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Dislocation me diate d dynamic tension-compression asymmetry of a Ni_(2)CoFeV_(0.5)Mo_(0.2) medium entropy alloy

Journal of Materials Science & technology 2023年第28期159卷 204-218页

作者： Ao Meng Xiang Chen Yazhou Guo Yiping Lu Yonghao Zhao Nano and Heterogeneous Materials Center School of Materials Science and EngineeringNanjing University of Science and TechnologyNanjing 210094China School of Aeronautics Northwestern Polytechnical UniversityXi’an 710072China Key Laboratory of Solidification Control and Digital Preparation Technology(Liaoning Province) School of Materials Science and EngineeringDalian University of TechnologyDalian 116024China

Although tension-compression(T-C)asymmetry in yield strength was rarely documented in coarse-grained face centered cubic(FCC)metals as critical resolved shear stress(CRSS)for dislocation slip differs little between tension and compression,the T-C asymmetry in strength,i.e.,higher strength when loaded in compression than in tension,was reported in some FCC high entropy alloys(HEAs)due to twinning and phase transitions activated at high strain regimes in *** this paper,we demonstrate a reversed and atypical tension-compression asymmetry(tensile strength markedly exceeds compressive strength)in a non-equiatomic FCC Ni_(2)CoFeV_(0.5)Mo_(0.2) medium entropy alloy(MEA)under dynamic loading,wherein dislocation slip governs dynamic deformation without twins or phase *** asymme-try can be primarily interpreted as higher CRSS and more hard slip modes(lower average Schmid factor)activated in grains under dynamic tension than ***,larger strain rate sensitivity in dy-namic tension overwhelmingly contributes to the higher flow stress,thanks to the occurrence of more immobile Lomer-locks,narrower spacing of planar slip bands and higher dislocation *** finding may provide some insights into designing MEAs/HEAs with desired properties under extreme conditions such as blast,impact and crash.

关键词： Medium entropy alloy Dynamic deformation Tension-compression asymmetry Slip trace analysis EBSD and TEM

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Enhancing mechanical properties and corrosion resistance of nickel-aluminum bronze via hot rolling process

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Journal of Materials Science & technology 2021年第2期61卷 186-196页

作者： Yanhua Zeng Fenfen Yang Zongning Chen Enyu Guo Minqiang Gao Xuejian Wang Huijun Kang Tongmin Wang Key Laboratory of Solidification Control and Digital Preparation Technology(Liaoning Province) School of Materials Science and EngineeringDalian University of TechnologyDalian 116024China

The mechanical properties and corrosion behavior of as-cast, as-annealed and hot-rolled nickelaluminum bronze(NAB) alloy(Cu-9 Al-10 Ni-4 Fe-1.2 Mn, all in wt.%) in 3.5 wt.% Na Cl solution were investigated. The results show that annealing introduces a large number of k phases to precipitate in the k phase. However, after further hot rolling, the original continuous k phases are spheroidized and dispersed, increasing the strength, hardness, and elongation of the alloy. In addition to the enhanced mechanical properties, the corrosion resistance of the NAB samples is also improved significantly by hot rolling, as revealed by the mass loss measurements, electrochemical impedance spectroscopy(EIS), and cross-sectional corrosion morphology. Selective phase corrosion occurs by the preferential corrosion of the k phase, which acts as an anode to the k phases, and the uncorroded k phases are retained in the corrosion product film. The interfaces between the k phases and the surrounding corrosion products become discontinuous caused by the spheroidization of k phases, reducing the corrosion of the substrate by the corrosive medium via the channels. As a result, the corrosion rate and the maximum local corrosion depth of the hot-rolled NAB sample are greatly reduced.

关键词： Nickel-aluminum bronze Hot rolling Mass loss EIS Selective phase corrosion

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Growth mechanism of primary Ti_(5)Si_(3) phases in special brasses and their effect on wear resistance

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Journal of Materials Science & technology 2021年第2期61卷 138-146页

作者： Xianlong Wang Jinchuan Jie Shichao Liu Zhuangzhuang Dong Guomao Yin Tingju Li Key Laboratory of Solidification Control and Digital Preparation Technology(Liaoning Province) School of Materials Science and EngineeringDalian University of TechnologyDalian116024China

In the present work, in-situ Ti_(5)Si_(3) reinforced special brasses were prepared by melt reaction method. The synthesized Ti_(5)Si_(3) phase shows various morphologies in brasses with different Ti_(5)Si_(3) content, and the3 D morphological evolution of primary Ti_(5)Si_(3)and its growth mechanism were investigated. The Ti_(5)Si_(3) crystal, which bears D8_(8) hexagonal crystal structure, grows along <0001> direction and is revealed by{1010} faces during growth. With the increase of Ti_(5)Si_(3) content in the brasses, the morphology of primary Ti_(5)Si_(3)significantly changes from fibers to hexagonal prisms to short-rods with hollow. In addition,the influence of Ti_(5)Si_(3) volume fraction and morphology on the wear behavior of special brass was also revealed. It was substantiated that the wear resistance increases with the increasing volume fraction of Ti_(5)Si_(3), and the corresponding wear mechanism changes from delamination to slight adhesive wear and abrasive wear. However, the friction coefficient shows an abnormal increase when most of the Ti_(5)Si_(3) containing hollows appears in the brass. That is mainly due to the fact that the Ti_(5)Si_(3) is easier to break and fall off resulted by the hollow as a crack source, which makes it unable to resist the plastic deformation of the contact surface during the sliding.

关键词： Ti_(5)Si_(3) Brass Morphology Growth mechanism Wear behavior

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A novel as-cast precipitation-strengthened Al_(0.5)V_(0.1)FeCrMnNi_(0.9) high-entropy alloy with high strength and plasticity

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Science China(Technological Sciences) 2021年第9期64卷 1920-1926页

作者： LI ChunHui WANG MingLiang ZHANG HuanZhi ZHANG GuoJia LI TianXin LU YiPing LI TingJu Key Laboratory of Solidification Control and Digital Preparation Technology(Liaoning Province) School of Materials Science and EngineeringDalian University of TechnologyDalian 116024China

A novel Al_(0.5)V_(0.1)FeCrMnNi_(0.9) high-entropy alloy was designed to achieve enhanced strength and plasticity. The as-cast Al_(0.5)V_(0.1)FeCrMnNi_(0.9) alloy shows a typical dendritic microstructure consisting of a body-centered cubic-structured matrix phase and a B2-structured nanoprecipitate phase. Nanoprecipitates are homogeneous and dispersed in the matrix. The as-cast Al_(0.5)V_(0.1)FeCrMnNi_(0.9) alloy exhibits a compressive yield strength of 1.104 GPa, a fracture strength of 2.926 GPa, and a fracture strain of 45.7%. The product of strength and plasticity of this alloy is 133.72 GPa%, which is superior to that of most of the reported high-entropy alloys. The strengthening mechanisms were evaluated in detail, which indicates that the coherent precipitation enhancement contributes to the unusually high strength and plasticity.

关键词： high-entropy alloy microstructure mechanical properties precipitation strengthening

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Microstructural evolution and its influence on mechanical and corrosion behaviors in a high-Al/Zn containing duplex Mg-Li alloy after friction stir processing

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Journal of Materials Science & technology 2024年第17期184卷 245-255页

作者： Yixing Zhu Mengran Zhou Yingxin Geng Shun Zhang Tongzheng Xin Gaoqiang Chen Yifan Zhou Xiaoyu Zhou Ruizhi Wu Qingyu Shi State Key Laboratory of Clean and Efficient Turbomachinery Power Equipment Department of Mechanical EngineeringTsinghua UniversityBeijing 100084China Key Laboratory for Advanced Materials Processing Technology Ministry of EducationBeijing 100084China Key Laboratory of Superlight Materials&Surface Technology(Ministry of Education) Harbin Engineering UniversityHarbin 150001China Key Laboratory of Solidification Control and Digital Preparation Technology(Liaoning Province) School of Materials Science and EngineeringDalian University of TechnologyDalian 116024China Beijing North Vehicle Group Corporation Beijing 100072China

Ultralight Mg-Li alloys offer promising applications across various ***-Li alloys enriched with Al and Zn hold theoretical potential for achieving excellent mechanical strength and corrosion ***,the structural and performance characteristics of such Mg-Li alloys,particularly after thermo-mechanical processing,remain inadequately explored and *** study investigated the mi-crostructural evolution of a Mg-9Li-5Al-4Zn alloy after friction stir processing and its consequent effects on the mechanical and corrosion *** grain size of the alloy was effectively refined and sta-bilized during friction stir processing at various heat *** yield strength of the alloy increased by 86.4%after friction stir processing under the highest heat input condition,which was attributed to fine grain strengthening,solid solution strengthening and dispersion ***,the alloy ex-perienced a slight decrease in elongation after the friction stir *** alloy subjected to friction stir processing with the highest heat input exhibited a minimal corrosion current density of 6.10×10^(−6) A/cm^(2),which was only 25%of the base *** enhanced anti-corrosion properties can be attributed to the dispersion and distribution of precipitated particles induced by friction stir processing,which hin-dered the micro-galvanic corrosion and promoted the generation of a compact surface film,leading to minimal and uniform *** investigation can be significant for understanding the metallurgical mechanisms and performance evolution of Mg-Li alloys during thermomechanical processes.

关键词： Mg-Li-Al-Zn alloy Friction stir processing Microstructure evolution Thermal-mechanical stability Corrosion behavior

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The electromagnetic response of composition-regulated honeycomb structural materials used for broadband microwave absorption

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Journal of Materials Science & technology 2021年第29期88卷 203-214页

作者： Huifang Pang Yuping Duan Xuhao Dai Lingxi Huang Xuan Yang Tuo Zhang Xiaoji Liu Key Laboratory of Solidification Control and Digital Preparation Technology(Liaoning Province) School of Materials Science and EngineeringDalian University of TechnologyDalian116085China

The undesirable absorption bandwidth is the main limitation for the application of microwave absorbing *** that the design of structure and composition of absorbing coating allows it to obtain a satisfying absorption bandwidth and to avoid weight increasing,honeycomb and its sandwich structures coated by various absorbant have been developed and measured using an arch measurement system over2-18 *** further understand the absorption mechanisms of honeycomb structural materials,simulation based on finite element method and transmission line theory is performed to analyze the different responses to the applied microwave between honeycomb structural materials and uniform-medium slab *** proper composition design allows control over the microwave loss mechanisms,which optimize the coating to possess both of the dielectric and magnetic *** the honeycomb structural materials,the magnetic resonation is found for the first time,which is resulting from the periodic honeycomb walls on both sides of the dielectric cavity(consisting of the aramid paper interlayer and vacuum hexagonal prisms).In addition,the conversion of structure from solid to honeycomb brings about changes in impedance,propagating path,effective wavelength,effective attenuation area,microwave phases,and inductive coupling effect,etc.,which result in a better microwave absorbing *** honeycomb sandwich structure coated by CIP/CB/EP with the weight ratio of 4:0.03:1 shows the absorption bandwidth of~9.8 GHz for reflection loss(RL)lower than-10 dB which covers part of the S and C bands and almost the whole X and Ku bands.

关键词： Microwave absorption Structural materials Honeycomb Electromagnetic response

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Tailoring the Microstructure and Mechanical Property of Mg-Zn Matrix Composite via the Addition of Al Element

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Acta Metallurgica Sinica(English Letters) 2024年第3期37卷 438-452页

作者： Chong Wang Fuyuan Liu Xuejian Wang Enyu Guo Zelong Du Kunkun Deng Zongning Chen Huijun Kang Guohao Du Tongmin Wang Key Laboratory of Solidification Control and Digital Preparation Technology(Liaoning Province) School of Materials Science and EngineeringDalian University of TechnologyDalian 116024China School of Mechanical Engineering Guizhou UniversityGuiyang 550025China Ningbo Institute of Dalian University of Technology Ningbo 315000China Shanxi Key Laboratory of Advanced Magnesium-Based Materials College of Materials Science and EngineeringTaiyuan University of TechnologyTaiyuan 030024China Shanghai Synchrotron Radiation Facility Shanghai Advanced Research Institute CASShanghai 201204China

The semi-solid stir casting method is adopted to prepare 10 wt%SiC_(p)/Mg-6Zn-0.5Ca-xAl(x=0,1,3 and 5 wt%)composites,and the microstructure evolution and mechanical property of composites with various Al content are *** results show that the addition of 3 wt%Al improves the distribution of SiC_(p),whereas the SiC_(p) cluster occurs again with Al content greater than 3%.An abnormal phenomenon of twinning is observed in the cast composites in this *** SiC_(p)/Mg-6Zn-0.5Ca composite possesses the highest twin content of~23%,for which tension twins(TTW)and compression twins(CTW)account for~19%and~3%,*** CTW is only observed in ZXA600 *** addition of Al has an inhibiting effect for the generation and growth of *** content of twin decreases firstly and then increases with increase of Al *** lowest twin content is obtained as Al increases to 3 wt%.It is found the existence of twin is detrimental to the mechanical property of ***-cast SiC_(p)/Mg-6Zn-0.5Ca-3Al composite with the lowest twin content exhibits the optimal mechanical property of yield strength,ultimate tensile strength and elongation for 100 MPa,188 MPa and 4.4%,*** outstanding mechanical property is attributed to the uniform distribution of SiC_(p),the low twin content and the well-distributed fine second phases.

关键词： Mg matrix composite Synchrotron tomography Twinning Liquid melt processing Mechanical property

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Bio-Inspired Microwave Modulator for High-Temperature Electromagnetic Protection,Infrared Stealth and Operating Temperature Monitoring

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Nano-Micro Letters 2022年第2期14卷 124-135页

作者： Xuan Yang Yuping Duan Shuqing Li Huifang Pang Lingxi Huang Yuanyuan Fu Tongmin Wang Key Laboratory of Solidification Control and Digital Preparation Technology(Liaoning Province) School of Materials Science and EngineeringDalian University of TechnologyDalian 116085People’s Republic of China Science and Technology On Power Beam Processes Laboratory AVIC Manufacturing Technology InstituteBeijing 100024People’s Republic of China

High-temperature electromagnetic(EM) protection materials integrated of multiple EM protection mechanisms and functions are regarded as desirable candidates for solving EM interference over a wide temperature *** this work,a novel microwave modulator is fabricated by introducing carbonyl iron particles(CIP)/resin into channels of carbonized wood(C-wood).Innovatively,the spaced arrangement of two microwave absorbents not only achieves a synergistic enhancement of magnetic and dielectric losses,but also breaks the translational invariance of EM characteristics in the horizontal direction to obtain multiple phase discontinuities in the frequency range of 8.2-18.0 GHz achieving modulation of reflected wave radiation ***,CIP/C-wood microwave modulator demonstrates the maximum effective bandwidth of 5.2 GHz and the maximum EM protection efficiency over 97% with a thickness of only 1.5 mm in the temperature range 298-673 ***,CIP/C-wood microwave modulator shows stable and low thermal conductivities,as well as monotonic electrical conductivity-temperature characteristics,therefore it can also achieve thermal infrared stealth and working temperature monitoring in wide temperature *** work provides an inspiration for the design of high-temperature EM protection materials with multiple EM protection mechanisms and functions.

关键词： Microwave modulator Electromagnetic protection High temperatures Temperature monitoring Carbonized wood

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Microstructure Design of High-Entropy Alloys Through a Multistage Mechanical Alloying Strategy for Temperature-Stable Megahertz Electromagnetic Absorption

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Nano-Micro Letters 2022年第9期14卷 49-62页

作者： Xiaoji Liu Yuping Duan Yuan Guo Huifang Pang Zerui Li Xingyang Sun Tongmin Wang Key Laboratory of Solidification Control and Digital Preparation Technology School of Materials Science and EngineeringDalian University of TechnologyDalianLiaoning 116085People’s Republic of China School of Physics Dalian University of TechnologyDalianLiaoning 116024People’s Republic of China

Developing megahertz(MHz)electromagnetic wave(EMW)absorption materials with broadband absorption,multi-temperature adaptability,and facile preparation method remains a ***,nanocrystalline FeCoNiCr_(0.4)Cu_(0.2) high-entropy alloy powders(HEAs)with both large aspect ratios and thin intergranular amorphous layers are constructed by a multistage mechanical alloying strategy,aiming to achieve excellent and temperature-stable permeability and EMW absorption.A single-phase face-centered cubic structure with good ductility and high crystallinity is obtained as wet milling precursors,via precisely controlling dry milling ***,HEAs are flattened to improve aspect ratios by synergistically regulating wet milling ***_(0.4)Cu_(0.2) HEAs with dry milling 20 h and wet milling 5 h(D20)exhibit higher and more stable permeability because of larger aspect ratios and thinner intergranular amorphous *** maximum reflection loss(RL)of D20/SiO_(2) composites is greater than-7 dB with 5 mm thickness,and EMW absorption bandwidth(RL<-7 dB)can maintain between 523 and 600 MHz from-50 to 150℃.Furthermore,relying on the“cocktail effect”of HEAs,D20 sample also exhibits excellent corrosion resistance and high Curie *** work provides a facile and tunable strategy to design MHz electromagnetic absorbers with temperature stability,broadband,and resistance to harsh environments.

关键词： Electromagnetic wave absorption Multistage mechanical alloying High-entropy alloys Temperature-stable Corrosion resistance

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GO/MgO/Mg interface mediated strengthening and electromagnetic interference shielding in AZ31 composite

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Journal of Magnesium and Alloys 2023年第10期11卷 3800-3814页

作者： Z.Y.Xu C.F.Fang C.J.Li R.Wang X.P.Zhang J.Tan Y.M.Wang Key Laboratory of Solidification Control and Digital Preparation Technology(Liaoning Province) School of Materials Science and EngineeringDalian University of TechnologyDalian 116024China Faculty of Materials Science and Engineering Kunming University of Science and TechnologyKunming 650093China College of Materials Science and Engineering Chongqing UniversityChongqing 400045China Key Laboratory of Materials Modification by Laser Ion and Electron Beams(Ministry of Education)School of Materials Science and EngineeringDalian University of TechnologyDalian 116023China

More requirements of electromagnetic interference(EMI) shielding performance are put forward for lightweight structural materials due to the development of aerospace and 5G communications. Herein, graphene oxide(GO) decorated with SnO_(2) coating is introduced as reinforcement into AZ31 Mg alloy. During the smelting process, the MgO layer is in situ gernerated at interface between GO and the molten Mg alloy matrix by consuming SnO_(2). In the solid state, such kind of interface structure can improve the GO-Mg interface bonding intensity,also significantly generate stacking faults. The AZ31 composite reinfoced by trace modified GO(0.1 wt%) exhibits high ultimate strength and almost the same elongation with AZ31 alloy. Compared with AZ31 alloy, the yield strength and ultimate tensile strength of composite are increased by 33.5% and 23.7%, respectively. Meanwhile, the multi-level electromagnetic reflection from the multi-layer structure of GO and the interface polarization caused by the MgO mid-layer can significantly improve EMI shielding performance. The appropriate interface design strategy achieves the effect of “two birds with one stone”.

关键词： Metal-matrix composites Mechanical properties EMI shielding Microstructures

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