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arXiv 2024年

作者： Shao, Sen Chiu, Wei-Chi Hossain, Md Shafayat Hou, Tao Wang, Naizhou Belopolski, Ilya Zhao, Yilin Ni, Jinyang Zhang, Qi Li, Yongkai Liu, Jinjin Yahyavi, Mohammad Jin, Yuanjun Feng, Qiange Cui, Peiyuan Zhang, Cheng-Long Yao, Yugui Wang, Zhiwei Yin, Jia-Xin Xu, Su-Yang Ma, Qiong Gao, Wei-Bo Bansil, Arun Hasan, M. Zahid Chang, Guoqing Division of Physics and Applied Physics School of Physical and Mathematical Sciences Nanyang Technological University 21 Nanyang Link Singapore637371 Singapore Department of Physics Northeastern University BostonMA02115 United States Quantum Materials and Sensing Institute Northeastern University BurlingtonMA01803 United States Department of Physics Princeton University PrincetonNJ08544 United States Wako Saitama351-0198 Japan School of Physics Beijing Institute of Technology Beijing100081 China Beijing Key Lab of Nanophotonics and Ultrafine Optoelectronic Systems Beijing Institute of Technology Beijing100081 China Material Science Center Yangtze Delta Region Academy of Beijing Institute of Technology Jiaxing314011 China Department of Physics Southern University of Science and Technology Shenzhen Guangdong518055 China Beijing National Laboratory for Condensed Matter Physics Institute of Physics Chinese Academy of Sciences Beijing100190 China Department of Chemistry and Chemical Biology Harvard University CambridgeMA United States Department of Physics Boston College Chestnut HillMA United States CIFAR Azrieli Global Scholars program CIFAR Toronto Canada

Implementing and tuning chirality is fundamental in physics, chemistry, and material science. Chiral charge density waves (CDWs), where chirality arises from correlated charge orders, are attracting intense interest due to their exotic transport and optical properties. However, a general framework for predicting chiral CDW materials is lacking, primarily because the underlying mechanisms remain elusive. Here, we address this challenge by developing the first comprehensive predictive framework, systematically identifying chiral CDWmaterials via first-principles calculations. The key lies in the previously overlooked phase difference of the CDW Q-vectors between layers, which is linked to opposite collective atomic displacements across different layers. This phase difference induces a spiral arrangement of the Q-vectors, ultimately giving rise to a chiral structure in real space. We validate our framework by applying it to the kagome lattice AV3Sb5 (A = K, Rb, Cs), successfully predicting emergent structural chirality. To demonstrate the generality of our approach, we extend it to predict chiral CDWs in the triangular-lattice NbSe2. Beyond material predictions, our theory uncovers a universal and unprecedented Hall effect in chiral CDW materials, occurring without external magnetic fields or intrinsic magnetization. Our experiments on CsV3Sb5 confirm this prediction, observing a unique signature where the Hall conductivity's sign reverses when the input current is reversed, a phenomenon distinct from known Hall effects. Our findings elucidate the mechanisms behind chiral CDWs and open new avenues for discovering materials with unconventional quantum properties, with potential applications in next-generation electronic and spintronic devices. © 2024, CC BY.

关键词： Optical properties

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The effect of organic acid hydrolysis on the properties of nanocellulose from edamame husk (Glycine max (L.) merill)

Case Studies in Chemical and Environmental Engineering

引用

Case Studies in Chemical and Environmental Engineering 2025年 11卷

作者： Wahyudi, Muhammad Sapto Holilah Bahruji, Hasliza Prasetyoko, Didik Asranudin Pratama, Agus Wedi Indriani, Dina Wahyu Suryanegara, Lisman Faradilla, RH Fitri Mahardika, Melbi Wardani, Ratih Kusuma Piluharto, Bambang Knight, Victor Feizal Norrrahim, Mohd Nor Faiz Research Center for Biomass and Bioproducts National Research and Innovation Agency of Indonesia (BRIN) Cibinong Indonesia Research Collaboration Center for Nanocellulose BRIN-Andalas University Padang Indonesia Study Program of Chemistry Faculty of Science and Technology UIN Sunan Kalijaga Yogyakarta Indonesia Centre of Advanced Material and Energy Sciences Universiti Brunei Darussalam Jl. Tungku Link BE 1410 Brunei Darussalam Department of Chemistry Faculty of Science and Data Analytics Institut Teknologi Sepuluh Nopember Surabaya Indonesia Research Center for Applied Microbiology National Research and Innovation Agency (BRIN) Cibinong Indonesia Department of Biosystem Engineering Faculty of Agricultural Technology Universitas Brawijaya Jalan Veteran Malang Indonesia Department of Food Science and Technology Faculty of Agriculture Universitas Halu Oleo Kendari Indonesia Academy Pharmacy of Surabaya Ketintang Gayungan Surabaya 60231 Indonesia Department of Chemistry Faculty of Mathematics and Natural Sciences University of Jember Jember Indonesia Research Center for Chemical Defence Defence Research Institute Universiti Pertahanan Nasional Malaysia Kem Sungai Besi Kuala Lumpur 57000 Malaysia

The increasing demand for sustainable materials has highlighted nanocellulose as a promising candidate due to its exceptional mechanical strength, thermal stability, and superior barrier properties. These attributes enable its application in diverse fields, including packaging, biomedical devices, and nanocomposites. This study investigates the valorization of edamame bean husks, a byproduct of the globally consumed legume snack, as a sustainable feedstock for nanocellulose production. Cellulose was extracted from the husks via delignification and bleaching, followed by a green and facile acid hydrolysis method employing organic acids (maleic acid, lactic acid, citric acid, and formic acid) to produce nanocellulose. The resulting nanocellulose exhibited a fibrillar morphology with particle sizes ranging from 7.59 to 17.51 nm, depending on the acid used. X-ray diffraction analysis revealed a crystallinity index ranging from 63.49 % to 67.24 %. Notably, acid hydrolysis significantly enhanced the thermal stability of the nanocellulose compared to both the raw husk and isolated cellulose. These findings demonstrate the potential of edamame agricultural waste as a valuable resource for sustainable and eco-friendly nanocellulose production, contributing to a circular bioeconomy. © 2025 The Authors

关键词： Characterization Edamame husk waste Green synthesis Nanocellulose Organic acids

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Concurrent operando neutron imaging and diffraction analysis revealing spatial lithiation phase evolution in an ultra-thick graphite electrode

arXiv

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arXiv 2024年

作者： Strobl, Markus Baur, Monica E. Samothraktis, Stavros Malamud, Florencia Zhang, Xiaolong Tung, Patrick K.M. Schmidt, Søren Woracek, R. Lee, J. Kiyanagi, Ryoji Kuhn, Luise Theil Segev, Inbal Gavish Ein-Eli, Yair PSI Center for Neutron and Muon Sciences Villigen5232 Switzerland Niels Bohr Institut University of Copenhagen Denmark Department of Energy Conversion and Storage Technical University of Denmark Kongens LyngbyDK-2800 Denmark Research Technology Services [ResTech UNSW Sydney Kensington2052 Australia DMSC European Spallation Source Lyngby Denmark European Spallation Source P.O. Box 176 LundS - 221 00 Sweden J-PARC Center Japan Atomic Energy Agency Tokai319-1195 Japan Soreq Nuclear Research Center [SNRC Yavne Israel Department of Material Science and Engineering Technion Israel Institute of Technology Haifa3200003 Israel Grand Technion Energy Program [GTEP Technion Haifa3200003 Israel Israel National Institute for Energy Storage [INIES Technion Haifa3200003 Israel

Energy efficient, safe and reliable Li-ion batteries (LIBs) are required for a wide range of applications. Charging capabilities of thick electrodes still holding their stored high-energy is a most desirable characteristic in future advanced LIBs. The introduction of ultra-thick graphite anode meets limitations in internal electrode transport properties, leading to Li-ion gradients with detrimental consequences for battery cell performance and lifetime. Yet, there is a lack of experimental tools capable of providing a complete view of local processes and evolving gradients within such thick electrodes. Here, we introduce a multi-modal operando measurement approach, enabling quantitative spatio-temporal observations of Li concentrations and intercalation phases in ultra-thick, graphite electrodes. Neutron imaging and diffraction concurrently provide correlated information from the macroscopic scale of the cell and electrode down to the crystallographic scale portraying the intercalation and deintercalation processes. In particular, the evolving formation of the solid electrolyte interphase (SEI), observation of gradients in total lithium content, as well as in the formation of ordered LixC6 phases and trapped lithium have been mapped throughout the first charge-discharge cycle of the cell. Different lithiation stages co-exist during charging and discharging of an ultra-thick composite graphite-based electrode;delayed lithiation and delithiation processes are observed at the central region of the electrode, while the SEI formation, potential plating and dead lithium are predominantly found closer to the interface with the separator. The study furthermore emphasizes the potential of the method to study Li ion diffusion and the kinetics of lithiation phase formation in advanced ultra-thick electrodes. Specifically, the relation of dead Li and SEI formation to the different Li phase stages can be mapped. Copyright © 2024, The Authors. All rights reserved.

关键词： Solid electrolytes

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Electronic ratchet effect in a moiré system: signatures of excitonic ferroelectricity

arXiv

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arXiv 2023年

作者： Zheng, Zhiren Wang, Xueqiao Zhu, Ziyan Carr, Stephen Devakul, Trithep de la Barrera, Sergio Paul, Nisarga Huang, Zumeng Gao, Anyuan Zhang, Yang Bérubé, Damien Evancho, Kathryn Natasha Watanabe, Kenji Taniguchi, Takashi Fu, Liang Wang, Yao Xu, Su-Yang Kaxiras, Efthimios Jarillo-Herrero, Pablo Ma, Qiong Department of Physics Massachusetts Institute of Technology CambridgeMA United States Stanford Institute of Materials and Energy Science SLAC National Accelerator Laboratory Menlo ParkCA94025 United States Brown Theoretical Physics Center Department of Physics Brown University ProvidenceRI United States Department of Physics Boston College Chestnut HillMA United States Department of Chemistry and Chemical Biology Harvard University CambridgeMA United States Department of Physics and Astronomy Clemson University ClemsonSC United States Research Center for Functional Materials National Institute for Materials Science Tsukuba Japan International Center for Material Nanoarchitectonics National Institute for Materials Science Tsukuba Japan Department of Physics Harvard University CambridgeMA United States CIFAR Azrieli Global Scholars program CIFAR Toronto Canada

Electronic ferroelectricity represents a new paradigm where spontaneous symmetry breaking driven by electronic correlations, in contrast to traditional lattice-driven ferroelectricity, leads to the formation of electric dipoles. Despite the potential application advantages arising from its electronic nature, switchable electronic ferroelectricity remains exceedingly rare. Here, we report the discovery of an electronic ratchet effect that manifests itself as switchable electronic ferroelectricity in a layer-contrasting graphene-boron nitride moiré heterostructure. Our engineered layer-asymmetric moiré potential landscapes result in layer-polarized localized and itinerant electronic subsystems. At particular fillings of the localized subsystem, we find a ratcheting injection of itinerant carriers in a non-volatile manner, leading to a highly unusual ferroelectric response. Strikingly, the remnant polarization can be stabilized at multiple (quasi-continuous) states with behavior markedly distinct from known ferroelectrics. Our experimental observations, simulations, and theoretical analysis suggest that dipolar excitons are the driving force and elementary ferroelectric units in our system. This signifies a new type of electronic ferroelectricity where the formation of dipolar excitons with aligned moments generates a macroscopic polarization and leads to an electronically-driven ferroelectric response, which we term excitonic ferroelectricity. Such new ferroelectrics, driven by quantum objects like dipolar excitons, could pave the way to innovative quantum analog memory and synaptic devices. Copyright © 2023, The Authors. All rights reserved.

关键词： Ferroelectricity

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Terahertz Landau Polaritons in Nano-slots: Ultrastrong Coupling under Extreme Spatial Confinement

Terahertz Landau Polaritons in Nano-slots: Ultrastrong Coupl...

引用

International Conference on Infrared and Millimeter Waves

作者： Dasom Kim Sunghwan Kim Dukhyung Lee Shuang Liang Fuyang Tay Michael J. Manfra Dai-Sik Kim Junichiro Kono Department of Electrical and Computer Engineering Rice University Houston TX USA Applied Physics Graduate Program Smalley-Curl Institute Rice University Houston TX USA Department of Physics Long-wavelength Nanotechnology Laboratory and Quantum Photonics Institute Ulsan National Institute of Science and Technology (UNIST) Ulsan South Korea Department of Physics and Astronomy Purdue University West Lafayette IN USA Birck Nanotechnology Center Purdue University West Lafayette IN USA Elmore Family School of Electrical and Computer Engineering Purdue University West Lafayette IN USA School of Materials Engineering Purdue University West Lafayette IN USA Department of Physics and Astronomy Rice University Houston TX USA Department of Material Science and NanoEngineering Rice University Houston TX USA

We report ultrastrong coupling of the cyclotron resonance of a two-dimensional electron gas in a GaAs quantum well to terahertz cavity photons under extreme confinement to the nanometer scale. This was realized by an array of nano-slots fabricated close to the quantum well layer on the GaAs substrate. Our terahertz magnetospectroscopic measurements revealed two polariton branches as a function of applied magnetic field. While the photon-like part of the two polariton branches was clearly observed, the matter-like part was generally elusive. Our electromagnetic simulations quantitatively reproduce our observation for the upper-polariton branch. However, for the lower-polariton branch, our simulations predict a pronounced resonance, which was absent in experimental spectra. This discrepancy may be a consequence of the breakdown of the dipole approximation in this extreme confinement situation.

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Regioisomeric effects regulating the physicochemical properties of complex copolymers in thin films

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European Polymer Journal 2025年 234卷

作者： Hyeji Lee Seungjun Kim Yun Hee Ko Juyoung Park Dahye Lee Yejin Ku Chanjae Ahn Yoonhyun Kwak Minsang Kim Jin-Kyun Lee Myungwoong Kim Department of Chemistry and Chemical Engineering Inha University Incheon 22212 Republic of Korea Program in Environment and Polymer Engineering Inha University Incheon 22212 Republic of Korea Department of Polymer Science and Engineering Inha University Incheon 22212 Republic of Korea Material Research Center Samsung Advanced Institute of Technology Samsung Electronics Suwon 16677 Republic of Korea

We demonstrate that minimal alterations to the chemical structure of a hydroxystyrene (HOST)-containing terpolymer lead to significant changes in its physicochemical properties, which in turn govern photolithographic pattern formation in chemical amplification mechanism. While the structures of the three repeating units, their compositions, and the molecular weight characteristics of the terpolymers were controlled to be similar, the location of the phenolic OH groups was adjusted by copolymerizing o -, m -, and p -acetoxystyrene, subsequently transformed into o -, m -, and p -HOST through deacetylation. In the studies to examine the physicochemical properties of the copolymers, the copolymer with p -HOST showed dissolution rate in n -butyl acetate ( n BA) of ≈ 15 nm/s, which was lower than that of copolymer with m -HOST (≈ 18 nm/s) and o -HOST (≈ 27 nm/s), further showing high linear correlation with the Hansen space distance between the copolymers and n BA. Moreover, the acid diffusions in the thin film, which plays a significant role in acid-catalyzed deprotection of the copolymers to solubility modulation, was affected by the location of the phenolic OH: the fastest and slowest acid diffusions were observed in the copolymers of p -HOST and o -HOST, respectively. The regioisomerism further affects the photolithographic performance collectively: (i) in contrast curve, light energy required to change the solubility was in order of p -HOST < m -HOST < o -HOST, and (ii) the height of the formed pattern was in order of p -HOST > m -HOST > o -HOST, highlighting the significance of chemical structure design and the fundamental understanding of structure–property relationships.

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Effects of gas grafting treatment with different amounts of palmitoyl chloride on properties of CNF-coated paper

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Palpu Chongi Gisul/Journal of Korea Technical Association of the Pulp and Paper Industry 2020年第1期52卷 55-65页

作者： Park, Min-A. Choi, Kyoung-Hwa Cho, Byoung-Uk Department of Paper Science and Engineering College of Forest and Environmental Sciences Kangwon National University Korea Republic of Changgang Institute of Paper Science and Technology Kangwon National University Korea Republic of Program of Paper Science and Engineering Division of Forest Material Science and Engineering College of Forest and Environmental Sciences Kangwon National University Korea Republic of

Effects of gas grafting treatment using palmitoyl chloride on properties of papers coated with three different types of CNFs whose crystalline structures are different were investigated. One type of cellulose I based CNF (cellulose nanofibril) and two types of cellulose II based CNFs were utilized for this study. Effects of the applied amount of palmitoyl chloride on the CNF coated papers were also investigated. It was found that tensile strength and stabilities of optical properties of the CNF coated papers such as color, brightness, and yellowness were deteriorated with the gas grafting treatment with palmitoyl chloride. Increasing the applied amount of palmitoyl chloride increased the degree of deterioration. Applying excess amount of palmitoyl chloride for gas grafting increased the roughness of the CNF coated paper. In addition, increasing the pick-up of CNF on paper increased air resistance while the applied amount of palmitoyl chloride did not show any significant effects on air permeability. © 2020 Korean Technical Assoc. of the Pulp and Paper Industry. All rights reserved.

关键词： Gases

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Highly Sensitive and Stable Non-Enzymatic Glucose Sensing Based on Nanostructure-Gated Organic Electrochemical Transistors with Self-Ph Calibration

SSRN

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SSRN 2025年

作者： Cheng, Huanyu Meng, Ke Zhu, Jia Zhang, Tianyao Zhang, Xianzhe Zhang, Yingying Chen, Xiangjie Li, Fan Tong, Yao Zhang, Senhao Qiu, Donghai Yang, Hongbo Liu, Shangbin Yin, Lan Zhao, Rui Huang, Libin Li, Tao Gao, Min Pan, Taisong Yang, Jian Lin, Yuan State Key Laboratory of Biotherapy and Cancer Center China School of Material and Energy University of Electronic Science and Technology of China Chengdu610054 China University of Electronics Science and Technology of China Quzhou324000 China Department of Engineering Science and Mechanics The Pennsylvania State University University ParkPA16802 United States Suzhou Institute of Biomedical Engineering and Technology Chinese Academy of Science Suzhou215011 China School of Materials Science and Engineering Tsinghua University Beijing100084 China Department of Gastroenterology West China Hospital Sichuan University Chengdu610041 China Research Center for Industries of the Future Biomedical Engineering Program School of Engineering Westlake University Zhejiang Hangzhou310030 China Medico-Engineering Cooperation on Applied Medicine Research Center University of Electronics Science and Technology of China Chengdu610054 China

Non-invasive, real-time, and continuous monitoring of the trace amount of glucose in near-neutral biofluids is significant for the daily care and treatment of diabetic patients or people with suboptimal health status. Despite improved sensing performance with novel low-dimensional materials or porous structures in various enzymatic and non-enzymatic electrochemical glucose sensors, they still suffer from high cost, poor long-term stability, and performance fluctuations in varied temperature and pH. This work synergistically combines an Au-modified porous laser-induced graphene (LIG) gate electrode with an organic electrochemical transistor (OECT) to create a flexible non-enzymatic glucose sensor. The resulting OECT-based non-enzymatic glucose sensor exhibits significantly enhanced sensitivity in near-neutral biofluids, the limit of detection (LOD) (0.08 μM in pH=7.4), excellent stability over time (degradation of ~10% in 180 days) and against temperature changes (30 °C - 40 °C), self-pH calibration capabilities, and uncompromised sensing performance with shrinking sizes. The highly consistent laser patterning technique and in situ galvanic reduction process for electrode modifications not only provide a simple yet versatile approach to creating low-cost, compact sensing platforms for precise and real-time sweat glucose measurements, but also support scalable production, allowing the correlation study of key biomarkers in sweat and blood. © 2025, The Authors. All rights reserved.

关键词： Coated wire electrodes

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Microscopic picture of paraelectric perovskites from structural prototypes

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Physical Review Research 2022年第1期4卷 L012042-L012042页

作者： Michele Kotiuga Samed Halilov Boris Kozinsky Marco Fornari Nicola Marzari Giovanni Pizzi Theory and Simulation of Materials (THEOS) National Centre for Computational Design and Discovery of Novel Materials (MARVEL) École Polytechnique Fédérale de Lausanne CH-1015 Lausanne Switzerland Designed Material Technologies LLC P.O. Box 14548 Richmond Virginia 23221-9998 USA John A. Paulson School of Engineering and Applied Sciences Harvard University 29 Oxford Street Cambridge Massachusetts 02138 USA Robert Bosch LLC Research and Technology Center Cambridge Massachusetts 02139 USA Department of Physics and Science of Advanced Materials Program Central Michigan University Mt. Pleasant Michigan 48859 USA

We highlight with first-principles molecular dynamics the persistence of intrinsic 〈111〉 Ti off-centerings for BaTiO3 in its cubic paraelectric phase. Intriguingly, these are inconsistent with the Pm3¯m space group often used to atomistically model this phase using density-functional theory or similar methods. Therefore, we deploy a systematic symmetry analysis to construct representative structural models in the form of supercells that satisfy a desired point symmetry but are built from the combination of lower-symmetry primitive cells. We define as structural prototypes the smallest of these that are both energetically and dynamically stable. Remarkably, two 40-atom prototypes can be identified for paraelectric BaTiO3; these are also common to many other ABO3 perovskites. These prototypes can offer structural models of paraelectric phases that can be used for the computational engineering of functional materials. Last, we show that the emergence of B-cation off-centerings and the primitive-cell phonon instabilities is controlled by the equilibrium volume, in turn, dictated by the filler A cation.

关键词： Crystal symmetry Ferroelectricity Structural order parameter Paraelectrics

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Two-step electronic response to magnetic ordering in a van der Waals ferromagnet

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Physical Review B 2024年第4期109卷 045416-045416页

作者： Han Wu Jian-Xin Zhu Lebing Chen Matthew W. Butcher Ziqin Yue Dongsheng Yuan Yu He Ji Seop Oh Bin Gao Jianwei Huang Shan Wu Cheng Gong Yucheng Guo Sung-Kwan Mo Jonathan Denlinger Donghui Lu Makoto Hashimoto Matthew B. Stone Alexander I. Kolesnikov Songxue Chi Junichiro Kono Andriy H. Nevidomskyy Robert J. Birgeneau Pengcheng Dai Ming Yi Department of Physics and Astronomy and Rice Center for Quantum Materials Rice University Houston Texas 77005 USA Theoretical Division Los Alamos National Laboratory Los Alamos New Mexico 87545 USA Center for Integrated Nanotechnologies Los Alamos National Laboratory Los Alamos New Mexico 87545 USA Department of Physics University of California at Berkeley Berkeley California 94720 USA Applied Physics Graduate Program Smalley-Curl Institute Rice University Houston Texas 77005 USA Materials Sciences Division Lawrence Berkeley National Laboratory Berkeley California 94720 USA National Institute for Materials Science 1-1 Namiki Tsukuba Ibaraki 305-0044 Japan Department of Applied Physics Yale University New Haven Connecticut 06511 USA Department of Electrical and Computer Engineering and Quantum Technology Center University of Maryland College Park Maryland 20742 USA Advanced Light Source Lawrence Berkeley National Laboratory Berkeley California 94720 USA Stanford Synchrotron Radiation Lightsource SLAC National Accelerator Laboratory Menlo Park California 94025 USA Neutron Scattering Division Oak Ridge National Laboratory Oak Ridge Tennessee 37831 USA Department of Electrical and Computer Engineering Rice University Houston Texas 77005 USA Smalley-Curl Institute Rice University Houston Texas 77005 USA Department of Material Science and Nanoengineering Rice University Houston Texas 77005 USA Department of Materials Science and Engineering University of California Berkeley California 94720 USA

The two-dimensional material Cr2Ge2Te6 is a member of the class of insulating van der Waals (vdW) magnets. Here, using high resolution angle-resolved photoemission spectroscopy in a detailed temperature dependence study, we identify a clear response of the electronic structure to a dimensional crossover in the form of two distinct temperature scales marking onsets of modifications in the electronic structure. Specifically, we observe Te p-orbital-dominated bands to undergo changes at the Curie transition temperature TC while the Cr d-orbital-dominated bands begin evolving at a higher temperature scale. Combined with neutron scattering, density functional theory calculations, and Monte Carlo simulations, we find that the electronic system can be consistently understood to respond sequentially to the distinct temperatures at which in-plane and out-of-plane spin correlations exceed a characteristic length scale. Our findings reveal the sensitivity of the orbital-selective electronic structure for probing the dynamical evolution of local moment correlations in vdW insulating magnets.

关键词： Electronic structure Magnetic order Magnetic phase transitions Van der Waals systems Angle-resolved photoemission spectroscopy

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