical diseases in skin. The GCMS result showed 2-.BETA.-PINENE and .gamma.-Terpinene as the major compound with values 34,46% and 30,28%.

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Corrigendum to "miR-29a-3p-dependent COL3A1 and COL5A1 expression reduction assists sulforaphane to inhibit gastric cancer progression" [Biochem. Pharmacol. 188 (2021) 114539]

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Biochemical pharmacology 2023年 208卷 115389页

作者： Sichong Han Zhe Wang Jining Liu Hui-Min David Wang Qipeng Yuan State Key Laboratory of Chemical Resource Engineering Beijing University of Chemical Technology Beijing 100029 PR China. Graduate Institute of Biomedical Engineering National Chung Hsing University Taichung City 402 Taiwan Department of Medical Laboratory Science and Biotechnology China Medical University Taichung City 404 Taiwan Graduate Institute of Medicine College of Medicine Kaohsiung Medical University Kaohsiung City 807 Taiwan College of Food and Biological Engineering Jimei University Xiamen City 361021 Fujia Province PR China Undergraduate Program Study of Biomedical Engineering Physics Department Airlangga University Surabaya City 60115 Indonesia. Electronic address: davidw@dragon.nchu.edu.tw. State Key Laboratory of Chemical Resource Engineering Beijing University of Chemical Technology Beijing 100029 PR China. Electronic address: yuanqp@***.

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The quality and quantity improvement efforts for Geblek Kulonprogo as a millennial healthy snack

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Journal of Physics: Conference Series 2020年第1期1446卷

作者： Ratnaningsih Devi, M K Sugati, D Food Processing Education Department Universitas Negeri Yogyakarta Indonesia Urban and Regional Planning Study Program Institut Teknologi Nasional Yogyakarta Indonesia Mechanical Engineering Department Institut Teknologi Nasional Yogyakarta Indonesia

Geblek is a traditional food made from wet cassava starch that has become an icon of Kulonprogo District, Special Region of Yogyakarta. The characteristics of geblek are white, number eight shapes, savory taste, and chewy texture. Some problems of Small and Medium Enterprises (SME), Patimurni Andani as the producer of geblek, are the cooking equipment for geblek dough, label and packaging that do not accordance with the goverment regulation. The objective of this community service is to improve the quality and quantity of geblek production as a milenial healthy snack. The method of this study consisted of the design and manufacture of the geblek dough cooker, the nutritional composition analysis, and the improvement of label and packaging. The results of this community service showed that the specifications for the geblek dough cooker were 75 cm in height and 45 cm in diameter, the material was from stainless steel 304, the maximum pressure was 5 kg/cm2, the maximum temperature was 145°C, the tank volume was 190 liters, the capacity was 150 kg, and the gas consumption was 0.8 kg/hour. These results suggested that the quality and quantity improvement of geblek could be implemented in SME to produce it as healthy snacks.

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The Design of Automatic Sprinkler based on Arduino Uno Microcontroller

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IOP Conference Series: Earth and Environmental Science 2019年第1期355卷

作者： A Priyati M Sahbandi GMD Putra DA Setiawati Study Program of Agricultural Engineering Faculty of Food and Agroindustrial Technology Universitas Mataram Mataram NTB Indonesia

The purpose of this study was to design a microcontroller based automatic plant watering system. The method used was an experimental method using two sensors, i.e. soil moisture sensor (measure soil moisture) and ultrasonic sensors (measure the distance of rotary direction regulator for DC motors). Arduino board is preferable as the main controller due to its simplicity. Tool testing was conducted through trials on soil samples and performance tests when the tool was operating. The parameters observed were solar intensity (Lux), ambient temperature (°C), RH (%), water discharge (ml/s), DC motor axis rotation (rpm), AC and DC voltage (Volt), and soil moisture (%). The tool testing showed that the designed watering system could works properly with less than 10% MAPE. When the sensor read the soil moisture value below 70% setting point, the pump and DC motor were turned on. Whereas, when the soil moisture value achieved 80% setting point, the pump and DC motor were turned off. Performance test was conducted for three days of observation. The founding shows that the designed automatic watering system could successfully provide as much as 2.52 litre of water during approximately 6 minutes of watering period.

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Remote monitoring systems in greenhouse based on NodeMCU ESP8266 microcontroller and Android

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AIP Conference Proceedings 2019年第1期2199卷

作者： Yuliana Astutik Murad Guyup Mahardian Dwi Putra Diah Ajeng Setiawati 1Study Program of Agricultural Engineering Faculty of Food and Agroindustrial Technology University of Mataram Indonesia

This study aimed to design a Greenhouse Remote Monitoring system and to immediately evaluate the monitoring system. The Monitoring system was designed based on the NodeMCU ESP8266 microcontroller to expectedly result an Android monitoring display as the output. This research was conducted in Greenhouse at Faculty of food and Agroindustrial Technology, University of Mataram. An experimental method using greenhouse and hydroponic system was applied to this research. The monitoring system consisted of components that functionally related to each other (NodeMCU ESP8266, Android, DHT11 (temperature and humidity sensor), BH1750 (light sensor), Total Dissolved Solid (TDS) sensors, and other components that further supported by programming language. The observed parameters were the greenhouse temperature (°C); humidity (%); light intensity (lux); and the amount of TDS (ppm). The experiment indicated that the designed monitoring system successfully displayed what the sensor had read then translated it into Android. The average percentage of the Light meter reading errors using the BH1750 sensor (shown) on Android was 2.13%; the average percentage of the hygrometer reading errors using DHT11 sensor on Android was 0.14%; the average value of the thermometer reading errors as well as DHT11 sensor on Android was 0.76%; while the average TDS reading error on Android was slightly above 5% due to increasing temperature inside the greenhouse, especially in the afternoon period.

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Effects of slurry concentration and rotational speeds of drum drier to the characteristics of pregelatinized breadfruit (Artocarpus altilis) flours

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IOP Conference Series: Materials Science and engineering 2019年第1期557卷

作者： T C Sunarti W S L Br. Sinaga C Pandji Department of Agroindustrial Technology Faculty of Agricultural Engineering and Technology Bogor Agricultural University Indonesia Program Study of Food Science Faculty of Science and Technology University of Pelita Harapan Tangerang Indonesia

Breadfruit is one alternative carbohydrate source in Indonesia. However, breadfruit is seasonal and climacteric crops; it should be processed immediately to produce flour. Native breadfruit flour has many limitations since it is difficult to be solubilized and swollen in cold water. The flour is modified physically by pregelatinization to improve its properties. Pragelatinized breadfruit flour can be used as instant food, porridge, and baby food. This research is aimed to investigate the effect of slurry concentration (20 and 30%) of native breadfruit flour and rotational speeds (4, 6 and 8 rpm) of double drum drier to the chemical composition and physico-chemical properties of the pregelatinized flours. The results showed that pregelatinization did not influence to the chemical composition. Pregelatinization of the flour improved the water solubility and swelling power on room (30°C) and hot (70°C) solutions, reduced the freeze-thaw stability, caused partial gelatinization which is monitored by losing the birefringence of starch granule, and darkened the flour. The pregelatinization also reduced the gelatinization temperature and had low final viscosity. Low concentration of slurry and low rotation speed of drum increased the gelatinized part of the flour, which is influenced to the cold and hot water solubility.

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Fungal diversity notes 1512–1610: taxonomic and phylogenetic contributions on genera and species of fungal taxa

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Fungal Diversity 2022年第6期117卷 1-272页

作者： Ruvishika S.Jayawardena Kevin D.Hyde Song Wang Ya‑Ru Sun Nakarin Suwannarach Phongeun Sysouphanthong Mohamed A.Abdel‑Wahab Faten A.Abdel‑Aziz Pranami D.Abeywickrama Vanessa P.Abreu Alireza Armand AndréAptroot Dan‑Feng Bao Dominik Begerow Jean‑Michel Bellanger Jadson D.P.Bezerra Digvijayini Bundhun Mark S.Calabon Ting Cao Taimy Cantillo João LVRCarvalho Napalai Chaiwan Che‑Chih Chen Régis Courtecuisse Bao‑Kai Cui Ulrike Damm Cvetomir M.Denchev Teodor T.Denchev Chun Y.Deng Bandarupalli Devadatha Nimali Ide Silva Lidiane Ados Santos Nawal K.Dubey Sylvain Dumez Himashi SFerdinandez André L.Firmino Yusufon Gaforov Achala J.Gajanayake Deecksha Gomdola Sugantha Gunaseelan Shucheng‑He Zin H.Htet Malarvizhi Kaliyaperumal Martin Kemler Kezhocuyi Kezo Nuwan DKularathnage Marco Leonardi Ji‑Peng Li Chunfang Liao Shun Liu Michael Loizides Thatsanee Luangharn Jian Ma Hugo Madrid S.Mahadevakumar Sajeewa S.N.Maharachchikumbura Dimuthu S.Manamgoda María P.Martín Niranjan Mekala Pierre‑Arthur Moreau Yan‑Hong Mu Pasouvang Pahoua Dhandevi Pem Olinto L.Pereira Wiphawanee Phonrob Chayanard Phukhamsakda Mubashar Raza Guang‑Cong Ren Andrea C.Rinaldi Walter Rossi Binu C.Samarakoon Milan CSamarakoon Vemuri V.Sarma Indunil C.Senanayake Archana Singh Maria F.Souza Cristina M.Souza‑Motta Adriano A.Spielmann Wenxin Su Xia Tang XingGuo Tian Kasun M.Thambugala Naritsada Thongklang Danushka S.Tennakoon Nopparat Wannathes DingPeng Wei Stéphane Welti Subodini N.Wijesinghe Hongde Yang Yunhui Yang Hai‑Sheng Yuan Huang Zhang Jingyi Zhang Abhaya Balasuriya Chitrabhanu SBhunjun Timur S.Bulgakov Lei Cai Erio Camporesi Putarak Chomnunti Y.S.Deepika Mingkwan Doilom Wei‑Jun Duan Shi‑Ling Han Naruemon Huanraluek EBGareth Jones NLakshmidevi Yu Li Saisamorn Lumyong Zong‑Long Luo Surapong Khuna Jaturong Kumla Ishara S.Manawasinghe Ausana Mapook Wilawan Punyaboon Saowaluck Tibpromma Yong‑Zhong Lu JiYe Yan Yong Wang Center of Excellence in Fungal Research Mae Fah Luang UniversityChiang Rai 57100Thailand School of Science Mae Fah Luang UniversityChiang Rai 57100Thailand Innovative Institute for Plant Health Zhongkai University of Agriculture and EngineeringGuangzhou 510225P.R.China Department of Plant Pathology College of AgricultureGuizhou UniversityGuiyang 550025GuizhouChina Research Center of Microbial Diversity and Sustainable Utilization Chiang Mai UniversityChiang Mai 50200Thailand Department of Biology Faculty of ScienceChiang Mai UniversityChiang Mai 50200Thailand Biotechnology and Ecology Institute Ministry of Agriculture and ForestryP.O.Box:811Vientiane CapitalLao PDR Department of Botany and Microbiology Faculty of ScienceSohag UniversitySohag 82524Egypt Beijing Key Laboratory of Environment-Friendly Management on Fruit Diseases and Pests in North China Institute of Plant ProtectionBeijing Academy of Agriculture and Forestry SciencesBeijing 100097China Departamento de Fitopatologia Universidade Federal de ViçosaViçosaMinas GeraisBrazil Laboratório de Botânica/Liquenologia Instituto de BiociênciasUniversidade Federal de Mato Grosso do SulAvenida Costa e Silva S/NBairro UniversitárioCampo GrandeMato Grosso do Sul CEP 79070-900Brazil College of Agriculture and Biological Sciences Dali UniversityDali 671003YunnanChina Department of Entomology and Plant Pathology Faculty of AgricultureChiang Mai UniversityChiang Mai 50200Thailand Institute of Plant Science and Microbiology Universität HamburgOrganismic Botany and MycologyOhnhorststr.1822609 HamburgGermany CEFE CNRSUniv.MontpellierEPHEIRDINSERM1919Route de Mende34293 Montpellier Cedex 5France Setor de Micologia Departamento de Biociências e TecnologiaInstituto de Patologia Tropical e Saúde PúblicaUniversidade Federal de GoiásRua 235S/NSetor UniversitárioGoiâniaGO CEP:74605-050Brazil Division of Biological Sciences College of Arts and SciencesUniversity of the Philippines Visayas5023 MiagaoIloiloPhilippines CA

This article is the 14th in the Fungal Diversity Notes series,wherein we report 98 taxa distributed in two phyla,seven classes,26 orders and 50 families which are described and *** in this study were collected from Australia,Brazil,Burkina Faso,Chile,China,Cyprus,Egypt,France,French Guiana,India,Indonesia,Italy,Laos,Mexico,Russia,Sri Lanka,Thailand,and *** are 59 new taxa,39 new hosts and new geographical distributions with one new *** 59 new species comprise Angustimassarina kunmingense,Asterina lopi,Asterina brigadeirensis,Bartalinia bidenticola,Bartalinia caryotae,Buellia pruinocalcarea,Coltricia insularis,Colletotrichum fexuosum,Colletotrichum thasutense,Coniochaeta caraganae,Coniothyrium yuccicola,Dematipyriforma aquatic,Dematipyriforma globispora,Dematipyriforma nilotica,Distoseptispora bambusicola,Fulvifomes jawadhuvensis,Fulvifomes malaiyanurensis,Fulvifomes thiruvannamalaiensis,Fusarium purpurea,Gerronema atrovirens,Gerronema favum,Gerronema keralense,Gerronema kuruvense,Grammothele taiwanensis,Hongkongmyces changchunensis,Hypoxylon inaequale,Kirschsteiniothelia acutisporum,Kirschsteiniothelia crustaceum,Kirschsteiniothelia extensum,Kirschsteiniothelia septemseptatum,Kirschsteiniothelia spatiosum,Lecanora immersocalcarea,Lepiota subthailandica,Lindgomyces guizhouensis,Marthe asmius pallidoaurantiacus,Marasmius tangerinus,Neovaginatispora mangiferae,Pararamichloridium aquisubtropicum,Pestalotiopsis piraubensis,Phacidium chinaum,Phaeoisaria goiasensis,Phaeoseptum thailandicum,Pleurothecium aquisubtropicum,Pseudocercospora vernoniae,Pyrenophora verruculosa,Rhachomyces cruralis,Rhachomyces hyperommae,Rhachomyces magrinii,Rhachomyces platyprosophi,Rhizomarasmius cunninghamietorum,Skeletocutis cangshanensis,Skeletocutis subchrysella,Sporisorium anadelphiae-leptocomae,Tetraploa dashaoensis,Tomentella exiguelata,Tomentella fuscoaraneosa,Tricholomopsis lechatii,Vaginatispora favispora and Wetmoreana *** new combin

关键词： 59 New taxa 39 New records Ascomycota Basidiomycota Dothideomycetes Lecanoromycetes Leotiomycetes Sordariomycetes Ustilaginomycotina

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A first-principles study on the quantum tunneling of methylhydroxycarbene isomerization in various solvents

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Journal of Physics: Conference Series 2020年第1期1568卷 012003-012003页

作者： E D Susanti F Rusydi I Puspitasari R N Fadilla N D Aisyah A Ahmad Research Center for Quantum Engineering Design Faculty of Science and Technology Universitas Airlangga Jl. Mulyorejo Surabaya 60115 Indonesia Department of Physics Faculty of Science and Technology Universitas Airlangga Jl. Mulyorejo Surabaya 60115 Indonesia Visiting Researcher at Precision Sciences & Technology and Applied Physics Graduate School of Engineering Osaka University Suita 565-0871 Japan Information System Study Program Faculty of Science and Technology Universitas Airlangga Jl. Mulyorejo Surabaya 60115 Indonesia School of Chemical Science and Food Technology Faculty of Science and Technology Universiti Kebangsaan Malaysia Bangi Selangor 43600 Malaysia

Quantum tunneling phenomenon allows a high-barrier reaction to occur even though thermal energy is not sufficient to surmount the barrier. The phenomenon has been suggested to exist in the isomerization of methylhydroxycarbene which occured at 11 K. Here we study the quantum tunneling that occured in the isomerization of methylhydroxycarbene to acetaldehyde and to vinyl alcohol based on density functional calculations. The isomerization pathways are determined under the effect of various solvents which are modeled by polarizable continuum model (PCM). We use Wentzel-Kramers-Brillouin (WKB) approximation to calculate the tunneling probability (T) and extend the usefulness of T into isomerization rate. The results show that the solvents give a significant effect on the isomerization rate of methylhydroxycarbene to acetaldehyde but an insignificant one on the isomerization rate to vinyl alcohol.

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