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Numerical study of growth competition between twin grains during directional solidification by using multi-phase field method

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Chinese Physics B 2022年第2期31卷 626-633页

作者： Chang-Sheng Zhu Ting Wang Li Feng Peng Lei Fang-Lan Ma School of Computer and Communication Lanzhou University of TechnologyLanzhou 730050China State Key Laboratory of Gansu Advanced Processing and Recycling of Non-Ferrous Metal Lanzhou University of TechnologyLanzhou 730050China

A multi-phase field model is established to simulate the growth competition and evolution behavior between seaweed and columnar dendrites during directional *** to the effects of surface tension and interfacial energy,we quantitatively analyze the influences of factors such as inclination angles,pulling velocity,and anisotropic strength on twin *** results demonstrate that the pulling velocity and anisotropic strength have an important influence on the morphology and evolution of the seaweed and dendritic *** low pulling velocity and anisotropic strength are both key parameters for maintaining the stable morphology of seaweed during competitive growth in a bicrystal,showing that the lateral branching behavior is the root of the dendrites that can ultimately dominate the *** it is clarified that the lateral branching behavior and lateral blocking are the root causes of the final dominant growth of *** the increase of anisotropy strength,the seaweed is eliminated fastest in case 1,the seaweed is transformed into degenerate dendritic morphology,and eliminates the seaweed by promoting the generation and lateral growth of the lateral branches of the *** increase of pulling velocity is to increase the undercooling of favorable oriented grain and accelerate the growth rate of dendrites,thus producing more new primary dendrites for lateral expansion and accelerating the elimination rate of unfavorable oriented grain.

关键词： multi-phase field simulation grain growth competition directional solidification twin grains

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Multiple Responsive Photonic Prints Through Localized Interpenetrating Polymer Network

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Chemical Research in Chinese Universities 2023年第5期39卷 803-808页

作者： ZHANG Tian JIA Xiaolu HOU Zaiyan XIE Ge ZHANG Lianbin ZHU Jintao Key Laboratory of Material Chemistry for Energy Conversion and Storage of Ministry of Education State Key Laboratory of Materials Processing and Mold TechnologySchool of Chemistry and Chemical EngineeringHuazhong University of Science and TechnologyWuhan 430074P.R.China School of Chemistry&Chemical Engineering Zhoukou Normal UniversityZhoukou 466001P.R.China

Multiple responsive photonic prints that can be revealed by a thermal or light stimulus are prepared by locally producing interpenetrating polymer network(IPN)within photonic ***-responsive poly-(N-isopropylacrylamide)(PNIPAM)photonic hydrogels with self-assembled monodisperse carbon-encapsulated Fe_(3)O_(4) nanoparticles(Fe_(3)O_(4)@C NPs)are first prepared by a photopolymerization *** photopolymerization of acrylamide(AM)is carried out within the photonic hydrogel with the help of a mask to generate an IPN structure *** of the regionally different network structure and the resulting varied responsiveness,responsive photonic prints are *** to the thermo-responsive capability of the PNIPAM and the photothermal conversion capability of the incorporated Fe_(3)O_(4)@C NPs,the as-prepared photonic prints with a localized IPN structure can shift the structural color in a broad spectrum range under thermal or light *** current multiple responsive photonic prints with a localized IPN structure can realize full-color pattern display under thermal and light stimulations,providing a new path for anti-counterfeiting,display,and information encoding.

关键词： Photonic crystal Photothermal Hydrogel Patterning Stimuli-responsive

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Highly efficient synthesis of boron nitride nanotubes by catalytic chemical vapor deposition of boron/nickel containing precursors

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Journal of Materiomics 2022年第6期8卷 1199-1204页

作者： Heng Wang Haoran Yang Yongzhi Peng Yulin Zheng Dongying Huang Pu Hu Yawei Li Zhengyi Fu Hubei Key Laboratory of Plasma Chemistry and Advanced Materials Key Laboratory of Green Chemical Engineering Process of Ministry of EducationWuhan Institute of TechnologyWuhan430205China State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of TechnologyWuhan430070China The State Key Laboratory of Refractories and Metallurgy Wuhan University of Science and TechnologyWuhan430081China

High-purity and high-yield boron nitride nanotubes with large aspect ratio were prepared by a facile two-step process,including the synthesis of boron/nickel containing precursors by precipitation reactions and subsequent thermally catalytic chemical vapor deposition *** influence of catalyst content and annealing temperature on the phase composition and microstructure of the products were *** results show that it is difficult to exert the catalytic effect of nickel-based catalyst at low temperatures(<1400℃).At appropriate temperatures(1400-1500℃),highly crystalline boron nitride nanotubes with a length of more than 50 mm and a diameter of 50 nm are *** content of catalyst in the precursor mainly affects the morphology of the boron nitride *** the content is too low,it is easy to form boron nitride particles;while high catalyst content can easily lead to catalyst aggregation and form a submicron one-dimensional boron nitride with unregular *** on microstructural evolutions,phase changes,and thermodynamic analysis,the vapor-liquid-solid(V-L-S)growth mechanism of the tip growth mode dominates the formation of boron nitride nanotubes has also been verified.

关键词： Boron nitride nanotubes Highly efficient synthesis Boron/nickel containing precursors Growth mechanism

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Hollow Zn/Co zeolitic imidazolate framework-implanted composite hydrogel for highly efficient uranium extraction from seawater

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Nano Research 2023年第7期16卷 10451-10461页

作者： Yucheng Song Xin Ma Huanhuan Tan Zhong Liu Chuntai Liu Changyu Shen Peipei Yang Songwei Li National Engineering Research Center for Advanced Polymer Processing Technology Key Laboratory of Materials Processing and Mold(Ministry of Education)Zhengzhou UniversityZhengzhou 450002China Key Laboratory of Comprehensive and Highly Efficient Utilization of Salt Lake Resources Qinghai Provincial Key Laboratory of Resources and Chemistry of Salt LakesQinghai Institute of Salt LakesChinese Academy of SciencesXining 810008China Henan Tuoren Medical Device Co. Ltd.Weiyuan Industrial ParkChangyuan 453400China

Efficient capture of uranium(VI)(U(VI))from seawater is of great significance to the sustainable development of nuclear energy and environmental protection,which is also a serious challenge at *** this study,hollow Zn/Co zeolitic imidazolate framework(H-ZIF)was decorated on polyacrylamide/sodium alginate(PAM/SA)hydrogel by chelating and covalently crosslinking,and a new type of PAM/SA/H-ZIF hydrogel was *** combination of PAM/SA and H-ZIF gives PAM/SA/H-ZIF hydrogel excellent mechanical properties,good stability,and abundant surface functional groups,which is beneficial to improving the adsorption *** extraction amount of U(VI)by PAM/SA/H-ZIF is 171.14 mg·g^(-1)at C_(0)=99.52 mg·L^(-1)and pH=*** adsorption equilibrium is reached in 120 min and the adsorption process fits well with Langmuir isotherm model and pseudo-second-order rate *** PAM/SA/H-ZIF also showed good recyclability and stability after 10 cycles of *** importantly,the rate of uranium adsorption is 0.196 mg·g^(-1)·day^(-1)after 30 days,which implies that the PAM/SA/H-ZIF could serve as a potential adsorbent for the development of uranium capture from seawater.

关键词： hydrogel hollow metal-organic framework uranium capture seawater

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Effect of cross rolling on the microstructure and mechanical performance of a dual-phase structured Mg-8Li-6Zn-1Y(in wt.%)alloy

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Journal of materials Science & technology 2024年第9期176卷 132-144页

作者： Dongliang Wang Daokui Xu Baojie Wang Changjian Yan Shuo Wang Xiangbo Xu Lan Zhang Cuilan Lu Key Laboratory of Nuclear Materials and Safety Assessment Institute of Metal ResearchChinese Academy of SciencesShenyang 110016China School of Materials Science and Engineering University of Science and Technology of ChinaShenyang 110016China Binzhou Institute of Technology Binzhou 256606China Shandong Key Laboratory of Advanced Aluminium Materials and Technology Binzhou 256606China School of Environmental and Chemical Engineering Shenyang Ligong UniversityShenyang 110159China Institute of Corrosion Science and Technology Guangzhou 510070China Key Lab of Electromagnetic Processing of Materials Ministry of EducationNortheastern UniversityShenyang 110819China

The microstructure and mechanical performance of the unidirectionally and cross-directionally rolled Mg-8Li-6Zn-1Y(in wt.%)sheets have been investigated and *** reveals that after the unidirectional rolling(UR),the broken I-phase particles are aggregated at theα-Mg/β-Li phase ***,the cross-rolling(CR)process can not only severely break the bulk I-phase,but also cause the obviously uniform distribution of I-phase particles in the matrix ***,the average grain size of the CR samples is 3.61μm and about 50%that of the UR *** maximum texture intensities ofα-Mg andβ-Li phases in the CR samples are slightly stronger than those in the UR *** results demonstrate that the CR process can effectively enhance the tensile properties and remarkably reduce the mechanical anisotropy of the *** the UR samples,the yield strength,ultimate tensile strength,and elongation ratio along the rolling direction(RD)are 164 MPa,198 MPa,and 16.4%,whereas those along the transverse direction(TD)are 157 MPa,185 MPa,and 22.0%,*** the CR samples,their mechanical properties are basically the same and the mechanical anisotropy is almost *** yield strength,ultimate tensile strength,and elongation ratio along the cross-rolling direction 1(CRD1)and 2(CRD2)are respectively measured to be 181 MPa and 182 MPa,220 MPa and 218 MPa,20.6%and 20.7%.Failure analysis indicates that for the UR samples being tensile tested along the RD and TD,microcracks are preferentially initiated in the region of aggregated I-phase *** the CR samples being tensile tested along both two cross-rolling directions,the initiation of micro-cracks mainly occurs at the I-phase/matrix phase interfaces and in the interior of matrix phases.

关键词： Magnesium-lithium alloy Cross-rolling I-phase Microstructure Mechanical performance

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Pushing the high-k scalability limit with a superparaelectric gate layer

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Journal of advanced Ceramics 2024年第4期13卷 539-547页

作者： Kun Wang Chao Liu Yuan Zhang Fuyu Lv Jun Ouyang Houbing Huang Rui-Long Yang Yu-Yao Zhao Hongbo Cheng Hanfei Zhu Xiaoming Shi Yun Tian Institute of Advanced Energy Materials and Chemistry Jinan Engineering Laboratory for Multi-scale Functional MaterialsSchool of Chemistry and Chemical EngineeringQilu University of Technology(Shandong Academy of Sciences)Jinan 250353China Key Laboratory for Liquid-Solid Structure Evolution and Processing of Materials(Ministry of Education) School of Materials Science and EngineeringShandong UniversityJinan 250061China China Tobacco Shandong Industrial Co. Ltd.Jinan 250104China Department of Materials Science and Engineering Southern University of Science and TechnologyShenzhen 518055China Key Laboratory of Key Film Materials&Application for Equipments(Hunan Province) School of Material Sciences and EngineeringXiangtan UniversityXiangtan 411105China Advanced Research Institute of Multidisciplinary Science and School of Materials Science and EngineeringBeijing Institute of TechnologyBeijing 100081China Key Laboratory of Magnetic Molecules and Magnetic Information Materials of Ministry of Education School of Chemistry and Materials ScienceShanxi Normal UniversityTaiyuan 030032China

To meet the expectation set by Moore’s law on transistors,the search for thickness-scalable high dielectric constant(k)gate layers has become an emergent research *** investigations have failed to solve the“polarizability–scalability–insulation robustness”*** this work,we show that this trilemma can be solved by using a gate layer of a high k ferroelectric oxide in its superparaelectric(SPE)*** the SPE,its polar order becomes local and is dispersed in an amorphous matrix with a crystalline size down to a few nanometers,leading to an excellent dimensional scalability and a good field-stability of the k *** an example,a stable high k value(37±3)is shown in ultrathin SPE films of(Ba_(0.95),Sr_(0.05))(Zr_(0.2),Ti_(0.8))O_(3)deposited on LaNiO_(3)-buffered Pt/Ti/SiO_(2)/(100)Si down to a 4 nm thickness,leading to a small equivalent oxide thickness of~0.46 *** aforementioned characteristic microstructure endows the SPE film a high breakdown strength(~10.5 MV·cm^(−1)for the 4 nm film),and hence ensures a low leakage current for the operation of the complementary metal oxide semiconductor(CMOS)***,a high electrical fatigue resistance is displayed by the SPE *** results reveal a great potential of superparaelectric materials as gate dielectrics in the next-generation microelectronics.

关键词： high-k transistors Moore's law superparaelectric insulation robustness

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3D multiphysic simulations of energy field and material process in radial ultrasonic rolling electrochemical micromachining

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Chinese Journal of Aeronautics 2022年第3期35卷 494-508页

作者： Minghuan WANG Yongchao SHANG Changshun LIU Jiajie WANG Jinsong ZHENG Xufeng XU College of Mechanical Engineering Zhejiang University of TechnologyHangzhou 310023ZhejiangChina Key Laboratory of Special Purpose Equipment and Advanced Processing Technology of Ministry of Education Zhejiang University of TechnologyHangzhou 310023ZhejiangChina

The radial ultrasonic rolling electrochemical micromachining(RUR-EMM)combined rolling electrochemical micromachining(R-EMM)and ultrasonic vibration was studied in this *** fundamental understanding of the machining process especially the interaction between multiphysics in the interelectrode gap(IEG)was investigated and discussed by the finite element *** multiphysics coupling model including flow field model,Joule heating model,material dissolution model and vibration model was built.3D multiphysics simulation based on micro dimples process in RUR-EMM and R-EMM was *** results showed that the electrolyte flowed into and out IEG periodically,gas bubbles were easy to squeeze out and the gas void fraction deceased about 16%to 54%,the maximum current density increased by 1.36 times in RUR-EMM than in R-EMM in one vibration period of *** application of the ultrasonic vibration increased the electrolyte temperature about 1.3–4.4%in *** experiments of the micro dimple process denoted better corrosion consistency of array dimples in RUR-EMM,there was no island at the micro dimple bottom which always formed in R-EMM,and an aggregated deviation of less than 8.7%for the micro dimple depth and 4%for the material removal amount between theory and experiment was obtained.

关键词： 3D Multiphysics simulation Electrochemical micromachining Energy field material process Micro dimple Ultrasonic vibration

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Crystalline@amorphous core-shell structure of WO3@WO_(3-x)S_(x) established via doping strategy for enhancing magnesium ions storage performance

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Journal of Magnesium and Alloys 2025年第3期13卷 1353-1363页

作者： Shiqi Ding Yuxin Tian Jiankang Chen Guofeng Wang Bing Sun He Lv Lei Wang Guicun Li Alan Meng Zhenjiang Li College of Materials Science and Engineering Key Laboratory of Optic-electric Sensing and Analytical Chemistry for Life ScienceMOEShandong Key Laboratory of Biochemical AnalysisCollege of Chemistry and Molecular EngineeringQingdao University of Science and TechnologyQingdao 266042ShandongPR China Qingdao Engineering Research Center for New Metallic Functional Materials Characteristic Laboratory of Advanced Metal Functional Materials and Processing in Universities of ShandongQingdao Binhai UniversityQingdao 266555ShandongPR China

Designing cathode possessing crystalline@amorphous core-shell structure with both active core and shell is a meaningful work for resolving the low speciﬁc capacity,unstable cycling performance and sluggish reaction kinetics issues of rechargeable magnesium batteries(RMBs)by providing more active sites as well as releasing inner stress during ***,WO_(3)@WO_(3-x)S_(x) owning crystalline@amorphous core-shell structure containing both active core and active shell is constructed successfully by introducing S into metastable WO3 structure under temperatureﬁeld *** such structure,amorphous shell would provide continuous Mg^(2+)diffusion channels due to its isotropy property for most Mg^(2+)migrating rapidly to interface and then adsorb at ions reservoir formed by interfacial electricﬁeld for increasing speciﬁc *** also makes security for stable structure of WO_(3)@WO_(3-x)S_(x) by alleviating volume expansion of crystalline core WO_(3) during cycling to prolong cycling ***,“softer”ions S^(2-)would weaken interaction between hard acid Mg^(2+) and ionic lattice to enhance Mg^(2+)storage ***,WO_(3)@WO_(3-x)S_(x) delivers the superior cycling performance(1000 cycles with 83.3%),rate capability(88.5 mAh g^(-1) at 1000 mA g^(-1))and speciﬁc capacity(about 150 mAh g^(-1) at 50 mA g^(-1)),which is near 2 times higher than that of *** is believed that the crystalline@amorphous core-shell structure with both active core and shell designing via doping strategy is enlightening for the development of high-performance RMBs,and such design can be extended to other energy storage devices for better electrochemical performance.

关键词： Doping Sulfuration Crystalline@amorphous core-shell structure WO_(3) Rechargeable magnesium batteries

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An efficient method to engage oxide ceramics in low-temperature interfacial reactions: Microstructure evolution and kinetics behaviors based on supercooling in a transient liquid phase bonding joint

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Journal of materials Science & technology 2023年第20期151卷 234-244页

作者： Jia Yang Wanqi Zhao Panpan Lin Qiuguang Zhang Xinfei Zhang Tiesong Lin Peng He Yanli Zhuang State Key Laboratory of Advanced Welding and Joining Harbin Institute of TechnologyHarbin 150001China AECC Shenyang Liming Aero-Engine Co. LtdShenyang 110043China Heilongjiang Provincial Key Laboratory of CO_(2) Resource Utilization and Energy Catalytic Materials School of Material Science and Chemical EngineeringHarbin University of Science and TechnologyHarbin 150040China

Ductile transient liquid phase(TLP)bonding joints reinforced by multiple precipitates were produced using novel pre-sintered coatings and Au-Si fillers;therefore,the highest strength of NiTi/sapphire joints brazed at 460℃ for 30 min reached 72 *** pre-sintering process improved the surface-active of sapphire by forming metastable Ti_(3)O and non-stoichiometric Al_(2)O_(3).The typical brazing seam consisted of O-rich compounds,TiSi_(2),and Ti-Ni-Si,wherein the O-rich phase featured different crystallinity depending on the oxygen *** sapphire/seam interface was either a nanoscale diffusion region or a Si-rich amorphous *** breakdown of the Stokes-Einstein relation(SER)occurred,and the deviation from SER increased with a higher cooling *** influence of coating thickness was reflected in(i)the supercooling related to the viscosity and fractional exponent of liquids and(ii)the microstructural change of the joint related to the driving force for crystal *** work presented a new strategy for joining ceramics to metals at lower temperatures but using the joint at higher temperatures;furthermore,gave an insight into the microstructure evolution and kinetics behaviors based on supercooling in a transient liquid phase bonding joint.

关键词： Reinforced ductile fillers Transient liquid phase bonding Surface modification Kinetic behaviors

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High-rate sodium metal batteries enabled by trifluormethylfullerene additive

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Nano Research 2022年第8期15卷 7172-7179页

作者： Pengju Li Xiaobo Huang Zhipeng Jiang Han Zhang Pengwei Yu Xing Lu Jia Xie State Key Laboratory of Materials Processing and Die&Mould Technology School of Materials Science and EngineeringHuazhong University of Science and TechnologyWuhan 430074China State Key Laboratory of Advanced Electromagnetic Engineering and Technology School of Electrical and Electronic EngineeringHuazhong University of Science and TechnologyWuhan 430074China

Sodium metal is a promising anode for sodium batteries due to its high theoretical capacity and low ***,the serious Na dendrite growth and low Coulombic efficiency,especially at high current densities/cycling capacities,severely limit the application of sodium metal ***,trifluoromethylfullerene,C_(60)(CF_(3))_(6),is designed as an electrolyte additive to enable the high-rate cycling of sodium metal anodes with high Coulombic *** CF3 groups contribute to the formation of stable NaF-rich solid electrolyte interface layer,while C_(60)cages induce the uniform distribution of sodium ions and promote the formation of smooth and compact ***,Na||Cu cell with C_(60)(CF_(3))_(6)can be cycled at 2 mA·cm^(−2)and 10 mAh·cm^(−2)over 180 cycles with an average Coulombic efficiency of 99.9%,and Na||Na cell can be cycled at 10 mA·cm^(−2)over 600 ***,Na||NaV2(PO_(4))_(3)@C full cell exhibits high capacity retention of 84%over 2,000 cycles at 20 C(~3 mA·cm^(−2)).

关键词： sodium metal anode fullerene trifluormethylfullerene high rate electrolyte additive

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