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Binuclear Macrocyclic Silver(I) Complex of a Bis(carbone) Pincer Ligand: Synthesis and Application as a Carbone-Transfer Agent

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Inorganic Chemistry 2023年第32期62卷 12664-12673页

作者： Aweke, Bamlaku Semagne Yu, Cheng-Han Shen, Jiun-Shian Wang, Sheng Yap, Glenn P. A. Chen, Wen-Ching Ong, Tiow-Gan Institute of Chemistry Academia Sinica Taipei11529 Taiwan Department of Applied Chemistry National Yang Ming Chiao Tung University Hsinchu30010 Taiwan Department of Chemistry National Taiwan University Taipei106216 Taiwan Department of Medicinal and Applied Chemistry National Taiwan University 10617 Kaohsiung Medical University Kaohsiung80708 Taiwan Sustainable Chemical Science and Technology Taiwan International Graduate Program Academia Sinica Taipei11529 Taiwan Department of Chemistry and Biochemistry University of Delaware NewarkDE19716 United States

A facile synthesis of a binuclear AgI complex 2 of a bis(carbone) ligand L and its application as a carbone-transfer agent for the generation of other transition-metal complexes of AuI (3), NiII (4), and PdII (5) is presented. Complex 2 was synthesized through multiple synthetic routes under mild reaction conditions using the tetracationic [LH4][OTf·Cl]2 precursor salt, the dicationic [LH2][OTf]2 ylide salt, and the free ligand L. The first two synthesis routes require no prior isolation of the air-, moisture-, and temperature-sensitive free ligand L, thus affording complex 2 with high yield and purity. Multinuclear NMR techniques, high-resolution mass spectrometry, and single-crystal X-ray diffraction analysis confirmed the identity of complex 2 as a binuclear AgI complex of L with a molecular formula of [L2Ag2][OTf]2 and a 16-membered-ring metallomacrocyclic structure. During the transmetalation reaction with AuI, the binuclear nature of complex 2 remains intact to give analogous complex 3 ([L2Au2][OTf]2). However, the dimeric structure was disrupted upon the carbone-transfer reaction with NiII and PdII, yielding mononuclear C-N-C pincer-type complexes 4 ([LNiCl][OTf]) and 5 ([LPdCl][OTf]), respectively. These results demonstrated the versatile use of complex 2 as a carbone-transfer agent to other transition metals regardless of the type or size of the metals or the geometry they prefer. © 2023 American Chemical Society.

关键词： Transition metals

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Incidence, prevalence, and medical costs of pressure injuries in Taiwan from 2001 to 2015: Results of a retrospective cohort study

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Journal of Clinical Nursing 2024年第4期34卷 1264-1276页

作者： Tai, Chia-Hui Wang, Jen-Hung Lo, Shu-Fen Tsay, Shwu-Feng Yang, Chao-Chih O Yang, An-Chi Chung, Hui-Chun Department of Nursing Hualien Tzu Chi Hospital Buddhist Tzu Chi Medical Foundation Hualien Taiwan Department of Nursing Tzu Chi University of Science and Technology Hualien Taiwan Department of Medical Research Hualien Tzu Chi Hospital Buddhist Tzu Chi Medical Foundation Hualien Taiwan Department of Nursing Tzu Chi University Hualien Taiwan General Department of Nursing and Health Care Ministry of Health and Welfare Taipei Taiwan Department of Health Services Administration College of Public Health China Medical University Taichung Taiwan Adjunct Rank Technical Expert School of Nursing National Taiwan University Taipei Taiwan Division of Plastic Surgery Department of Surgery Taichung Tzu Chi Hospital Buddhist Tzu Chi Medical Foundation Taichung Taiwan Department of Nursing Tzu Chi University and Doctoral Program Student School and Graduate Institute of Nursing National Taiwan University Taipei Taiwan

Aims and Objectives: This study aims to analyse the trends in the incidence, prevalence and medical costs of pressure injuries (PIs) among genders in Taiwan. Background: The treatment of PIs is complex and costly, often leading to complications and increased mortality. This issue significantly impacts healthcare quality and incurs substantial medical and social costs, warranting attention. Methods: A retrospective cohort study was conducted using data from Taiwan's National Health Insurance Database to obtain and calculate the incidence, prevalence, and medical costs of PIs in the country between 2001 and 2015 as well as to analyse high-risk groups and the medical care utilisation of patients following the STROBE reporting guidelines. Results: Between 2001 and 2015, 15,327 incident case of PIs were diagnosed. During the study period, the prevalence rate of PIs per 100,000 population rose from 26.3 to 189.6, with approximately 11.5%–16.3% of patients undergoing surgical debridement. The PIs prevalence rate increased by 7.2-fold, and hospitalisation costs accounted for 91.7%–96.0% of the total medical costs. Patients with older age, comorbidities, poorer financial status and lower education levels were found to be likely to develop PIs. These predisposing factors differed between males and females. The prevalence of PIs was higher in patients ≥75 years old than in patients from other age groups. Moreover, PI-related medical expenses have been increasing annually. Conclusions: In Taiwan, the rising incidence of PIs is driving up medical costs. Effective care and prevention of PIs necessitate a comprehensive plan from the entire healthcare system. Relevance to Clinical Practice: This research fills a gap in the available data on the incidence, prevalence, and medical costs of PIs in Taiwan and Asia. Patient or Public Contribution: The findings can be used to help develop clinical guidelines for preventive education and treatment of PIs. © 2024 John Wiley & Sons Ltd.

关键词： comorbidity diagnosis incidence medical care costs population health pressure injuries prevalence

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CASE REPORT: A SPORADIC BOVINE PAPULAR STOMATITIS VIRUS INFECTION IN DAIRY CALVES IN SOUTH TAIWAN

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Taiwan Veterinary Journal 2024年第03N04期49卷 109-115页

作者： Huan-Yu Hsu Yu-Ching Chuang Wei-Yu Hsu Chih-Wei Huang Guan-Ming Ke Veterinary Medical Teaching Hospital National Pingtung University of Science and Technology Neipu Pingtung Taiwan International Degree Program in Animal Vaccine Technology International College National Pingtung University of Science and Technology Neipu Pingtung Taiwan Veterinary Research Institute Ministry of Agriculture Tamsui New Taipei Taiwan Department of Veterinary Medicine College of Veterinary Medicine National Pingtung University of Science and Technology Neipu Pingtung Taiwan Graduate Institute of Animal Vaccine Technology College of Veterinary Medicine National Pingtung University of Science and Technology Neipu Pingtung Taiwan

An outbreak of a disease with multiple erosive papules and ulcers on the lips, noses, and tongues of calves was reported in Taiwan in August 2023. Five of 11 2–4-month-old dairy calves were affected. Oral swabs, nasal swabs, and esophageal–pharyngeal fluid were collected and tested positive for bovine papular stomatitis virus (BPSV) via quantitative real-time polymerase chain reaction assay (qPCR) for all of the affected calves. All of the positive calves remained positive for BPSV after 1 month of the outbreak, and the viral loads of the affected calves did not decrease within this period. To determine the genetic characteristics of this outbreak strain, phylogenetic analysis was performed with the partial B2L sequence of BPSV. The results revealed that the virus strain was closely related to isolates from Japan, the United States, and France. This is the first report on an outbreak in this particular region since 1988 and the first molecular characterization of BPSV in Taiwan.

关键词： Bovine papular stomatitis virus Phylogenetic analysis Taiwan

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NIR-Responsive Methotrexate-Modified Iron Selenide Nanorods for Synergistic Magnetic Hyperthermic, Photothermal, and Chemodynamic Therapy

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ACS Applied Materials and Interfaces 2024年第20期16卷 25622-25636页

作者： Thirumurugan, Senthilkumar Muthiah, Kayalvizhi Samuvel Lin, Yu-Chien Dhawan, Udesh Liu, Wai-Ching Wang, An-Ni Liu, Xinke Hsiao, Michael Tseng, Ching-Li Chung, Ren-Jei No. 1 Section 3 Zhongxiao East Road Taipei10608 Taiwan Centre for the Cellular Microenvironment Division of Biomedical Engineering James Watt School of Engineering Mazumdar-Shaw Advanced Research Centre University of Glasgow GlasgowG116EW United Kingdom Faculty of Science and Technology Technological and Higher Education Institute of Hong Kong Hong Kong New Territories999077 Hong Kong Scrona AG Grubenstrasse 9 Zürich8045 Switzerland College of Materials Science and Engineering Chinese Engineering and Research Institute of Microelectronics Shenzhen University Shenzhen518060 China Department of Electrical and Computer Engineering National University of Singapore Singapore117583 Singapore Genomics Research Center Academia Sinica Taipei115 Taiwan Department and Graduate Institute of Veterinary Medicine School of Veterinary Medicine National Taiwan University Taipei10617 Taiwan Graduate Institute of Biomedical Materials and Tissue Engineering College of Biomedical Engineering Taipei Medical University Taipei11031 Taiwan International Ph.D. Program in Biomedical Engineering College of Biomedical Engineering Taipei Medical University Taipei11031 Taiwan Research Center of Biomedical Device College of Biomedical Engineering Taipei Medical University Taipei11031 Taiwan International Ph.D. Program in Cell Therapy and Regenerative Medicine College of Medicine Taipei Medical University Taipei11031 Taiwan Taipei10608 Taiwan

Breast cancer is a malignant tumor with a high mortality rate among women. Therefore, it is necessary to develop novel therapies to effectively treat this disease. In this study, iron selenide nanorods (FeSe2 NRs) were designed for use in magnetic hyperthermic, photothermal, and chemodynamic therapy (MHT/PTT/CDT) for breast cancer. To illustrate their efficacy, FeSe2 NRs were modified with the chemotherapeutic agent methotrexate (MTX). MTX-modified FeSe2 (FeSe2-MTX) exhibited excellent controlled drug release properties. Fe2+ released from FeSe2 NRs induced the release of •OH from H2O2 via a Fenton/Fenton-like reaction, enhancing the efficacy of CDT. Under alternating magnetic field (AMF) stimulation and 808 nm laser irradiation, FeSe2-MTX exerted potent hyperthermic and photothermal effects by suppressing tumor growth in a breast cancer nude mouse model. In addition, FeSe2 NRs can be used for magnetic resonance imaging in vivo by incorporating their superparamagnetic characteristics into a single nanomaterial. Overall, we presented a novel technique for the precise delivery of functional nanosystems to tumors that can enhance the efficacy of breast cancer treatment. © 2024 The Authors. Published by American Chemical Society

关键词： Magnetic resonance imaging

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Ohwia caudata extract relieves the IL-17A-induced inflammatory response of synoviocytes through modulation of SOCS3 and JAK2/STAT3 activation

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Environmental Toxicology 2023年第8期38卷 1914-1924页

作者： Lu, Cheng-You Kuo, Chia-Hua Kuo, Wei-Wen Hsieh, Dennis Jine-Yuan Wang, Tso-Fu Shih, Cheng-Yen Lin, Pi-Yu Lin, Shinn-Zong Ho, Tsung-Jung Huang, Chih-Yang Department of Post-Baccalaureate Medicine College of Medicine National Chung Hsing University Taichung Taiwan Department of Sports Sciences University of Taipei Taipei Taiwan Department of Biological Science and Technology China Medical University Taichung Taiwan Ph.D. Program for Biotechnology Industry China Medical University Taichung Taiwan School of Medical Laboratory and Biotechnology Chung Shan Medical University Taichung Taiwan Clinical Laboratory Chung Shan Medical University Hospital Taichung Taiwan Department of Hematology and Oncology Hualien Tzu Chi Hospital Buddhist Tzu Chi Medical Foundation Hualien Taiwan Department of Medicine Hualien Tzu Chi Hospital Buddhist Tzu Chi Medical Foundation Tzu Chi University Hualien Taiwan Buddhist Tzu Chi Medical Foundation Hualien Taiwan Buddhist Compassion Relief Tzu Chi Foundation Hualien Taiwan Bioinnovation Center Buddhist Tzu Chi Medical Foundation Hualien Taiwan Department of Neurosurgery Hualien Tzu Chi Hospital Buddhist Tzu Chi Medical Foundation Hualien Taiwan Integration of Chinese Medicine and Modern Medicine Hualien Tzu Chi Hospital Buddhist Tzu Chi Medical Foundation Hualien Taiwan Department of Chinese Medicine Hualien Tzu Chi Hospital Buddhist Tzu Chi Medical Foundation Hualien Taiwan Cardiovascular and Mitochondrial Related Disease Research Center Hualien Tzu Chi Hospital Buddhist Tzu Chi Medical Foundation Hualien Taiwan Graduate Institute of Biomedical Sciences China Medical University Taichung Taiwan Department of Biological Science and Technology Asia University Taichung Taiwan Center of General Education Buddhist Tzu Chi Medical Foundation Tzu Chi University of Science and Technology Hualien Taiwan

Fibroblast-like synoviocytes accumulation, proliferation and activation, and the subsequent inflammatory mediators production play a key role in the progression of rheumatoid arthritis (RA). It is well established that Janus kinase 2/signal transducer and activator of transcription 3 (JAK2/STAT3) signaling triggers inflammation, and induces cytokine levels in RA. Ohwia caudata have long been used against many disorders. However, in RA, the effects of O. caudata have not been elucidated. In the current study, synoviocytes were used to evaluate the suppressive effects of O. caudate extract (OCE) on the pro-inflammatory cytokines production. In vitro, the underlying mechanisms by which OCE inhibits inflammatory response through regulation of suppressors of cytokine signaling 3 (SOCS3) and JAK2/STAT3 expression in IL-17A-treated HIG-82 synoviocytes were investigated. The results demonstrated that the proliferation of IL-17A-challenged cells were increased in comparison with non-stimulated control cells. The synoviocyte proliferation was decreased significantly of OCE concentrations in dose dependent manner. The p-JAK2, p-STAT3, interleukin (IL)-1β, and IL-6 were reduced in IL-17A-challenged cells treated with OCE. Furthermore, AZD1480 (a JAK2-specific inhibitor) or WP1066 (a STAT3-specific inhibitor) affected the inflammatory mediators production in IL-17A-challenged synoviocytes, and OCE failed to mitigate the IL-17A-induced inflammatory mediators and SOCS3, acting as a feedback inhibitor of the JAK/STAT3 pathway, in the presence of SOCS3 siRNA, indicating that the beneficial effects of OCE on the regulation of inflammatory response homeostasis were dependent on SOCS3 and the JAK2/STAT3 signaling pathway. Our study also showed that SOCS3 was markedly activated by OCE in RA fibroblast-like synoviocytes, thereby decreasing the JAK/STAT3 pathway, and the IL-1β, and IL-6 activation. Thus, O. caudate should be further investigated as a candidate anti-inflammatory and anti-a

关键词： Chemical activation

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Contour Detection from Ultrasound Kidney Images with A Coarse-to-Fine Approach

Contour Detection from Ultrasound Kidney Images with A Coars...

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2023 IEEE International Conference on Systems, Man, and Cybernetics, SMC 2023

作者： Peng, Tao Gu, Yidong Xu, Yanqing Wang, Caishan Zhang, Lei Cai, Jing School of Future Science and Engineering Soochow University Suzhou China UT Southwestern Medical Center Department of Radiation Oncology DallasTX United States The Affiliated Suzhou Hospital of Nanjing Medical University Department of Medical Ultrasound Suzhou Municipal Hospital Jiangsu Suzhou China University of Texas Southwestern Medical Center McDermott Center for Human Growth and Development DallasTX United States The Second Affiliated Hospital of Soochow University Department of Ultrasound Suzhou China Duke Kunshan University Graduate Program of Medical Physics and Data Science Research Center Jiangsu Kunshan China The Hong Kong Polytechnic University Department of Health Technology and Informatics Hong Kong Hong Kong

ISBN: (纸本)9798350337020

Ultrasound kidney image segmentation presents significant challenges due to missing or ambiguous boundaries. In this study, we introduce a coarse-to-refinement approach incorporating four novel aspects. Firstly, we leverage the properties of a principal curve (PC) to automatically fine-tune the curve shape and employ a neural network's learning ability to reduce model error. Secondly, a deep fusion learning network is utilized for the coarse segmentation step, incorporating a parallel architecture to enhance deep-learning performance. Thirdly, addressing the limitation of standard PC-based methods in determining the number of vertices automatically, we propose an automatic searching polygon tracking method using a mean shift clustering-based approach to replace the projection and vertex extension step in standard PC-based methods. Lastly, we develop an explainable mathematical map function for the kidney contour, as denoted by the neural network output (i.e., optimized vertices), which aligns well with the ground truth contour. We conducted various experiments to evaluate our method's performance, demonstrating its effectiveness in ultrasound kidney image segmentation. © 2023 IEEE.

关键词： Artificial intelligence Explainable mathematical model Ultrasound kidney segmentation

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Hybrid Intelligent-Annotation Organ Segmentation on medical Datasets

Hybrid Intelligent-Annotation Organ Segmentation on Medical ...

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2023 IEEE International Conference on Systems, Man, and Cybernetics, SMC 2023

作者： Peng, Tao Zhao, Jing Gu, Yidong Di, Gongye Zhang, Lei Cai, Jing School of Future Science and Engineering Soochow University Suzhou China Ut Southwestern Medical Center Department of Radiation Oncology DallasTX United States Tsinghua University Affiliated Beijing Tsinghua Changgung Hospital Department of Ultrasound Beijing China The Affiliated Suzhou Hospital of Nanjing Medical University Suzhou Municipal Hospital Department of Medical Ultrasound Jiangsu Suzhou China The Affiliated Taizhou People's Hospital of Nanjing Medical University Department of Ultrasonic Taizhou China Duke Kunshan University Graduate Program of Medical Physics Data Science Research Center Jiangsu Kunshan China The Hong Kong Polytechnic University Department of Health Technology and Informatics Hong Kong

ISBN: (纸本)9798350337020

Ultrasound image segmentation is crucial for early disease detection and treatment planning but remains a challenging task due to the low contrast of organ boundaries and varying image quality. Current methods often require manual intervention or have limited accuracy. In this paper, we propose a novel hybrid framework that combines an automatic option polygon segment (AOPS) algorithm and a distributed- and memory-based evolution (DME) algorithm for precise ultrasound organ segmentation. Our pipeline consists of two cascaded stages: (1) a coarse segmentation step using the AOPS algorithm, which determines the number of vertices/clusters without human intervention, and (2) a refinement step using the DME algorithm to hunt for the optimal neural network, which is then used to represent a smooth, explainable mathematical expression of the organ boundary. We employ the fractional backpropagation learning network with L2 regularization (FBLN) for training and use the scaled exponential linear unit (SELU) activation function to address the vanishing gradient problem. This is a new attempt such a hybrid framework is applied to ultrasound organ segmentation tasks, and it demonstrates significant contributions in terms of accuracy, smoothness, and computational efficiency. © 2023 IEEE.

关键词： distributed-evolution learning network Multi-organs segmentation principal curve SEL U-based explainable mathematical model ultrasound

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Verification of the Inactivation Effect of Near-UV LEDs using a Pulsed Lighting System on Staphylococcus aureus

Verification of the Inactivation Effect of Near-UV LEDs usin...

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Sustainable Smart Lighting World Conference & Expo (LS18), IEEE

作者： Hiroki Nomura Seiji Kihara Akinori Zukeran Jun Sawai Takayuki Misu Graduate School of Engineering Master's Degree Program in Electrical and Electronic Engineering Kanagawa Institute of Technology Atsugi Kanagawa Japan Department of Electrical and Electronic Engineering Faculty of Engineering Kanagawa Institute of Technology Atsugi Kanagawa Japan Department of Nutrition and Life Science Faculty of Health and Medical Sciences Kanagawa Institute of Technology Atsugi Kanagawa Japan

ISBN: (数字)9798331540197

ISBN: (纸本)9798331540203

The purpose of this study is to investigate the disinfection effect of Near-UV LED light, which is pulsed using PWM control, on Staphylococcus aureus. To evaluate the disinfection effect of Near-UV LED light, three types of Near-UV LEDs with wavelengths of 395 nm, 385 nm, and 365 nm were installed within a sealed space inside an incubator and energized with a forward current of 1000 mA and a forward voltage of 3.6 V, and the disinfection rate under each type of light was assessed. Additionally, the disinfection effect was evaluated when the same three types of Near-UV LEDs were pulsed with a 50% duty cycle. As a result, 100% disinfection was achieved with 365 nm Near-UV LED direct-current irradiation for 120 seconds, and a 93% disinfection rate was obtained with pulsed irradiation for 150 seconds.

关键词： Radiation effects Power demand Lighting Pulse width modulation Aerospace electronics Light emitting diodes

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A Label-Free Electrochemical Biosensor for the Detection of Alpha-Thalassemia 1 (Sea Deletion) Carriers Using Screen-Printed Carbon Electrodes

SSRN

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SSRN 2023年

作者： Chomean, Sirinart Thamwarokun, Areenuch Kaset, Chollanot Karuwan, Chanpen Kamsong, Wichayaporn Attapong, Jirapat Graduate Program in Biomedical Sciences Faculty of Allied Health Sciences Thammasat University Pathumtani Thailand Department of Medical Technology Faculty of Allied Health Sciences Thammasat University Pathumtani Thailand Thammasat University Research Unit in Medical Technology and Precision Medicine Innovation Thammasat University Pathumtani Thailand Phahonyothin Thailand

A label-free electrochemical DNA biosensor based on screen-printed carbon electrodes (SPCEs) coupled with H33258 dye has been extensively developed to diagnose human genetic diseases. However, many developed methods are still limited to simulated target DNA. In the present study we aimed to develop a label-free electrochemical DNA biosensor based on SPCEs for identifying carriers of α-thalassemia 1 (SEA deletion), which is the most common inherited blood disorder worldwide. Twenty samples of known normal α-globin gene and α-thalassemia 1 (SEA deletion) carriers were assessed;the criterion cut-off values were more than 26.84 kΩ (negative imaginary impedance, -Z") and 48.83 kΩ (charge transfer resistance, Rct). Reliability analysis between -Z" and Rct showed a strong correlation, with a Pearson’s correlation coefficient value of 0.88 and a mean difference between Rct and -Z′′, determined by Bland–Altman plot analysis, of 55.8 kΩ. The diagnostic potency of the developed EIS biosensor based on SPCEs was evaluated in 81 clinical blood samples. The results demonstrate that the biosensor had 100% sensitivity, 88.2% specificity, 83.3% positive predictive value (PPV), 100% negative predictive value (NPV) and 92.6% accuracy for Rct measurement. The developed EIS biosensor based on SPCEs is an attractive alternative method to gel electrophoresis for the detection of α-thalassemia 1 (SEA deletion) carriers. It is simple, inexpensive and can reduce turnaround time 45-fold. Identification of an α-thalassemia 1 (SEA deletion) carrier is the most effective approach for the management of thalassemia and for the prevention of Hb Bart’s hydrops fetalis, the most severe form of thalassemia. © 2023, The Authors. All rights reserved.

关键词： Biosensors

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Spray-pyrolysis synthesis of CuMnO₂ with the potential for photoelectrocatalysis

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Journal of the Chinese Chemical Society 2024年第10期71卷 1203-1210页

作者： Martinez, Benjamin Kuo, Chun-Hong Chiang, Ming-Hsi Institute of Chemistry Academia Sinica Taipei Taiwan Sustainable Chemical Science and Technology Taiwan International Graduate Program Academia Sinica and National Yang Ming Chiao Tung University Hsinchu Taiwan Department of Applied Chemistry National Yang Ming Chiao Tung University Hsinchu Taiwan Center for Emergent Functional Matter Science National Yang Ming Chiao Tung University Hsinchu Taiwan National Synchrotron Radiation Research Center Hsinchu Taiwan Department of Medicinal and Applied Chemistry Kaohsiung Medical University Kaohsiung Taiwan

Amidst the global endeavor toward sustainable energy sources, photocatalysis appears as a promising gateway toward the production of solar fuels, in particular hydrogen. Hydrogen is currently a crucial reagent for vital industries such as petrol desulfurization, iron reduction and ammonia production, so the decarbonization of its production is a major challenge. CuMnO₂ (CMO), a p-type semiconductor, has been shown to enhance the efficiency of catalysts such as TiO₂ for the photoelectrocatalytic water splitting reaction. However, since pure CMO thin films have never been reported, its potential and limitations remain elusive. We used spray pyrolysis as a low-cost synthesis technique to simplify and accelerate the synthesis of CMO thin films directly on FTO substrates. CMO prepared in this manner exhibits activity toward photoeletrocatalytic water splitting and O₂ reduction. The activity has been found to be highly dependent on synthesis conditions, especially on the ratio and volume of precursors. © 2024 The Chemical Society Located in Taipei & Wiley-VCH GmbH.

关键词： crednerite hydrogen oxygen reduction p-type semiconductor water splitting

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