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Distinct microstructure and property evolution of 0.76(Bi_(0.5)Na_(0.5))TiO_(3)-0.24SrTiO_(3) ferroelectric ceramics synthesized with different TiO_(2) reactants

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Journal of Materials Science & technology 2023年第20期151卷 73-79页

作者： Jian Guo Ji Zhang Jing Wang Shan-Tao Zhang National Laboratory of Solid State Microstructures College of Engineering and Applied Sciences&Jiangsu Key Laboratory of Artificial Functional Materials&Collaborative Innovation Center of Advanced MicrostructuresNanjing UniversityNanjing 210093China School of Materials Science and Engineering Nanjing University of Science&TechnologyNanjing 210094China State Key Laboratory of Mechanics and Control of Mechanical Structures College of Aerospace EngineeringNanjing University of Aeronautics and AstronauticsNanjing 210016China

Single phase 0.76(Bi_(0.5)Na_(0.5))TiO_(3)–0.24SrTiO_(3) ferroelectric ceramics have been synthesized with homogenous anatase and hierarchical rutile TiO_(2) raw reactants(BNST-A and BNST-R).Either calcined powder persists the microstructure characteristics of raw *** the result,when the sintering temperature increases from 1000 to 1200℃,the average grain size and density of BNST-A increase from 0.49 to 1.48μm and 5.02 to 5.61 g/cm^(3),while those of BNST-R from 0.86 to 1.44μm and 5.37 to 5.61 g/cm^(3).BNST-A illustrates a predominant ergodic relaxor state,and BNST-R prefers a non-ergodic relaxor state,as evidenced by the distinct polarization-electric field loops and current-electric field ***,such a distinct ferroelectric state is independent of sintering *** is believed that the special hierarchical microstructure of rutile TiO_(2) reactant is beneficial to form denser ceramics with larger grains,and thus suppresses the contributions of polar nanoregions and defect-induced built-in field to ferroelectric property,leading to non-ergodic relaxor *** work clearly demonstrates the nonnegligible effects of TiO_(2) reactants on the microstructure and properties of BNST ferroelectric ceramics.

关键词： BNST ferroelectric ceramics TiO_(2)raw reactants Microstructure and property evolution

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Wearable multichannel pulse condition monitoring system based on flexible pressure sensor arrays

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Microsystems & Nanoengineering 2022年第1期8卷 249-258页

作者： Jie Wang Yirun Zhu Zhiyong Wu Yunlin Zhang Jian Lin Tao Chen Huicong Liu Fengxia Wang Lining Sun Jiangsu Provincial Key Laboratory of Advanced Robotics School of Mechanical and Electric EngineeringSoochow UniversitySuzhou 215123China Micro Nano System Research Center Key Laboratory of Advanced Transducers and Intelligent Control System of Ministry of Education and Shanxi Province&College of Information EngineeringTaiyuan University of TechnologyTaiyuan 030024China Suzhou Institute of Nano-tech and Nanobionics Chinese Academy of SciencesSuzhou 215123China

Pulse diagnosis is an irreplaceable part of traditional Chinese medical ***,application of the traditional pulse monitoring method was restricted in the modernization of Chinese medical science since it was difficult to capture real signals and integrate obscure feelings with a modern data ***,a novel multichannel pulse monitoring platform based on traditional Chinese medical science pulse theory and wearable electronics was *** pulse sensing platform simultaneously detected pulse conditions at three pulse positions(Chi,Cun,and Guan).These signals were fitted to smooth surfaces to enable 3-dimensional pulse mapping,which vividly revealed the shape of the pulse length and width and compensated for the shortcomings of traditional single-point pulse ***,the pulse sensing system could measure the pulse signals from different individuals with different conditions and distinguish the differences in pulse *** addition,this system could provide full information on the temporal and spatial dimensions of a person’s pulse waveform,which is similar to the true feelings of doctors’*** innovative,cost-effective,easily designed pulse monitoring platform based on flexible pressure sensor arrays may provide novel applications in modernization of Chinese medical science or intelligent health care.

关键词： multichannel system replace

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Implications of 1.5 K climate warming on warm-season ozone exposure and atmospheric oxidation capacity in China

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Atmospheric and Oceanic Science Letters 2024年第6期17卷 53-61页

作者： Zhihao Shi Lin Huang Xiaodong Xie Momei Qin Jingyi Li Bingye Xu Lingling Jin Jianlin Hu College of Environment Henan Normal UniversityXinxiangChina Jiangsu Key Laboratory of Atmospheric Environment Monitoring and Pollution Control Collaborative Innovation Center of Atmospheric Environment and Equipment TechnologyNanjing University of Information Science&TechnologyNanjingChina Ecological and Environmental Monitoring Center of Zhejiang Province HangzhouChina

Surface ozone(O_(3))poses significant threats to public health,agricultural crops,and plants in natural *** warming is likely to increase future O_(3)mainly by altering atmospheric photochemical reactions and enhancing biogenic volatile organic compound(BVOC)*** assess the impacts of the future 1.5 K climate target on O_(3)concentrations and ecological O_(3)exposure in China,numerical simulations were conducted using the CMAQ(Community Multiscale Air Quality)model during April-October *** O_(3)exposure was estimated using six indices(i.e.,M7,M24,N100,SUM60,W126,and AOT40f).The results show that the temperature rise increases the MDA8 O_(3)(maximum daily eight-hour average O_(3))concentrations by∼3 ppb and the number of O_(3)exceedance days by 10-20 days in the North China Plain(NCP),Yangtze River Delta(YRD),and Sichuan Basin(SCB)*** O_(3)exposure indices show substantial increases.M24 and M7 in eastern and southern China will rise by 1-3 ppb and 2-4 ppb,respectively.N100 increases by more than 120 h in the surrounding regions of ***60 increases by greater than 9 ppm h^(−1),W126 increases by greater than 15 ppm h^(−1)in Shaanxi and SCB,and AOT40f increases by 6 ppm h^(−1)in NCP and *** temperature increase also promotes atmospheric oxidation capacity(AOC)levels,with the higher AOC contributed by OH radicals in southern China but by NO_(3)radicals in northern *** change in the reaction rate caused by the temperature increase has a greater influence on O_(3)exposure and AOC than the change in BVOC emissions.

关键词： Temperature increase Ozone exposure Biogenic emissions Atmospheric oxidation capacity

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Chemical characteristics and sources apportionment of volatile organic compounds in the primary urban area of Shijiazhuang,North China Plain

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Journal of Environmental Sciences 2025年第3期149卷 465-475页

作者： Xiao Zhang Junfeng Wang Jiangwei Zhao Junliang He Yali Lei Kai Meng RuiWei Xue Zhang Miaomiao Zhang Shuangying Ni Eleonora Aruffo College of geographical sciences and Environment Shijiazhuang UniversityShijiazhuang 050035China Jiangsu Key Laboratory of Atmospheric Environment Monitoring and Pollution Control Collaborative Innovation Center of Atmospheric Environment and Equipment TechnologySchool of Environmental Science and EngineeringNanjing University of Information Science and TechnologyNanjing 210044China Hebei Province Ecology Environmental Monitoring Center Shijiazhuang 050037China Key Lab of Geographic Information Science of the Ministry of Education School of Geographic SciencesEast China Normal UniversityShanghai 200241China Hebei Provincial Institute of Meteorological Sciences Shijiazhuang 050021China Key Laboratory of Meteorology and Ecological Environment of Hebei Province Shijiazhuang 050021China Hebei Provincial Academy of Ecological Environmental Science Shijiazhuang 050037China Department of Advanced Technologies in Medicine&Dentistry University“G.d’Annunzio”of Chieti-PescaraChieti 66100Italy Center for Advanced Studies and Technology-CAST Chieti 66100Italy

VOCs(Volatile organic compounds)exert a vital role in ozone and secondary organic aerosol production,necessitating investigations into their concentration,chemical characteristics,and source apportionment for the effective implementation of measures aimed at preventing and controlling atmospheric *** to October 2020,onlinemonitoringwas conducted in the main urban area of Shijiazhuang to collect data on VOCs and analyze their concentrations and ***,the PMF(positive matrix factorization)method was utilized to identify the VOCs *** indicated that the TVOCs(total VOCs)concentration was(96.7±63.4μg/m^3),with alkanes exhibiting the highest concentration of(36.1±26.4μg/m^3),followed by OVOCs(16.4±14.4μg/m^3).The key active components were alkenes and aromatics,among which xylene,propylene,toluene,propionaldehyde,acetaldehyde,ethylene,and styrene played crucial roles as reactive *** sources derived from PMF analysis encompassed vehicle emissions,solvent and coating sources,combustion sources,industrial emissions sources,as well as plant sources,the contribution of which were 37.80%,27.93%,16.57%,15.24%,and 2.46%,***,reducing vehicular exhaust emissions and encouraging neighboring industries to adopt low-volatile organic solvents and coatings should be prioritized to mitigate VOCs levels.

关键词： Volatile organic compounds Pollution characteristics Ozone formation potential OH radical loss rate Source apportionment

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Interfacial behavior of a thermoelectric film bonded to a graded substrate

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Applied Mathematics and Mechanics(English Edition) 2023年第11期44卷 1853-1870页

作者： Juan PENG Dengke LI Zaixing HUANG Guangjian PENG Peijian CHEN Shaohua CHEN School of Materials Science and Physics State Key Laboratory for Geomechanics and Deep Underground EngineeringSchool of Mechanics and Civil EngineeringChina University of Mining and TechnologyXuzhou 221116Jiangsu ProvinceChina State Key Laboratory of Mechanics and Control of Mechanical Structures Nanjing University of Aeronautics and AstronauticsNanjing 210016China College of Mechanical Engineering Zhejiang University of TechnologyHangzhou 310014China State Key Laboratory of Solid Lubrication Lanzhou Institute of Chemical PhysicsChinese Academy of SciencesLanzhou 730000China Institute of Advanced Structure Technology Beijing Institute of TechnologyBeijing 100081China Beijing Key Laboratory of Lightweight Multi-functional Composite Materials and Structures Beijing Institute of TechnologyBeijing 100081China Collaborative Innovation Center of Electric Vehicles in Beijing Beijing Institute of TechnologyBeijing 100081China

To improve the thermoelectric converting performance in applications such as power generation,reutilization of heat energy,refrigeration,and ultrasensitive sensors in scramjet engines,a thermoelectric film/substrate system is widely designed and applied,whose interfacial behavior dominates the strength and service life of thermoelectric ***,a theoretical model of a thermoelectric film bonded to a graded substrate is *** interfacial shear stress,the normal stress in the thermoelectric film,and the stress intensity factors affected by various material and geometric parameters are comprehensively *** is found that adjusting the inhomogeneity parameter of the graded substrate,thermal conductivity,and current density of the thermoelectric film can reduce the risk of interfacial failure of the thermoelectric film/graded substrate *** a stiffer and thicker thermoelectric film is advantageous to the reliability of the thermoelectric film/graded substrate *** results should be of great guiding significance for the present and upcoming applications of thermoelectric materials in various fields.

关键词： thermoelectric film graded substrate interfacial behavior singular integral equation shear stress intensity factor

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Effect of PyC Interface Thickness on the Heat-stability of Cansas-ⅡSiC_(f)/SiC Composites

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Journal of Wuhan University of technology(Materials Science) 2023年第4期38卷 725-734页

作者：韩笑于国强张盛 SHI Jian GAO Xiguang SONG Yingdong WANG Fang Key Laboratory of Aero-Engine Thermal Environment and Structure Ministry of Industry and Information TechnologyCollege of Energy and Power EngineeringNanjing University of Aeronautics and AstronauticsNanjing210016China College of Chemical Engineering Nanjing Forestry UniversityNanjing210016China Jiangsu Province Key Laboratory of Aerospace Power System College of Energy and Power EngineeringNanjing University of Aeronautics and AstronauticsNanjing210016China State Key Laboratory of Mechanics and Control of Mechanical Structures Nanjing University of Aeronautics and AstronauticsNanjing210016China AECC Sichuan Gas Turbine Establishment Chengdu610500China

The effect of the pyrolytic carbon(PyC)interface thickness on the heat-stability of CansasⅡSiC_(f)/SiC composites under Ar up to 1500℃was studied in *** the heat treatment at 1500℃for 50 h,the interface bonding strength of the thin interface(about 200 nm)decreases from 74.4 to 20.1 MPa(73.0%),while that of the thick interface(about 2μm)declines from 7.3 to 3.2 MPa(52.7%).At the same time,the decline fraction of strength of the composites with the thin interface is 12.1%,less than that with the thick interface(42.0%).The fiber strength also decreases after heat treatment,which may be due to the significant growth ofβ-SiC grains and critical *** different heat-stability of the interface with the thin and thick thickness might be related to the inconsistency of the degree of the graphitization of *** with the composites with the thick interface,the composites with the thin interface remained higher tensile strength after heat treatment due to the better interface bonding *** interface with strong bonding strength could protect the fiber by postponing the decomposition of amorphous phases SiC_(x)O_(y) and hindering the generation of fiber defects.

关键词： SiC_(f)/SiC mini-composites heat-stability interface thickness mechanical properties microstructure

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Excellent energy storage properties in non-stoichiometric Bi_(0.5)Na_(0.5)TiO_(3)-based relaxor ferroelectric ceramics

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Chinese Chemical Letters 2024年第7期35卷 470-472页

作者： Shunshun Jiang Ji Zhang Jing Wang Shan-Tao Zhang School of Materials Science and Engineering Nanjing University of Science&TechnologyNanjing 210094China State Key Laboratory of Mechanics and Control of Mechanical Structures College of Aerospace EngineeringNanjing University of Aeronautics and AstronauticsNanjing 210016China National Laboratory of Solid State Microstructures Department of Materials Science and EngineeringCollege of Engineering and Applied Science&Jiangsu Key Laboratory of Artificial Functional Materials&Collaborative Innovation Center of Advanced MicrostructuresNanjing UniversityNanjing 210093China

The rapid development of high-power and pulsed-power techniques inspires extensive investigates on high-performance ceramic-based ***,the low recoverable energy density(Wrec)hampers their wider ***,the non-stoichiometric Bi_(0.5)Na_(0.5)TiO_(3)-based ceramics were designed and *** proper introduction of oxygen vacancies facilitated activating defect dipole,giving rise to reduced remanent ***,the optimal composition exhibited an exceptional high Wrec of 8.3 J/cm^(3),a high efficiency of 85%,and excellent anti-fatigue and thermal *** work provides an efficient approach to explore ceramic capacitors with high capacitive energy storage performances.

关键词： Non-stoichiometric Bi_(0.5)Na_(0.5)TiO_(3) Ceramic capacitor Energy density Thermal stability

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Mission segment division of the whole aeroengine loading spectrum based on flight actions

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Chinese Journal of Aeronautics 2022年第2期35卷 164-174页

作者： Yu JIN Zhigang SUN Yingdong SONG Xin LIN Xuming NIU Junjie DING Jiangsu Province Key Laboratory of Aerospace Power System College of Energy and Power EngineeringNanjing University of Aeronautics and AstronauticsNanjing 210016China Key Laboratory of Aero-engine Thermal Environment and StructureMinistry of Industry and Information TechnologyNanjing 210016China State Key Laboratory of Mechanics and Control Mechanical Structures Nanjing University of Aeronautics and AstronauticsNanjing 210016China

This paper studies on a division method of the whole aeroengine loading spectrum flight mission segment and rotor speed mission segment,which is based on the actual flight actions and related to the flight operations of aeroengine and is suitable for the variable-speed aeroengines such as turbojet and *** the research,the aeroengine loading spectrum operation-related mission segments can be divided,which can provide important data basis for the life research on the structures which are sensitive to flight maneuver(such as the main shaft,large gearbox and installation section),lay a foundation for the simulation,compilation and prediction of the whole aeroengine loading ***,based on the summary of basic flight actions in actual flight,the division of flight mission segment was realized by ***,the aeroengine rotor speed mission segments,associated with flight actions and missions,were divided based on the flight mission segment division ***,the efficiency and accuracy of the mission segment division results were verified by adopting measured loading spectrum ***,the characteristics of speed mission segment division results were compared and analyzed in tables and *** comparison results show that the characteristics of similar speed mission segments are similar,while the characteristics of different speed mission segments are *** the shapes of similar mission segments vary to the change of flight actions and operations,which can reflect the operation-related feature of the segments.

关键词： Aircraft engine Flight mission segment Mission segment division Rotor speed mission segment Spectrum analysis

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Synthesis,Crystal Structure,Fungicidal Activities and Molecular Docking of Acyl Urea Derivatives Containing 2-Chloronicotine Motif

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Chinese Journal of Structural Chemistry 2022年第2期41卷 114-122,I0010页

作者： SUN Guo-Xiang WANG Qiao MIN Li-Jing HAN Liang LIU Xing-Hai School of Chemistry and Chemical Engineering Yancheng Institute of TechnologyJiangsu 224051China College of Chemical Engineering Zhejiang University of TechnologyHuzhou 313000China College of Life Science Key Laboratory of Vector Biology and Pathogen Control of Zhejiang ProvinceHuzhou UniversityHangzhou 310014China

Eighteen new acyl urea derivatives containing 2-chloronicotine moiety were synthesized using2-chloronicotinic acid as starting material via 4 steps *** 2-chloronicotine acyl urea structures were confirmed by ^(1)H NMR,^(13)C NMR and *** 4r was further confirmed by X-ray *** crystallizes in the orthorhombic system,space group Pbca with a=7.2960(3),b=14.8546(6),c=25.2840(11)?,V=2740.3(2)?^(3),Z=8,the final R=0.0442 and w R=0.1033 for 4028 observed reflections with I>2σ(I).The antifungal activity results demonstrate that some of these compounds possessed good activity against ***,***,***,and *** at 50 *** molecular docking results indicated that the key group is urea bridge and pyridine ring.

关键词： acyl urea compounds crystal structure synthesis antifungal activity docking

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Enhancing lithium-ion and electric conductive Li_(2)FeSiO_(4)cathode through in situ boron-doping and carbon-coating strategy

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Rare Metals 2022年第12期41卷 4055-4064页

作者： Hao-Xiang Li Jia-Hui Zhu Xiao-Bing Huang Tao Zhou Yu-Rong Ren Hunan Provincial Key Laboratory of Chemical Power Sources College of Chemistry and Chemical EngineeringCentral South UniversityChangsha 410083China Hunan Provincial Key Laboratory of Water Treatment Functional Materials Hunan Provincial Key Laboratory for Control Technology of Distributed Electric Propulsion AircraftCollege of Chemistry and Materials EngineeringHunan University of Arts and ScienceChangde 415000China Jiangsu Province Engineering Research Center of Intelligent Manufacturing Technology for the New Energy Vehicle Power Battery Changzhou Key Laboratory of Intelligent Manufacturing and Advanced Technology for Power BatterySchool of Materials Science and EngineeringChangzhou UniversityChangzhou 213164China

The extremely low electrical conductivity and ion-diffusion coefficient of Li_(2)FeSiO_(4)limits its application as a cathode material in lithium-ion ***,in situ boron-doped Li_(2)FeSi_(1)-xB_(x)O_(4-δ)/C(x=0,0.01,0.03,0.05 and 0.07)at the Si site was prepared via the solid-state reaction method using pitch as the c arbon source.B doping in the lattice structure and a c arbon coating on the surface of the composites could effectively enhance the Li^(+)/electron ***,the reduced particle size of the active material with the relatively high specific area via borondoped modification could improve the wettability between the electrolyte and *** the synergistic effect of appropriate boron doping and carbon coating,it exhibits a good rate performance,specific capacity,and cycling *** a result,the as-prepared Li_(2)FeSi_(0.95)B_(0.05)O_(4-δ)/C cathode showed a high discharge capacity of 160.7mAh·g^(-1)at 0.2C,and the capacity retention rate was 96%after 100 cycles at *** work presents an effective path for designing advanced cathode materials for lithium-ion batteries.

关键词： Li_(2)FeSiO_(4) Carbon coating Boron doping Synergistic effect Lithium-ion battery

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