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Evidence of microstructural evolution linked to non-monotonic distribution of micromechanical properties induced by shot peening

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材料科学技术（英文版） 2025年第4期207卷 238-245页

作者： Guoxin Lu Qiang Wang Bonnie Attard Huhu Su Shijian Zheng Key Laboratory for Liquid-Solid Structural Evolution and Processing of Materials Ministry of EducationSchool of Materials Science and EngineeringShandong UniversityJinan250061China Aviation Key Laboratory of Science and Technology on Advanced Corrosion and Protection for Aviation Material AECC Beijing Institute of Aeronautical MaterialsBeijing100095China Department of Metallurgy and Materials Engineering University of MaltaMSD2080Malta Tianjin Key Laboratory of Materials Laminating Fabrication and Interface Control Technology School of Materials Science and EngineeringHebei University of TechnologyTianjin300130China

The residual stress field induced by surface strengthening processes such as mechanical shot peening and other forms of plastic deformation does not generally exhibit a simple"monotonic"distribution *** researchers have analyzed this fact from a mechanical perspective based on Hertz ***,the micro/nano-scale microstructural changes corresponding to the distribution of residual stress fields still appear to be *** this study,we focused on a widely used material in aviation manufacturing,namely nickel-based superalloy GH4169,as our experimental *** subjected GH4169 alloy to me-chanical strengthening treatment using a shot peening intensity of 0.25 mmA,followed by quantitative testing of micromechanical performance indicators such as microhardness and residual *** thor-oughly investigate the relationship between micromechanical properties and microstructure changes,we utilized transmission electron microscopy(TEM)to observe and analyze shot-peened materials at differ-ent *** findings revealed that the most severe microstructural distortion induced by mechanical shot peening in GH4169 alloy was likely to occur within a depth range of 25 to 75 *** observation aligns with the actual phenomenon that the maximum microhardness and maximum residual compres-sive stress did not manifest on the outermost surface of the *** presenting a detailed analysis of deformation defects such as dislocations,stacking faults,and twinning in different depths of mechan-ically strengthened layers,our study contributes to a deeper understanding and practical application of post-processing technologies based on plastic deformation.

关键词： Mechanical shot peening Surface strengthening Residual stress Microstructure

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An experimental study on effects of temperature gradient on microstructure of a 308L stainless steel manufactured by directed energy deposition

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Journal of Iron and Steel Research International 2024年第8期31卷 2031-2040页

作者： Ting Dai De-yu Gu Yu-wen Qiu Wei Guo Hui Ding Yi-wei Sun School of Materials Science and Engineering Jiangsu Key Laboratory of Advanced Metallic MaterialsSoutheast UniversityNanjing 211189JiangsuChina

The effect of spatial temperature gradient on the microstructural evolution of a 308L stainless steel during the directed energy deposition(DED)process was experimentally investigated.A novel cooling system was designed and incorporated to a DED system in order to control the temperature gradient along the deposition direction during *** deposition,the workpiece was placed on a lifting platform,and as the deposition process proceeded,the platform and workpiece were gradually lowered into cooling water so that the temperature gradient along the deposition direction could be controlled and maintained stable during the deposition *** microstructure characterization results indicated that a deposition strategy with higher G and G/R values(where G is temperature gradient and R is solidification rate)produced finer cellular grains that were better aligned with the deposition direction,while a deposition strategy with lower G and G/R values produced columnar grains with larger primary arm spacing and less aligned with the deposition direction.

关键词： Additive manufacturing Directed energy deposition Stainless steel Microstructure Temperature gradient

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A facile data-driven battery capacity estimation framework for on-road plug-in hybrid electric vehicle

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Progress in Natural science:materials International 2025年第1期35卷 166-176页

作者： Jianlu Li Yanming Chen Tongxing Lei Jianguo Liu Guizheng Liu Zhaoyang Deng Xuebiao Wu Zhiyu Ding Yinghe Zhang Junwei Wu Yanan Chen Guangzhou Automobile Group Co. Ltd. School of Materials Science and Engineering Harbin Institute of Technology School of Materials and Environmental Engineering Shenzhen Polytechnic University School of Science Shenzhen Key Laboratory of Flexible Printed Electronics Technology Shenzhen Key Laboratory of Advanced Functional Carbon Materials Research and Comprehensive Application Harbin Institute of Technology School of Materials Science and Engineering Key Laboratory of Advanced Ceramics and Machining Technology of Ministry of Education Tianjin Key Laboratory of Composite and Functional Materials Tianjin University

A data-driven framework with strong generalization capabilities is proposed to effectively extract features and easily access battery capacity. This framework can make highly accurate predictions for the battery capacities of plug-in electric vehicles. The feature extraction process is entirely based on statistics, which are always available and can be generalized to various types of battery data. An improved ampere-hour integral method can easily access battery capacity with just short-charging segments lasting 500 s. Several machine-learning models are trained to verify the framework's effectiveness, with the best model achieving a test error of 0.84 % based on leave-one-out validation. SHAP values are used to provide a reasonable interpretation of the relationships between the constructed features and model outputs. The proposed framework offers advantages such as reduced computational resources, wide generalization, and high prediction accuracy, showing great potential for battery management.

关键词： Battery capacity estimation Data-driven framework Lithium-ion battery Machine learning Plug-in hybrid electric vehicle

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ZIF-8 modified by isocyanate as a photocatalytic antibacterial agent

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Rare Metals 2024年第6期43卷 2708-2718页

作者： Yi-Ning Zhang Zhen Pei Zi-Hao Wang Chong-En Wang Fen-Fen Liang Li-Qiao Wei College of Architecture Taiyuan University of TechnologyTaiyuan 030024China Key Laboratory of Interface Science and Engineering in Advanced Materials of Taiyuan University of Technology Ministry of EducationTaiyuan 030024China Department of Materials Science and Engineering Shanxi Institute of TechnologyYangquan 045000China Shanxi-Zheda Institute of Advanced Materials and Chemical Engineering Taiyuan 030000China

Zeolite imidazole skeleton(ZIF-8)is a promising option for self-cleaning of building exterior walls due to its large specific surface area,high antibacterial activity and low ***,it suffers from low antibacterial efficiency and yield under visible light *** address the issues,we developed the photocatalytic materials T-ZIF-8-TDI(thermally treated-ZIF-8-toluene 2,4-diisocyanate)by modifying ZIF-8 with thermal oxygen sensitization and chemical *** results show that the yield of T-ZIF-8-TDI photocatalytic antibacterial agent is increased to 11.5 times of that of T-ZIF-8,while maintaining the crystal structure of T-ZIF-8 and thermal stability up to 60℃.Furthermore,T-ZIF-8-TDI exhibits extended optical response range to the nearinfrared region,significantly narrowed band gap,improved photogenerated elec tron-hole separation efficiency,reduced recombination rate,and excellent photocatalytic *** the concentration of antibacterial agent is 600 mg·L^(-1),the antibacterial rate of Escherichia coli(***)reaches 99.99%irradiated by visible light for30 min,and when the concentration of antibacterial agent is 200 mg·L^(-1),the antibacterial rate of Staphylococcus aureus(***)reaches 99.99%irradiated by visible light for 25 *** also analyzed the reasons in detail from the aspects of bacterial species and antibacterial mechanism,and proposed the antibacterial mechanism of·O_(2)^(-)and h^(+)as the main active *** findings suggest that T-ZIF-8-TDI photocatalytic antibacterial agent has potential for use in self-cleaning of building exterior walls.

关键词： ZIF-8 Hot oxygen sensitization Modified by isocyanate Antimicrobial performance Photocatalytic antibacterial mechanism

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Prediction of BOF endpoint carbon content and temperature via CSSA-BP neural network model

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Journal of Iron and Steel Research International 2025年第3期32卷 578-593页

作者： Xiao-feng Qiu Run-hao Zhang Jian Yang State Key Laboratory of Advanced Special Steel School of Materials Science and EngineeringShanghai UniversityShanghai200444China

To predict the endpoint carbon content and temperature in basic oxygen furnace (BOF), the industrial parameters of BOF steelmaking are taken as input values. Firstly, a series of preprocessing works such as the Pauta criterion, hierarchical clustering, and principal component analysis on the original data were performed. Secondly, the prediction results of classic machine learning models of ridge regression, support vector machine, gradient boosting regression (GBR), random forest regression, back-propagation (BP) neural network models, and multi-layer perceptron (MLP) were compared before and after data preprocessing. An improved model was established based on the improved sparrow algorithm and BP using tent chaotic mapping (CSSA-BP). The CSSA-BP model showed the best performance for endpoint carbon prediction with the lowest mean absolute error (MAE) and root mean square error (RMSE) values of 0.01124 and 0.01345 mass% among seven models, respectively. And the lowest MAE and RMSE values of 8.9839 and 10.9321 ℃ for endpoint temperature prediction were obtained among seven models, respectively. Furthermore, the CSSA-BP and GBR models have the smallest error fluctuation range in both endpoint carbon content and temperature predictions. Finally, in order to improve the interpretability of the model, SHapley additive interpretation (SHAP) was used to analyze the results.

关键词： BOF steelmaking Principal component analysis Hierarchical clustering CSSA-BP SHapley additive interpretation

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Effect of Al content on nanoprecipitates, austenite grain growth and toughness in coarse-grained heat-affected zones of Al–Ti–Ca deoxidized shipbuilding steels

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International Journal of Minerals,Metallurgy and materials 2025年第4期32卷 879-891页

作者： Tingting Li Jian Yang Yinhui Zhang Han Sun Yanli Chen Yuqi Zhang State Key Laboratory of Advanced Special Steel School of Materials Science and EngineeringShanghai UniversityShanghai 200444China

This work focuses on the influence of Al content on the precipitation of nanoprecipitates,growth of prior austenite grains(PAGs),and impact toughness in simulated coarse-grained heat-affected zones (CGHAZs) of two experimental shipbuilding steels after being subjected to high-heat input welding at 400 kJ·cm^(-1).The base metals (BMs) of both steels contained three types of precipitates Type Ⅰ:cubic (Ti,Nb)(C,N),Type Ⅱ:precipitate with cubic (Ti,Nb)(C,N) core and Nb-rich cap,and Type Ⅲ:ellipsoidal Nb-rich *** the BM of 60Al and 160Al steels,the number densities of the precipitates were 11.37×10^(5) and 13.88×10^(5) mm^(-2),respectively The 60Al and 160Al steel contained 38.12% and 6.39% Type Ⅲ precipitates,*** difference in the content of Type Ⅲ precipitates in the 60Al steel reduced the pinning effect at the elevated temperature of the CGHAZ,which facilitated the growth of PAGs The average PAG sizes in the CGHAZ of the 60Al and 160Al steels were 189.73 and 174.7μm,*** the 60Al steel,the low lattice mismatch among Cu_(2)S,TiN,and γ-Al_(2)O_(3)facilitated the precipitation of Cu_(2)S and TiN onto γ-Al_(2)O_(3)during welding,which decreased the number density of independently precipitated (Ti,Nb)(C,N) particles but increased that of γ-Al_(2)O_(3)–Ti N–Cu_(2)S *** abnormally large PAGs formed in the CGHAZ of the 60Al steel,and they reached a maximum size of 1 *** PAGs greatly reduced the microstructural homogeneity and consequently decreased the impact toughness from 134 (0.016wt%Al) to 54 J (0.006wt%Al)at-40℃.

关键词： oxide metallurgy Al–Ti–Ca deoxidization Al content precipitates coarse-grained heat-affected zone

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Revealing the influential mechanism of electromagnetic vibration on the bulk solidification and the upward continuous casting of Cu-15Ni-8Sn Alloy

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Journal of materials science & Technology 2024年第22期189卷 166-182页

作者： Ganpei Tang Zhe Sun Zhongze Lin Tianxiang Zheng Bangfei Zhou Peijian Shi Qiang Li Chunmei Liu Haibiao Lu Zhe Shen Biao Ding Yunbo Zhong State Key Laboratory of Advanced Special Steel&Shanghai Key Laboratory of Advanced Ferrometallurgy&School of Materials Science and Engineering Shanghai UniversityShanghai 200444China

The effect of electromagnetic vibration(EMV)on the solidification structure of Cu-15Ni-8Sn alloy during bulk solidification and the upward continuous casting was investigated experimentally and *** bulk solidification results indicated that in the case of B=0.5 T and J=1.27×10^(5)A/m^(2),the most effective grain refinement frequency was at f=10 Hz,where fine non-dendrites were *** solidification structure became coarser at f=0.1 Hz and f=1 Hz compared to the case of f=10 Hz,while no grain refinement was observed at f=100 *** numerical simulations showed that at f=10 Hz,the strong melt convection surrounding the primary solid phase promotes the diffusion of the rejected solute,consequently,resulting in a reduction of the solute boundary layer,which leads to the decrease in the nucleation-free zone(NFZ)and the grain ***,the most effective grain refinement frequency transformed to 1 Hz when the electromagnetic force was reduced by five ***,we proposed that the most effective grain refinement frequency range aligns with the EMV-induced relative displacement in the range of 10^(2)–10^(3)μ***,the upward continuous casting was conducted to validate the relative displacement range,and the experimental results matched well.

关键词： Electromagnetic vibration Grain refinement Solidification structure Upward continuous casting

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The Kirkendall effect on erosion resistance of chrome-coated 25Cr3Mo2WNiV and 30SiMn2MoV gun barrel steels

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Journal of materials science & Technology 2024年第10期177卷 246-255页

作者： C.H.Dou P.F.Jin C.Z.Wang J.J.Li C.Zhang J.F.Huang C.Zhang Key Laboratory for Advanced Materials Processing State State Key Laboratory for Advanced Metals and MaterialsUniversity of Science and Technology BeijingBeijing 100083China National Joint Engineering Research Center for Abrasion Control and Molding of Metal Materials School of Materials Science and EngineeringHenan University of Science and TechnologyLuoyang 471003China

This study aimed to investigate the erosion behavior and mechanism of a newly developed 25Cr3Mo2WNiV steel with a chrome coating using promoted ignition combustion *** erosion threshold pressure and temperature of the chrome-coated 25Cr3Mo2WNiV steel were determined to be 0.2 MPa and 254.3 K higher than those of traditional chrome-coated 30SiMn2MoV ***,Kirkendall voids and inter-diffusion between the Cr coating and matrix were first observed before *** improved erosion resistance of the chrome-coated 25Cr3Mo2WNiV steel was attributed to the suppression of the Kirkendall effect,which minimized heat generation at the Cr/matrix interface by pre-venting oxygen diffusion and reducing oxygen affinity.

关键词： Erosion resistance Kirkendall effect Cr coating Gun steel

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Deciphering and overcoming the high-voltage limitations of halide and sulfide-based all-solid-state lithium batteries

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Journal of Energy Chemistry 2025年第4期103卷 926-935页

作者： Xiang Qi Gang Wu Meng Wu Dabing Li Chao Wang Lei Gao Shichao Zhang Li-Zhen Fan Beijing Advanced Innovation Center for Materials Genome Engineering Beijing Key Laboratory for Advanced Energy Materials and TechnologiesUniversity of Science and Technology BeijingBeijing 100083China School of Materials Science and Engineering Beihang UniversityBeijing 100191China

Adopting high-voltage Ni-rich cathodes in halide and sulfide-based all-solid-state lithium batteries(ASSLBs)holds great promise for breaking through the 400 Wh kg^(-1)***,both cell configurations are confronted with intricate interfacial challenges in high-voltage regines(>4.5 V),resulting in inadequate cathode utilization and premature cell ***,contrary to previous studies,coupled with LiNi_(0.85)Co_(0.1)Mn_(0.05)O_(2)cathodes,typical halide(Li_(2)ZrCl_(6))-based cells at 4.5 V feature unlimited interfacial degradation and poor long cycle stability,while typical sulfide(Li_(6)PS_(5)Cl)-based cells feature self-limited interfacial degradation and poor initial cycle ***,this work addresses the high-voltage limitations of Li_(2)ZrCl_(6)and Li_(6)PS_(5)Cl catholyte-based cells by manipulating electrode mass fraction and tailoring interfacial composition,thereby effectively improving interfacial charge-transfer kinetics and(electro)chemical stability within *** appropriate interface design,both optimized cells at 4.5 V demonstrate remarkably increased initial discharge capacities(>195 mA h g^(-1)at0.1 C),improved cycle stabilities(>80%after 600 cycles at 0.5 C),and enhanced rate performances(>115 mA h g^(-1)at 1.0 C).This work deepens our understanding of high-voltage applications for halide/sulfide electrolytes and provides generalized interfacial design strategies for advancing high-voltage ASSLBs.

关键词： All-solid-state lithium batteries Halide solid electrolytes Sulfide solid electrolytes High voltage interface design

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Mg/Fe site-specific dual-doping to boost the performance of cobalt-free nickle-rich layered oxide cathode for high-energy lithium-ion batteries

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Journal of Energy Chemistry 2024年第4期91卷 670-679页

作者： Yunting Wang Gaohui Du Di Han Wenhao Shi Jiahao Deng Huayu Li Wenqi Zhao Shukai Ding Qingmei Su Bingshe Xu Materials Institute of Atomic and Molecular Science Shaanxi University of Science and TechnologyXi'an 710021ShanxiChina Shanxi-Zheda Institute of Advanced Materials and Chemical Engineering Taiyuan 030024ShanxiChina Key Laboratory of Interface Science and Engineering in Advanced Materials Taiyuan University of TechnologyTaiyuan 030024ShanxiChina

Layer-type LiNi0.9Mn0.1O2is promising to be the primary cathode material for lithium-ion batteries(LIBs)due to its excellent electrochemical ***,the cathode with high nickel content suffers from severely detrimental structural transformation that causes rapid capacity ***,site-specific dual-doping with Fe and Mg ions is proposed to enhance the structural stability of *** Fe3+dopants are inserted into transition metal sites(3b)and can favorably provide additional redox potential to compensate for charge and enhance the reversibility of anionic *** Mg ions are doped into the Li sites(3a)and serve as O_(2)^(-)-Mg^(2+)-O_(2)^(-)pillar to reinforce the electrostatic cohesion between the two adjacent transition-metal layers,which further suppress the cracking and the generation of harmful phase transitions,ultimately improving the *** theoretical calculations,including Bader charge and crystal orbital Hamilton populations(COHP)analyses,confirm that the doped Fe and Mg can form stable bonds with oxygen and the electrostatic repulsion of O_(2)^(-)-O_(2)^(-)can be effectively suppressed,which effectively mitigates oxygen anion loss at the high delithiation *** dual-site doping strategy offers new avenues for understanding and regulating the crystalline oxygen redox and demonstrates significant potential for designing high-performance cobalt-free nickel-rich cathodes.

关键词： Cobalt-free Layered oxide Cathode Dual dopants Density functional theory calculation

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