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Phase transition of multi-component(TiZrVNb)C ceramics—Part I:Phase decomposition induced by carbon content

Journal of advanced Ceramics 2024年第5期13卷 679-688页

作者： Qingyi Kong Rao Zhang Lei Chen Sijia Huo Wenyu Lu Yujin Wang Boxin Wei Yu Zhou Institute for Advanced Ceramics School of Materials Science and EngineeringHarbin Institute of TechnologyHarbin 150080China Key Laboratory of Advanced Structure‒Function Integrated Materials and Green Manufacturing Technology Harbin Institute of TechnologyHarbin 150001China School of Materials Science and Chemical Engineering Harbin University of Science and TechnologyHarbin 150001China National Key Laboratory of Precision Hot Processing of Metals Harbin Institute of TechnologyHarbin 150001China

Phase decomposition can effectively enhance the mechanical properties of carbide ceramics and can overcome the difficulty of enhancing the mechanical properties of single-phase multicomponent carbide *** this work,a series of nonstoichiometric(TiZrVNb)Cx ceramics were prepared by spark plasma sintering(SPS)at different *** effects of the carbon content on the phase composition,microstructure evolution,and mechanical properties were investigated in *** decomposition occurred with decreasing carbon *** different solid solutions of(Ti,V)-rich and Zr-rich phases formed from the decomposition of equimolar single-phase solid solutions,namely,the Zr-poor phase and Zr-rich phase,*** distribution of Nb element is relatively *** semicoherent interfaces between the Zr-poor phase and the Zr-rich phase can harden and strengthen effectively under the synergistic effect of grain *** with phase decomposition structures have apparent advantages compared to single-phase high-entropy *** work provides an important train of thought for the microstructure tailoring and properties optimization of multi-component carbide ceramics.

关键词： multicomponent ceramics nontoichiometry microstructure evolution phase decomposition mechanical properties

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The precipitation behaviours and strengthening mechanism of a Cu-0.4 wt% Sc alloy

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Journal of materials Science & technology 2022年第3期98卷 1-13页

作者： Zifan Hao Guoliang Xie Xinhua Liu Qing Tan Rui Wang State Key Laboratory for Advanced Metals and Materials University of Science and Technology BeijingBeijing100083China Key Laboratory for Advanced Materials Processing of Ministry of Education Institute of Advanced Materials and TechnologyUniversity of Science and Technology BeijingBeijing100083China Beijing Laboratory of Metallic Materials and Processing for Modern Transportation University of Science and Technology BeijingBeijing100083China

The precipitation behaviours during the aging process and the corresponding strengthening mechanism of a Cu-0.4 wt%Sc alloy were systematically investigated in this *** phase transformation sequence of the precipitation in the aging process of the Cu-0.4 wt%Sc alloy was found to be:supersaturated solid solution→Sc-enriched atomic clusters→metastable phase→Cu4Sc *** tetragonal structured lamellar Cu4Sc precipitates,with a habit plane parallel to the{111}plane of the Cu matrix and orientation relationships of(022)_(α)//(211)_(Cu4Sc)and[011]_(α)//[113]_(Cu4Sc),are found homogeneously distributed in the matrix.A combined process of cryogenic rolling(CR)and aging was designed for optimization of the mechanical and electrical *** integration of yield strength(696 MPa)and electrical conductivity(62.8%IACS)of this alloy was achieved by cryogenic rolling and subsequent aging process at 400℃for 4 *** significant precipitation strengthening effect of this alloy is attributed to the Cu4Sc precipitates with an extremely small size of only 1.5–3 *** leading strengthening mechanism is considered as the superposition of both coherent strengthening and Orowan strengthening effects.

关键词： Cu-Sc alloy Precipitation Aging process Strengthening mechanism

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Electronic structure and carrier mobility of BSb nanotubes

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Chinese Physics B 2025年第3期34卷 183-188页

作者： Lantian Xue Chennan Song Miaomiao Jian Qiang Xu Yuhao Fu Pengyue Gao Yu Xie State Key Laboratory of High Pressure and Superhard Materials College of PhysicsJilin UniversityChangchun 130012China Key Laboratory of Material Simulation Methods&Software of Ministry of Education College of PhysicsJilin UniversityChangchun 130012China Key Laboratory of Physics and Technology for Advanced Batteries of Ministry of Education College of PhysicsJilin UniversityChangchun 130012China

High-mobility semiconductor nanotubes have demonstrated great potential for applications in high-speed transistors,single-charge detection,and memory *** we systematically investigated the electronic properties of single-walled boron antimonide(BSb)nanotubes using first-principles *** observed that rolling the hexagonal boron antimonide monolayer into armchair(ANT)and zigzag(ZNT)nanotubes induces compression and wrinkling effects,significantly modifying the band structures and carrier mobilities through band folding andπ^(*)-σ^(*)*** the chiral index increases,the band gap and carrier mobility of ANTs decrease monotonically,where electron mobility consistently exceeds hole *** contrast,ZNTs exhibit a more complex trend:the band gap first increases and then decreases,and the carrier mobility displays oscillatory *** particular,both ANTs and ZNTs could exhibit significantly higher carrier mobilities compared to hexagonal monolayer and zinc-blende BSb,reaching 10^(-3)-10^(-7) cm^(-2)·V^(-1)·s^(-1).Our findings highlight strong curvature-induced modifications in the electronic properties of single-walled BSb nanotubes,demonstrating the latter as a promising candidate for high-performance electronic devices.

关键词： ab initio calculations nanotubes electronic structure carrier mobility

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Unveiling the surface-interface properties of perovskite crystals and pivotal regulation strategies

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Nano Research 2024年第5期17卷 3950-3981页

作者： Qin Li Ziyu Wang Junjie Ma Mengqi Han Peng Gao Meng Cai Yiqiang Zhang Yanlin Song Shou Peng Henan Institute of Advanced Technology College of ChemistryZhengzhou UniversityZhengzhou 450001China Key Laboratory of Green Printing Institute of ChemistryChinese Academy of Sciences(ICCAS)Beijing 100190China China National Building Material Group Co. Ltd.Beijing 100036China State Key Laboratory of Advanced Technology for Float Glass Beijing 100036China

Metal-halide perovskite solar cells have garnered significant research attention in the last decade due to their exceptional photovoltaic performance and potential for *** achieving remarkable power conversion efficiency of up to 26.1%,a substantial discrepancy persists when compared to the theoretical Shockley-Queisser(SQ)*** of the most serious challenges facing perovskite solar cells is the energy loss incurred during photovoltaic conversion,which affects the SQ limits and stability of the *** significant than the energy loss occurring in the bulk phase of the perovskite is the energy loss occurring at the ***,we provide a systematic overview of the physical and chemical properties of the ***,we delve into the underlying mechanism causing the energy deficit and structural degradation at the surface-interface,aiming to enhance the understanding of carrier transport processes and structural chemical ***,we systematically summarized the primary modulating pathways,including surface reconstruction,dimensional construction,and electric-field ***,we propose directions for future research to advance the efficiency of perovskite solar cells towards the radiative limit and their widespread commercial application.

关键词： perovskite solar cells surface-interface treatment defect modification dimensional design energy regulation heterojunction and homojunction

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Self-sensing tribological coating with phosphor particles for wear indicator

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Rare Metals 2023年第7期42卷 2462-2469页

作者： Ling He Xue-Yan Wu Wen-Sheng Li Mi-Na Zhang Shu-Jie Liu State Key Laboratory of Advanced Processing and Recycling of Nonferrous Metals Lanzhou University of TechnologyLanzhou730050China School of Materials Science and Engineering Lanzhou University of TechnologyLanzhou730050China

Monitoring of coating health was achieved by embedding sensor materials(MAl_(2)O_(4):Eu^(2+),Dy^(3+),M=Sr,Ba)in tribological *** the luminescence disappears under ultraviolet(UV)light,it means that the functional coating is worn out and that recoating is *** this work,four types of alloy(Cu-14Al-X,Cu,Cu-Al,Al)composite coatings were investigated by vacuum pres sure-as sis ted sintering *** composite coatings with different copper-aluminium alloy matrixes were compared by phase composition,microstructure,luminescence properties and tribological *** results indicate that the Cu-14Al-X matrix composite coating shows not only good resistance to wear but also exhibits strong green light emitting under ultraviolet(UV)*** is the best wear-resistant self-sensitive coating which has potential industrial *** the coating wore or broke,the emitting intensity will decrease or disappear.

关键词： Copper-aluminium alloy coatings Luminescent powders Wear indicator Luminescent spectroscopy Tribology

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Microstructure and Mechanical Properties of Extruded Mg-Y-Zn-Ni-Co Alloy 75

Microstructure and Mechanical Properties of Extruded Mg-Y-Zn...

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75th World Foundry Congress, WFC 2024

作者： An, Binxin Jiang, Jing Xu, Haobin Li, Yuandong Chen, Tijun Bi, Guangli Key Laboratory of Advanced Processing and Recycling of Nonferrous Metals Lanzhou University of Technology Lanzhou730050 China School of Material Science and Engineering Lanzhou University of Technology Lanzhou730050 China

Microstructure and mechanical properties of Mg-2Y-0.5Zn-0.5Ni-0.5Co (MYZNC, at.%) alloy were investigated in the as-cast, homogeneous and extruded states. The as-cast MYZNC alloy mainly consisted of α-Mg matrix, gray lamellar 18R LPSO phase, and white irregular Mg2Y, MgY(Co,Zn,Ni)4, and granular Mg3(Co,Zn,Ni,Y) phases. After homogenization treatment, a large number of strip-like 14H LPSO phases precipitated in the grain interior. After hot extrusion, the alloy occured obvious dynamic recrystallization with a significant grain refinement from 46.5 μm in the homogenized state to 2.98 μm in the extruded state, while the second phases were fragmented and distributed along the extrusion direction. The tensile testing results indicated that the extruded MYZNC alloy exhibited the good tensile strengths as compared with the as-cast and homogenized alloys, whose ultimate tensile strength (σb), yield strength (σ0.2) and elongation to failure (Εf) of were 280 MPa, 225 MPa and 11.7%, respectively. The high tensile properties of the extruded alloy were mainly attributed to the grain refinement and the second-phase strengthening by the high volume fraction of LPSO phase. In addition, the homogenized appeared a more pronounced strain hardening behavior, attributed to its large grain size and higher dislocation density arised from the presence of numerous fine particles and LPSO phases. © 2024 75th World Foundry Congress, WFC 2024. All rights reserved.

关键词： Tensile strength

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Loosely coordinating diluted highly concentrated electrolyte toward -60℃ Li metal batteries

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Journal of Energy Chemistry 2024年第3期90卷 380-387,I0009页

作者： Han Zhang Ziqi Zeng Qiang Wu Xinlan Wang Mingsheng Qin Sheng Lei Shijie Cheng Jia Xie State Key Laboratory of Advanced Electromagnetic Technology School of Electrical and Electronic EngineeringHuazhong University of Science and TechnologyWuhan 430074HubeiChina State Key Laboratory of Materials Processing and Die&Mould Technology School of Materials Science and EngineeringHuazhong University of Science and TechnologyWuhan 430074HubeiChina

Lithium metal batteries(LMBs) promise energy density over 400 Wh kg^(-1).However,they suffer severe electrochemical performance deterioration at sub-zero *** failure behavior highly correlates to inferior lithium metal anode(LMA) compatibility and sluggish Li^(+) ***,we demonstrate that cyclopentylmethyl ether(CPME) based diluted high-concentration electrolyte(DHCE)enables-60℃ LMBs *** leveraging the loose coordination between Li^(+) and CPME,such developed electrolyte boosts the formation of ion clusters to derive anion-dominant interfacial chemistry for enhancing LMA compatibility and greatly accelerates Li^(+) desolvation *** resulting electrolyte demonstrates high Coulombic efficiencies(CE),providing over 99.5%,99.1%,98.5% and 95% at 25,-20,-40,and-60℃*** assembled Li-S battery exhibits remarkable cyclic stability in-20,and-40℃ at 0.2 C charging and 0.5 C *** at-60℃,Li-S cell with this designed electrolyte retains> 70% of the initial capacity over 170 ***,lithium metal coin cell and pouch cell with10 mg cm^(-2) high S cathode loading exhibit cycling stability at-20℃.This work offers an opportunity for rational designing electrolytes toward low temperature LMBs.

关键词： Lithium metal batteries -60℃operation Lithium metal anode compatibility Li^(+) desolvation kinetics

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Enhanced strength of a high-conductivity Cu-Cr alloy by Sc addition

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Rare Metals 2024年第11期43卷 6054-6067页

作者： Tao Huang Chao-Min Zhang Ying-Xuan Ma Shu-Guo Jia Ke-Xing Song Yan-Jun Zhou Xiu-Hua Guo Zhen-Peng Xiao Hui-Wen Guo School of Materials Science and Engineering Henan University of Science and TechnologyLuoyang 471023China Henan Key Laboratory of Non-Ferrous Materials Science and Processing Technology Luoyang 471023China Henan Academy of Sciences Zhengzhou 450046China Henan Key Laboratory of Advanced Conductor Materials Zhengzhou 450046China Chinaclo Luoyang Copper Processing Co.Ltd. Luoyang 471023China

A new Cu-Cr-Sc alloy was designed,prepared and subjected to deformation heat *** electron microscopy(TEM),electron backscatter diffraction(EBSD)and X-ray diffraction(XRD)were employed to investigate the effects of Sc on the microstructural changes in the Cu-Cr alloy in different states,examine the changes in the precipitates during aging,reveal the intrinsic correlation between the structure and property in the peak aging state,and evaluate the Sc distribution in the Cu-Cr *** addition of Sc significantly increased the yield strength of the Cu-Cr alloy by~24.6%after aging at 480℃for 1 h,while it had a high electrical conductivity of81.5%international annealed copper standard(IACS).This enhancement was attributed to the effective inhibition of Cr phase coarsening and recrystallization through the addition of Sc,which strengthened the ***,in the Cu-Cr-Sc alloy,most of the Sc atoms precipitated as the Cu_(4)Sc phase,with a small amount of Sc segregating at the grain boundaries to pin *** grain boundary pinning helped to inhibit grain growth and further improve the *** main strengthening mechanisms identified in Cu-Cr-Sc alloys were dislocation strengthening and precipitation strengthening.

关键词： Cu-Cr-Sc alloy High strength and high conductivity Precipitation strengthening Cr precipitates

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NiSe nanoparticles anchored on hollow carbon nanofibers with enhanced rate capability and prolonged cycling durability for sodium-ion batteries

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Rare Metals 2025年第1期44卷 185-194页

作者： Li-Jun Xu Xue-Jie Wang Guo-Yu Tang Bi-Cheng Zhu Jia-Guo Yu Liu-Yang Zhang Tao Liu Faculty of Materials Science and Chemistry China University of GeosciencesWuhan 430078China School of Chemistry and Physics Queensland University of TechnologyBrisbaneQLD 4000Australia State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of TechnologyWuhan 430070China

Nickel selenides have been studied as potential anode materials for sodium-ion batteries due to their high theoretical ***,the low electrical conductivity and the large volumetric variation during the charging/discharging process greatly reduce the specific capacity and cycling lifespan of the *** this paper,a simple strategy to fabricate NiSe nanoparticles enclosed in carbon hollow nanofibers(NiSe/C@CNF)is proposed,involving the preparation of Ni-precursor nanofibers by electrospinning,the coating of polydopamine and the formation of NiSe/C@CNF by calcination and *** combination of NiSe nanoparticles and porous carbon hollow nanofibers creates a strong conductive environment,which enhances the dynamic ability of sodium-ion transport and improves charge storage *** fabricated NiSe/C@CNF material exhibits excellent *** demonstrates a high rate capability,with specific capacities of 406.8 and 300.1 mAh·g^(-1)at 0.1 and 5.0 A·g^(-1),*** results highlight the potential of NiSe/C@CNF as an anode material for sodium-ion batteries,offering a large capacity and long life.

关键词： Nickel selenide Hollow porous structure Sodium storage Anode material

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Titanium nitrides as novel reactants for in-situ synthesis of TiB_(2)-based composites with improved properties

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Journal of materials Science & technology 2023年第14期145卷 48-55页

作者： Ji Zou Huayue Liang Jingjing Liu Weimin Wang Fan Zhang Wei Ji Zhengyi Fu State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of TechnologyWuhan 430070China Hubei Longzhong Laboratory Xiangyang 441000China School of Materials Science and Engineering Wuhan University of TechnologyWuhan 430070China

A novel in-situ reactive approach based on the reactions among TiN,aluminum and boron has been developed to synthesize TiB_(2)-based composites including TiB_(2)-h BN(TB)and TiB_(2)-h BN-AlN(TBA).Fully dense ceramics with fine-grained microstructure were successfully obtained via spark plasma sintering at 1850℃/60 MPa/5 *** analysis suggests h BN flakes were homogenously distributed in the TiB_(2)*** AlN,however,they were elongated into plate-like grains during sintering,in which lots of defects in terms of stacking faults and twinning structures were *** mechanical and thermophysical properties of as-sintered ceramics were comprehensively investigated and ***-corporating AlN significantly improved the flexure strength,hardness,fracture toughness and thermal conductivity of TiB_(2)-h BN *** electrical conductivity of TB(3.06×10^(6)S/m)is larger than that of TBA(2.35×10^(6)S/m)at room temperature,but the value(6×10^(5)S/m)was lower than that of TBA(6.9×10^(5)S/m)at 1173 *** on the measurement of electrical and thermal conductivity,electron and phonon contributions to thermal conductivities of TB and TBA were calculated and their temperature dependences were illustrated.

关键词： Borides Microstructure Spark plasma sintering Mechanical property Thermo-physics property

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