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Optimizing temperature coefficient of Sm_(2)Co_(17)-type magnets through adjusting the isothermal aging process

Journal of Rare Earths 2024年第11期42卷 2097-2104,I0004页

作者： Chao Wang Die Hu Qiangfeng Li Yikun Fang Meng Zheng Lei Wang Hongsheng Chen Lei Zhao Haizhou Wang Minggang Zhu Wei Li Division of Functional Materials Research Central Iron and Steel Research InstituteBeijing100081China Shanghai Aerospace Control Technology Institute Shanghai201109China Beijing Advanced Innovation Center for Materials Genome Engineering Central Iron and Steel Research InstituteBeijing100081China Beijing Key Laboratory of Metal Materials Characterization Central Iron and Steel Research InstituteBeijing100081China

The high-temperature magnetic perfo rmance and micro structure of Sm_(1-x)Gd_(x)(Co_(bal)Fe_(0.09)Cu_(0.09)Zr_(0.025))_(7.2)(x=0.3,0.5) magnets were *** the isothermal aging time decreasing from 11 to 3 h,the temperature coefficient of intrinsic coercivity in the temperature range of 25-500℃,β_(25-500℃),was optimized from -0,167%/℃ to-0.112%/℃ for x=0.3 *** noticeable enhancement(~33%) of temperature stability is correlated with the increased content of 1:5H cell boundary phase and its relatively high Curie temperature as ***,for the x=0.5 magnet,it is found that the presence of Sm_(5)Co_(19) phases and wider nanotwin variants hinder the formation of 1:5H cell boundary *** insufficient 1:5H is not beneficial to the proper redistribution of Cu in cell boundary,making the x=0.5 magnet difficult to achieve higher temperature ***,the approach of adjusting the isothermal aging process can offer guidance for attaining superior magnetic performance in the temperature range from 25 to 500℃ for Gd-substituted Sm_(2)Co_(17)-type magnets.

关键词： Rare earths Sm_(2)Co_(17)-type magnets Isothermal aging process Temperature coefficient of intrinsic coercivity

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Effects of Welding Factors on Liquid Metal Embrittlement Cracking during Resistance Spot Welding of Zinc-coated High-strength steel

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ISIJ International 2025年第1期65卷 117-126页

作者： Yu, Yang Zhang, Yongqiang Zhang, Tianyue Cao, Guangxiang Chen, Weixuan Research Institute of Technology of Shougang Group Co. Ltd. Beijing100043 China Beijing Key Laboratory of Green Recycling Process for Iron & Steel Production Technology Beijing100043 China Beijing Engineering Research Center of Energy Steel Beijing100043 China Shougang Jingtang United Iron and Steel Co. Ltd. Tangshan063200 China National Key Laboratory of Advanced Vehicle Integration & Control China FAW Group Co. Ltd Changchun130013 China

During resistance spot welding of zinc-coated advanced high-strength steels (AHSS), cracks which are promoted by liquid metal embrittlement (LME) may occur. According to previous researches, welding current, welding time, electrode tip diameter and electrode misalignment angle are significant factors on LME cracking. In this study, the effects of these four factors on LME cracking were compared with an orthogonal design experiment. After welding, numbers and lengths of cracks were measured, and Crack Index (CI) of each experiment group was calculated for comparison. As the result, two types of LME cracks, i.e., Type A cracks located at the indentation of electrode tip and Type B cracks located at the indentation of electrode shoulder were observed. The order of influence degree on CI of Type A crack from high to low was welding current > electrode tip diameter > electrode misalignment angle > welding time. The order of influence degree on CI of Type B crack was electrode tip diameter > electrode misalignment angle > welding time > welding current. The result reveals that modifying welding current is the most effective way to reduce Type A cracks and optimizing the electrode tip diameter is significant for preventing Type B cracks. © 2025 The iron and steel Institute of Japan.

关键词： Zinc coatings

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Influence mechanism of different elements and alloy phases on the corrosion resistance of Zn-Al-Mg coated steel in the atmospheric environment: A review

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Corrosion Communications 2024年第1期13卷 49-59页

作者： Xin He Xun Zhou Ting Shang Wuhua Liu Guangrui Jiang Chao Liu Xuequn Cheng Xin Zhang Xiaogang Li Institute of Advanced Materials&Technology University of Science and Technology Beijing National Materials Corrosion and Protection Data Center University of Science and Technology Beijing Technology Research Institute Shougang Group Co.Ltd. Beijing Key Laboratory of Green Recyclable Process for Iron&steel Production Technology Shougang Jingtang United Iron&Steel Co. Ltd. Institute of New Energy Technology State Power Investment Corporation Central Research Institute

Sacrificial metallic coatings are an effective strategy for mitigating corrosion in steel operating in industrial environments. This review article focuses on examining the protection mechanism of zinc-aluminum-magnesium(Zn-Al-Mg) coatings on steel substrates. Specifically, it investigates the effects of various elements and their corrosion products on the corrosion resistance of Zn-Al-Mg coatings. Furthermore, this review summarizes the formation mechanisms of various specialized corrosion modes that occur following the corrosion of Zn-Al-Mg coatings, based on previous experimental findings. It also includes suggestions for further research areas that could contribute to the development of highly corrosion-resistant and long-lasting coatings. These suggestions are based on published laboratory and field test results available in literature.

关键词： Zn-Al-Mg coated steel Corrosion resistance Corrosion products Black rust Filiform corrosion

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Coordinated control of decarbonization efficiency and oxygen absorption rate in Ruhrstahl–Heraeus degasser based on mechanism model and BP neural network

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Journal of iron and steel Research International 2025年第3期32卷 606-618页

作者： Lu-heng Jiang Min Wang Jia-qi Zhao Cheng Yao Li-dong Xing Xin-gang Ai State Key Laboratory of Advanced Metallurgy University of Science and Technology BeijingBeijing100083China Technical Support Centre for Prevention and Control of Disastrous Accidents in Metal Smelting University of Science and Technology BeijingBeijing100083China Institute of Research of Iron&Steel Zhangjiagang215600JiangsuChina School of Materials and Metallurgy University of Science and Technology LiaoningAnshan114051LiaoningChina

A mathematical model of the decarburization reaction zone was established for the Ruhrstahl–Heraeus (RH) forced oxygen blowing decarburization process by Matlab R2022b software. For the problem of inaccurate prediction due to the large variation range of oxygen absorption rate under different process conditions, we statistically analyzed the main factors affecting the oxygen absorption rate. The backpropagation neural network was used to train and predict the oxygen absorption rate and was used to calculate the RH decarburization reaction zone model. We designed and developed a mathematical modeling software with process control of decarburization in RH degasser, which can realize the change of operating process parameters in the dynamic prediction process. The optimized mathematical model has more than 95% of the furnaces whose absolute error in calculation of carbon content is within ± 5 × 10^(−6), more than 90% of the heats whose relative error in calculation of oxygen content is within ± 15%, and the average absolute error of calculation of oxygen content is 26.4 × 10^(−6). Finally, we studied the influence of oxygen blowing timing, oxygen blowing volume and initial oxygen content on the forced decarburization process.

关键词： Ruhrstahl-Heraeus degasser Mathematical model Forced decarburization Oxygen absorption rate process control

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Effect of traveling-wave magnetic field on dendrite growth of high-strength steel slab: Industrial trials and numerical simulation

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International Journal of Minerals,Metallurgy and Materials 2023年第9期30卷 1716-1728页

作者： Cheng Yao Min Wang Youjin Ni Dazhi Wang Haibo Zhang Lidong Xing Jian Gong Yanping Bao State Key Laboratory of Advanced Metallurgy University of Science and Technology BeijingBeijing 100083China Technical Support Center for Prevention and Control of Disastrous Accidents in Metal Smelting University of Science and Technology BeijingBeijing 100083China Qianshun Technology Center Shougang Qian’an Iron and Steel CompanyQian’an 064404China

The dendrite growth behavior of high-strength steel during slab continuous casting with a traveling-wave magnetic field was studied in this paper. The morphology of the solidification structure and composition distribution were analyzed. Results showed that the columnar crystals could deflect and break when the traveling-wave magnetic field had low current intensity. With the increase in current intensity, the secondary dendrite arm spacing and solute permeability decreased, and the columnar crystal transformed into an equiaxed crystal. The electromagnetic force caused by the traveling-wave magnetic field changed the temperature gradient and velocity magnitude and promoted the breaking and fusing of dendrites. Dendrite compactness and composition uniformity were arranged in descending order as follows:columnar-toequiaxed transition (high current intensity), columnar crystal zone (low current intensity), columnar-to-equiaxed transition (low current intensity), and equiaxed crystal zone (high current intensity). Verified numerical simulation results combined with the boundary layer theory of solidification front and dendrite breaking–fusing model revealed the dendrite deflection mechanism and growth process. When thermal stress is not considered, and no narrow segment can be found in the dendrite, the velocity magnitude on the solidification front of liquid steel can reach up to 0.041 m/s before the dendrites break.

关键词： high-strength steel traveling-wave magnetic field dendrite growth numerical simulation

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Boron promoted Fe^(3+)/peracetic acid process for sulfamethazine degradation:Efficiency,role of boron,and identification of the reactive species

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Journal of Environmental Sciences 2024年第1期135卷 72-85页

作者： Yanhong Zhang Guangbing Liu Yuzhu Xue Lichun Fu Yawei Qian Minhui Hou Xiang Li Chen Ling Ying Zhang Yuwei Pan Jiangsu Provincial Key Laboratory of Environmental Engineering Jiangsu Provincial Academy of Environmental ScienceNanjing 210036China College of Biology and the Environment Nanjing Forestry UniversityNanjing 210037China School of Iron and Steel Soochow UniversitySuzhou 215000China School of the Environment Nanjing UniversityNanjing 210023China SUMEC Complete Equipment&Engineering Co. LTD.Nanjing 211500China Key Laboratory of Pollution Process and Environmental Criteria Ministry of EducationCollege of Environmental Science and EngineeringNankai UniversityTianjin 300350China School of Environment Key Laboratory for Yellow River and Huai River Water Environmental and Pollution ControlMinistry of EducationHenan Key Laboratory for Environmental Pollution ControlHenan Normal UniversityXinxiang 453007China

In this work,boron(B)was used to promote Fe^(3+)/peracetic acid(Fe^(3+)/PAA)for the degradation of sulfamethazine(SMT).An SMT degradation efficiency of 9.1%was observed in the Fe^(3+)/PAA system over 60 min,which was significantly increased to 99.3%in the B/Fe^(3+)/PAA system over 10 *** B/Fe^(3+)/PAA process also exhibited superior resistance to natural substances,excellent adaptability to different harmful substances,and good removal of antibiotics in natural fresh water *** mechanism of action of boron for Fe^(3+)reduction was determined using scanning electron microscopy(SEM),X-ray photoelectron spectroscopy(XPS),Fourier transform infrared(FT-IR)spectroscopy,density functional theory(DFT)calculations,and electrochemical *** dominant role of^(·)OH was confirmed using quenching experiments,electron spin resonance(EPR)spectroscopy,and quantitative *** radicals(R-O^(·))and Fe(IV)also significantly contribute to the removal of *** calculations on the reaction between Fe^(2+)and the PAA were conducted to further determine the contribution from ^(·)OH,R-O^(·),and Fe(IV)from the perspective of thermodynamics and the reaction *** boron dosages,Fe^(3+)dosages,and initial pH values were also investigated in the B/Fe^(3+)/PAA system to study their effect of SMT removal and the production of the reactive ***(IV)production determined the k_(R-O·+Fe(IV))value suggesting that Fe(IV)may play a more important role than R-O^(·).A comparison of the results with other processes has also proved that the procedure described in this study(B/Fe^(3+)/PAA)is an effective method for the degradation of antibiotics.

关键词： Boron Peracetic acid Sulfamethazine DFT Reactive species

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Growth mechanism for zinc coatings deposited by vacuum thermal evaporation

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Journal of iron and steel Research International 2021年第8期28卷 1047-1053页

作者： Xiao-pan Qiu Xin Liu She-ming Jiang Guang-rui Jiang Qi-fu Zhang National Engineering Laboratory of Advanced Coating Technology for Metals Central Iron and Steel Research InstituteBeijing 100081China Beijing Key Laboratory of Green Recyclable Process for Iron and Steel Production Technology Shougang Group Co.Ltd.Research Institute of TechnologyBeijing 100043China

The vacuum thermal evaporation technique was used to simultaneously deposit zinc coatings onto interstitial free steel plates and single-crystal silicon wafers in a high vacuum *** effect of substrate temperature on the mor-phology and crystal orientation of zinc coatings was *** the substrate temperature was 25 and 50℃,the zinc crystallites were plate-like and grew under a particular angle to the substrate *** the substrate was heated to 100℃,the zinc crystallites were regular hexagonal and arranged almost parallel to the substrate *** addition,observation of pure zinc coatings with different thicknesses showed that the growth of zinc coating was mainly in the Volmer-Weber *** the process parameters were appropriate,the zinc coating was composed of closely arranged columnar crystallites,and the crystallites grew preferentially along[0001]direction.

关键词： Vacuum thermal evaporation Zinc coating Deposition temperature Growth mechanism

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Multimodal process Monitoring Based on Dynamic Extended K-means-VAE-RF

Multimodal Process Monitoring Based on Dynamic Extended K-me...

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第35届中国控制与决策会议

作者： Shiwei Su Kaixiang Peng Xueyi Zhang Key Laboratory for Advanced Control of Iron and Steel Process of Ministry of Education School of Automation and Electrical Engineering University of Science and Technology Beijing

With the development of customization and flexibility of manufacturing industry,intelligent manufacturing process gradually presents multimodal characteristics,which are reflected in the strong coupling,nonlinear,multi working conditions and other characteristics of the *** this paper,a multi-modal process monitoring method based on dynamic expansion is *** view of the dynamic characteristics of process data,the process data is dynamically expanded through the amplification matrix,and then the multi-modal process data is modal divided through the improved K-means *** divided multi-modal process data is monitored using Variational Autoencoder,and relevant statistics and control limits are ***,the multi-modal process monitoring is constructed by introducing the method of random forest for modal *** validity of the algorithm is verified by real data of steel rolling process.

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3D bioprinting of in vitro porous hepatoma models:establishment,evaluation,and anticancer drug testing

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Bio-Design and Manufacturing 2024年第2期7卷 137-152页

作者： Xiaoyuan Wang Zixian Liu Qianqian Duan Boye Zhang Yanyan Cao Zhizhong Shen Meng Li Yanfeng Xi Jianming Wang Shengbo Sang Shanxi Key Laboratory of Micro Nano Sensors and Artificial Intelligence Perception College of Electronic Information and Optical EngineeringTaiyuan University of TechnologyTaiyuan 030024China Key Lab of Advanced Transducers and Intelligent Control System of the Ministry of Education Taiyuan University of TechnologyTaiyuan 030024China Shanxi Institute of 6D Artificial Intelligence Biomedical Science Taiyuan 030031China Shanxi-Zheda Institute of Advanced Materials and Chemical Engineering Taiyuan 030024China Department of Pathology Shanxi Provincial Cancer HospitalTaiyuan 030024China General Hospital of Taiyuan Iron and Steel Company Taiyuan 030809China

Traditional tumor models do not tend to accurately simulate tumor growth in vitro or enable personalized treatment and are particularly unable to discover more beneficial targeted *** address this,this study describes the use of threedimensional(3D)bioprinting technology to construct a 3D model with human hepatocarcinoma SMMC-7721 cells(3DP-7721)by combining gelatin methacrylate(GelMA)and poly(ethylene oxide)(PEO)as two immiscible aqueous phases to form a bioink and innovatively applying fluorescent carbon quantum dots for long-term tracking of *** GelMA(10%,mass fraction)and PEO(1.6%,mass fraction)hydrogel with 3:1 volume ratio offered distinct pore-forming characteristics,satisfactorymechanical properties,and biocompatibility for the creation of the 3DP-7721 *** analysis and quantitative real-time fluorescence polymerase chain reaction(PCR)were used to evaluate the biological properties of the *** with the two-dimensional culture cell model(2D-7721)and the 3D mixed culture cell model(3DM-7721),3DP-7721 significantly improved the proliferation of cells and expression of tumor-related proteins and ***,we evaluated the differences between the three culture models and the effectiveness of antitumor drugs in the three models and discovered that the efficacy of antitumor drugs varied because of significant differences in resistance proteins and genes between the three *** addition,the comparison of tumor formation in the three models found that the cells cultured by the 3DP-7721 model had strong tumorigenicity in nude *** evaluation of the levels of biochemical indicators related to the formation of solid tumors showed that the 3DP-7721 model group exhibited pathological characteristics of malignant tumors,the generated solid tumors were similar to actual tumors,and the deterioration was *** research therefore acts as a foundation for the application of 3DP-7721 models in drug devel

关键词： 3D bioprinting Hepatoma tumor models Drug screening Antitumor drug development

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Improved Digital Costas Loop Design in Spread Spectrum Communication

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Chinese Journal of Electronics 2023年第2期20卷 299-302页

作者： Hongbo Wang Li Deng Zhonggui Ma Xuyan Tu School of Information Engineering University of Science and Technology Beijing Beijing China Key Laboratory of Advanced Control of Iron and Steel Process (Ministry of Education) University of Science and Technology Beijing Beijing China

Based on software radio technique, a novel improved design structure of digital Costas loop for spread spectrum communication is put forward in the paper. Main practical works includes: (1) For carrier recovery in the traditional Costas central, it improves a way applicable to the spread spectrum communication and gives a detailed mathematical deduction; (2) As for traditional QPSK modern methods, it joins the encoding, interleaving, de-interlacing, decoding, balanced module in the QPSK modulation and demodulation process in spread spectrum communications to reduce the system Bit error rate (BER); (3) a PN code magna-scope demodulator and two low power filers are added in order to get sensitive weighing signal. Simulation contrast results show that the improvement is feasible.

关键词： Phase shift keying Codes Voltage-controlled oscillators Bit error rate Spread spectrum communication Encoding Decoding

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