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Investigating long term storage stability and drug release behavior of polypeptide based fibrous scaffold for tissue engineering application

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materials Chemistry and Physics 2024年 321卷

作者： Chang, Chun-Yu Su, An-Jey A. Lin, Meng-Fang Hsiao, Kai-Chi Lee, Chia-Hsien Lin, Yu-Ting Hsiao, Yu-Sheng Wu, Ming-Chung Huang, Yu-Ching Su, Wei-Fang Bachelor Program in Semiconductor Materials and Fabrication Ming Chi University of Technology Taiwan Dept. of Surgery Anschutz Medical Campus University of Colorado AuroraCO United States Dept. of Materials Engineering Ming Chi University of Technology Taiwan Dept. of Chemical and Materials Engineering Chang Gung University Taiwan Dept. of Materials Science and Engineering National Taiwan University of Science and Technology Taipei City Taiwan Dept. of Materials Science and Engineering National Taiwan University Taiwan

Electrospun poly (γ-benzyl-L-glutamate) (PBG) scaffold felt with aligned fibers shows promising nerve regeneration and neurite growth capability due to the nerve stimulating moiety of glutamate in the PBG material. The nerve regeneration capability can be further enhanced by incorporating 4 wt% minocycline hydrochloride (MH) in the scaffold (PBGMH4). They are useful in the nerve tissue engineering to repair and regeneration damaged nerves in central nerve system or peripheral nerve system. Here we investigate the ambient storage capability of PBG and PBGMH4 by monitoring the changes over time of fiber dimension, mechanical properties of both scaffolds and amount of drug release of PBGMH4. It is interesting to observe the diameter of fibers and mechanical strength of scaffolds increases but the amount of drug release decrease with time. By carefully examining the top view of the scaffolds using scanning electron microscopy (SEM), the fiber diameter of PBG increased by 58 % over the 12 months storage period, which is larger than the 32 % increase observed for PBGMH4. Furthermore, after storage for 12 months, the difference in fiber diameter between the top and bottom sides of PBG scaffold is 25.9 %, whereas for PBGMH4 is only 6.3 %. These results demonstrate that the PBGMH4 scaffold exhibits superior storage stability compared to that of PBG. Because the fibers of the scaffolds are aligned without any crosslinkage, the scaffolds are porous structure of felts. The porosity of PBGMH4 scaffold is decreased from 90 % to 72 % which can be accountable for the decrease of drug release from initial 42 % to a stabilized 26 % after 9 months of storage. The results indicate the specific surface area of the scaffolds play an important role in governing drug release kinetics. This study thoroughly investigates the storage stability of PBG and PBGMH4 electrospun fibrous scaffolds. The observed correlations between fiber diameter, mechanical properties, and drug release behavior hol

关键词： Electrospinning

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Brownian motion of poly(divinylbenzene) nanoparticles in water

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Journal of Applied Physics 2023年第11期133卷

作者： Lin, Ching-Bin Lee, Chia-Wei Ouyang, Hao Yang, Fuqian Lee, Sanboh Mechanical and Electro-Mechanical Engineering Tamkang University New Taipei City251301 Taiwan Department of Materials Science and Engineering National Tsing Hua University Hsinchu300 Taiwan Materials Program Department of Chemical and Materials Engineering University of Kentucky LexingtonKY40506 United States

Understanding the motion of nanoparticles in liquid is of practical importance for drug delivery and fluid flow in nanofluidic systems. In this work, we use a nanoparticle tracking analyzer to investigate the Brownian motion of polydivinylbenzene (PDVB) nanoparticles in water and a video camera to record the aggregation of PDVB aggregates on the water surface. Using water as the liquid medium precludes the possible complex interaction between the liquid medium and the PDVB nanoparticles, which can possibly alter the random characteristics of the motion of the PDVB nanoparticles. The diffusivity of the PDVB nanoparticles determined from the mean square displacements of the PDVB nanoparticles has the same activation energy as that for the intrinsic viscosity of the corresponding aqueous suspension of the PDVB nanoparticles. The correlation between the diffusivity for the motion of the PDVB nanoparticles in water and the intrinsic viscosity of the corresponding aqueous suspension follows the Stokes-Einstein relation. The capillary effect and the interaction between PDVB aggregates and the liquid media enable the aggregation of the PDVB aggregates on the water surface, which follows the first-order reaction with activation energy larger than that for the random motion of the PDVB nanoparticles in water. © 2023 Author(s).

关键词： Nanoparticles

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First principles derivation of a Rayleigh Gans Debye model for scattering from anisotropic inhomogeneities

arXiv

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arXiv 2023年

作者： Shachar, M.H. Garay, J.E. Materials Science & Engineering Program Mechanical & Aerospace Engineering Department University of California San Diego La Jolla CA United States

Scattering problems are important in describing light propagation in wide ranging media such as the atmosphere, colloidal solutions, metamaterials, glass ceramic composites, transparent polycrystalline ceramics, and surfaces. The Rayleigh-Gans-Debye (RGD) approximation has enjoyed great success in describing a wide range of scattering phenomena. We derive a generalized RGD formulation from the perturbation of Maxwell’s equations. In contrast to most treatments of RGD scattering, our formulation can model any soft scattering phenomena in linear media, including scattering by stochastic process, lossy media, and by anisotropic inhomogeneities occurring at multiple length scales. Our first-principles derivation makes explicit underlying assumptions and provides jumping-off points for more general treatments. The derivation also facilitates a deeper understanding of soft scattering. It is demonstrated that sources of scattering are not interfaces as is often presumed, but excess accelerating charges emitting uncompensated radiation. Approximations to the equations are also presented and discussed. For example, the scattering coefficient in the large-size RGD limit is shown to be proportional to the correlation length and the variance of a projected phase shift. © 2023, CC BY.

关键词： Random processes

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Methane reforming reactions for hydrogen production using hydrotalcite precursors and nanofibers based catalysts 12

Methane reforming reactions for hydrogen production using hy...

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12th International Renewable Energy Congress, IREC 2021

作者： Silva, Thamyscira Chaghouri, Muriel Tidahy, Lucette Haingomalala Gennequin, Cedric Abi-Aad, Edmond Cesario, Moises MacEdo, Daniel Dunkerque France Federal University Of Paraiba Materials Science And Engineering Postgraduate Program Joao Pessoa Brazil

ISBN: (纸本)9781665432900

CoNiMg4Al2 catalysts were synthesized using two different methods: solution blow spinning to produce nanofibers (NF), and co-precipitation to produce hydrotalcite precursors (HT). Part of the hydrotalcite sample was ground (GR) using mechanical milling to determine the effect of grinding on the catalytic performance. The three materials (NF, HT and GR) were tested in the dry and steam reforming of methane (DRM, SRM respectively) reactions during 12h stability tests at 700°C. The calcined and the used catalysts were characterized using XRD and DTA/TG analysis. All catalysts were active during the SRM and DRM tests;however, nanofibers showed a slightly higher activity in both reactions. The dry reforming of methane reaction was more susceptible to the formation of carbon deposition leading to the deactivation of the ground catalyst. © 2021 IEEE.

关键词： Methane

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Optically-generated focused ultrasound for noninvasive brain stimulation with ultrahigh precision

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Light(science & Applications) 2022年第11期11卷 2817-2831页

作者： Yueming Li Ying Jiang Lu Lan Xiaowei Ge Ran Cheng Yuewei Zhan Guo Chen Linli Shi Runyu Wang Nan Zheng Chen Yang Ji-Xin Cheng Department of Mechanical Engineering Boston UniversityBostonMA 02215USA Graduate Program for Neuroscience Boston UniversityBostonMA 02215USA Department of Electrical and Computer Engineering Boston UniversityBostonMA 02215USA Department of Chemistry Boston UniversitBostonMA 02215USA Department of Biomedical Engineering Boston UniversityBostonMA 02215USA Division of Materials Science and Engineering Boston UniversityBostonMA 02215USA Department of Biological Engineering Massachusetts Institute of TechnologyCambridgeMA 02142USA

High precision neuromodulation is a powerful tool to decipher neurocircuits and treat neurological *** non-invasive neuromodulation methods offer limited precision at the milimeter ***,we report opticallygenerated focused ultrasound(OFUS)for non-invasive brain stimulation with ultrahigh *** is generated by a soft optoacoustic pad(SOAP)fabricated through embedding candle soot nanoparticles in a curved polydimethylsiloxane *** generates a transcranial ultrasound focus at 15 MHz with an ultrahigh lateral resolution of 83μm,which is two orders of magnitude smaller than that of conventional transcranial-focused ultrasound(tFUS).Here,we show effective OFUS neurostimulation in vitro with a single ultrasound *** demonstrate submillimeter transcranial stimulation of the mouse motor cortex in *** acoustic energy of 0.6 mJ/cm?,four orders of magnitude less than that of tFUS,is suffcient for successful OFUS *** offers new capabilities for neuroscience studies and disease treatments by delivering a focus with ultrahigh precision noninvasively.

关键词： SOAP stimulation precision

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Growth of Wafer-Scale Single-Crystal 2D Semiconducting Transition Metal Dichalcogenide Monolayers

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Advanced science 2024年第11期11卷 e2307839页

作者： Singh, Jitendra Astarini, Nadiya Ayu Tsai, Meng-Lin Venkatesan, Manikandan Kuo, Chi-Ching Yang, Chan-Shan Yen, Hung-Wei Department of Materials Science and Engineering National Taiwan University of Science and Technology Taipei City106335 Taiwan Department of Physics Udit Narayan Post Graduate College Padrauna Uttar Pradesh Kushinagar274304 India Department of Molecular Science and Engineering Institute of Organic and Polymeric Materials National Taipei University of Technology Taipei City106344 Taiwan Institute and Undergraduate Program of Electro-Optical Engineering National Taiwan Normal University Taipei City11677 Taiwan Department of Materials Science and Engineering National Taiwan University Taipei City106319 Taiwan

Due to extraordinary electronic and optoelectronic properties, large-scale single-crystal two-dimensional (2D) semiconducting transition metal dichalcogenide (TMD) monolayers have gained significant interest in the development of profit-making cutting-edge nano and atomic-scale devices. To explore the remarkable properties of single-crystal 2D monolayers, many strategies are proposed to achieve ultra-thin functional devices. Despite substantial attempts, the controllable growth of high-quality single-crystal 2D monolayer still needs to be improved. The quality of the 2D monolayer strongly depends on the underlying substrates primarily responsible for the formation of grain boundaries during the growth process. To restrain the grain boundaries, the epitaxial growth process plays a crucial role and becomes ideal if an appropriate single crystal substrate is selected. Therefore, this perspective focuses on the latest advances in the growth of large-scale single-crystal 2D TMD monolayers in the light of enhancing their industrial applicability. In the end, recent progress and challenges of 2D TMD materials for various potential applications are highlighted. © 2023 The Authors. Advanced science published by Wiley-VCH GmbH.

关键词： Single crystals

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NIR-Responsive Methotrexate-Modified Iron Selenide Nanorods for Synergistic Magnetic Hyperthermic, Photothermal, and Chemodynamic Therapy

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ACS Applied materials and Interfaces 2024年第20期16卷 25622-25636页

作者： Thirumurugan, Senthilkumar Muthiah, Kayalvizhi Samuvel Lin, Yu-Chien Dhawan, Udesh Liu, Wai-Ching Wang, An-Ni Liu, Xinke Hsiao, Michael Tseng, Ching-Li Chung, Ren-Jei No. 1 Section 3 Zhongxiao East Road Taipei10608 Taiwan Centre for the Cellular Microenvironment Division of Biomedical Engineering James Watt School of Engineering Mazumdar-Shaw Advanced Research Centre University of Glasgow GlasgowG116EW United Kingdom Faculty of Science and Technology Technological and Higher Education Institute of Hong Kong Hong Kong New Territories999077 Hong Kong Scrona AG Grubenstrasse 9 Zürich8045 Switzerland College of Materials Science and Engineering Chinese Engineering and Research Institute of Microelectronics Shenzhen University Shenzhen518060 China Department of Electrical and Computer Engineering National University of Singapore Singapore117583 Singapore Genomics Research Center Academia Sinica Taipei115 Taiwan Department and Graduate Institute of Veterinary Medicine School of Veterinary Medicine National Taiwan University Taipei10617 Taiwan Graduate Institute of Biomedical Materials and Tissue Engineering College of Biomedical Engineering Taipei Medical University Taipei11031 Taiwan International Ph.D. Program in Biomedical Engineering College of Biomedical Engineering Taipei Medical University Taipei11031 Taiwan Research Center of Biomedical Device College of Biomedical Engineering Taipei Medical University Taipei11031 Taiwan International Ph.D. Program in Cell Therapy and Regenerative Medicine College of Medicine Taipei Medical University Taipei11031 Taiwan Taipei10608 Taiwan

Breast cancer is a malignant tumor with a high mortality rate among women. Therefore, it is necessary to develop novel therapies to effectively treat this disease. In this study, iron selenide nanorods (FeSe2 NRs) were designed for use in magnetic hyperthermic, photothermal, and chemodynamic therapy (MHT/PTT/CDT) for breast cancer. To illustrate their efficacy, FeSe2 NRs were modified with the chemotherapeutic agent methotrexate (MTX). MTX-modified FeSe2 (FeSe2-MTX) exhibited excellent controlled drug release properties. Fe2+ released from FeSe2 NRs induced the release of •OH from H2O2 via a Fenton/Fenton-like reaction, enhancing the efficacy of CDT. Under alternating magnetic field (AMF) stimulation and 808 nm laser irradiation, FeSe2-MTX exerted potent hyperthermic and photothermal effects by suppressing tumor growth in a breast cancer nude mouse model. In addition, FeSe2 NRs can be used for magnetic resonance imaging in vivo by incorporating their superparamagnetic characteristics into a single nanomaterial. Overall, we presented a novel technique for the precise delivery of functional nanosystems to tumors that can enhance the efficacy of breast cancer treatment. © 2024 The Authors. Published by American Chemical Society

关键词： Magnetic resonance imaging

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The effects of growth environments on WS2 in electrocatalytic hydrogen evolution reaction

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Journal of Physics and Chemistry of Solids 2024年 185卷

作者： Chang, Yung-Huang Huang, Chien-Sheng Chen, Yuan-Tsung Chiang, Chia-Yu Bachelor Program in Industrial Technology National Yunlin University of Science and Technology Yunlin Taiwan Department of Electronic Engineering National Yunlin University of Science and Technology Yunlin Taiwan Graduate School of Materials Science National Yunlin University of Science and Technology Yunlin Taiwan

Transition metal dichalcogenides (TMDs) recently have attracted much attention because of their outstanding catalytic activity, low cost, and earth abundance in the hydrogen evolution reaction (HER). Among these TMDs, MoS2 and WS2 are recognized as promising HER electrocatalysts and have been explored to be one of the candidates for replacing precious metals. In this work, the electrocatalytic activity of WS2 grown in Ar-only, Ar + H2, and ambient environments were studied, where the WS2 was synthesized by thermolysis from (NH4)2WS4 precursor. Different surface morphologies are shown under the different growth atmospheres. The structures of pure WS2, WS2 and WO3 mixed, and almost WO3 were prepared in different growth atmospheres of Ar-only, Ar + H2, and ambient environment, respectively. All the materials prepared in these different environments exhibit high crystalline characteristic. Especially, the pure WS2 grown in an Ar-only environment presents the preferred (103) lattice plane. The pure WS2 performs the best H2 evolution efficiency, indicating that high crystallinity and preferred (103) lattice plane could be relative to the electrocatalytic activity. The studies provide fundamental insight for further design and preparation of electrocatalysts, useful in the development of clean energy. © 2023 Elsevier Ltd

关键词： Electrocatalysts

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Detailed dynamics of a moving magnetic skyrmion lattice in MnSi observed using small-angle neutron scattering under an alternating electric current flow

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Physical Review B 2024年第1期110卷 014431-014431页

作者： D. Okuyama M. Bleuel Q. Ye J. Krzywon N. Nagaosa A. Kikkawa Y. Taguchi Y. Tokura J. D. Reim Y. Nambu T. J. Sato Institute of Multidisciplinary Research for Advanced Materials (IMRAM) Institute of Materials Structure Science (IMSS) National Institute of Standards and Technology 100 Bureau Drive Gaithersburg Maryland 20899-8562 USA Department of Materials Science and Engineering (CEMS) Wako 351-0198 Japan Fundamental Quantum Science Program TRIP Headquarters RIKEN Wako 351-0198 Japan Tokyo College and Department of Applied Physics (IMR) Organization for Advanced Studies FOREST

Lattice formation of swirling textures is ubiquitous in solid-state materials, such as a magnetic skyrmion lattice in chiral magnets. In the magnetic skyrmion lattices, their moving states and dynamics under external perturbations are still unrevealed, although a detailed understanding of the dynamics is crucial to realizing spintronic applications, such as magnetic domain-wall racetrack memory [Parkin et al., science 320, 190 (2008); Fert et al., Nat. Nanotechnol. 8, 152 (2013)]. Here, we report in detail on the transient state of a moving magnetic skyrmion lattice in bulk single-crystalline MnSi under alternating current (AC) using small-angle neutron scattering. A rotation and concomitant broadening of the spot width in the azimuthal direction of the magnetic skyrmion reflections originating from the plastic deformation of the magnetic skyrmion lattice were found only at low AC frequencies [Okuyama et al., Commun. Phys. 2, 79 (2019)], whereas above the threshold AC frequency (ft∼0.12Hz) the rotation was not observed, and the spot width becomes sharper. The observed complex response of the magnetic skyrmion reflections can be explained by the change in dislocation density in the magnetic skyrmion lattice. At frequencies higher than ft, the magnetic skyrmions oscillate removing the dislocations, indicating that the dislocation density is controlled by the AC frequency.

关键词： Magnetic texture Topological defects Chiral magnets Neutron diffraction

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Two-dimensional MXenes:New frontier of wearable and flexible electronics

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InfoMat 2022年第4期4卷 1-28页

作者： Abbas Ahmed Sudeep Sharma Bapan Adak Md Milon Hossain Anna Marie LaChance Samrat Mukhopadhyay Luyi Sun Polymer Program Institute of Materials ScienceUniversity of ConnecticutStorrsConnecticutUSA Advanced Sensor and Energy Research(ASER)Lab Department of Electronic EngineeringKwangwoon UniversitySeoulSouth Korea Department of Textile and Fiber Engineering Indian Institute of TechnologyNew DelhiIndia Department of Textile Engineering Chemistry and ScienceNorth Carolina State UniversityRaleighNorth CarolinaUSA Department of Textile Engineering Khulna University of Engineering&TechnologyKhulnaBangladesh Department of Chemical and Biomolecular Engineering University of ConnecticutStorrsConnecticutUSA

Wearable electronics offer incredible benefits in mobile healthcare monitoring,sensing,portable energy harvesting and storage,human-machine interactions,etc.,due to the evolution of rigid electronics structure to flexible and stretchable ***,transition metal carbides and nitrides(MXenes)are highly regarded as a group of thriving two-dimensional nanomaterials and extraordinary building blocks for emerging flexible electronics platforms because of their excellent electrical conductivity,enriched surface functionalities,and large surface *** article reviews the most recent developments in MXene-enabled flexible electronics for wearable *** MXeneenabled electronic devices designed on a nanometric scale are highlighted by drawing attention to widely developed nonstructural attributes,including 3D configured devices,textile and planer substrates,bioinspired structures,and printed ***,the unique progress of these nanodevices is highlighted by representative applications in healthcare,energy,electromagnetic interference(EMI)shielding,and humanoid control of *** emerging prospects of MXene nanomaterials as a key frontier in nextgeneration wearable electronics are envisioned and the design challenges of these electronic systems are also discussed,followed by proposed solutions.

关键词： flexible electronics MXene nanostructures wearable electronics

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