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作者： Ahn, Seok Hwan Seok, Kum Cheol Nam, Ki Woo School of Mechanical Engineering Pukyong National University San 100 Yongdang-dong Namgu 608-739 Busan Korea Republic of Department of UR Interdisciplinary Program Mechanical Engineering Graduate School Pukyong National University San 100 Yongdang-dong Nam-gu 608-739 Busan Korea Republic of Division of Materials Science and Engineering Pukyong National University San 100 Yongdang-dong Nam-gu 608-739 Busan Korea Republic of

The locally wall thinned phenomenon of pipes is simulated as metal loss due to erosion/corrosion. Therefore, fracture behaviors of pipes with local wall thinning are very important for the integrity of nuclear power plant. In this study, monotonic bending tests without internal pressure are conducted on 1.91-inch diameter Schedule 80 STS370 full-scale carbon steel pipe specimens. We investigated fracture strengths and failure modes of locally wall thinned pipes that welded and unwelded by four point bending test. From test results, we could be divided three types of failure modes.

关键词： Steel pipe

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Waters network's potential to transform environmental engineering education

Waters network's potential to transform environmental engine...

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114th Annual ASEE Conference and Exposition, 2007

作者： Eschenbach, Elizabeth Montgomery, Jami Johnson, James Brus, Chris Carlson, Patricia Giammar, Dan Grauer, Bette Hotaling, Liesl Oguntimein, Gbekeloluwa Safferman, Steven Wentling, Tim Humboldt State University United States Department of Environmental Resources Engineering Humboldt State University United States WATERS Network - CLEANER Project Office Network Howard University United States Department of Environmental Engineering College of Engineering Architecture and Computer Sciences Howard University United States American Academy of Environmental Engineers United States University of Iowa United States Program University of Iowa United States Rose-Hulman Institute of Technology United States Department of Rhetoric Rose-Hulman Institute of Technology United States National Research Council U. S. Air Force United States NASA's Classroom of the Future Wheeling WV United States Washington University United States Department of Energy Environmental and Chemical Engineering Washington University St. Louis United States Environmental Studies Program Center for Materials Innovation United States McPherson High School United States McPherson High School McPherson KS United States Stevens Institute of Technology United States Stevens Institute of Technology United States Morgan State University United States Michigan State University United States Biosystems and Agricultural Engineering Department Michigan State University United States University of Dayton United States Education Planning Committee National Center for Supercomputing Applications United States Department of Information Science Graduate School of Library and Information Science National Center for Supercomputing Applications University or Illinois United States Knowledge and Learning Systems Group NCSA United States

The WATERS Network (WATer and Environmental Research Systems Network) will be an integrated real-time distributed observing system which will enable academic and government scientists, engineers, educators, and practitioners to advance effective management of our nation's water resources by understanding human interactions with water and the natural and built environment. WATERS will provide easily accessible real time environmental data as well as analysis tools to engineers, scientists, educators, K- graduate students and policymakers so they can better understand how water quantity, quality and related components of the hydrologic cycle are impacted by natural and human influences. The WATERS strategic plan will be completed by July 2007 and requires constituent input. This paper describes the draft Conceptual Design and the Education Plan of WATERS Network. This paper will highlight the potential impact of WATERS on undergraduate and graduate environmental engineering education in order to elicit input from the environmental engineering education community on how WATERS Network could better meet the future needs of undergraduate and graduate students and educators. More information can be found at ***. © American Society for engineering Education, 2007.

关键词： Water resources

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Synthetic Paper from Plastic Waste: The Effect of CaCO3on Physical, Surface Properties and Printability

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Macromolecular Symposia 2007年第1期245-246卷

作者： Ana Carolina Corrêa Cristiano Ribeiro de Santi Sati Manrich Graduate Program of Materials Science and Engineering Federal University of São Carlos Brazil Department of Materials Engineering Federal University of São Carlos 3R- Residue Recycling Center Rod Washington Luís Km 235 13565-905 São Carlos-SP Brazil

This article is a description of recent work in the development of composite sheet materials from blends of recycled high-impact polystyrene (HIPS) and high-density polyethylene (HDPE), with a view to using them as synthetic paper for the printing trade. Four monolayer films of differing composition were characterized in terms of their physical and surface properties. They were further evaluated compared with each other and with commercial synthetic and cellulose papers, to discover relationships between CaCO 3 filler loadings, film structure and properties that could lead to improvements. In terms of their whiteness and water base inks printing properties, these sheets were generally inferior to the cellulose and synthetic papers. Notwithstanding this, in some tests they showed superior quality; thus, in offset printing, the high surface gloss, probably due to the HIPS content, made the colors brighter in some mono-oriented film samples.

关键词： fillers film surface properties polystyrene blends recycling waste

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Cover Picture: Influence of Plasma Stimulation on Si Nanowire Nucleation and Orientation Dependence (Adv. Mater. 18/2007)

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Advanced materials 2007年第18期19卷

作者： P. Aella S. Ingole W. T. Petuskey S. T. Picraux School of Materials Arizona State University Tempe AZ 85287 (USA) Department of Chemistry and Biochemistry Science and Engineering of Materials Graduate Program Arizona State University Tempe AZ 85287 (USA) Center for Integrated Nanotechnologies Los Alamos National Laboratory Los Alamos NM 87545 (USA)

On p. 2603, Tom Picraux and co‐workers report on the use of plasma excitation to strongly enhance the nucleation of Si nanowires by the vapor–liquid–solid growth method. This control allows the preferential formation of very small diameter [110] oriented nanowires, as well as significant enhancements in low temperature nanowire growth.

关键词： Nanowires, inorganic Plasmas Silicon Synthesis

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Aqueous tape casting of LZSA glass ceramics

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6th Pacific Rim Conference on Ceramic and Glass Technology, PacRim6

作者： Gomes, C.M. Biscaia, F.N. Quinaud, J.T. Montedo, O.R.K. Oliveira, A.P.N. Hotza, D. Graduate Program in Materials Science and Engineering - PGMAT Chemical Engineering Department - EQA Federal University of Santa Catarina Florianópolis SC 88040-900 Brazil

ISBN: (纸本)0470080507

The effect of sodium alginate, as binder, and polyethyleneglicol, as plasticizer, on rheological and mechanical properties of suspensions used in water-based tape casting of LZSA glass ceramics was studied. The investigation was carried out using a statistical design approach. An aqueous suspension of a parent glass from the LZSA (Li2O-ZrO2SiO 2-Al2O3) system was used. Viscosity, thixotropy and yield stress behavior were measured for the aqueous suspensions as a function of additive composition. Tensile strength of cast tapes was also measured. The experiments were shown to be statistically significant.

关键词： Glass ceramics

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Characterizations of trimetallic heteronuclear Bi1-xLa x[Fe(CN)6]·n(H2O) complexes and their thermal decomposition products

Characterizations of trimetallic heteronuclear Bi1-xLa x[Fe(...

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作者： Aono, Hiromichi Kondo, Nobuyuki Katagishi, Haruo Kurihara, Masato Sakamoto, Masatomi Sadaoka, Yoshihiko Department of Materials Science and Engineering Faculty of Engineering Ehime University Matsuyama 790-8577 Japan Graduate Program of Human Sensing and Functional Sensor Engineering Graduate School of Science and Engineering Yamagata University Yamagata 990-8560 Japan Department of Material and Biological Chemistry Faculty of Science Yamagata University Yamagata 990-8560 Japan

Heteronuclear Bi1-x La x [Fe(CN)6] &middotnH2O complexes were synthesized, and their crystal structures and thermal decomposition process were investigated by X-ray diffraction (XRD), thermogravimetry analysis (TG... 详细信息

Heteronuclear Bi1-x La x [Fe(CN)6] ·nH2O complexes were synthesized, and their crystal structures and thermal decomposition process were investigated by X-ray diffraction (XRD), thermogravimetry analysis (TGA), Auger electron spectroscopy (AES) with scanning electron microscope (SEM), and transmission electron microscopy (TEM). The crystal system of the complexes was orthorhombic having n = 4 for x = 0-0.7 and was hexagonal having n = 5 for x = 1.0. Their mixture was confirmed for x = 0.8 and 0.9. The lattice parameters for the orthorhombic increased with increasing the x value for the complexes. The single phase of trimetallic perovskite-type Bi1-x La x FeO3 was obtained by its thermal decomposition at low temperature. The crystal system was hexagonal for BiFeO3 (x = 0) and orthorhombic for x = 0.1-1.0. In the case of the decomposed perovskite sample, the lattice parameters decreased with increasing x values for Bi1-x La x FeO3. The particle size was ca. 30 nm for Bi0.2La0.8FeO3 obtained by thermal decomposition at 500 °C and it grew with an increase in decomposition temperature. For the Bi0.5La0.5FeO 3, AES showed that the elemental distributions of Bi, La, and Fe on the surface were very homogeneous for the sample decomposed at 700 °C.

关键词： Bismuth compounds

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Low-temperature sintered LZSA cellular glass ceramics

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6th Pacific Rim Conference on Ceramic and Glass Technology, PacRim6

作者： Sousa, E. Rambo, C.R. Hotza, D. De Oliveira, A.P. Novaes Fey, T. Graduate Program on Materials Science and Engineering - PGMAT Department of Chemical Engineering - EQA Federal University of Santa Catarina P.O. Box 476 88040-900 Florianópolis SC Brazil Department of Materials Science Glass and Ceramics University of Erlangen-Nuremberg Martensstrasse 5 D-91058 Erlangen Germany

ISBN: (纸本)0470080507

Commercial polyurethane foams with a monomodal pore size distribution were used to produce LZSA glass ceramic foams by the polymeric sponge method. A suspension containing LZSA glass ceramic, bentonite and sodium silicate, was prepared in water and isopropanol media to impregnate the polymeric foams by dip coating. The suspension was characterized by Theological measurements. The effect of the solvent on the microstructure and physical properties on the LZSA foams was also evaluated. The cellular microstructure of the glass-ceramic foams was characterized by scanning electron microscopy (SEM) and micro-computer X-ray tomography (μ-CT). The LZSA foam prepared with isopropanol suspension exhibited higher mechanical strength under compression than those prepared with water.

关键词： Glass ceramics

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In situ characterization of Ti-peroxy gel during formation on titanium surfaces in hydrogen peroxide containing solutions

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materials science and engineering C 2006年第8期26卷 1408-1411页

作者： Muyco, Julie J. Gray, Jeremy J. Ratto, Timothy V. Orme, Christine A. McKittrick, Joanna Frangos, John Lawrence Livermore National Laboratory Chemistry and Materials Science 7000 East Ave. L-350 Livermore CA 94550 United States University of California Mechanical and Aerospace Engineering Materials Science and Engineering Graduate Program 9500 Gilman Dr La Jolla CA 92093 United States La Jolla Bioengineering Institute 505 Coast Blvd. S. Ste. #405 La Jolla CA 92037 United States

Three possible functions of Ti-peroxy gel are: reduction of the inflammatory response through the reduction of hydrogen peroxide and other reactive oxygen species;creation of a favorable surface for calcium phosphate nucleation;and as a transitional layer between the compliant surrounding tissue and the stiff titanium. Traditional surface characterization techniques operate in high vacuum environments that alter the actual sample-solution interface. Our studies used techniques that allowed samples to remain in solution and be observed over time. Atomic force microscopy (AFM) force-distance curves, electrochemical impedance spectroscopy (EIS), and Raman spectroscopy were each used in situ to define kinetic and mechanical properties of Ti-peroxy gel as it formed over time on titanium during exposure to hydrogen peroxide. Our studies enabled us to monitor real-time changes in the native oxide layer on titanium in hydrogen peroxide containing solution, including the formation of a Ti-peroxy gel layer above the native oxide. Peaks attributed to Ti-peroxy gel were seen to emerge over the course of several hours using in situ Raman spectroscopy. Force-distance curves suggest a layer that thickens with time on the titanium sample surface. EIS data showed that changes in the surface layers could be monitored in solution over time. © 2005 Elsevier B.V. All rights reserved.

关键词： Gels

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Chitosan for biofunctionalization of microsystems

Chitosan for biofunctionalization of microsystems

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2006 IEEE/NLM Life science Systems and Applications Workshop, LiSA 2006

作者： Koev, Stephan T. Powers, Michael A. Badilita, Vlad Yi, Hyunmin Bentley, William E. Payne, Gregory F. Rubloff, Gary W. Ghodssi, Reza Department of Electrical and Computer Engineering University of Maryland College Park MD 20742 Department of Materials Science and Engineering University of Maryland College Park MD 20742 Department of Chemical Engineering University of Maryland College Park MD 20742 University of Maryland College Park MD 20742 University of Maryland College Park MD 20742 Bioengineering Graduate Program University of Maryland College Park MD 20742

ISBN: (纸本)1424402786

We present the use of the polysaccharide chitosan for immobilizing biomolecules on microfabricated device surfaces. The main advantages of chitosan are its abundance of primary amine groups and its ability to be electrodeposited. Biomolecules are easily attached to chitosan's amines by standard glutaraldehyde chemistry. The electrodeposition of chitosan allows accurate spatial and temporal control of biomolecule placement. We have demonstrated this biofunctionalization method for two different BioMEMS devices: a biophotonic sensor and a micromechanical biosensor. We have successfully assembled probe DNA on each of them and detected hybridization with target DNA as a demonstration of sensor operation. Here, we briefly present the fabrication procedure and testing results for both of these BioMEMS sensing devices. © 2006 IEEE.

关键词： Microsystems

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Ottenimento di silice amorfa a partire da pula di riso madiante estrazione

C e Ca

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C e Ca 2006年第2期36卷 141-145页

作者： Junkes, J.A. Della, V.P. Acchar, W. Oliveira, A.P.N. Hotza, D. Materials Science and Engineering Graduate Program Federal University of Santa Catarina Florianopolis Brazil Department of Physics Federal University of Rio Grande do Norte Natal Brazil Department of Chemical Engineering Federal University of Santa Catarina Florianopolis Brazil

Rice husk can be an interesting source of raw material for obtaining silica, due to its composition, availability and cost. The extraction process of silica from rice husk can be divided in two parts. First some components of rice husk are removed by acid leaching, using HCl, H2SO4, or a mixture of them, followed by calcination for burning out carbon compounds. The residue obtained after calcination is composed of about 95% amorphous silica. In this work, silica was produced from rice husk following the steps previously described, using leaching solutions of 10% HCl, 10% H 2SO4 and a mixture of 10% HCl and 10% H2SO 4. Calcination of leached materials was carried out at 600 or 700°C for 3 h. The silica powder obtained presented a mean particle size of 18 μm, around 98% amorphous SiO2 with a specific surface area of about 300 m2/g.

关键词： Hulls (seed coverings)

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