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Effect of Free-End Torsion on the Corrosion and mechanical Properties for Mg-3Zn-0.2Ca Alloy

Acta Metallurgica Sinica(English Letters) 2025年第1期38卷 59-70页

作者： Li-Lan Gao Jiang Ma Yan-Song Tan Xiao-Hao Sun Qi-Jun Gao De-Bao Liu Chun-Qiu Zhang Tianjin Key Laboratory for Advanced Mechatronic System Design and Intelligent Control School of Mechanical EngineeringTianjin University of TechnologyTianjin300384China National Demonstration Center for Experimental Mechanical and Electrical Engineering Education Tianjin University of TechnologyTianjin300384China School of Materials Science and Engineering Tianjin University of TechnologyTianjin300384China

Magnesium alloys with excellent degradability and biocompatibility are promising materials for biomedical implants,saving patients the burden of second ***,their mechanical properties and corrosion resistance are significantly below the requirements for implant *** study aims to improve the mechanical and corrosion resistance properties of Mg-3Zn-0.2Ca alloy by pre-torsion treatment,and find out the optimal shear *** rod-shaped Mg-3Zn-0.2Ca alloy specimens were pre-torsion treated at different torsion *** effect of free-end torsion on Mg-3Zn-0.2Ca alloy was characterized through microstructure analysis,mechanical testing,and corrosion ***-torsion treatment can refine grain and induce twins and dislocations in Mg-3Zn-0.2Ca *** surface hardness increases with the increase in torsion *** yield strength and ultimate strength initially increase and then decrease with increasing torsion angle,while ductility decreases with increasing torsion *** with a shear strain of 30%exhibit the highest tensile strength,reaching 284.78±10.62 MPa,with an elongation of 19.37±1.66%.Furthermore,they show a significant improvement in fatigue lives both before and after *** the stress amplitude is 120 MPa,the fatigue lives for specimens without pre-torsion treatment are 54,275 cycles and 4324 cycles before and after pre-corrosion,while they increased significantly to 92,015 cycles and 5050 cycles with the 30%shear strain,***,the 30%shear strain specimens show a significant reduction in corrosion *** conclusion,pre-torsion treatment can effectively modify the microstructure of Mg-3Zn-0.2Ca alloy,enhancing both mechanical properties and corrosion *** optimal shear strain for this improvement is 30%.This study provides a practical method to enhance the mechanical properties and corrosion resistance of Mg-3Zn-0.2Ca alloy,making it more suitable for biomedical implan

关键词： Magnesium alloy Pre-torsion Microstructure mechanical property Corrosion resistance

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Contact-reactive brazing mechanism of Al_(0.3)CoCrFeNi high-entropy alloys using a niobium interlayer

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Journal of Iron and Steel Research International 2024年第10期31卷 2546-2554页

作者： Yu Lei Yi-nan Li Xiao-guo Song Sheng-peng Hu Wei-min Long Hai-chuan Shi Zu-bin Chen School of Mechanical and Automotive Engineering Qingdao University of TechnologyQingdao266000ShandongChina State Key Laboratory of Precision Welding and Joining of Materials and Structures Harbin Institute of TechnologyHarbin150001HeilongjiangChina State Key Laboratory of Advanced Brazing Filler Metals and Technology Zhengzhou Research Institute of Mechanical EngineeringZhengzhou450001HenanChina School of Materials Science and Engineering Shanghai University of Engineering ScienceShanghai201620China Yantai Research Institute Harbin Engineering UniversityYantai264006ShandongChina

The contact-reactive brazing of Al_(0.3)CoCrFeNi high-entropy alloys with a Nb interlayer was *** effects of Nb thickness and brazing temperature on the interfacial microstructure and mechanical properties of Al_(0.3)CoCrFeNi joints were *** results show that with Nb thickness increasing from 10 to 100μm,the average width of Al_(0.3)CoCrFeNi joints is increased from 127 to 492μm and the erosion volume of Al_(0.3)CoCrFeNi base metals(BMs)by face-centered cubic-Nb eutectic liquid is enlarged *** increasing brazing temperature from 1280 to 1360℃,the intergranular penetration of eutectic liquid into Al_(0.3)CoCrFeNi BMs becomes more severe and lamellar Laves phase is broken-up and *** shear strength of joint is increased gradually from 374 to 486 MPa and then decreased to 475 *** maximum shear strength value of 486 MPa is obtained when brazing at 1340℃ for 10 min,reaching about 78% of the shear strength of Al_(0.3)CoCrFeNi ***,the brazing mechanism was analyzed in details.

关键词： Contact-reactive brazing High-entropy alloy Intergranular penetration Shear strength Mechanism

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Heat-resistant Al_(2)O_(3) nanowire-polyetherimide separator for safer and faster lithium-ion batteries

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Journal of materials science & Technology 2023年第11期142卷 112-120页

作者： Wenqiang Hu Wenbin Fu Samik Jhulki Liang Chen Aashray Narla Zhijian Sun Fujia Wang Alexandre Magasinski Gleb Yushin School of Materials Science and Engineering Georgia Institute of TechnologyAtlantaGA 30332USA Institute of Materials Science and Engineering School of Mechanical and Electronic Control EngineeringBeijing Jiaotong UniversityBeijing 100044China Sila Nanotechnologies Inc AlamedaCA 94501USA School of Chemistry and Chemical Engineering Hunan Institute of Science and TechnologyYueyangHunan 414006China

Poor heat/flame-resistance of polyolefin(e.g.,polyethylene and polypropylene)separators and high flammability of organic electrolytes used in today’s lithium-ion batteries(LIBs)may trigger rare yet potentially catastrophic safety ***,we mitigate this challenge by developing a heat-resistant and flame-retardant porous composite membrane composed of polyetherimide(PEI)and Al_(2)O_(3) nanowires(NWs).The membranes are fabricated based on an industrially scalable non-solvent-induced phase separation process,which results in an intimately interconnected porous network of Al_(2)O_(3) NWs and *** produced composite membranes exhibit excellent flexibility,thermal stability,and ***,the composite membranes exhibit minimal thermal shrinkage and superior tensile strength(16 MPa)at temperatures as high as 200℃,significantly exceeding the performance of conventional polyolefin *** with commercial separators,their superior wettability and higher ionic conductivity(by up to 2.4 times)when filled with the same electrolyte,larger electrolyte uptake(-190 wt.%),as well as improved cycle and rate performance demonstrated in LiNiMnCoO_(2)(NCM)-based LIBs make them attractive choices for a variety of electrochemical energy storage devices.

关键词： Lithium-ion batteries Separators Al_(2)O_(3)NWs Polyetherimide Thermal resistance

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mechanically robust and dynamic supramolecular polymer networks enabled by[an]daisy chain backbones

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science China Chemistry 2024年第12期67卷 4234-4241页

作者： Yongming Wang Yi Ding Yuhang Liu Shaolei Qu Wenbin Wang Wei Yu Zhaoming Zhang Feng Liu Xuzhou Yan School of Chemistry and Chemical Engineering Frontiers Science Center for Transformative MoleculesShanghai Jiao Tong UniversityShanghai 200240China State Key Laboratory for Mechanical Behavior of Materials Shaanxi International Research Center for Soft MatterSchool of Materials Science and EngineeringXi’an Jiaotong UniversityXi’an 710049China

Supramolecular polymer networks(SPNs)have garnered significant research interest due to their dynamic ***,while current developments primarily focus on managing supramolecular crosslinks,the role of polymer backbones—equally crucial to SPN properties—has not yet been sufficiently ***,we utilize mechanically interlocked[an]daisy chain as backbone to prepare a class of SPNs,where the force-induced motion of successive mechanical bonds toughens and reinforces the *** specific,the[an]daisy chain backbones connect with polynorbornene chains through quadruple H-bonding in the SPN *** to the control with non-slidable backbone,The representative SPN-2 exhibits a robust feature in tensile tests with high maximum stress(14.7 vs.7.89 MPa)and toughness(83.8 vs.48.6 MJ/m^(3)).Moreover,it also has superior performance in energy dissipation benefitting from the[an]daisy chain backbones as well as supramolecular ***,the SPN-2 displayed exceptional self-healing and reprocessing capabilities due to their dynamic quadrable H-bonding *** findings demonstrate the untapped potential of[an]daisy chain as a polymer skeleton to develop SPNs and open the door to design mechanically robust supramolecular materials with diverse smart functions.

关键词： supramolecular polymer networks mechanical bond [an]daisy chains self-healing dynamic materials

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Challenges and approaches of single-crystal Ni-rich layered cathodes in lithium batteries

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National science Review 2023年第12期10卷 203-222页

作者： Jiangtao Hu Hongbin Wang Biwei Xiao Pei Liu Tao Huang Yongliang Li Xiangzhong Ren Qianling Zhang Jianhong Liu Xiaoping Ouyang Xueliang Sun Graphene Composite Research Center College of Chemistry and Environmental EngineeringShenzhen University GRINM(Guangdong) Institute for Advanced Materials and Technology School of Materials Science and Engineering Xiangtan University Department of Mechanical and Materials Engineering University of Western Ontario Eastern Institute for Advanced Study Eastern Institute of Technology

High energy density and high safety are incompatible with each other in a lithium battery, which challenges today's energy storage and power applications. Ni-rich layered transition metal oxides(NMCs) have been identified as the primary cathode candidate for powering next-generation electric vehicles and have been extensively studied in the last two decades, leading to the fast growth of their market share, including both polycrystalline and single-crystal NMC cathodes. Single-crystal NMCs appear to be superior to polycrystalline NMCs, especially at low Ni content(≤60%). However, Ni-rich single-crystal NMC cathodes experience even faster capacity decay than polycrystalline NMC cathodes, rendering them unsuitable for practical application. Accordingly, this work will systematically review the attenuation mechanism of single-crystal NMCs and generate fresh insights into valuable research pathways. This perspective will provide a direction for the development of Ni-rich single-crystal NMC cathodes.

关键词： single-crystal NMC attenuation mechanism modification strategy developing route

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Effect of cerium addition on non-metallic inclusions in a high-carbon chromium bearing steel

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Journal of Iron and Steel Research International 2023年第11期30卷 2254-2266页

作者： Hao Li Qiang Ren Li-feng Zhang State Key Lab of Metastable Materials Science and Technology Yanshan UniversityQinhuangdao066004HebeiChina School of Mechanical Engineering Yanshan UniversityQinhuangdao066004HebeiChina School of Mechanical and Materials Engineering North China University of TechnologyBeijing100144China

Effects of varied levels of cerium(28×10-6,65×10^(-6) and 150×10^(-6))on inclusions in a high-carbon chromium bearing steel at different stages(before adding cerium,after adding cerium for 1,5,10 min and ingot)were studied using laboratory *** automatic scanning electron microscope system with energy-dispersive spectroscopy was used to analyze the amount,composition,size and morphology of inclusions in the steel at different *** the cerium content in the molten steel increased from 0 to 150×10^(-6),the evolution sequence of inclusions was as follows:Al_(2)O_(3)→CeAl11O18→CeAlO_(3)→Ce_(2)O_(2)*** 28×10^(-6) cerium was added,Al_(2)O_(3) inclusions were modified into CeAl_(11)O_(18) inclusions in the molten steel and then were further transformed into Al2O3 and CeAlO3 inclusions in the solid steel during *** the addition of 65×10^(-6) cerium,inclusions in the molten steel were modified into CeAlO_(3) and a small number of Ce2O2S *** the addition amount of cerium increased to 150×10^(-6),inclusions were transformed to Ce_(2)O_(2)*** size of inclusions in the molten steel decreased obviously with cerium *** the other hand,the size of inclusions increased during the cooling process in solid steels of No.1 steel(with 28×10^(-6) cerium)and No.2 steel(with 65×10^(-6) cerium).During the cooling process,unmodified MnS inclusions were precipitated in the solid steel of No.1 steel and wrapped outside the Al2O3 and CeAlO_(3) inclusions to form large complex *** the cooling process of No.2 steel,the inclusion size of CeAlO_(3) increased due to the collision and *** the No.3 steel(with 150×10^(-6) cerium),the average size of inclusions decreased rapidly and remained at a lower size during the cooling process,which was beneficial to improving the fatigue life of the steel.

关键词： Cerium Inclusion Transformation High-carbon chromium bearing steel Modification

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Morphable 3D architectures enabled by shear-guided approach

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materials Today 2025年 86卷 28-41页

作者： Li, Kan Liu, Zhi Hu, Xiaonan Xu, Zijian Zhou, Yunlei Chen, Lin Huang, Yonggang Bo, Renheng Zhang, Yihui AML Department of Engineering Mechanics State Key Laboratory of Flexible Electronics Technology Tsinghua University Beijing100084 China State Key Laboratory of Digital Manufacture Equipment and Technology Huazhong University of Science and Technology Wuhan430074 China State Key Laboratory for Mechanical Behavior of Materials School of Materials Science and Engineering Xi'an Jiaotong University Shaanxi Xi'an710000 China Departments of Mechanical Engineering Civil and Environmental Engineering Materials Science and Engineering and Center for Bio-Integrated Electronics Northwestern University EvanstonIL60208 United States

3D structures and electronic devices assembled through mechanically guided approaches have found important applications in a wide spectrum of emerging fields, including healthcare, biomedical engineering, wearable devices, robotics, among others. To broaden the obtainable functional 3D architectures via mechanical pathways, in this work, a shear-guided assembly approach is demonstrated. A series of structures in forms of ribbon, membrane and hybrid configurations with previously inaccessible geometrical features, such as reversible local flips and centrosymmetric charity are showcased. Finite element analysis (FEA) is performed, suggesting that such shear-induced structures are capable of reversible post-assembly shape transformation among different modes. Given the above, a facile design, consisting of two ribbon-like 3D units (dual-3D-unit design), is introduced and carefully calibrated for shear sensing. Notably, such design is capable of translating the hard-to-measure shear deformation into easily-accessed vertical displacements while insensitive to finite tensile loadings. A multifunctional arrayed electronic interface is fabricated using such dual-3D-unit design, suggesting promising potentials in human–machine interactions. © 2025 Elsevier Ltd

关键词： Shear deformation

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Unusual twin induced recrystallization and corresponding texture optimization in a cold rolled Mg-Gd-Zr alloy during annealing

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Journal of Magnesium and Alloys 2025年第3期13卷 1099-1115页

作者： Ning Lv Lingyu Zhao Hong Yan Boyu Liu Rongshi Chen Zhiwei Shan Shi-changxu Innovation Center for Advanced Materials Institute of Metal ResearchChinese Academy of Sciences72 Wenhua RoadShenyang 110016China School of Materials Science and Engineering University of Science and Technology of China72 Wenhua RoadShenyang 110016China School of Materials Science and Engineering Shenyang Ligong UniversityShenyang110159China School of Materials Science and Engineering Shandong University of Science and TechnologyQingdaoShandong 266590China Center for Advancing Materials Performance From the Nanoscale(CAMP-Nano)&Hysitron Applied Research Center in China(HARCC) State Key Laboratory for Mechanical Behavior of MaterialsXi’an Jiaotong UniversityXi’an 710049China

Twins play an important role in the texture transition during *** a cold rolled high rare earth content magnesium(Mg)alloys with{10–12}extension twins,{11–21}extension twins,{10–11}compression twins and{10–11}-{10–12}double twins and frequent twin-twin interactions,quasi-in-situ electron backscatter diffraction method was used to observe the twin induced static recrystallization(SRX)and related effect on texture during *** results show that basal component was consumed owing to the SRX occurred in basal oriented{10–12}twins and SRXed grains with several speciﬁc orientations show preferential grain *** widely operated in the{10–12}extension and{11–21}extension twins,but absent in most{10–11}compression and{10–11}-{10–12}double twins,which is different to traditional twin induced *** compression/double twins detwinned while only partial tension twins *** of{11–21}twins and resultant twin-twin interaction facilitate the formation of serrated twin boundaries,which can serve as nucleation *** ofdislocation and related dislocation interaction in high dislocation density areas promote the formation of new grain boundaries and related ***dislocations in basal oriented twins release the strain accumulation in compression/double twins and thus result in the absence of *** twin size difference,storage energy and dislocation-twin interaction commonly functioned to the detwinning during *** near-coincide site lattice boundaries that show high mobility were considered to be the important contributor to the preferential grain growth of SRXed grains.

关键词： Magnesium alloy {11–21}twin Texture Static recrystallization Detwinning

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Enhancing the thermal conductivity of semiconductor thin films via phonon funneling

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npj Computational materials 2024年第1期10卷 1414-1422页

作者： C.Jaymes Dionne Sandip Thakur Nick Scholz Patrick Hopkins Ashutosh Giri Department of Mechanical Industrialand Systems EngineeringUniversity of Rhode IslandKingston02881 RIUSA Department of Mechanical and Aerospace Engineering University of VirginiaCharlottesville22904 VAUSA Department of Materials Science and Engineering University of VirginiaCharlottesville22904 VAUSA Department of Physics University of VirginiaCharlottesville22904 VAUSA

The second law of thermodynamics asserts that energy diffuses from hot to *** resulting temperature gradients drive the efficiencies and failures in a plethora of ***,as the dimensionalities of materials shrink to the nanoscale regime,proper heat dissipation strategies becomemore challenging since the mean free paths of phonons become larger than the characteristic length *** leads to temperature gradients that are dependent on interfaces and boundaries,which ultimately can lead to severe thermal ***,we uncover a phenomenon which we refer to as‘phonon funneling’,that allows the control of phonon transport to preferentially direct phonon energy away from geometrically confined interfacial thermal bottlenecks and into localized colder *** phenomenon supersedes heat diffusion based on the macroscale temperature gradients,thus introducing a nanoscale regime in which boundary scattering increases the phonon thermal conductivity of thin films,an opposite effect than what is traditionally *** work advances the fundamental understanding of phonon transport at the nanoscale and the role of efficient scattering methods for enhancing thermal transport.

关键词： thermal conductivity films

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Selective laser melted AZ91D magnesium alloy with superior balance of strength and ductility

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Journal of Magnesium and Alloys 2023年第12期11卷 4644-4658页

作者： Xinzhi Li Xuewei Fang Shuaipeng Wang Siqing Wang Min Zha Ke Huang State Key Laboratory for Manufacturing Systems Engineering School of Mechanical EngineeringXi’an Jiaotong UniversityXi’an 710049ShaanxiPR China School of Materials Science and Engineering Jilin UniversityChangchunPR China

In the context of global carbon neutrality, the application of lightweight magnesium alloys is becoming increasingly attractive. In this study, selective laser melting(SLM) was employed to achieve nearly full dense and crack-free AZ91D components with fine equiaxed grain structure. The formation mechanism of typical pore defects(gas pore, lack-of-fusion pore and keyhole pore) and melting modes(keyhole mode and conduction mode) were systematically studied by varying the laser power and scanning speed. The morphology and volume fraction of the pores under different processing conditions were characterized. A criterion based on the depth-to-width ratio of the melt pool was established to identify different melting modes. The strength and ductility(tensile strength up to 340 MPa and uniform elongation of 8.9%)of the as deposited AZ91D are far superior to those of the casting components and are comparable to those of its wrought *** superior balance of strength and ductility of SLMed AZ91D, as well as the negligible anisotropic properties are mainly ascribed to the extremely fine equiaxed grain structure(with average grain size of ~1.2 μm), as well as the discontinuous distribution of β-Al_(12)Mg_(17) phases. It thus provides an alternative way to fabricate high-strength magnesium alloys with complex geometry.

关键词： Magnesium alloy Selective laser melting Melting mode Defects Equiaxed grain structure mechanical properties

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