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arXiv 2024年

作者： Rennich, Emily Sung, Suk Hyun Agarwal, Nishkarsh Gates, Maya Kerns, Robert Hovden, Robert Baggari, Ismail El The Rowland Institute at Harvard Harvard University CambridgeMA02142 United States Department of Mechanical Engineering University of Michigan Ann ArborMI48109 United States Department of Materials Science and Engineering University of Michigan Ann ArborMI48109 United States Michigan Center for Materials Char-acterization University of Michigan Ann ArborMI48109 United States Applied Physics Program University of Michigan Ann ArborMI48109 United States

Cryogenic transmission electron microscopy has revolutionized structural biology and materials science, but achieving temperatures below the boiling point of liquid nitrogen remains a long-standing aspiration. We introduce an ultra-cold liquid helium transmission electron microscope specimen holder, featuring continuous cryogen flow and vibration decoupling. This instrument is compatible with modern aberration-corrected microscopes and achieves sub-25 K base temperature, ±2 mK thermal stability over many hours, and atomic resolution—setting the stage for a new era of cryogenic electron microscopy. © 2024, CC BY.

关键词： High resolution transmission electron microscopy

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Noble metal-free plasmonic Cu/WO3-x@ZNC bi-functional composite for ciprofloxacin photocatalytic degradation and photothermal water evaporation via visible-infrared exposure

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Chemosphere 2024年 364卷 143309页

作者： Zakaria, Hossam Li, Yi Wei, Hongyu Fathy, Mohamed M. Zhang, Chi College of Mechanical and Electrical Engineering Nanjing University of Aeronautics and Astronautics Nanjing210016 China Key Laboratory of Integrated Regulation and Resource Development on Shallow Lake of Ministry of Education College of Environment Hohai University Nanjing210098 China Cairo Egypt Department of Biophysics Faculty of Science Cairo University Giza Egypt College of Materials Science and Engineering Hohai University Changzhou213200 China

Herein, coupling of noble metal-free plasmonic copper nanoparticles with tungsten suboxide and supporting on zeolite nanoclay (Cu/WO3-x@ZNC) composite will be introduced for bi-functional photocatalytic ciprofloxacin (CIP) degradation and water photothermal evaporation under visible/infrared (Vis/IR) exposure. Reduced band-gap of WO3-x via oxygen vacancies creation and localized surface plasmon resonance (LSPR) formation by Cu nanoparticles contributed significantly the extension and intensification of composite's photo-absorption range. Furthermore, small mesoporous structure of ZNC enhanced CIP adsorption and charge carriers separation where the reported photocatalytic efficiencies were 88.3 and 81.7% upon IR and Vis light exposure respectively. It was evidenced that plasmonic hot electrons (e−.s) and hydroxyl radicals (OH•-) performed the basic functions of the photocatalytic process. At the other side, oxygen vacancies existence, plasmonic effect, and confining thermal characteristics of WO3-x, Cu, and ZNC correspondingly induced water photothermal evaporation with efficiencies up to 97.5 and 72.8% under IR and Vis illumination respectively. This work introduces synthesis of a novel bi-functional photocatalytic-photothermal composite by metal sub-oxide and non-noble metal plasmonic coupling and supporting on naturally-derived carrier for water restoration under broad spectral exposure. © 2024 Elsevier Ltd

关键词： Zinc chloride

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Ferroelectric tuning of the valley polarized metal-semiconductor transition in Mn2P2S3Se3/Sc2CO2 van der Waals heterostructures and application to nonlinear Hall effect devices

arXiv

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arXiv 2024年

作者： Sun, Hanbo Ren, Yewei Wu, Chao Dong, Pengqiang Zhang, Weixi Wu, Yin-Zhong Li, Ping State Key Laboratory for Mechanical Behavior of Materials School of Materials Science and Engineering Xi’an Jiaotong University Shaanxi Xi’an710049 China Department of Physics and Electronic Engineering Tongren University Tongren554300 China School of Physical Science and Technology Suzhou University of Science and Technology Suzhou215009 China State Key Laboratory for Surface Physics Department of Physics Fudan University Shanghai200433 China State Key Laboratory of Silicon and Advanced Semiconductor Materials Zhejiang University Hangzhou310027 China

In order to promote the development of the next generation of nano-spintronic devices, it is of great significance to tune the freedom of valley in two-dimensional (2D) materials. Here, we propose a mechanism for manipulating the valley and nonlinear Hall effect by the 2D ferroelectric substrate. The monolayer Mn2P2S3Se3 is a robust antiferromagnetic valley polarized semiconductor. Importantly, the valley polarized metal-semiconductor phase transition of Mn2P2S3Se3 can be effectively tuned by switching the ferroelectric polarization of Sc2CO2. We reveal the microscopic mechanism of phase transition, which origins from the charge transfer and band alignment. Additionally, we find that transformed polarization direction of Sc2CO2 flexibly manipulate the Berry curvature dipole. Based on this discovery, we present the detection valley polarized metal-semiconductor transition by the nonlinear Hall effect devices. These findings not only offer a scheme to tune the valley degree of freedom, but also provide promising platform to design the nonlinear Hall effect devices. © 2024, CC BY.

关键词： Van der Waals forces

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Tailoring the structure of silicon-based materials for lithium-ion batteries via electrospinning technology

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escience 2021年第2期1卷 141-162页

作者： Aoming Huang Yanchen Ma Jian Peng Linlin Li Shu-lei Chou Seeram Ramakrishna Shengjie Peng College of Materials Science and Technology Nanjing University of Aeronautics and AstronauticsNanjing210016China Institute for Superconducting and Electronic Materials Australian Institute for Innovative MaterialsUniversity of Wollongong Innovation CampusSquires WayNorth WollongongNSW2522Australia Center for Nanofibers and Nanotechnology Department of Mechanical EngineeringNational University of SingaporeSingapore117576Singapore

Silicon(Si)is one of the most promising anode materials for the next generation of lithium-ion battery(LIB)due to its high specific capacity,low lithiation potential,and natural ***,the huge variation in volume during the storage of lithium,along with the low conductivity of element,are the main factors hindering its commercial *** micro-nano structures as well as composites of heterogeneous materials have proven to be effective strategies to overcome these *** technology is an affordable and scalablemethod for easily constructing a unique hierarchical micro-nano structurewhile realizing composites of *** far,many efforts have been made to solve the problems of Si-based anodes with general *** review considers the technical fundamental and design strategies for electrospun Si-based nanofibers,including preparation processes,structural engineering,and lithiumstorage *** structure-performance relationship of various materials and the effects of compositing with heterogeneous materials are explored in ***,the remaining challenges are discussed,along with directions for future *** review will provide inspiration for researchers in the design and manufacture of electrospun Si-based nanofibers for LIBs.

关键词： Lithium-ion batteries Anodes Silicon Electrospinning Composites

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Methods of Printing Copper for PCB Repair

Methods of Printing Copper for PCB Repair

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Electronic Components and Technology Conference (ECTC)

作者： Dylan J. Richmond Emuobosan Enakerakpo Mohammed Alhendi Peter McClure Mark D. Poliks Materials Science &#x0026 Engineering Program Binghamton University Binghamton NY Department of Systems Science Industrial Engineering Binghamton University Binghamton NY Universal Instruments Corporation Conklin NY

Damage and defects that occur in printed circuit board assembly (PCBA) often lead to the disposal of expensive components. In cases where laminate and circuitry have been removed, traditional repairs in the manufacturing process have not been able to return devices into service. This study examines the use of aerosol jet printing (AJP) and traditional engineering fluid dispensing (EFD) as methods to service repairs of damaged *** mount component failures on PCBAs may occur as a result of a bad solder joint or problems with the component. In order to salvage such a PCBA, the component must be physically removed from the board and a new be attached. During the removal of PCBA components, pad cratering may occur, where the pad and laminate are damaged/removed along with the component. This leaves behind a crater in place of the pad, rendering the board unrepairable and thus, unusable. Trace damage is another common failure in PCBs. A repair to either sort of damage often requires reconnections of intricate circuitry to be made. Trace repair has traditionally been serviced by soldering a wire between the undamaged regions, rerouting the connection. In the case of fine conductive traces, as seen in devices which are becoming smaller as heterogeneous packaging innovations continue to progress, traditional methods will not be able to service this sort of *** jet printing, a direct-write additive manufacturing process commonly used in flexible hybrid electronics, could save expensive PCBs by repairing cratered pads and damaged traces. The use of AJP has been successful in repairing damaged modules, however the process has not been optimized for general repairs on FR4. The use of AJP and EFD to repair damaged circuitry on FR4 laminate and to fill pad craters with copper nanoparticle ink is demonstrated. Copper ink structures are uniformly sintered to achieve a solderable surface and good adhesion to the exposed laminate and remaining copper on the PCB. P

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A Size-Dependent Ideal Solution Model for Liquid-Solid Phase Equilibria Prediction in Aqueous Organic Solutions

arXiv

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arXiv 2024年

作者： Alliston, Spencer P. Dames, Chris Powell-Palm, Matthew J. Department of Mechanical Engineering University of California Berkeley BerkeleyCA94720 United States J. Mike Walker '66 Department of Mechanical Engineering Texas A&M University 400 Bizzell St College StationTX77840 United States Department of Materials Science and Engineering Texas A&M University 400 Bizzell St College StationTX77840 United States Department of Biomedical Engineering Texas A&M UNiversity 400 Bizzell St College StationTX77840 United States

Predictive synthesis of aqueous organic solutions with desired liquid-solid phase equilibria could drive progress in industrial chemistry, cryopreservation, and beyond, but is limited by the predictive power of current solution thermodynamics models. In particular, few analytical models enable accurate liquidus and eutectic prediction based only on bulk thermodynamic properties of the pure components, requiring instead either direct measurement or costly simulation of solution properties. In this work, we demonstrate that a simple modification to the canonical ideal solution theory accounting for the entopic effects of dissimilar molecule sizes can transform its predictive power, while offering new insight into the thermodynamic nature of aqueous organic solutions. Incorporating a Flory-style entropy of mixing term that includes both the mole and volume fractions of each component, we derive size-dependent equations for the ideal chemical potential and liquidus temperature, and use them to predict the binary phase diagrams of water and 10 organic solutes of varying sizes. We show that sizedependent prediction outperforms the ideal model in all cases, reducing average error in the predicted liquidus temperature by 59%, eutectic temperature by 45%, and eutectic composition by 43%, as compared to experimental data. Furthermore, by retaining the ideal assumption that the enthalpy of mixing is zero, we demonstrate that for aqueous organic solutions, much of the deviation from ideality that is typically attributed to molecular interactions may in fact be explained by simple entropic size effects. These results suggest an underappreciated dominance of mixing entropy in these solutions, and provide a simple approach to predicting their phase equilibria. © 2024, CC BY.

关键词： Entropy

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Second law of thermodynamics: Spontaneous cold-to-hot heat transfer in a nonchaotic medium

arXiv

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arXiv 2023年

作者： Qiao, Yu Shang, Zhaoru Program of Materials Science and Engineering University of California La Jolla San DiegoCA92093 United States Department of Structural Engineering University of California La Jolla San DiegoCA92093-0085 United States

It has long been known that, fundamentally different from a large body of rarefied gas, when a Knudsen gas is immersed in a thermal bath, it may never reach thermal equilibrium. The root cause is nonchaoticity: as the particle-particle collisions are sparse, the particle trajectories tend to be independent of each other. Usually, this counterintuitive phenomenon is studied through kinetic theory and is not considered a thermodynamic problem. In current research, we show that if incorporated in a compound setup, such an intrinsically nonequilibrium behavior has nontrivial consequences and cannot circumvent thermodynamics: cold-to-hot heat transfer may happen spontaneously, either continuously (with an energy barrier) or cyclically (with time-dependent entropy barriers). It allows for production of useful work by absorbing heat from a single thermal reservoir without any other effect. As the system obeys the first law of thermodynamics, it breaks the boundaries of the second law of thermodynamics. © 2023, CC BY.

关键词： Energy barriers

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Sensing property of Ga2O3-based extended-gate field-effect transistors for a living cell viability sensor

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Sensors and Actuators A: Physical 2023年 349卷

作者： Chou, Hsin-Yu Chiang, Jung-Lung Yu, Chang-Tze Ricky Chen, Jo-Mei Maureen Wuu, Dong-Sing Department of Materials Science and Engineering National Chung Hsing University Taichung40227 Taiwan Ph.D. Program Prospective Technology of Electrical Engineering and Computer Science National Chin-Yi University of Technology Taichung411030 Taiwan Department of Applied Chemistry National Chi-Nan University Nantou54561 Taiwan Department of Applied Materials and Optoelectronic Engineering National Chi Nan University Nantou54561 Taiwan

In this study, gallium oxide (Ga2O3) nanorods were deposited onto an indium tin oxide (ITO) glass substrate to develop a real-time living cell viability sensor. Ga2O3 nanorods had characteristics of cell population sensing based on cellular metabolism to detect cell viability. The pH sensing characteristics of Ga2O3-based extended-gate field-effect transistors (EGFETs) with and without the annealing process were measured from pH 1–11. Three different sensor heads, ITO/glass, GaOOH/ITO/glass, and Ga2O3/ITO/glass, were produced as EGFETs and immersed into a pH standard buffer and high-glucose Dulbecco's modified Eagle's medium (DMEM) to investigate hydrogen ion sensing. Results showed that the Ga2O3/ITO/glass probe had the best hydrogen ion sensing sensitivity and stability in different sample buffers. In contrast, GaOOH/ITO/glass had instability and lower sensitivity due to interference with other components in the medium. The drift characteristic of sensors was analyzed to detect long-term stability. The Ga2O3/ITO/glass probe showed lower drift properties, which can potentially monitor the DMEM situation in real-time for a long-term period. During in vitro detection, the Ga2O3/ITO/glass probe revealed a 70 μA/cells change in IDS-VDS analysis and a 10 μV/cells change in IDS-VGS analysis, which was superior linearly dependent within 10,000 cells. The biocompatibility of the Ga2O3/ITO/glass probe was also detected by 3-(4,5-dimethylthiazol-2-yl)− 2,5-diphenyltetrazolium bromide assay and showed no cytotoxicity. Overall, the Ga2O3/ITO/glass EGFET sensor has potential applications as a living cell viability device in microenvironmental studies in the future. © 2022 Elsevier B.V.

关键词： Nanorods

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Nanoarchitectonics of europium vanadate nanoparticles decorated carbon nanofibers for electrochemical detection of fungicide in fruits

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Journal of the Taiwan Institute of Chemical Engineers 2024年 161卷

作者： Huang, Song-Jeng Gokulkumar, Kumar Govindasamy, Mani Albaqami, Munirah D. Wabaidur, Saikh Mohammad Department of Mechanical Engineering National Taiwan University of Science and Technology Taipei City106335 Taiwan Department of Research and Innovation Saveetha School of Engineering SIMATS Chennai602105 India International Ph.D. Program in Innovative Technology of Biomedical Engineering and Medical Devices Ming Chi University of Technology New Taipei City243303 Taiwan Department of Chemistry College of Science King Saud University Riyadh11451 Saudi Arabia

Background: Fungicides, like carbendazim, have effects on male fertility. There have been sufficient studies conducted on certain chemical compounds to indicate a selective action at the epididymis level. To prevent contamination of food products with fungicides, most of the governments have established rules for the use of fungicides. However, even though this type of fungicide is primarily used in agriculture. More probably, it's contaminated with fruits and vegetables. In particular, carbendazim is one of the major fungicides in the agricultural usage Methods: This research work developed a europium vanadate (EuVO4) nanoparticle decorated carbon nanofiber (CNF) composites by hydrothermal-sonochemical approach. Based on this composite, Carbendazim sensing is developed through electrochemical oxidation based on EuVO4/f-CNF modified Glassy Carbon Electrode (GCE). By combining EuVO4 and f-CNF with the GCE, carbendazim detection can be highly effective. GCEs are rigid, making them ideal for depositing EuVO4/f-CNF, while their expansive surface area makes it possible to immobilize a greater amount of EuVO4/f-CNF, which could increase the Carbendazim sensing ability of the resulting modified GCEs with EuVO4/f-CNF. Main Findings: : The carbendazim sensing was actualized by the electrocatalytic oxidation of carbendazim on the composite modified electrode, and it is demonstrating a linear range of 0.125 to 23.875 – 33.81 to 131.375 µM with a remarkably limit of detection of 0.00612 µM. The EuVO4/f-CNF /GCE also showcased an excellent degree of stability, retaining 96.5 % of its initial activity even after 30 days. This research highlights the potential of EuVO4/f-CNF modified GCEs as robust, and efficient platform for the carbendazim detection under electrochemical approach. © 2024 Taiwan Institute of Chemical Engineers

关键词： Carbon nanofibers

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Electro osmotically flow of fourth-grade fluid in complex channel with porous medium and lubricated walls: applications in petroleum industry

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Waves in Random and Complex Media 2023年

作者： Nazeer, Mubbashar Pasha, Amjad Ali Hussain, Farooq Adil, Mohammad Mechanical Engineering Program Physical Science and Engineering Division King Abdullah University of Science and Technology Thuwal Saudi Arabia BUITEMS Quetta Pakistan KAUST Clean Combustion Research Center King Abdullah University of Science and Technology Thuwal Saudi Arabia Department of Mathematics Institute of Arts and Sciences Government College University Faisalabad Chiniot Campus Pakistan Aerospace Engineering Department King Abdulaziz University Jeddah Saudi Arabia

This article offers a distinct survey of a multiphase flow through a uniform channel. The electro-osmotic phenomenon is the main source of the flow. Fourth-grade fluid model is used as the base liquid which is suspended with metallic particles to form a bi-phase viscous suspension. Skin friction effects are tackled by employing lubrication effects on the opposite walls of the channel. Porous media is governed by the modified Darcy’s law and the Poisson differential equation is considered for electric double-layer effects. An approximate solution is achieved for the nonlinear fluid flow. The obtained findings are also compared with the existing literature for the limiting case. It is inferred that the shear thickness effects cause the momentum of the bi-phase flow to decline, gradually. However, the motion of the metallic particles is supported by the lubrication effects on the walls of the channel. © 2023 Informa UK Limited, trading as Taylor & Francis Group.

关键词： Porous materials

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