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Enhanced and Tunable Visible-Light and Near-Infrared Transmittance of VO_(2)/ATO Composite Coatings for Smart Windows

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Journal of Wuhan University of technology(materials Science) 2025年第3期40卷 627-634页

作者： HAN Tao YAN Yuqing WANG Yanhang YANG Penghui LI Xianzi ZHANG Rui ZU Chengkui Building Material Industrial Key Laboratory for Special Glass Preparation and Processing China Building Materials AcademyBeijing 100024China School of Chemical Safety North China Institute of Science and TechnologySanhe 065201China

We synthesized tungsten-doped vanadium dioxide(W-VO_(2))particles via a one-step hydrothermal method,followed by their integration with antimony-doped tin oxide(ATO)nanoparticles to formulate a composite ***,the VO_(2)/ATO composite coating was fabricated through a spin-coating *** impact of varying W-VO_(2) content and coating thickness on the performance of the composite coatings was systematically investigated by employing X-ray diffraction,particle size distribution analysis,spectrometry,and other pertinent test *** findings revealed that an escalation in both W-VO_(2) content and coating thickness retained high transmittance in the near-infrared band at lower ***,as the temperature increased,a notable reduction in transmittance in the near-infrared band was observed,alongside a slight decrease in transmittance within the visible ***,when the W-VO_(2) content reached 5%and the coating thickness was 1253 nm,the transmittance of the composite coating surpassed 80%.Furthermore,the heat insulation effect achieved a remarkable 10.0℃***,the synthesized composite coating demonstrates significant potential for smart glass applications,particularly in the realm of heat-insulating glass.

关键词： VO_(2) ATO composite coating transmittance thermal insulation performance

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Study on Synergistic Extraction of Iron from Carbide Slag and Nickel Slag

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Journal of Sustainable Metallurgy 2025年 1-10页

作者： Yang, Lushun Li, Bin Du, Xueyan Han, Mengyao School of Materials Science and Engineering Lanzhou University of Technology Lanzhou730050 China State Key Laboratory of Advanced Processing and Recycling of Nonferrous Metals Lanzhou University of Technology Lanzhou730050 China

Iron recovery from nickel slag, a significant byproduct generated during nickel pyrometallurgical process, represents a pivotal aspect of advancing sustainable utilization of metallurgical solid waste. This study explores the potential of utilizing carbide slag as a fluxing modifier to enhance iron extraction from nickel slag through the melting oxidation process. Thermodynamic simulations were conducted with FactSage software to predict phase equilibria and reaction pathway, while experimental analyses were performed to investigate phase composition, microstructural morphologies, and iron recovery efficiencies. The results indicate that in the FeO–SiO2–CaO–MgO slag system, predominant magnetite emerges as the primary iron-bearing phase in the spinel region. Increasing the slag’s basicity shifts the corresponding phase area of spinel increases first and then decreases. Thermodynamic predictions and experimental data corroborate that the addition of carbide slag facilitates the transformation of the fayalite phase into magnetite and pyroxene phases. Optimal basicity levels enhance the precipitation and crystal growth of magnetite, as well as promote the separation of iron from the slag matrix. Specifically, at a basicity of 0.5, the oxidized samples displayed the highest magnetite precipitation, with a recovery rate of 93.2%. Detailed microstructural analysis revealed the formation of well-defined dendritic magnetite crystals. These findings suggest that the introduction of carbide slag not only optimizes the phase transformation processes but also significantly enhances iron recovery, offering a viable pathway for the synergistic reutilization of nickel and calcium carbide slags. © The Minerals, Metals & materials Society 2025.

关键词： Magnetite

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Anion-induced electrolyte chemistry enables high energy density primary battery for ultralow-temperature conditions

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Science China Chemistry 2025年第5期68卷 2051-2058页

作者： Zi-Hang Xue Hao-Jie Liang Yong-Li Heng Jia-Lin Yang Edison Huixiang Ang Hong-Yan Lü Hong Yu Dongmei Dai Dai-Huo Liu Chuan-Yu Zheng Wei Guo Xing-Long Wu Department of Chemistry Northeast Normal University MOE Key Laboratory for UV Light-Emitting Materials and Technology Northeast Normal University Natural Sciences and Science Education National Institute of EducationNanyang Technological University State Key Laboratory of Solidification Processing Center of Advanced Lubrication and Seal MaterialsNorthwestern Polytechnical University School of Chemistry and Chemical Engineering Henan Normal University Key Laboratory of Organo-Pharmaceutical Chemistry of Jiangxi Province Gannan Normal University

Lithium/fluorinated-carbon（Li/CFx） primary batteries are widely used in defense and military fields due to their stable discharge plateau,low self-discharge rate,and adaptability across a wide temperature ***,enhancing their overall energy density and discharge capacity at low temperatures remains a critical ***,we report a strategically designed LiBF4-based sulfite/carboxylate electrolyte,where the anion-involved solvation structure significantly enhances electrochemical kinetics by reducing the desolvation ***,it introduces a radical reaction mechanism that contributes to additional *** a result,the Li/CFxprimary batteries with this formulated electrolyte deliver a specific capacity of 2,257.15 mAh g-1at 25 ℃.More importantly,when operating at -40 ℃,the batteries exhibit an exceptionally high discharge capacity of 1,549.4 mAh g-1and an energy density of 2,868.6 Wh *** at -60 ℃,the Li/CFxcells achieve a specific capacity of 444.3 mAh g-1and an energy density of 821.8 Wh kg-1at 0.1 C,significantly outperforming previously reported organic-based liquid *** work offers a viable strategy for enhancing the specific capacity and energy density of primary batteries in extreme environments,providing valuable insights for future developments.

关键词： Li/CFx primary batteries radical reaction mechanism desolvation barrier low-temperature

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Ultrasensitive conductive hydrogels conferred by nanoscale synergistic effect

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Science China materials 2025年第1期68卷 226-235页

作者： Gangrong Wang Xin Jing Binghan Niu Liya Lin Yaoxun Zhang Jiazhou Zeng Peiyong Feng Yuejun Liu Hao-Yang Mi Key Laboratory of Advanced Packaging Materials and Technology of Hunan Province Hunan University of TechnologyZhuzhou 412007China National&Local Joint Engineering Research Center for Advanced Packaging Material and Technology Hunan University of TechnologyZhuzhou 412007China National Engineering Research Center for Advanced Polymer Processing Technology Zhengzhou UniversityZhengzhou 450000China

The inherent limitations of hydrogels,such as low electrical conductivity and inadequate sensitivity,present considerable challenges in flexible electronic *** address these issues,we proposed an innovative synthesis technique that synergistically leveraged the nanoscale properties of the conductive fillers including one-dimensional polyaniline and two-dimensional reduced graphene oxide to fabricate hydrogels with exceptional *** advanced hydrogel exhibited an extraordinary sensitivity with a gauge factor of 27.55,impressive electrical conductivity(7.2 mS/cm),and outstanding ***,the hydrogel demonstrated excellent self-adhesion and robust selfhealing properties,attributed to its abundant catechol functionalities,hydrogen bonding interactions,andπ-π***,the flexible,strain-sensitive,self-powered sensors derived from these hydrogels displayed unparalleled sensing performance,positioning them as highly promising candidates for advanced human-computer interaction systems and sophisticated information transmission applications.

关键词： conductive hydrogels sodium alginate polyaniline sensitivity reduced graphene oxide

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Recent advances in photopolymerization 3D printing of alumina-ceramic

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Progress in Natural Science:materials International 2025年第1期35卷 1-30页

作者： M.Irfan Hussain Min Xia XiaoNa Ren Zhen Shen Muhammad Jamil Changchun Ge Institute of Powder Metallurgy and Advanced Ceramics School of Material Science and Engineering University of Science and Technology Beijing State Key Laboratory of Multimodal Artificial Intelligence Systems Beijing Engineering Research Center of Intelligent Systems and Technology Institute of AutomationChinese Academy of Sciences College of Mechanical and Electrical Engineering Nanjing University of Aeronautics and Astronautics

Digital light processing(DLP) 3D printing has a huge potential for manufacturing intricate and customized ceramic parts with high precision and cost-effectiveness. Research in this field contributes to material innovation,opening the avenues for new process designs in both scientific and industrial sectors. However, the implementation of DLP 3D printing technology in ceramic research has not yet reached the maturity level as that in polymer and tissue engineering. Necessarily, a holistic in-depth literature reporting the successful integration of alumina ceramics within DLP 3D printing technology is urgently needed. This review, systematic examines recent progress in DLP technology, focusing on photopolymer resins that incorporate UV-sensitive monomers, photoinitiators, and dispersants, as well as their synergistic effects on achieving high-quality printing, desirable material properties, and enhanced performance. Further, the review discusses key factors including post-processing characteristics such as debinding and sintering, which influence microstructure, and defect formation including microcracks, porosity and voids. Finally, the challenges associated with printing and sintering are highlighted,aiming to identify focused focused development pathways and potential solution to optimize outcomes. This analysis clarifies existing challenges and also propsoes future applications for DLP technology in the aluminaceramic field.

关键词： Al2O3 ceramics Applications Digital light processing (DLP) Post-processing Resin

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Electrochemical dissolution, reduction, and nucleation mechanisms of molybdenum in NaCl-KCl molten salt systems

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Journal of materials Science and technology 2025年 238卷 45-54页

作者： Lv, Hongzhan Zhang, Liwen Xi, Xiaoli Nie, Zuoren Collaborative Innovation Center of Capital Resource-Recycling Material Technology Beijing University of Technology Beijing100124 China Key Laboratory of Advanced Functional Materials Ministry of Education Faculty of Materials and Manufacturing Beijing University of Technology Beijing100124 China National Engineering Laboratory for Industrial Big-data Application Technology Beijing University of Technology Beijing100124 China

This study investigates the anodic dissolution and electrochemical behavior of molybdenum in a NaCl-KCl molten salt system at 1023 K. The anodic dissolution process was systematically analyzed, revealing a sequential oxidation pathway of molybdenum into high-valence ions (Mo6+, Mo5+, Mo4+) under varying electrolysis potentials. Electrochemical Impedance Spectroscopy (EIS) demonstrated that the dissolution is governed by both charge transfer and diffusion mechanisms, with reduced impedance at higher potentials facilitating molybdenum dissolution. The reduction behavior of dissolved molybdenum ions was further explored using cyclic voltammetry (CV) and square wave voltammetry (SWV), confirming a multi-step reduction process controlled by diffusion and high reversibility. Nucleation studies using chronoamperometry established that molybdenum deposition follows an instantaneous nucleation mechanism. Morphological analysis of cathodic deposits revealed that current density significantly influences particle size, transitioning from nano-sized spherical particles to larger equiaxed crystals with increasing current density. These findings provide a comprehensive understanding of molybdenum's electrochemical properties in molten salts, offering valuable insights for optimizing electrolysis processes and advancing molybdenum-based material production. © 2025

关键词： Cyclic voltammetry

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Enhanced reactive oxygen species generation:Synergic process of three-electron oxygen reduction and electrochemical ozone production by bimetallic La-Nb oxides

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Journal of Energy Chemistry 2025年第5期104卷 155-165页

作者： Xiaoge Peng Xu Liu Xiaosa Wang Yuanan Li Suiqin Li Yuhang Wang Zhikang Bao Haoqiang Cao Yunyi Cao Xing Zhong Jianguo Wang Institute of Industrial Catalysis State Key Laboratory Breeding Base of Green-Chemical Synthesis TechnologyZhejiang University of TechnologyHangzhou 310032ZhejiangChina Innovation Research Center for Advanced Environmental Technology Eco-Industrial Innovation InstituteZJUTQuzhou 324400ZhejiangChina Advanced Technology Center Wuxi Little Swan Electric Co.LtdWuxi 214125JiangsuChina College of Chemical and Material Engineering Quzhou UniversityQuzhou 324000ZhejiangChina

The anodic electrochemical ozone production(EOP)and the cathodic three-electron oxygen reduction reaction(3e^(-)ORR)are effective processes for generating active oxygen species(ROS).However,the activation of ozone(O_(3))by hydroxyl radical(OH)to form ROS poses significant *** micelle balllike bimetallic La-Nb oxides(LNOx)have been developed as a bifunctional electrocatalyst for both the EOP and 3e^(-)ORR *** LNO20 demonstrated a 9.8%of Faradaic efficiency(FE)in O_(3)production and a transfer number of 2.8 electrons in the 3e^(-)*** calculations support the notion that the five-membered ring mechanism in LNO20 facilitates O_(3)***,the incorporation of La provides active sites that enhance the activation of hydrogen peroxide(^(*)H_(2)O_(2))and the generation of *** innovative approach synergistically integrates EOP and 3e^(-)ORR,enhancing the activation of O_(3)to produce ROS,demonstrating exceptional efficacy in the degradation of organic pollutants and antimicrobial *** study paves the way for designing advanced electrocatalysts for EOP and 3e^(-)ORR and offers insights into utilizing electrochemical method to support other antibacterial strategies.

关键词： Three electron oxygen reduction reaction Electrochemical ozone production Synergistic electrosynthesis Reactive oxygen species Antibacterial

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Improvement of Mechanical Properties and Wall Thickness Uniformity of Hollow Ceramic Spheres by Biaxial Rotation Slurry Injection technology

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Journal of Wuhan University of technology(materials Science) 2025年第3期40卷 619-626页

作者： WANG Qiuyang ZHOU Jian LIU Guizhen WANG Lin DING Zhongjun State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of TechnologyWuhan 430070China National Deep Sea Center Qingdao 266237China

Ceramic hollow spheres have great potential for deep-sea ***,the irregularity of the conventional molding process,among other reasons,results in low wall thickness uniformity of hollow *** solve this problem,in this work,we developed a biaxial rotation grouting process for deep-sea ceramic hollow buoyancy spheres,which improves the drawbacks of the traditional rotary grouting method that results in poor wall thickness uniformity of the hollow spheres due to its irregular rotational *** this paper,an experimental study was carried out to investigate the effects of different rotational methods,rotational speeds,rotational time,solid phase content,*** the wall thickness uniformity of ceramic hollow *** results show that the hollow floating balls prepared by the biaxial rotation method have the lowest wall thickness standard deviation(0.04)when the rotation speed is 60 rpm,the molding time is 8 min,and the solid phase content is 70 wt%.After the hydrostatic pressure test of 120 MPa,the hydrostatic compressive strength of hollow spheres prepared by the biaxial rotation method was increased by 31.67%compared with that of the traditional process.

关键词： ceramic hollow sphere biaxial rotation monolithic molding wall thickness uniformity

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Robust interface and excellent as-built mechanical properties of Ti–6Al–4V fabricated through laser-aided additive manufacturing with powder and wire

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International Journal of Minerals,Metallurgy and materials 2025年第1期32卷 154-168页

作者： Fei Weng Guijun Bi Youxiang Chew Shang Sui Chaolin Tan Zhenglin Du Jinlong Su Fern Lan Ng Key Laboratory for Liquid-Solid Structural Evolution and Processing of Materials Ministry of EducationShandong Engineering&Technology Research Center for Superhard MaterialSchool of Materials Science and EngineeringShandong UniversityJinan 250061China Institute of Intelligent Manufacturing Guangdong Academy of SciencesGuangzhou 510095China Singapore Institute of Manufacturing Technology 5 Cleantech Loop636732Singapore

The feasibility of manufacturing Ti-6Al-4V samples through a combination of laser-aided additive manufacturing with powder(LAAM_(p))and wire(LAAM_(w))was explored.A process study was first conducted to successfully circumvent defects in Ti-6Al-4V deposits for LAAM_(p) and LAAM_(w),*** the optimized process parameters,robust interfaces were achieved between powder/wire deposits and the forged substrate,as well as between powder and wire *** characterization results revealed the epitaxial prior β grains in the deposited Ti-6Al-4V,wherein the powder deposit was dominated by a finerα′microstructure and the wire deposit was characterized by lamellar α *** mechanisms of microstructure formation and correlation with mechanical behavior were analyzed and *** mechanical properties of the interfacial samples can meet the requirements of the relevant Aerospace material Specifications(AMS 6932)even without post heat *** fracture occurred within the interfacial area,further suggesting the robust *** findings of this study highlighted the feasibility of combining LAAM_(p) and LAAM_(w) in the direct manufacturing of Ti-6Al-4V parts in accordance with the required dimensional resolution and deposition rate,together with sound strength and ductility balance in the as-built condition.

关键词： laser-aided additive manufacturing powder deposition wire deposition interfacial characteristic mechanical behavior

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Plasma-assisted fabrication of multiscale materials for electrochemical energy conversion and storage

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Carbon Energy 2025年第2期7卷 144-171页

作者： Chen Li Tengfei Zhang Zhong Qiu Beirong Ye Xinqi Liang Xin Liu Minghua Chen Xinhui Xia Chen Wang Wangjun Wan Yongqi Zhang Institute of Fundamental and Frontier Sciences University of Electronic Science and Technology of ChinaChengduChina Key Laboratory of Engineering Dielectric and Applications(Ministry of Education) School of Electrical and Electronic EngineeringHarbin University of Science and TechnologyHarbinChina State Key Laboratory of New Textile Materials and Advanced Processing Technology Wuhan Textile UniversityWuhanChina College of Materials Science and Engineering Zhejiang University of TechnologyHangzhouChina School of Materials Science and Engineering Zhejiang UniversityHangzhouChina Zhejiang Academy of Science and Technology for Inspection and Quarantine HangzhouChina

Plasma,the fourth state of matter,is characterized by the presence of charged particles,including ions and *** has been shown to induce unique physical and chemical ***,there have been increased applications of plasma technology in the field of multiscale functional materials'preparation,with a number of interesting *** review will begin by introducing the basic knowledge of plasma,including the definition,typical parameters,and classification of plasma *** this,we will provide a comprehensive review and summary of the applications(phase conversion,doping,deposition,etching,exfoliation,and surface treatment)of plasma in common energy conversion and storage systems,such as electrocatalytic conversion of small molecules,batteries,fuel cells,and *** article summarizes the structure-performance relationships of electrochemical energy conversion and storage materials(ECSMs)that have been prepared or modified by *** also provides an overview of the challenges and perspectives of plasma technology,which could lead to a new approach for designing and modifying electrode materials in ECSMs.

关键词： electrocatalysts energy conversion and storage nanomaterials plasma

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