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Flexible, self-cleaning, and high-performance ceramic nanofiber-based moist-electric generator enabled by interfacial engineering

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science China(Technological sciences) 2022年第2期65卷 450-457页

作者： WANG LiMing FENG LanLan SUN Zhao Yang HE XinYang WANG RongWu QIN XiaoHong YU JianYong Key Laboratory of Textile Science&Technology Ministry of EducationCollege of TextilesDonghua UniversityShanghai 201620China Innovation Center for Textile Science and Technology Donghua UniversityShanghai 201620China

Due to their long-term stability, even under extreme conditions, oxide ceramics have attracted significant attention in emerging fields like moist-electric generation. However, the inherent brittleness and low voltage output of oxide ceramic-based moistelectric generators(MEGs) limit their applications in wearable electronics. Herein, a facile strategy involving the combination of sol-gel electrospinning and calcination is used to fabricate flexible and freestanding Ti O_(2)/Zr O_(2)(TZ) composite nanofiber-based MEGs. The excellent flexibility of the TZ nanofiber membranes can be attributed to the suppression of their crystal structure transformation, dispersion of stress concentration, and reduction of crack propagation via interfacial engineering. The porous structure of the electrospun nanofiber membrane features an abundance of charged narrow channels for the diffusion of water molecules and generates a streaming potential. The optimal voltage output reached ~0.8 V, which is the highest value reported for an oxide ceramic-based MEG. Furthermore, the as-fabricated nanofiber-based MEG exhibits good self-cleaning capability to degrade organic pollutants under ultraviolet irradiation. By integrating mechanical flexibility, high performance, and a selfcleaning effect, this work presents a new idea for exploring diverse, efficient, and wearable oxide ceramic-based MEGs.

关键词： moist-electric generation ceramic nanofiber electrospinning flexible self-cleaning

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Reconfiguration and self-healing integrated Janus electrospinning nanofiber membranes for durable seawater desalination

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Nano Research 2023年第1期16卷 489-495页

作者： Huijie Liu Jiatai Gu Ye Liu Lei Yang Liming Wang Jianyong Yu Xiaohong Qin Key Laboratory of Textile Science&Technology of Ministry of Education College of TextilesDonghua UniversityShanghai 201620China State Key Laboratory for Modification of Chemical Fibers and Polymer Materials International Joint Laboratory for Advanced Fiber and Lowdimension MaterialsCollege of Materials Science and EngineeringDonghua UniversityShanghai 201620China Innovation Center for Textile Science and Technology Donghua UniversityShanghai 201620China

Janus electrospinning nanofiber membranes have attracted extensive attention in the fields such as solar-driven interfacial desalination,liquid filtration,and waterproof and breathable ***,the Janus structures suffer from weak interfacial bonding and vulnerability to damage,making the durability and sustainability are highly sought after in real-word ***,we fabricate the simply reconfigurable and entirely self-healing Janus evaporator by electrospinning polypropylene glycol based polyurethane(PPG@PU)and polydimethylsiloxane based polyurethane-CNTs(PDMS@PU-CNTs)with different wettability,which are both designed based on dynamic Diels–Alder(DA)*** interface of the Janus membrane is stitched by the covalent bonds to directly improve the interface adhesion to 22 N·m−1,constructing an integrated evaporator,and thereby achieving a stable desalination rate of 1.34 kg·m−2·h−1 under one *** dissociation of DA networks allows the evaporators for self-healing and reconfiguration abilities,after which the photothermal performance is *** is the first work for the crosslinked self-healing polymer to be directly electrospun,achieving the improved interfacial bond and reconfiguration of entire evaporators,which presented promising new design principles and materials for interfacial solar seawater desalination.

关键词： Janus nanofiber membrane electrospinning interfacial bonding solar steam generation seawater desalination

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Bioconversion of lignocellulosic biomass into bacterial nanocellulose:challenges and perspectives

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Green Chemical Engineering 2023年第2期4卷 160-172页

作者： Wenchao Li Yuqing Shen Huan Liu Xinxin Huang Bin Xu Cheng Zhong Shiru Jia State Key Laboratory of Food Nutrition&Safety Tianjin University of Science&Technology300457TianjinChina Key Laboratory of Industrial Fermentation Microbiology(Ministry of Education) Tianjin University of Science&Technology300457TianjinChina

Nanocellulose has various outstanding properties and great potential for replacing petrochemical *** utilization of lignocellulose to produce nanocellulose is of great significance to the sustainable development of the economy and ***,the direct extraction of nanocellulose from lignocellulose by chemical method is challenged by toxic chemicals utilization,energy and time consumption,and waste water ***,this paper addressed the conversion of lignocellulosic biomass into bacterial nanocellulose(BNC)by the biological ***,this article highlights the recent advances in potentials and challenges of lignocellulosic biomass for BNC production through the bioconversion process,including biomass pretreatment,enzymatic hydrolysis,glucose and xylose fermentation,GA accumulation,and inhibitor *** development in metabolic and evolutionary engineering to enhance the production capacity of BNC-producing strain is also *** is expected to provide guidance on the effective bioproduction of nanocellulose from lignocellulosic biomass.

关键词： Bioconversion Lignocellulose Bacterial nanocellulose Pretreatment Fermentation

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Ultra-broadband microwave absorber and high-performance pressure sensor based on aramid nanofiber,polypyrrole and nickel porous aerogel

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International Journal of Minerals,Metallurgy and Materials 2024年第8期31卷 1912-1921页

作者： Leyi Zhang Hongyu Jin Hanxin Liao Rao Zhang Bochong Wang Jianyong Xiang Congpu Mu Kun Zhai Tianyu Xue Fusheng Wen State Key Laboratory of Metastable Materials Science&Technology Yanshan UniversityQinhuangdao 066004China Key Laboratory for Microstructural Material Physics of Hebei Province School of ScienceYanshan UniversityQinhuangdao 066004China

Electronic devices have become ubiquitous in our daily lives,leading to a surge in the use of microwave absorbers and wearable sensor devices across various sectors.A prime example of this trend is the aramid nanofibers/polypyrrole/nickel(APN)aerogels,which serve dual roles as both microwave absorbers and pressure *** this work,we focused on the preparation of aramid nanofibers/polypyrrole(AP15)aerogels,where the mass ratio of aramid nanofibers to pyrrole was 1:*** employed the oxidative polymerization method for the preparation *** this,nickel was thermally evaporated onto the surface of the AP15 aerogels,resulting in the creation of an ultralight(9.35 mg·cm^(-3)).This aerogel exhibited a porous *** introduction of nickel into the aerogel aimed to enhance magnetic loss and adjust impedance matching,thereby improving electromagnetic wave absorption *** minimum reflection loss value achieved was-48.7 dB,and the maximum effective absorption bandwidth spanned 8.42 GHz with a thickness of 2.9 *** impressive metrics can be attributed to the three-dimensional network porous structure of the aerogel and perfect impedance ***,the use of aramid nanofibers and a three-dimensional hole structure endowed the APN aerogels with good insulation,flame-retardant properties,and compression *** under a compression strain of 50%,the aerogel maintained its resilience over 500 *** incorporation of polypyrrole and nickel particles further enhanced the conductivity of the ***,the final APN aerogel sensor demonstrated high sensitivity(10.78 kPa-1)and thermal *** conclusion,the APN aerogels hold significant promise as ultra-broadband microwave absorbers and pressure sensors.

关键词： porous aerogel aramid nanofibers microwave absorbers pressure sensor porous structure

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Design and simulation of a silicon-based hybrid integrated optical gyroscope system

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Chinese Physics B 2023年第4期32卷 397-404页

作者：孙道鑫张东亮鹿利单徐涛郑显通周哲海祝连庆 Key Laboratory of the Ministry of Education for Optoelectronic Measurement Technology and Instrument Beijing Information Science&Technology UniversityBeijing 100192China Beijing Laboratory of Optical Fiber Sensing and System Beijing Information Science&Technology UniversityBeijing 100016China

By combining a silicon-based lithium niobate modulator and a silicon-based Si3N4resonator with silicon-based photonics technology,a highly systematic design of a hybrid integrated optical gyroscope with enhanced reciprocity sensitivity and a dual micro-ring structure is proposed for the first time in this *** relationship between the device's structural parameters and optical performance is also analyzed by constructing a complete simulation link,which provides a theoretical design reference to improve the system's *** the wavelength is 1550 nm,the conversion frequency of the dual-ring optical path is 50 MHz,the coupling coefficient is 0.2,and the radius R is 1000μm,the quality factor of the silicon-based Si_(3)N_(4)resonator is 2.58×10^(5),which is 1.58 times that of the silicon-on-insulator ***,the effective number of times the light travels around the ring before leaving the micro-ring is 5.93,which is 1.62 times that of the silicon-on-insulator *** work fits the gyro dynamic output diagram,and solves the problem of low sensitivity at low speed by setting the phase *** results provide a basis for the further optimization of design and chip processing of the integrated optical gyroscope.

关键词： silicon photonics integrated optical gyroscope micro-ring resonator Sagnac effect

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Cu-Zn-based alloy/oxide interfaces for enhanced electroreduction of CO_(2) to C_(2+) products

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Journal of Energy Chemistry 2023年第8期83卷 90-97,I0004页

作者： Zi-Yang Zhang Hao Tian Lei Bian Shi-Ze Liu Yuan Liu Zhong-Li Wang Tianjin Key Laboratory of Applied Catalysis Science&Technology School of Chemical Engineering and TechnologyTianjin UniversityTianjin 300072China

The electrochemical CO_(2)reduction reaction to produce multi-carbon(C_(2+)) hydrocarbons or oxygenate compounds is a promising route to obtain a renewable fuel of high energy ***,producing C_(2+)at high current densities is still a ***,we develop a Cu-Zn alloy/Cu-Zn aluminate oxide composite electrocatalytic system for enhanced conversion of CO_(2)to C_(2+)*** Cu-Zn-Al-Layered Double Hydroxide(LDH) is used as a precursor to decompose into uniform Cu-Zn oxide/Cu-Zn aluminate *** electrochemical reduction,Cu-Zn oxide generates Cu-Zn alloy while Cu-Zn aluminate oxide remains *** alloy and oxide are closely stacked and arranged alternately,and the aluminate oxide induces the strong electron interaction of Cu,Zn and Al,creating a large number of highly active reaction interfaces composed of 0 to+3 valence metal *** the help of the interface effect,the optimized Cu_(9)Zn_(1)/Cu_(0.8)Zn_(0.2)Al_(2)O_(4)catalyst achieves a Faradaic efficiency of 88.5% for C_(2+)products at a current density of 400 mA cm^(-2)at-1.15 V versus reversible hydrogen *** in-situ Raman and attenuate total reflectance-infrared absorption spectroscopy(ATR-IRAS) spectra show that the aluminate oxide at the interface significantly enhances the adsorption and activation of CO_(2)and the dissociation of H2O and strengthens the adsorption of CO intermediates,and the alloy promotes the C-C coupling to produce C_(2+)*** work provides an efficient strategy to construct highly active reaction interfaces for industrial-scale electrochemical CO_(2)RR.

关键词： Electrochemical CO_(2)reduction reaction C_(2+)products Cu-Zn alloy Cu-Zn aluminate oxide Interface

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Evolution of Deformation Substructure and Mg_(x)Zn_(y)Ca_(z) Metastable Phase in Fine-Grained Mg Alloys

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Acta Metallurgica Sinica(English Letters) 2025年第1期38卷 71-85页

作者： Zhen-Liang Li Xin-Lei Zhang School of Materials Science and Engineering Inner Mongolia University of Science&TechnologyBaotou014010China Inner Mongolia Key Laboratory of New Metal Material Baotou014010China

The spray-deposition was used to produce billets of Mg-4Al-1.5Zn-3Ca-1Nd(A alloy)and Mg-13Al-3Zn-3Ca-1Nd(B alloy),and evolution of deformation substructure and Mg_(x)Zn_(y)Ca_(z)metastable phase in fine-grained(3μm)Mg alloys was investigated by scanning electron microscopy(SEM),transmission electron microscopy(TEM),X-ray diffraction(XRD),and electron backscattered diffraction(EBSD).It was found that different dislocation configurations were formed in A and B *** free dislocations(RFDs)and dislocation tangles were the ways to form deformation substructure in A alloy,no RFDs except dislocation tangles were found in B *** interaction between nano-scale second phase particles(nano-scale C15 andβ-Mg_(17)(Al,Zn)_(12)phase)and different dislocation configurations had a significant effect on the deformation substructures *** mass transfer of Mg_(x)Zn_(y)Ca_(z)metastable phases and the stacking order of stacking faults were conducive to the Mg-Nd-Zn typed long period stacking ordered(LPSO)phases ***-scale C15 phases,Mg-Nd-Zn typed LPSO phases,c/a ratio,β-Mg_(17)(Al,Zn)_(12)phases were the key factors influencing the formation of *** textures and grain boundary features(GB features)had a significant effect on *** non-basal textures were the main factor affecting k-value in A alloy,while the high-angle grain boundary(HAGB)was the main factor affecting k-value in B alloy.

关键词： Deformation substructures Metastable phase Textures k-value Fine-grained Mg alloys

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Impact of Annealing on the Melt Recrystallization of a-PDLA/α-PLLA Double-layered Films

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Chinese Journal of Polymer science 2024年第2期42卷 230-238,I0009页

作者： Yun-Peng Li Hao-Ran Shen Shao-Juan Wang Hao Zhang Jian Hu Rui Xin Xiao-Li Sun Shou-Ke Yan Key Laboratory of Rubber-Plastics Ministry of Education/Shandong Provincial Key Laboratory of Rubber-plasticsQingdao University of Science&TechnologyQingdao266042China State Key Laboratory of Chemical Resource Engineering Beijing University of Chemical TechnologyBeijing100029China

Poly(lactic acid)(PLA) as a bio-based polymer with biodegradability and biocompatibility has attracted much attention. To manipulate its properties for different applications, regulation of crystal structure and crystalline morphology becomes an attractive research topic. In this work, the structure evolution of layered samples containing an amorphous poly(D-lactide)(PDLA) layer and a crystalline poly(L-lactide)(PLLA)layer with highly oriented edge-on α lamellar crystals after annealing at 150 ℃ or/and after melt-recrystallization has been studied by AFM, FTIR,and TEM combined with electron diffraction. The results demonstrate that melt recrystallization of the as-prepared sample leads to the formation of abundant randomly oriented PLA stereo-complex(PLA SC) crystals. Annealing at 150 ℃ results in the formation of a small amount of oriented PLA SC crystals at the interface. These PLA SC crystals show great impact on the recrystallization behavior of sample after melting at 190 ℃ and then crystallizing at 90 ℃. First, they impede the mutual diffusion of the overlying PDLA and underlying PLLA, and thus reduce their stereocomplexation ability as manifested by the decreased amount of PLA SC crystals. Second, they act as substrate to initiate the epitaxial crystallization of the overlying PDLA and underlying PLLA, which ensures the production of a highly oriented structure of PDLA and PLLA after melt recrystallization again.

关键词： Poly(L-lactide) Poly(D-lactide) Double layer Stereocomplex

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Rational design of robust and transparent superrepellent surfaces for long-term marine antifouling

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science China(Technological sciences) 2024年第7期67卷 2031-2039页

作者： CHEN Hui WANG Zhi WANG DaHeng XIAO Feng FU Guang-En BU XueLing ZHAO Lei ZHANG Tao WU DaHeng PU JiBin The State Key Laboratory of Refractories and Metallurgy Wuhan University of Science&TechnologyWuhan 430081China Key Laboratory of Advanced Marine Materials Ningbo Institute of Materials Technology and EngineeringChinese Academy of SciencesNingbo 315201China

Superhydrophobic surfaces have demonstrated exceptional efficacy in combatting biofouling contaminations of optical devices and equipment in marine applications. However, the fabrication of highly transparent superhydrophobic materials remains a formidable challenge due to the inherent trade-off between surface roughness for superhydrophobicity and optical ***, we design a robust and transparent superhydrophobic coating(Si-POSS) embedded silica nanoparticles(200 nm) with fluorinated polyhedral oligomeric silsesquioxanes(F-POSS) and zinc pyrithione(ZPT). The Si-POSS coating exhibits excellent water repellence toward diverse liquids and optical transmittance exceeding 90% in the visible spectrum. Moreover, the Si-POSS coating sustains long-term anti-bacterial(> 99.11%) and anti-algal effects for over 30 days, accompanied by mechanical,chemical, and thermal stability. This research asserts that the Si-POSS coating with outstanding combined characteristics holds significant potential for marine applications, particularly in self-cleaning and antifouling endeavors.

关键词： superhydrophobic surface transparent marine antifouling nanoparticles

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Conductive fibers for biomedical applications

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Bioactive Materials 2023年第4期22卷 343-364页

作者： Leqian Wei Shasha Wang Mengqi Shan Yimeng Li Yongliang Wang Fujun Wang Lu Wang Jifu Mao Key Laboratory of Textile Science&Technology Ministry of EducationCollege of TextilesDonghua UniversityShanghai201620China Key Laboratory of Textile Industry for Biomedical Textile Materials and Technology Donghua UniversityShanghai201620China School of Health and Life Sciences University of Health and Rehabilitation SciencesQingdao CityShandong Province266071China

Bioelectricity has been stated as a key factor in regulating cell activity and tissue function in electroactive ***,various biomedical electronic constructs have been developed to interfere with cell behaviors to promote tissue regeneration,or to interface with cells or tissue/organ surfaces to acquire physiological status via electrical *** from the outstanding advantages of flexibility,structural diversity,customizable mechanical properties,and tunable distribution of conductive components,conductive fibers are able to avoid the damage-inducing mechanical mismatch between the construct and the biological environment,in return to ensure stable functioning of such constructs during physiological ***,this review starts by presenting current fabrication technologies of conductive fibers including wet spinning,microfluidic spinning,electrospinning and 3D printing as well as surface modification on fibers and fiber *** provide an update on the biomedical applications of conductive fibers and fiber assemblies,we further elaborate conductive fibrous constructs utilized in tissue engineering and regeneration,implantable healthcare bioelectronics,and wearable healthcare *** conclude,current challenges and future perspectives of biomedical electronic constructs built by conductive fibers are discussed.

关键词： Conductive fibers Conductive biomaterials Tissue repair Implantable bioelectronics Wearable bioelectronics

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