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Microstructure and wear resistance of AlCrFeNiMo_(0.5)Si_(x) high-entropy alloy coatings prepared by laser cladding

China Foundry 2022年第6期19卷 473-480页

作者： Xiao-cong Li Hui Liang Yan-zhou Zhao Li Gao Li Jiang Zhi-qiang Cao Key Laboratory of Solidification Control and Digital Preparation Technology(Liaoning Province) School of Materials Science and EngineeringDalian University of TechnologyDalian 116024LiaoningChina School of Physics and Electronic Technology Liaoning Normal UniversityDalian 116029LiaoningChina

In recent years,the coating prepared by laser cladding has attracted much attention in the field of wear *** this work,AlCrFeNiMo_(0.5)Si_(x)(x=0,0.5,1.0,1.5,2.0)high-entropy alloy coatings were designed and prepared on Q235 steel by laser *** effect of Si content on microstructure,microhardness and wear resistance of the coatings was studied in *** results indicate that the AlCrFeNiMo_(0.5)Si_(x) highentropy alloy coatings show an excellent bonding between substrate and the cladding *** AlCrFeNiMo_(0.5)Si_(x) coatings are composed of nano-precipitated phase with BCC structure and matrix with ordered B2 *** the addition of Si,the white phase(Cr,Mo)_(3)Si with cubic structure appears in the interdendritic,and the morphology of the coating(x=2.0)transforms into lamellar eutectic-like *** addition of Si enhances the microhardness and significantly improves the wear resistance of the *** x increases from 0 to 2.0,the average hardness of the cladding zone increases from 632 HV to 835 HV,and the wear rate decreases from 1.64×10^(-5) mm^(3)·(N·m)^(-1) to 5.13×10^(-6) mm^(3)·(N·m)^(-1).When x≥1.5,the decreasing trend of the wear rate gradually slows *** wear rates of Si1.5 and Si2.0 coatings are 5.85×10^(-6) mm^(3)·(N·m)^(-1) and 5.13×10^(-6) mm^(3)·(N·m)^(-1),respectively,which is an order of magnitude lower than that of Q235 steel.

关键词： high-entropy alloy coatings laser cladding microstructure wear resistance

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High thermoelectric properties of Cu_(2)TeeAg_(2)Te composite with Fe addition and non-stoichiometric Te

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Journal of Materiomics 2024年第1期10卷 37-44页

作者： Wenxiu Li Su Dun Bin Xiao Jun Wang Xinba Yaer Chun Ying Ye Li Xiaohuan Wang Huijun Kang School of Materials Science and Engineering Inner Mongolia University of TechnologyHohhot010051China Research and Development Center HUA Cloud Intelligent Healthcare Co.LtdShenzhen518000China College of Sciences Inner Mongolia University of TechnologyHohhot010051China Key Laboratory of Solidification Control and Digital Preparation Technology(Liaoning Province) School of Materials Science and EngineeringDalian University of TechnologyDalian116024China

Cu_(2)Te-based materials are a type of superionic conductor belonging to the class of phonon-liquid elec-tron-crystal materials and have achieved high ZT values by doping and ***,it is easy to form copper vacancies in Cu_(2)Te which leads to an excessive carrier concentration and then results in a low Seebeck ***,controlling copper ion migration and optimizing carrier concen-tration is essential to improve the thermoelectric performance of Cu_(2)*** paper reports high-performance Cu_(2)TeeAg_(2)Te composite with high application value in the low-middle temperature re-gion,which is achieved by fine tuning the carrier concentration using Fe addition and non-stoichiometric Te,as well as controlling the thermal conductivity of composite.A high ZT of~1.2 is obtained in AgCu_(0.97)Fe_(0.03)Te_(0.96)at a low temperature of 573 ***,the phase transition mechanism of Cu_(2)TeeAg_(2)Te and its effect on the thermoelectric transport performance are revealed that go beyond nanostructuring and single-doping,which provides a strong theoretical basis for research and perfor-mance improvement of thermoelectric materials in this system.

关键词： Thermoelectric AgCuTe Fe addition Non-stoichiometric Te

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Maximizing the scattering of multiwavelength phonons in novel biphasic high-entropy ZrCoSb-based half-Heusler alloys

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Journal of Materiomics 2024年第1期10卷 45-56页

作者： Rongchun Chen Yu Yan Guangshu Li Ruonan Min Huijun Kang Enyu Guo Zongning Chen Xiong Yang Tongmin Wang Key Laboratory of Solidification Control and Digital Preparation Technology(Liaoning Province) School of Materials Science and EngineeringDalian University of TechnologyDalian116024China Ningbo Institute of Dalian University of Technology Ningbo315000China

The thermoelectric(TE)performance of p-type ZrCoSb-based half-Heusler(HH)alloys has been improved tremendously in recent years;however,it remains challenging to find suitable n-type ZrCoSb-based HH alloys due to their high lattice thermal conductivity(κ_(L)).In this work,n-type Zr_(1−x)Ta_(x)Co_(1−x)Ni_(x)Sb HH alloys were firstly designed by multisite *** evolution of the Raman peak proved that alloy scattering,phonon softening,anharmonicity,entropy-driven disorder,and precipitates had a combined effect on decreasingκ_(L)by 46.7%compared to that of pristine ***,Hf_(0.75)Zr_(0.25)NiSn_(0.99)Sb_(0.01)was introduced into Zr_(0.88)Ta_(0.12)Co_(0.88)Ni_(0.12)Sb to further suppressκ_(L).Remarkably,the grain size of the biphasic HH alloys was refined by at least one order of magnitude.A biphasic high-entropy HH alloy with y=0.2 exhibited the minimumκ_(L)of∼2.44 W/(m·K)at 923 K,reducing by 67.7%compared to that of ***,(Zr_(0.88)Ta_(0.12)Co_(0.88)Ni_(0.12)Sb)_(0.9)(Hf_(0.75)Zr_(0.25)NiSn_(0.99)Sb_(0.01))_(0.1)exhibited the highest TE figure of merit(∼0.38)at 923 *** cooperation between the entropy and biphasic microstructure resulted in multiscale defects,refined grains,and biphasic interfaces,which maximized the scattering of the multiwavelength phonons in HH *** work provides a new strategy for further reducing the grain size andκ_(L)of medium-and high-entropy HH alloys.

关键词： Biphasic half-Heusler alloys Thermoelectric properties Entropy engineering Multiscale defects

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Direct synthesis of Fe-Si-B-C-Cu nanocrystalline alloys with superior soft magnetic properties and ductile by melt-spinning

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Journal of Materials Science & technology 2022年第13期108卷 186-195页

作者： Xingjie Jia Bojun Zhang Wei Zhang Yaqiang Dong Jiawei Li Aina He Run-Wei Li Zhejiang Province Key Laboratory of Magnetic Materials and Application Technology CAS Key Laboratory of Magnetic Materials and DevicesNingbo Institute of Materials Technology&EngineeringChinese Academy of SciencesNingbo 315201China Key Laboratory of Solidification Control and Digital Preparation Technology(Liaoning Province) School of Materials Science and EngineeringDalian University of TechnologyDalian 116024China University of Chinese Academy of Sciences Beijing 100049China

Structure,magnetic properties and ductile of melt-spun Fe_(83-x)Si_(4)B_(13-y)C_(y)Cu_(x)(x=0-1.7;y=0-8)alloys were *** addition of 1.7 at.%Cu in a Fe_(83)Si_(4)B_(13) amorphous alloy generates abundantα-Fe crystals by providing nucleation sites,and further C doping promotes the growth of the crystals by suitable turning amorphous-forming ability,hence they increase saturation magnetic flux density(B_(s))and slightly worse magnetic softness of the as-spun *** as-spun Fe_(81.3)Si_(4)B_(7)C_(6)Cu_(1.7) alloy possesses a combined structure of a fully amorphous layer in wheel side surface and predominating nanocrystalline structure with gradually enlargedα-Fe crystal,whose average size and volume fraction are determined as about 12 nm and 32%,respectively,therefore superior soft magnetic properties and ductile with a high B_(s)of 1.74 T,coercivity(H_(c))of 32.7 A/m,effective permeability(μ_(e),at 1 kHz)of 3200 and high relatively strain at fracture(ε_(f))of 3.61%can be achieved directly in this alloy by only using *** annealing at 578 K releases internal stress,promotes the growth of theα-Fe crystals and remains the amorphous layer of the Fe_(81.3)Si_(4)B_(7)C_(6)Cu_(1.7) alloy,then improves the soft magnetic properties and maintains the superior ductile with increasing the B_(s)andμ_(e)to 1.80 T and 14,100,respectively,lowering the H_(c)to9.4 A/m and slightly reducing theε_(f)to 2.39%.The combination of superior soft magnetic properties and ductile and simplified synthesis process entitles the Fe-Si-B-C-Cu nanocrystalline alloys great potentials in high performance electromagnetic applications.

关键词： Fe-based nanocrystalline alloys High saturation magnetic flux density Direct synthesis Melt-spinning Ductile

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Effect of secondary phases on corrosion behavior of Mg−7Sn−1Zn−1Y alloys

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Transactions of Nonferrous Metals Society of China 2025年第2期35卷 446-459页

作者： Xue-jian WANG Hua-qiang XIAO Chong WANG En-yu GUO Tong-min WANG Bo LIN School of Mechanical Engineering Guizhou UniversityGuiyang 550000China Key Laboratory of Solidification Control and Digital Preparation Technology(Liaoning Province) School of Materials Science and EngineeringDalian University of TechnologyDalian 116024China Ningbo Institute of Dalian University of Technology Ningbo 315000China

Microstructural characterization,mass loss tests,hydrogen evolution tests,electrochemical measurements,and corrosion morphology observations were conducted to investigate the effect of the secondary phases on the corrosion behavior of the as-cast Mg−7Sn−1Zn−1Y(TZW711)alloy after solution treatment(T4)and aging treatment(T6).The results show that the T4-TZW711 alloy possesses the highest corrosion resistance in the early corrosion *** is because the dissolution of Mg2Sn reduces the cathodic current density and increases the charge transfer resistance(Rct).When the corrosion time is prolonged,the undissolved and clustered MgSnY phase will peel off from the T4-TZW711 alloy surface,thereby increasing the corrosion rate of the *** aging treatment,the undissolved MgSnY phase is dispersed,which results in a lower localized corrosion sensitivity of T6-TZW711 alloy than that of the T4-TZW711 alloy,suggesting that the T6 treatment can enhance the corrosion resistance of Mg−7Sn−1Zn−1Y alloys.

关键词： Mg−Sn−Zn−Y alloy heat treatment MgSnY phase electrochemical test corrosion behavior

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Excellent strength-ductility combination of Cr_(26)Mn_(20)Fe_(20)Co20Ni_(14) high-entropy alloy at cryogenic temperatures

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Journal of Materials Science & technology 2023年第23期154卷 166-177页

作者： Xuzhou Gao Wei Jiang Yiping Lu Zhigang Ding Jizi Liu Wei Liu Gang Sha Tongming Wang Tingju Li Isaac T.H.Chang Yonghao Zhao Nano and Heterogeneous Materials Center School of Materials Science and Engineering Nanjing University of Science and Technology Nanjing 210094 China Key Laboratory of Solidification Control and Digital Preparation Technology (Liaoning Province) School of Materials Science and Engineering Dalian University of Technology Dalian 116024 China Herbert Gleiter Institute of Nanoscience Nanjing University of Science and Technology Nanjing 210094 China Metallurgy and Head of Liquid Metal Engineering (LiME) Doctoral Training Centre Brunel Centre for Advanced Solidification Technology (BCAST) Brunel University London Uxbridge UB8 3PH UK

In the present study,a face-centered cubic non-equiatomic Cr_(26)Mn_(20)Fe_(20)Co20Ni_(14) high-entropy alloy(HEA)with a low stacking fault energy of 17.6 mJ m^(−2) was prepared by vacuum induction melting,forging and annealing *** recrystallized sample is revealed to exhibit an excellent combination of strength and ductility over a wide temperature range of 4.2–293 *** decreasing temperature from 293 to 77 K,the ductility and ultimate tensile strength(UTS)gradually increase by 30% to 95% and 137% to 1020 MPa,*** the lowest temperature of 4.2 K,the ductility keeps 65% and the UTS increases by 200% to 1300 MPa,which exceed those published in the literature,including conventional 300 series stainless *** microstructural analyses of this alloy reveal a change of deformation mechanisms from dislocation slip and nano-twinning at 293 K to nano-phase transformation at 4.2 *** cooperation and competition of multiple nano-twinning and nano-phase transformation are responsible for the superior tensile properties at cryogenic *** study provides experimental evidence for potential cryogenic applications of HEAs.

关键词： High-entropy alloys Strength and ductility Cryogenic temperature Twinning Phase transformation

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Effect of microstructure evolution on wear resistance of equal molar CoCrFeNi high-entropy alloy

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Rare Metals 2023年第11期42卷 3797-3805页

作者： Hai-Tao Zhang Cheng-Lin Wang Jun-Wei Miao Shu-Yan Shi Ting-Ju Li Hong-Wei Yan Yong-An Zhang Yi-Ping Lu Key Laboratory of Solidification Control and Digital Preparation Technology(Liaoning Province) School of Materials Science and EngineeringDalian University of TechnologyDalian116024China Engineering Research Center of High Entropy Alloy Materials(Liaoning Province) School of Materials Science and EngineeringDalian University of TechnologyDalian116024China Key Laboratory for Light-Weight Materials Nanjing Technology UniversityNanjing210009China State Key Laboratory of Nonferrous Metals and Processes GRINM Group Co.Ltd.Beijing100088China General Research Institute for Nonferrous Metals Beijing100088China

Face-centered-cubic high-entropy alloys have excellent ductility and great potential for engineering ***,few studies have reported on the wear behavior under different *** study aimed to investigate the tribological behavior of CoCrFeNi highentropy alloy under different *** wear rate increased with the load,and the main wear behavior was abrasive *** cross-sectional microstructure of worn surface consisted of oxide,nanocrystalline,nanolaminated,and deformation *** the higher loads,the deformation mechanism included dislocation slip and deformation twins,and shear bands also *** was unexpectedly found that the wear rate increased sharply under high load,which was attributed to the formation of shear bands and microcracks in the nanocrystalline *** results successfully revealed the great influence of microstructure evolution on the wear rate,providing theoretical guidance for improving the wear resistance of face-centered-cubic high-entropy alloys in the future.

关键词： High-entropy alloys(HEAs) Microstructure evolution Wear mechanism Shear bands

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Thermo-driven oleogel-based self-healing slippery surface behaving superior corrosion inhibition to Mg-Li alloy

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Journal of Magnesium and Alloys 2023年第12期11卷 4710-4723页

作者： Yibo Ouyang Huijun Kang Enyu Guo Ri Qiu Keqiang Su Zongning Chen Tongmin Wang Key Laboratory of Solidification Control and Digital Preparation Technology(Liaoning Province) School of Materials Science and EngineeringDalian University of TechnologyDalian 116024PR China Ningbo Institute of Dalian University of Technology Ningbo 315000PR China College of Safety and Environmental Engineering Shandong University of Science and TechnologyQingdao 266590PR China State Key Laboratory for Marine Corrosion and Protection Luoyang Ship Material Research InstituteQingdao 266101PR China Institute of Yellow River Delta Earth Surface Processes and Ecological Integrity Shandong University of Science and TechnologyPR China

Bioinspired by Nepenthes, lubricant infused surfaces(LIS) have attracted widespread attention in the field of anticorrosion. However,the lubricant coating has some disadvantages such as complex construction processing and easy loss of oil phase in air or dynamic water phase. In this study, oleogel is infused into a lotus leaf inspired super-hydrophobic matrix to form an oleogel infused surface(OIS) for enhancing corrosion resistance of active Mg-Li alloy. For reserving oleogel, firstly, a facile one-step electrodeposition method is used to construct super-hydrophobic surface(SHS) composed by samarium/myristic acid complex micro-nano flower structure onto Mg-Li *** coating exhibits excellent superhydrophobic property at a static contact angle of 160° by applying 30 V electrolysis for 30 min. The protection efficiency of single SHS highly relates with the metal itself. For short period immersion in water phase, SHS can afford protection to Mg-Li alloy. However, the long-term immersion will see the rapid failure of SHS, and the high activity of Mg-Li alloy is one main *** assume that SHS cannot be a good choice for protecting Mg-Li alloy. Then, a Nepenthes inspired liquid coating is formed by infusing oleogel into the micro-nano structure by a spin-coating method. The liquid coating performs prominent corrosion resistance with Rctreaching as high as 1.51 × 10^(10)Ω cm^(2). After the mechanical damage from the external environment, the liquid coating can realize self-repair through thermal assistance, and the liquid coating can still restore Rctup to 1.24 × 10^(10)Ω cm^(2) after healing. The corrosion resistance of the liquid coating remains strong by showing Rctas high as 1.14 × 10^(9)Ω cm^(2), even after immersion in representative corrosive 3.5 wt% Na Cl solution for 30 d.

关键词： Mg-Li alloy Oleogel Superhydrophobic Self-healing Corrosion

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Antibacterial activities of a novel Cu-bearing high-entropy alloy against multi-drug-resistant Acinetobacter baumannii and Staphylococcus aureus

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Rare Metals 2022年第2期41卷 570-579页

作者： En-Ze Zhou Guang-Yu Ren Yun-Ling Sun Yong-Qiang Fan Yi Yang Ming-Yue Sun Da-Ke Xu Yi-Ping Lu Jian-Jun Wang Hua-Bing Li Fu-Hui Wang Shenyang National Laboratory for Materials Science Key Laboratory for Anisotrotropy and Texture of Materials(Ministry of Education)School of Materials Science and EngineeringNortheastern UniversityShenyang 110819China Key Laboratory of Solidification Control and Digital Preparation Technology(Liaoning Province) School of Materials Science and EngineeringDalian University of TechnologyDalian 116024China General Hospital of Northern Theater Command Shenyang 110819China School of Metallurgy Northeastern UniversityShenyang 110819China

Acinetobacter baumannii and methicillin-resistant Staphylococcus aureus(MRSA)are two prevalent pathogens and have developed high resistant to most ***,it is a pressing need to develop a new method to inhibit the spread of drug-resistant *** containing high-entropy alloy(HEA,Al0.4CoCr-CuFeNi)is a new kind of alloy material,which shows extensive antibacterial activity and mechanical properties in our previous *** study further develops another HEA(CoCrCuFeNi)and evaluates its resistance against gram-negative *** and Gram-positive *** antibacterial tests show that the antibacterial rate of the HEA toward both bacteria reached nearly 99%,far better than the traditional copper-bearing 304 stainless steel(304 Cu-SS).The biofilm observation shows that the HEA could not only kill the planktonic bacteria,but also effectively inhibit the formation of *** data demonstrate that CoCrCuFeNi HEA possesses effective antibacterial and antibiofilm activities,making it a potential candidate for using in hospital,food industry,and domestic kitchens.

关键词： High-entropy alloy Acinetobacter baumannii Methicillin-resistant Staphylococcus aureus(MRSA) Antibacterial activity Antibiofilm activity

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Microwave absorption performance of FeCoNiAlCr_(0.9)alloy powders by adjusting the amount of process control agent

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Journal of Materials Science & technology 2021年第18期77卷 209-216页

作者： Yuping Duan Huifang Pang Xin Wen Xuefeng Zhang Tongmin Wang Key Laboratory of Solidification Control and Digital Preparation Technology(Liaoning Province) School of Materials Science and EngineeringDalian University of TechnologyDalian 116085China Innovative Center for Advanced Materials Hangzhou Dianzi UniversityHangzhou 310018China

Different amounts of absolute ethanol(0-50 mL)are used as process control agents(PCA)to prepare FeCoNiAlCr0.9 high entropy alloy(HEA)powders via 90 h ball *** results show that the increased amount of PCA plays an active role in the crystallinity of powders,and regulate the thickness and size distribution of flake *** the volume of PCA increases,the real and imaginary parts(ε′andε″)of complex permittivity get increased by the enhancement of the interface polarization and surface polarization,while the increase in the real and imaginary parts(μ′andμ″)of complex permeability arises from the increased anisotropic *** addition of PCA not only promotes the reflection loss but also extends the effective bandwidth(up to 4.28 GHz).Here,the performance adjustment of HEA electromagnetic absorber is realized by forthrightly changing the process parameters of ball milling.

关键词： FeCoNiAlCr_(0.9) Ball milling Electromagnetic performance Process control agent

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