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Effect of water loss during curing on hydration reaction and hydrates conversion in calcium aluminate cement-bonded castables

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Journal of Iron and Steel Research International 2024年第9期31卷 2133-2141页

作者： Zhong-zhuang Zhang Xiao-yu Wang Song-zhu Chu Jin-yan Zeng Yuan-dong Mu You-qi Li Zhong-tao Luo Guo-tian Ye Henan Key Laboratory of High Temperature Functional Ceramics School of Materials Science and EngineeringZhengzhou UniversityZhengzhou450001HenanChina School of Materials Science and Engineering Key Laboratory of Materials Processing and Mold Ministry of EducationZhengzhou UniversityZhengzhou450000HenanChina Jiangsu Jingxin New Materials Co. Ltd.Yangzhou225000JiangsuChina

Free water available in calcium aluminate cement(CAC)-bonded castables is crucial for the hydration of CAC and the conversion of hydration products in the curing and drying processes,as both the hydration and conversion reactions are dissolution–precipitation *** elucidate the effect of different levels of free water loss upon the hydration of CAC,the conversion of hydration products and the mechanical strength of the CAC-bonded castables,the CAC-bonded castables were subjected to sealed and unsealed curing conditions at 50℃ and drying at 110℃.The results demonstrate that the fast removal of free water during unsealed curing would hinder the conversion from 2CaO·Al_(2)O_(3)·8H_(2)O to 3CaO·Al_(2)O_(3)·6H_(2)O and consequently prevent the deterioration of *** a comparison,although sealed-cured samples have less water loss and high degree of hydration of CAC,they still show lower strength than the unsealed samples after *** following drying process further accelerates the hydration of residual calcium aluminate clinkers for both the sealed and unsealed samples,but still does not favor the conversion from 2CaO·Al_(2)O_(3)·8H_(2)O to 3CaO·Al_(2)O_(3)·6H_(2)O in the unsealed-cured samples.

关键词： Water loss Hydration Conversion Mechanical strength Calcium aluminate cement

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Effect of surface modification on thermal expansion of Zr_(2)WP_(2)O_(12)/aromatic polyimides based composites

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Tungsten 2023年第1期5卷 179-188页

作者： Xin-Wei Shi Sen Zhang Qiang Zhou Jing Li Bai-Lin Zhu Liu-Jie Xu Qi-Long Gao School of Physics and Microelectronics Zhengzhou UniversityZhengzhou 450001China The State Key Laboratory of Refractories and Metallurgy Wuhan University of Science and TechnologyWuhan 430081China Henan Key Laboratory of High-Temperature Structural and Functional Materials Henan University of Science and TechnologyLuoyang 471003China

Surface modification is a fascinating way to improve the compounding effect between inorganic fillers and *** this study,zirconium tungsten phosphate(ZWP) with negative thermal expansion was surface modified by silane coupling agent 3-(Trimethoxysilyl)propyl *** effects of surface modification and the modification mechanism were analyzed in detail by X-ray diffractometer,scanning electron microscopy,Fourier transform infrared spectroscopy and thermal mechanical *** surface modification could effectively reduce the thermal expansion properties of the *** the added amount of 3-methacryloxypropyl trimethoxysilaneSilane(trade name:KH570) is 0.50 wt%,the thermal expansion coefficient of ZWP/Aromatic polyimide composite decreased by 9.76%.The surface modification also can effectively improve the dielectric performance of aromatic *** present work provides one new way to improve the thermal expansion behavior of composites.

关键词： Negative thermal expansion Tungsten Surface modification Polyimide composite Silane coupling agent

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Binder Effect on Properties of Cr_(2)O_(3)-bearing Corundum-based Refractory Castables

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China's Refractories 2023年第3期32卷 36-41页

作者： ZHANG Hongrui CHEN Liugang Henan Key Laboratory of High Temperature Functional Ceramics School of Materials Science and EngineeringZhengzhou UniversityZhengzhou 450052China

Cr_(2)O_(3)-bearing castables bonded with reactive MgO(RM)or calcium aluminate cement(CAC)were studied to evaluate the binder effect on their performance in corrosive *** properties of the as-prepared castables were compared with respect to the differences in phase composition and *** corrosion behavior of the as-prepared castables by CaO-Al_(2)O_(3)-Fe_(2)O_(3)-SiO_(2)-based slag was systematically compared viarefractory cup testing at 1600℃with respect to the differences in phase composition and *** analysis indicates that RM bonded castables show higher apparent porosity,lower bulk density and strengths after drying at 110℃and firing at 1300℃,and higher permanent linear change after firing at 1300℃,but better slag corrosion and infiltration resistance compared with CAC bonded castables.

关键词： corrosion resistance Cr_(2)O_(3)-bearing castables refractories reactive MgO Mg(Al,Cr)2O4 spinel

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Properties and microstructure of oxide dispersion strengthened tungsten alloy prepared by liquid-phase method:a review

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Tungsten 2023年第4期5卷 481-502页

作者： Liu-Jie Xu Zhou Li Fang-Nao Xiao Yun-Chao Zhao Yu-Cheng Zhou Shi-Zhong Wei National Joint Engineering Research Center for Abrasion Control and Molding of Metal Materials Henan University of Science and TechnologyLuoyang471003China Henan Key Laboratory of High-temperature Structural and Functional Materials Henan University of Science and TechnologyLuoyang471003China College of Material Science and Technology Nanjing University of Aeronautics and AstronauticsNanjing201116China

The addition of the second phase into tungsten can significantly refine the grain size of tungsten alloys,and also play a role in dispersion strengthening,thus improving the properties of tungsten *** a preparation method of tungsten alloy powder,liquid-phase method avoids the disadvantage of mechanical alloying,and the obtained powder composition is accurate and controllable,with high purity and excellent *** present,the second phase particles used for dispersion strengthening tungsten alloys are mainly composed of *** particles can be synthesized and precipitated in nitrate solution through in situ chemical reaction,and are uniformly distributed in composite powder by mixing and ***,the oxide dispersion strengthened tungsten alloy(ODS-W)was obtained by reduction and ***-phase methods for preparing ODS-W alloys include azeotropic distillation,sol-gel methods,freeze-drying,hydrothermal synthesis,spray-drying,*** this paper,several liquid-phase methods for preparing tungsten alloy composite powder precursors are reviewed,and their latest research progresses are *** addition,the morphologies and properties of tungsten alloys prepared by different methods are compared,which provides guidance for preparing high-performance tungsten alloys.

关键词： Tungsten alloy ODS-W Liquid-phase method Microstructure Property

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Pore Control and Mechanical Properties of Alumina Ceramics Using Direct Ink Writing

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China's Refractories 2024年第4期33卷 19-28页

作者： ZHU Kai ZHAO Xiang YANG Lianghua YANG Daoyuan YUAN Huiyu Intelligent Manufacturing Institute Henan PolytechnicZhengzhou 450000China Henan Key Laboratory of High Temperature Functional Ceramics School of Materials Science and EngineeringZhengzhou UniversityZhengzhou 450002China

Ceramics with proper pore sizes and geometry are critical to many applications,so that lots of efforts have been made to achieve the *** ink writing(DIW),an additive manufacturing technique,is cost-effective and *** is interesting to study the ability to control the pore size and geometry by the DIW *** this study,alumina ceramics were prepared with special focus on the pore configuration and the performance of printed samples was *** porous structures with different pore sizes(minimum pore size of 200μm)and different shapes(honeycomb,lattice and triangle)were *** printed structures shrunk uniformly and maintained the original geometry after firing,they did not show any visible defects or deformations,and the microstructure was uniform and *** was found the honeycomb structures exhibited superior mechanical strength at the same porosity compared to lattice and triangle structures,which reached 55 MPa with a porosity of 70%.The high strength with the high porosity was attributed to the highly controlled microstructure,i.e.,uniform pore sizes,pore shapes and interconnectivity.

关键词： direct ink writing porous structures high porosity mechanical strength

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Effect of Zircon Addition on Properties of Corundum Porous materials

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China's Refractories 2024年第1期33卷 7-13页

作者： CHEN Haonan LIU Xin ZHANG Shiming LI Ying WANG Di JIA Quanli Henan Key Laboratory of High Temperature Functional Ceramics School of Materials Science and EngineeringZhengzhou UniversityZhengzhou 450052China Henan Building Materials Research and Design Institute Co. Ltd.Zhengzhou 450002China

This paper aims to improve the corrosion resistance of dispersive purging *** fused corundum particles and fine powder,α-Al_(2)O_(3) micropowder,Cr_(2)O_(3) micropowder,Guangxi clay and zircon powder were used as the main raw *** mass ratio of white fused corundum particles and fine powder was fixed at 85:15,and 0,1%,2%,or 3%(by mass)of zircon fine powder was added to replace the same amount of white fused corundum fine *** corundum porous material was prepared by the particle stacking pore-forming method at 1650℃for 3 *** effect of the zircon addition on the properties and microstructure of porous materials was *** results show that:after adding zircon,the permeability of the porous material increases,the cold and hot strengths increase obviously,and the expansion rate after firing *** the addition of zircon is 2%,the comprehensive performance of the specimen is optimal with the smallest linear change rate and the highest permeability.

关键词： porous materials zircon fines purging plug permeability

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Improved material descriptors for bulk modulus in intermetallic compounds via machine learning

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Rare Metals 2023年第7期42卷 2396-2405页

作者： De-Xin Zhu Kun-Ming Pan Yuan Wu Xiao-Ye Zhou Xiang-Yue Li Yong-Peng Ren Sai-Ru Shi Hua Yu Shi-Zhong Wei Hong-Hui Wu Xu-Sheng Yang National Joint Engineering Research Center for Abrasion Control and Molding of Metal Materials Henan Key Laboratory of High-Temperature Structural and Functional MaterialsHenan University of Science and TechnologyLuoyang471003China Longmen Laboratory Luoyang471003China State Key Laboratory for Advanced Metals and Materials University of Science and Technology BeijingBeijing100083China Guangdong Province Key Laboratory of Durability for Marine Civil Engineering School of Civil EngineeringShenzhen UniversityShenzhen518060China Department of Industrial and Systems Engineering The Hong Kong Polytechnic UniversityHong Kong999077China

Bulk modulus is an important mechanical property in the optimal design and selection of intermetallic *** this study,bulk modulus datasets of intermetallic compounds were collected,and the features affecting the bulk modulus of intermetallics were screened via feature *** features B_(cal),dB_(avg),and TIE(corresponding to calculated bulk modulus,mean bulk modulus,and third ionization energy,respectively)were found to be the dominant factors influencing bulk modulus and can be extended to other multi-component ***,we predicted the bulk modulus with an accuracy of 95%using surrogate machine learning models with the selected features,and these features were also demonstrated to be effective for high-entropy ***,symbolic regression provided an expression for the relationship between bulk modulus and the screened *** machine learning models provide a new approach for optimizing and predicting the bulk moduli of intermetallic compounds.

关键词： Bulk modulus Intermetallic compounds Machine learning Symbolic regression

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Molten salt synthesis,morphology modulation,and lithiation mechanism of high entropy oxide for robust lithium storage

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Journal of Energy Chemistry 2023年第11期86卷 536-545,I0011页

作者： Xuefeng Liu Honghong Wang Long Dong Kezhuo Li Haijun Zhang Quanli Jia Shaowei Zhang Wen Lei The State Key Laboratory of Refractories and Metallurgy Wuhan University of Science and TechnologyWuhan 430081HubeiChina Henan Key Laboratory of High Temperature Functional Ceramics Zhengzhou UniversityZhengzhou 450052HenanChina College of Engineering Mathematics and Physical SciencesUniversity of ExeterExeter EX44QFUK Key Laboratory of Advanced Energy Materials Chemistry(Ministry of Education) Nankai UniversityTianjin 300071China

high entropy oxides(HEOs)with ideal element tunability and enticing entropy-driven stability have exhibited unprecedented application potential in electrochemical lithium ***,the general control of dimension and morphology remains a major ***,scalable HEO morphology modulation is implemented through a salt-assisted strategy,which is achieved by regulating the solubility of reactants and the selective adsorption of salt ions on specific crystal *** electrochemical properties,lithiation mechanism,and structure evolution of composition-and morphology-dependent HEO anode are examined in *** importantly,the potential advantages of HEOs as electrode materials are evaluated from both theoretical and experimental *** from the high oxygen vacancy concentration,narrow band gap,and structure durability induced by the multi-element synergy,HEO anode delivers desirable reversible capacity and reaction *** particular,Mg is evidenced to serve as a structural sustainer that significantly inhibits the volume expansion and retains the rock salt *** new perspectives are expected to open a window of opportunity to compositionally/morphologi cally engineer high-performance HEO electrodes.

关键词： high-entropy oxide Lithium-ion battery anode Molten salt Morphology modulation Structure stability

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Application of Ag-based materials in high-performance lithium metal anode:A review

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材料科学技术（英文版） 2023年第2期133卷 165-182页

作者： Zhongxiu Liu Sihu Ha Yong Liu Fei Wang Feng Tao Binrui Xu Renhong Yu Guangxin Wang Fengzhang Ren Hongxia Li Provincial and Ministerial Co-Construction of Collaborative Innovation Center for Non-Ferrous Metal New Materials and Advanced Processing Technology Henan Key Laboratory of Non-Ferrous Materials Science & Processing TechnologySchool of Materials Science and EngineeringHenan University of Science and TechnologyLuoyang 471023China Provincial and Ministerial Co-Construction of Collaborative Innovation Center for Non-Ferrous Metal New Materials and Advanced Processing Technology Henan Key Laboratory of Non-Ferrous Materials Science & Processing TechnologySchool of Materials Science and EngineeringHenan University of Science and TechnologyLuoyang 471023China National Joint Engineering Research Center for Abrasion Control and Molding of Metal Materials Henan Key Laboratory of High-Temperature Structural and Functional MaterialsHenan University of Science and TechnologyLuoyang 471003China School of Electrical Engineering Henan University of Science and TechnologyLuoyang 471023China State Key Laboratory of Advanced Refractories Sinosteel Luoyang Institute of Refractories Research Co.Ltd.Luoyang 471039China

Li metal is a promising candidate for battery anodes due to its high theoretical specific capacity(3860 mAh g-1)and low electrochemical potential(-3.04 V).Nevertheless,the challenges for Li metal include uncontrolled dendrites growth,unstable solid electrolyte interface,and infinite volume expansion during Li plating and stripping,which limit the further development of lithium metal anodes(LMAs).Intro-ducing Ag-based materials in LMAs is regarded as one of the most effective solutions to solve the above-mentioned problems,which have received considerable attention because of their superior characteristics,such as high electrical conductivity,outstanding lithiophilicity,and excellent mechanical ***,we review the recent progress on the application of Ag-based materials in ***,the theo-retical mechanism of Ag-based materials and their advantages in LMAs are *** addition,the relationship between their fabrication strategies,micro/nanostructures,and electrochemical performances is systematically ***,the challenges and opportunities for the future research and appli-cation of Ag-based materials in lithium metal batteries are proposed based on the available academic knowledge.

关键词： Ag-based materials Nucleation sites Current collectors Lithium metal anodes Electrochemical performance

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Shining light on transition metal tungstate-based nanomaterials for electrochemical applications:Structures,progress,and perspectives

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Nano Research 2022年第8期15卷 6924-6960页

作者： Kaijia Feng Zhefei Sun Yong Liu Feng Tao Junqing Ma Han Qian Renhong Yu Kunming Pan Guangxin Wang Shizhong Wei Qiaobao Zhang National Joint Engineering Research Center for Abrasion Control and Molding of Metal Materials Henan Key Laboratory of Non–Ferrous Materials Science&Processing TechnologySchool of Materials Science and EngineeringHenan University of Science and TechnologyLuoyang 471023China Provincial and Ministerial Co–construction of Collaborative Innovation Center for Non-ferrous Metal New Materials and Advanced Processing Technology Henan Key Laboratory of High-temperature Structural and Functional MaterialsHenan University of Science and TechnologyLuoyang 471023China Department of Materials Science and Engineering College of MaterialsXiamen UniversityXiamen 361005China Fujian Key Laboratory of Surface and Interface Engineering for High Performance Materials Xiamen UniversityXiamen 361005China

Transition metal tungstate-based nanomaterials have become one of the research hotspots in electrochemistry due to their abundant natural resources,low costs,and environmental *** studies have demonstrated their significant potentials for electrochemical applications,such as supercapacitors,Li-ion batteries,Na-ion batteries,electrochemical sensing,and *** the rapidly growing research enthusiasm for this topic over the last several years,herein,a critical review of recent progress on the application of transition metal tungstates and their composites for electrochemical applications is *** relationships between synthetic methods,nano/micro structures and electrochemical properties are systematically ***,their promising prospects for future development are also *** is anticipated that this review will inspire ongoing interest in rational designing and fabricating novel transition metal tungstate-based nanomaterials for high-performance electrochemical devices.

关键词： transition metal tungstates supercapacitors lithium-ion batteries sodium-ion batteries electrochemical sensing electrocatalysis

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