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Food Chemistry Advances 2023年 3卷

作者： de Oliveira, Caroline Beatriz Queiroz, Betânia Branco Tiago Delalibera, Priscila Navarro, José Pérez Gómez-Alonso, Sérgio Pertuzatti, Paula Becker Graduate Program in Materials Science Institute of Exact and Earth Sciences Federal University of Mato Grosso Avenida Valdon Varjão 6390 Barra do Garças 78600-000 Brazil Graduate Program in Immunology and Basic Parasitology Federal University of Mato Grosso Avenida Valdon Varjão 6390 Barra do Garças 78600-000 Brazil Department of Food Engineering Institute of Exact and Earth Sciences Federal University of Mato Grosso Avenida Valdon Varjão 6390 Barra do Garças 78600-000 Brazil Regional Institute for Applied Scientific Research Castilla-La Mancha University Ronda de Calatrava 7 Ciudad Real 13071 Spain

Anacardium humile, known as “cajuzinho-do-cerrado,” is a native Brazilian Cerrado fruit similar to the cashew but less studied, particularly its phenolic compound content and profile. This study used a factorial design to examine how A. humile concentration and maturation time affect the liqueur's physicochemical attributes, phenolic content, antioxidant capacity, and sensory appeal. The liqueurs exhibited low antioxidant capacities as determined by the 2,2-diphenyl-1-picrylhydrazyl radical scavenging capacity assay (DPPH), ferric ion reducing antioxidant power (FRAP), and 2,2′-azinobis(3-ethylbenzothiazoline-6-sulfonic acid). This is likely attributable to a reduction in phenolic compounds within the liqueurs compared to A. humile. The phenolic compound profile of A. humile showed 11 compounds, comprising 5 flavonols, 3 hydroxycinnamic acids, and 2 hydrolyzable tannins. Treatment 8 (500 g of A. humile and 17 days of maturation) showed the highest value for phenolic compound content. However, with regard to sensory analysis, this was the darkest liqueur and the least accepted test, while Treatment 5 (147.5 g of A. humile and 10 days of maturation) was one of the most accepted and chosen as the best liqueur due to the highest antioxidant capacity by FRAP and DPPH methods. The fusion of technology and factorial design proved efficacious in formulating functional liqueurs. © 2023

关键词： Antioxidant capacity Cajuzinho-do-cerrado Factorial design Phenolic compounds

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Topological Surface State Evolution in Bi2Se3 via Surface Etching

arXiv

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arXiv 2024年

作者： Yue, Ziqin Huang, Jianwei Wang, Ruohan Li, Jia-Wan Rong, Hongtao Guo, Yucheng Wu, Han Zhang, Yichen Kono, Junichiro Zhou, Xingjiang Hou, Yusheng Wu, Ruqian Yi, Ming Department of Physics and Astronomy Rice University HoustonTX77005 United States Applied Physics Graduate Program Smalley-Curl Institute Rice University HoustonTX77005 United States Guangdong Provincial Key Laboratory of Magnetoelectric Physics and Devices Center for Neutron Science and Technology School of Physics Sun Yat-Sen University Guangzhou510275 China Institute of Physics Chinese Academy of Sciences Beijing100190 China Department of Electrical and Computer Engineering Rice University HoustonTX77005 United States Department of Materials Science and NanoEngineering Rice University HoustonTX77005 United States Department of Physics and Astronomy University of California Irvine IrvineCA92697 United States

Topological insulators are materials with an insulating bulk interior while maintaining gapless boundary states against back scattering. Bi2Se3 is a prototypical topological insulator with a Dirac-cone surface state around Γ. Here, we present a controlled methodology to gradually remove Se atoms from the surface Se-Bi-Se-Bi-Se quintuple layers, eventually forming bilayer-Bi on top of the quintuple bulk. Our method allows us to track the topological surface state and confirm its robustness throughout the surface modification. Importantly, we report a relocation of the topological Dirac cone in both real space and momentum space, as the top surface layer transitions from quintuple Se-Bi-Se-Bi-Se to bilayer-Bi. Additionally, charge transfer among different surface layers is identified. Our study provides a precise method to manipulate surface configurations, allowing for the fine-tuning of the topological surface states in Bi2Se3, which represents a significant advancement towards nano-engineering of topological states. Copyright © 2024, The Authors. All rights reserved.

关键词： Topological insulators

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The biocompatibility and hemostatic efficacy of silk fibroin nanofibrils fabricated by Shear-Induced phase separation process

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Chemical engineering Journal 2023年 474卷

作者： Lu, Po-Wen Wu, Yu-Tzu Chang, Liang-Yu Lu, Tzu-Wei Jaihao, Chonlachat Huang, Ching-Shuan Murphy Chuang, Mo-Fei Lin, Chunche Chen, Innie Brangule, Agnese Zarkov, Aleksej Kareiva, Aivaras Yang, Jen-Chang Graduate Institute of Biomedical Materials and Tissue Engineering College of Biomedical Engineering Taipei Medical University Taipei11052 Taiwan Division of Gastroenterology and Hepatology Department of Internal Medicine Shuang Ho Hospital Taipei Medical University Zhongzheng Rd. Taipei Zhonghe23561 Taiwan Graduate Institute of Nanomedicine and Medical Engineering College of Biomedical Engineering Taipei Medical University 250 Wu-Hsing Street Taipei11031 Taiwan Department of Dentistry Taipei Medical University Hospital Taipei11031 Taiwan Institute of Organic and Polymeric Materials National Taipei University of Technology Taipei106344 Taiwan Research and Development Center for Smart Textile Technology National Taipei University of Technology Taipei106344 Taiwan Innie Chen Department of Obstetrics and Gynecology University of Ottawa OttawaONK1H 7W9 Canada Department of Pharmaceutical Chemistry Riga Stradins University RīgaLV-1007 Latvia Institute of Chemistry Vilnius University Naugarduko 24 VilniusLT-03225 Lithuania International Ph.D. Program in Biomedical Engineering College of Biomedical Engineering Taipei Medical University Taipei11031 Taiwan Research Center of Biomedical Device Taipei Medical University Taipei11031 Taiwan Research Center of Digital Oral Science and Technology Taipei Medical University Taipei11031 Taiwan

The objectives of this study were to investigate the biocompatibility and hemostatic efficacy of silk fibroin nanofibrils (SFNFs). Unlike a conventional dialysis/freeze-drying process, SFNFs were prepared using a novel shear-induced phase-separation method. The morphology, particle size distribution, protein secondary structures, and crystalline structures of the resulting SFNFs were respectively investigated by scanning electron microscopy (SEM), transmission electron microscopy (TEM), laser diffraction (LD), Fourier-transform infrared (FTIR) spectroscopy, and x-ray diffraction (XRD) deconvolution analyses. Polar and non-polar extractants of SFNFs under a bath ratio of 0.2 g/mL were collected after individually soaking them into 0.9% normal saline and cottonseed oil. In vitro hemolysis ratios, biocompatibility, and sensitization tests were carried out. Then, the hemostatic efficacy was assayed using a rat liver punch biopsy model. Compared to dialyzed/freeze-dried SF, the harvested SFNFs revealed high surface area in morphology. The median particle size distribution, D50, was 294 μm for SFNFs. Shear-induced hydrogen bonding, crystallization, and phase separation tended to give the SFNFs a high crystalline index (CI) and degree of crystallinity (DC). The hemolysis ratio of SFNFs was 0.86 ± 0.40%, and it was classified as being non-hemolytic (0%∼2%). The test results of toxicity and skin sensitization were both negative. The hemostasis time for SFNFs (2.8 ± 0.6 min) was statistically less than that of oxidized cellulose (4.3 ± 0.9 min) (p © 2023 Elsevier B.V.

关键词： Biocompatibility

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Precision measurements of muonium and muonic helium hyperfine structure at J-PARC

arXiv

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arXiv 2025年

作者： Strasser, Patrick Abe, Mitsushi Asai, Kanta Fukumura, Seiso Fushihara, Mahiro Goto, Yu Ino, Takashi Iwai, Ryoto Kanda, Sohtaro Kawamura, Shiori Kitaguchi, Masaaki Nishimura, Shoichiro Oku, Takayuki Okudaira, Takuya Powell, Adam Sasaki, Ken-Ichi Shimizu, Hirohiko M. Shimomura, Koichiro Tada, Hiroki Torii, Hiroyuki A. Yamanaka, Takashi Yamazaki, Takayuki 1-1 Oho Ibaraki Tsukuba305-0801 Japan Materials and Life Science Division J-PARC Center 2-4 Shirakata Tokai-mura Naka-gun Ibaraki319-1195 Japan Materials Structure Science Program Graduate Institute for Advanced Studies SOKENDAI 1-1 Oho Ibaraki Tsukuba305-0801 Japan 1-1 Oho Ibaraki Tsukuba305-0801 Japan Graduate School of Science Nagoya University Furo-cho Chikusa-ku Aichi Nagoya464-8601 Japan Department of Physics Niigata University 8050 Ikarashi 2-no-cho Nishi-ku Niigata-shi Niigata950-2181 Japan Facility for Rare Isotope Beams Michigan State University 640 South Shaw Lane East LansingMI48824 United States Kobayashi-Maskawa Institute Nagoya University Furo-cho Chikusa-ku Aichi Nagoya464-8601 Japan 2-4 Shirakata Tokai-mura Naka-gun Ibaraki319-1195 Japan Graduate School of Science and Engineering Ibaraki University 2-1-1 Bunkyo Ibaraki Mito310-8512 Japan Department of Physics and Astronomy University of Calgary 2500 University Drive NW CalgaryABT2N 1N4 Canada School of Science The University of Tokyo 7-3-1 Hongo Bunkyo-ku Tokyo113-0033 Japan Faculty of Arts and Science Kyushu University 744 Motooka Nishi Fukuoka819-0395 Japan

At the J-PARC Muon science Facility (MUSE), the MuSEUM collaboration is now performing new precision measurements of the ground state hyperfine structure (HFS) of both muonium and muonic helium atoms. High-precision measurements of the muonium ground-state HFS are recognized as one of the most sensitive tools for testing bound-state quantum electrodynamics theory to precisely probe the standard model and determine fundamental constants of the positive muon magnetic moment and mass. The same technique can also be employed to measure muonic helium HFS, obtain the negative muon magnetic moment and mass, and test and improve the theory of the three-body atomic system. Measurements at zero magnetic field have already yielded more accurate results than previous experiments for both muonium and muonic helium atoms. High-field measurements are now ready to start collecting data using the world’s most intense pulsed muon beam at the MUSE H-line. We aim to improve the precision of previous measurements ten times for muonium and a hundred times or more for muonic helium. We review all the key developments for these new measurements, focusing on the high-field experiment, and report the latest results and prospects. Copyright © 2025, The Authors. All rights reserved.

关键词： Microwave spectroscopy

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Interface Rotation in Cu/Nb Accumulative Roll Bonded (ARB) Nanolaminates

SSRN

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SSRN 2022年

作者： Radchenko, Ihor Zhu, Wenxin Qing, Liu Navarro, Etienne Sahay, Rahul Lee, Pooi See Raghavan, Nagarajan Thomas, Olivier Budiman, Arief Suriadi Chen, Kai State Key Laboratory for Mechanical Behavior of Materials Xi’an Jiaotong University Xi’an China School of Materials Science and Engineering Nanyang Technological University Singapore639798 Singapore Nanyang Technological University Temasek Laboratories@NTU 637553 Singapore Aix Marseille Université Université de Toulon CNRS IM2NP Marseille France Xtreme Mechanics Lab 8 Somapah Road Singapore487372 Singapore Singapore487372 Singapore Department of Manufacturing and Mechanical Engineering and Technology Oregon Institute of Technology Klamath FallsOR97601 United States Industrial Engineering Department BINUS Graduate Program—Master of Industrial Engineering Bina Nusantara University Jakarta11480 Indonesia

Metal-metal nanolaminates made by accumulative roll bonding (ARB) is a developing new class of structural nanocomposites that possesses high strength, good ductility, and can also be produced in bulk. These nanolaminates exhibit strong crystallographic textures and mechanical anisotropy. Yet, their mechanical properties are often measured only along rolling direction (RD). Using in situ pillar compression, we show that in-plane shear deformation mechanism in Cu(63 nm)/Nb(63 nm) ARB nanolaminate strongly depends on the shear direction. Plastic shear along the RD abruptly changes into crystallographic rotation and later into interface shear as the shear direction deviates away from the RD. The observed shear mechanisms are driven by competition between different slip systems in Cu layers and at the interface. We expect similar deformation anisotropy to happen in other ARB nanolaminates with sharp texture and interface orientation. Comprehensive characterization of such nanolaminates may require considering more than just the usual rolling/transverse/normal direction anisotropy. © 2022, The Authors. All rights reserved.

关键词： Anisotropy

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The Japanese Vision for the Black Hole Explorer Mission

arXiv

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arXiv 2024年

作者： Akiyama, Kazunori Niinuma, Kotaro Hada, Kazuhiro Doi, Akihiro Hagiwara, Yoshiaki Higuchi, Aya E. Honma, Mareki Kawashima, Tomohisa Kolev, Dimitar Koyama, Shoko Masui, Sho Ohsuga, Ken Sano, Hidetoshi Takami, Hideki Tsunetoe, Yuh Uzawa, Yoshinori Akahori, Takuya Akiyama, Yuto Galison, Peter Hayashi, Takayuki J. Hirota, Tomoya Inoue, Makoto Iwata, Yuhei Johnson, Michael D. Kino, Motoki Kofuji, Yutaro Mizuno, Yosuke Moriyama, Kotaro Nagai, Hiroshi Nakamura, Kenta Notsu, Shota Ono, Fumie Oya, Yoko Oyama, Tomoaki Rana, Hannah Saida, Hiromi Saito, Ryo Saito, Yoshihiko Sasada, Mahito Sawada-Satoh, Satoko Takahashi, Mikiya M. Takamura, Mieko Tong, Edward Tsuji, Hiroyuki Yoshioka, Shogo Watanabe, Yoshimasa Massachusetts Institute of Technology Haystack Observatory WestfordMA01886 United States Mizusawa VLBI Observatory National Astronomical Observatory of Japan Iwate023-0861 Japan Black Hole Initiative Harvard University CambridgeMA02138 United States Graduate School of Sciences and Technology for Innovation Yamaguchi University Yamaguchi753-8512 Japan The Graduate School of Science Nagoya City University Aichi467-0001 Japan Institute of Space and Astronautical Science Japan Aerospace Exploration Agency Kanagawa252-5210 Japan Department of Space and Astronautical Science The Graduate University for Advanced Studies SOKENDAI Kanagawa229-8510 Japan Natural Science Laboratory Toyo University Tokyo112-8606 Japan Division of Science School of Science and Engineering Tokyo Denki University Saitama350-0394 Japan Department of Astronomy Graduate School of Science The University of Tokyo Tokyo113-0033 Japan Institute for Cosmic Ray Research The University of Tokyo Chiba277-8582 Japan Space Communication Systems Laboratory Wireless Networks Research Center National Institute of Information and Communications Technology Tokyo184-8795 Japan Graduate School of Science and Technology Niigata University Niigata950-2181 Japan Advanced Technology Center National Astronomical Observatory of Japan Tokyo181-8588 Japan Center for Computational Sciences University of Tsukuba Ibaraki305-8577 Japan Faculty of Engineering Gifu University Gifu501-1193 Japan Harvard University CambridgeMA02138 United States Azabu Junior and Senior High School Tokyo106-0046 Japan Astronomical Science Program The Graduate University for Advanced Studies SOKENDAI Tokyo181-8588 Japan Institute of Astronomy and Astrophysics Academia Sinica Taipei10617 Taiwan Center for Astrophysics Harvard & Smithsonian CambridgeMA02138 United States Kogakuin University of Technology & Engineering Academic Support Center 2665-1 Nakano Hachioji Tokyo192-0015 Japan Tsung-Dao Lee Institut

The Black Hole Explorer (BHEX) is a next-generation space very long baseline interferometry (VLBI) mission concept that will extend the ground-based millimeter/submillimeter arrays into space. The mission, closely aligned with the science priorities of the Japanese VLBI community, involves an active engagement of this community in the development of the mission, resulting in the formation of the Black Hole Explorer Japan Consortium. Here we present the current Japanese vision for the mission, ranging from scientific objectives to instrumentation. The Consortium anticipates a wide range of scientific investigations, from diverse black hole physics and astrophysics studied through the primary VLBI mode, to the molecular universe explored via a potential single-dish observation mode in the previously unexplored 50-70 GHz band that would make BHEX the highest-sensitivity explorer ever of molecular oxygen. A potential major contribution for the onboard instrument involves supplying essential elements for its high-sensitivity dual-band receiving system, which includes a broadband 300 GHz SIS mixer and a space-certified multi-stage 4.5K cryocooler akin to those used in the Hitomi and XRISM satellites by the Japan Aerospace Exploration Agency. Additionally, the Consortium explores enhancing and supporting BHEX operations through the use of millimeter/submillimeter facilities developed by the National Astronomical Observatory of Japan, coupled with a network of laser communication stations operated by the National Institute of Information and Communication Technology. Copyright © 2024, The Authors. All rights reserved.

关键词： Radio astronomy

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Tessellated granular metamaterials with tunable elastic moduli

arXiv

引用

arXiv 2023年

作者： Pashine, Nidhi Wang, Dong Zhang, Jerry Patiballa, Sree Kalyan Witthaus, Sven Shattuck, Mark D. O’Hern, Corey S. Kramer-Bottiglio, Rebecca Department of Mechanical Engineering & Materials Science Yale University New HavenCT06520 United States Department of Physics Yale University New HavenCT06520 United States Department of Applied Physics Yale University New HavenCT06520 United States Graduate Program in Computational Biology & Bioinformatics Yale University New HavenCT06520 United States Benjamin Levich Institute Physics Department The City College of the City University of New York New YorkNY10031 United States

Most granular packings possess shear moduli (G) that increase with the applied external pressure, and bulk moduli (B) that increase or remain constant with pressure. This paper presents "tessellated" granular metamaterials for which both G and the ratio G/B decrease with increasing pressure. The granular metamaterials are made from flexible tessellations forming a ring of closed cells, each containing a small number of solid particles. For under-constrained tessellations, the dominant contributions to G and B are the particle-particle and particle-cell interactions. With specific particle configurations in the cells, we limit the number of possible particle rearrangements to achieve decreasing G as we increase the pressure difference between the inside and outside of the tessellation, leading to G/B 1 at large pressures. We further study tessellated granular metamaterials with cells containing a single particle and many particles to determine the variables that control the mechanical response of particle-filled tessellations as a function of pressure. © 2023, CC BY.

关键词： Metamaterials

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Spin Seebeck effect at low temperatures in the nominally paramagnetic insulating state of vanadium dioxide

arXiv

引用

arXiv 2022年

作者： Luo, Renjie Zhao, Xuanhan Chen, Liyang Legvold, Tanner J. Navarro, Henry Schuller, Ivan K. Natelson, Douglas Department of Physics and Astronomy Rice University HoustonTX77005 United States Applied Physics Graduate Program Rice University HoustonTX77005 United States Department of Physics Center for Advanced Nanoscience University of California-San Diego La Jolla CA92093 United States Department of Electrical and Computer Engineering Department of Materials Science and NanoEngineering Rice University HoustonTX77005 United States

The low temperature monoclinic, insulating phase of vanadium dioxide is ordinarily considered nonmagnetic, with dimerized vanadium atoms forming spin singlets, though paramagnetic response is seen at low temperatures. We find a nonlocal spin Seebeck signal in VO2 films that appears below 30 K and which increases with decreasing temperature. The spin Seebeck response has a non-hysteretic dependence on in-plane external magnetic field. This paramagnetic spin Seebeck response is discussed in terms of prior findings on paramagnetic spin Seebeck effects and expected magnetic excitations of the monoclinic ground state. Copyright © 2022, The Authors. All rights reserved.

关键词： Vanadium dioxide

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Magneto-optics in a van der Waals magnet tuned by self-hybridized polaritons

arXiv

引用

arXiv 2023年

作者： Dirnberger, Florian Quan, Jiamin Bushati, Rezlind Diederich, Geoffrey Florian, Matthias Klein, Julian Mosina, Kseniia Sofer, Zdenek Xu, Xiaodong Kamra, Akashdeep García-Vidal, Francisco J. Alù, Andrea Menon, Vinod M. Department of Physics City College of New York New YorkNY10031 United States Department of Physics The Graduate Center City University of New York New YorkNY10016 United States Photonics Initiative CUNY Advanced Science Research Center New YorkNY10031 United States Department of Electrical Engineering City College of the City University of New York New YorkNY10031 United States Intelligence Community Postdoctoral Research Fellowship Program University of Washington SeattleWA United States Department of Physics Department of Materials Science and Engineering University of Washington SeattleWA United States Department of Electrical and Computer Engineering Department of Physics University of Michigan Ann ArborMI48109 United States Department of Materials Science and Engineering Massachusetts Institute of Technology CambridgeMA02139 United States Department of Inorganic Chemistry University of Chemistry and Technology Prague Technickaá 5 Prague 6166 28 Czech Republic Universidad Autónoma de Madrid MadridE- 28049 Spain

Controlling quantum materials with light is of fundamental and technological importance. By utilizing the strong coupling of light and matter in optical cavities [1–3], recent studies were able to modify some of their most defining features [4–6]. In this work, we study the magneto-optical properties of a van der Waals magnet that supports strong coupling of photons and excitons even in the absence of external cavity mirrors. In this material – the layered magnetic semiconductor CrSBr – emergent light-matter hybrids called polaritons are shown to significantly increase the spectral bandwidth of correlations between the magnetic, electronic, and optical properties, enabling largely tunable optical responses to applied magnetic fields and magnons. Our results highlight the importance of exciton-photon self-hybridization in van der Waals magnets and motivate novel directions for the manipulation of quantum material properties by strong light-matter coupling. © 2023, CC BY.

关键词： Van der Waals forces

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Effects of sodium alginate-poly(acrylic acid) cross-linked hydrogel beads on soil conditioner in the absence and presence of phosphate and carbonate ions

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Case Studies in Chemical and Environmental engineering 2024年 9卷

作者： Hidayat, Endar Sarbani, Nur Maisarah Mohamad Lahiri, Sudip Kumar Samitsu, Sadaki Yonemura, Seiichiro Mitoma, Yoshiharu Harada, Hiroyuki Graduate School of Comprehensive Scientific Research Program in Biological System Sciences Prefectural University of Hiroshima Shobara 727-0023 Japan Department of Life System Science Faculty of Bioresources Science Prefectural University of Hiroshima Shobara 727-0023 Japan Data-driven Polymer Design Group Research Center for Macromolecules and Biomaterials National Institute for Materials Science 1−2−1 Sengen Tsukuba 305-0047 Japan Department of Mechanical & Industrial Engineering University of Toronto Toronto M5S 3G8 ON Canada Faculty of Allied Health Sciences Chettinad Hospital and Research Institute Chettinad Academy of Research and Education Tamil Nadu Kelambakkam 603103 India

Hydrogel beads, composed of polymers, possess the ability to absorb substantial quantities of water simultaneously and gradually release it in dry conditions. In this work, hydrogel beads were synthesized using sodium alginate (S-Alg) and poly (acrylic acid) (P-Acc), either in the absence or presence of phosphate (PO₄ ³⁻) (S-Alg/P-Acc@PO₄ ³⁻) and carbonate (CO₃ ²⁻) anionic ions (S-Alg/P-Acc@CO₃ ²⁻). Subsequently, these beads were crosslinked with Ca²⁺ ions. The scanning electron microscopy (SEM) images demonstrated that the presence of anionic ions has an impact on the structure of the hydrogel beads and enhances porosity expansion while concurrently reducing the concentration of carboxyl (COOH) groups. The hydrogel beads exhibited a great swelling behavior, with S-Alg/P-Acc@CO₃ ²⁻ capable of absorbing up to 73.5 % of water in acidic conditions, but decreased under neutral and basic conditions. Soil water loss (SWL) experiments confirmed the ability of hydrogel beads to retain water in the soil. Additionally, observations of soil characteristics after a 14-day treatment revealed no significant difference in pH and C/N ratio (P-value <0.05). However, soil's available Fe and N–NO₃ ^- significantly reduced (P-value <0.05) while substantially promoting soil N–NH₄ ⁺, available phosphorus (P), cation exchange capacity (CEC), soil organic carbon (SOC), and exchangeable cation (Ca²⁺, K⁺ and Mg²⁺). The presence of hydroxyl (-OH) and –COOH groups was found to be crucial for enhancing soil properties. © 2024 The Authors

关键词： Anionic ions Hydrogel beads Poly (acrylic acid) Sodium alginate Soil characteristics Soil water retention Swelling

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