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Fabrication and Characterization of Willemite Scaffolds Using Corn Stalk as a Novel Bio Template for Bone Tissue engineering Applications

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Journal of Bionic engineering 2023年第1期20卷 16-29页

作者： Zahra Yahay Seyed Mehdi Mirhadi Fariborz Tavangarian Department of Cellular Biotechnology Cell Science Research CenterRoyan Institute for BiotechnologyACECRIsfahan81593-58686Iran Department of Materials Engineering Shahreza BranchIslamic Azad UniversityShahrezaIsfahan86145-311Iran Mechanical Engineering Program School of ScienceEngineering and TechnologyPennsylvania State UniversityHarrisburgMiddletownPA17057USA

In this paper,we used Corn Stalk(CS)as a renewable and economical bio template to fabricate willemite scaffolds with the potential application in skull bone *** was used as a sacrificial template to synthesize the *** scaffolds with the chemical formula of Zn2SiO4 and pore size in the range of 3 to 10µm could be successfully synthesized by soaking CS in the willemite solution for 24 h and sintering at 950°C for 5 *** porosity of the samples was controlled by the soaking time(between 12 and 48 h)in the willemite solution from 5 to 35%,*** properties of these scaffolds showed a good approximation with cranial bone *** addition,cytotoxicity assays(MTT)were performed on Human Bone Marrow Stromal cells(HBMSc)and A172 human glioblastoma cell lines by direct and indirect culture methods to estimate their toxicity for bone and nerve cells,*** Phosphatase(ALP)activity and DAPI/Phalloidin cell staining were also performed to investigate the efficiency of the scaffolds for bone tissue engineering *** results showed that the scaffolds had good biocompatibility with both HBMSC and A172 cells,noticeable improvement on ALP activity,and great apatite formation ability in Simulated Body Fluid(SBF).All the evidence ascertained that willemite scaffolds made by corn stalks could be a useful candidate for bone tissue engineering applications.

关键词： Corn stalk Bio template Bioactive ceramics-Scaffolds Bone tissue engineering

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Crafting chirality in three dimensions via a novel fabrication technique for bound states in the continuum metasurfaces

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Light(science & Applications) 2024年第3期13卷 390-392页

作者： Zaid Haddadin Anna My Nguyen Lisa V.Poulikakos Department of Electrical&Computer Engineering University of California San DiegoLa JollaCAUSA Department of Mechanical&Aerospace Engineering University of California San DiegoLa JollaCAUSA Program of Materials Science&Engineering University of California San DiegoLa JollaCAUSA

An additional deposition step was added to a multi-step electron beam lithographic fabrication process to unlock the height dimension as an accessible parameter for resonators comprising unit cells of quasi-bound stat... 详细信息

关键词： dimensions dimension intrinsic

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Excitations in layered materials from a non-empirical Wannier-localized optimally-tuned screened rangeseparated hybrid functional

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npj Computational materials 2024年第1期10卷 132-140页

作者： María Camarasa-Gómez Stephen E.Gant Guy Ohad Jeffrey B.Neaton Ashwin Ramasubramaniam Leeor Kronik Department of Molecular Chemistry and Materials Science Weizmann Institute of ScienceRehovoth7610001Israel Department of Physics University of CaliforniaBerkeleyCA94720USA Materials Sciences Division Lawrence Berkeley National LaboratoryBerkeleyCA94720USA Kavli Energy NanoSciences Institute at Berkeley University of CaliforniaBerkeleyCA94720USA Department of Mechanical and Industrial Engineering University of Massachusetts AmherstAmherstMA01003USA Materials Science and Engineering Graduate Program University of MassachusettsAmherstAmherstMA01003USA

Accurate prediction of electronic and optical excitations in van der Waals(vdW)materials is a long-standing challenge for density functional *** recent Wannier-localized optimally-tuned screened range-separated hybrid(WOT-SRSH)functional has proven successful in non-empirical determination of electronic band gaps and optical absorption spectra for covalent and ionic ***,for vdW materials the tuning of the material-and structure-dependent functional parameters has only been attained ***,we present a non-empirical WOT-SRSH approach applicable to vdW materials,with the optimal functional parameters transferable between monolayer and *** apply this methodology to prototypical vdW materials:black phosphorus,molybdenum disulfide,and hexagonal boron nitride(in the latter case including zero-point renormalization).We show that the WOT-SRSH approach consistently achieves accuracy levels comparable to experiments and many-body perturbation theory(MBPT)calculations for band structures and optical absorption spectra,both on its own and as an optimal starting point for MBPT calculations.

关键词： theory optimal functional

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INTER- AND INTRA-LAMINAR PROPERTIES OF AN AFP POST-PROCESSED THERMOPLASTIC COMPOSITE

INTER- AND INTRA-LAMINAR PROPERTIES OF AN AFP POST-PROCESSED...

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SAMPE 2024 Conference and Exhibition

作者： Yap, Timothy S. Heathman, Nathaniel M. Kirchhoff, Joseph G. Tehrani, Mehran Walker Department of Mechanical Engineering The University of Texas at Austin AustinTX United States Department of Structural Engineering University of California La Jolla San DiegoCA United States Program in Materials Science and Engineering University of California La Jolla San DiegoCA United States

ISBN: (纸本)9781934551455

Transitioning to high-performance thermoplastic composites (TPCs) carries great potential due to their enhanced toughness, ease of repairability, and the possibility of bypassing the need for autoclaves that are essential for curing thermosetting composites. Full consolidation of parts may be achieved in-situ using automated fiber placement (AFP) at slow rates;alternatively, with higher rates, consolidation may only occur following vacuum-bag oven processing (vacuum-bag only or VBO) or compression molding (CM) post-processing. This study investigates the CM of AFP carbon fiber LM-PAEK™ composites at a low pressure of 0.2 MPa to simulate VBO post-processing, focusing on their intra- and inter-laminar behavior. Short-beam strength, fracture toughness modes I and II, and transverse tensile and compressive samples were manufactured via AFP using a fast layup rate, followed by low-pressure CM. As compared to previous studies, post-processing resulted in greater interlaminar bonding. This study demonstrates the viability of TPCs for the next generation of aerospace structures with a relatively simple oven post-processing. © 2024 Soc. for the Advancement of Material and Process engineering. All rights reserved.

关键词： Compression molding

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Bayesian optimization with active learning of design constraints using an entropy-based approach

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npj Computational materials 2023年第1期9卷 1866-1879页

作者： Danial Khatamsaz Brent Vela Prashant Singh Duane D.Johnson Douglas Allaire Raymundo Arróyave J.Mike Walker’66 Department of Mechanical Engineering Texas A&M UniversityCollege StationTX 77843USA Department of Materials Science and Engineering Texas A&M UniversityCollege StationTX 77843USA Ames Laboratory U.S.Department of EnergyIowa State UniversityAmesIA 50011USA Department of Materials Science&Engineering Iowa State UniversityAmesIA 50011USA Department of Industrial and Systems Engineering Texas A&M UniversityCollege StationTX 77843USA

The design of alloys for use in gas turbine engine blades is a complex task that involves balancing multiple objectives and *** alloys must be ductile at room temperature and retain their yield strength at high temperatures,as well as possess low density,high thermal conductivity,narrow solidification range,high solidus temperature,and a small linear thermal expansion *** Integrated Computational materials engineering(ICME)methods are not sufficient for exploring combinatorially-vast alloy design spaces,optimizing for multiple objectives,nor ensuring that multiple constraints are *** this work,we propose an approach for solving a constrained multi-objective materials design problem over a large composition space,specifically focusing on the Mo-Nb-Ti-V-W system as a representative Multi-Principal Element Alloy(MPEA)for potential use in next-generation gas turbine *** approach is able to learn and adapt to unknown constraints in the design space,making decisions about the best course of action at each stage of the *** a result,we identify 21 Pareto-optimal alloys that satisfy all *** proposed framework is significantly more efficient and faster than a brute force approach.

关键词： alloys solidification alloy

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Microencapsulated paraffin as a tribological additive for advanced polymeric coatings

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Friction 2023年第10期11卷 1939-1952页

作者： Reza GHEISARI Mariela VAZQUEZ Vasilis TSIGKIS Ali ERDEMIR Karen L.WOOLEY Andreas A.POLYCARPOU J.Mike Walker’66 Department of Mechanical Engineering Texas A&M UniversityCollege Station 77843USA Department of Chemistry Texas A&M UniversityCollege Station 77843USA Department of Materials Science&Engineering Texas A&M UniversityCollege Station 77843USA Department of Chemical Engineering Texas A&M UniversityCollege Station 77843USA

Numerous tribological applications,wherein the use of liquid lubricants is infeasible,require adequate dry *** the use of polymers as an effective solution for dry sliding tribological applications,their poor wear resistance prevents the utilization in harsh industrial *** methods are typically implemented to tackle the poor wear performance of polymers,however sacrificing some of their mechanical/tribological ***,we discussed the introduction of a novel additive,namely microencapsulated phase change material(MPCM)into an advanced polymeric ***,paraffin was encapsulated into melamine-based resin,and the capsules were dispersed in an aromatic thermosetting co-polyester(ATSP)*** found that the MPCM-filled composite exhibited a unique tribological behavior,manifested as“zero wear”,and a super-low coefficient of friction(COF)of *** developed composite outperformed the state-of-the-art polytetrafluoroethylene(PTFE)-filled coatings,under the experimental conditions examined herein.

关键词： microencapsulated phase change material(MPCM) friction reduction additive advanced polymeric coating

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Controlling the morphology of 2D Laser-induced Periodic Surface Structures (LIPSS) for Surface-enhanced Raman Spectroscopy applications 19

Controlling the morphology of 2D Laser-induced Periodic Surf...

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Laser-based Micro- and Nanoprocessing XIX 2025

作者： Baskar, Balaji Ahad, Atiqul Islam Berrospe-Rodriguez, Carla Aguilar, Guillermo J. Mike Walker’66 Department of Mechanical Engineering Texas A&M University College Station United States Department of Materials Science & Engineering Texas A&M University College Station United States

ISBN: (纸本)9781510684508

The creation of laser-induced periodic surface structures (LIPSS) with near-submicron dimensions has significantly altered the surface properties of materials, as demonstrated in the past decade. These properties, particularly the hydrophobic characteristics, can be enhanced when combined with the dense nanostructures in LIPSS, making them ideal for highly sensitive surface-enhanced Raman spectroscopy (SERS) applications. However, a key challenge lies in precisely controlling the morphology of these nanostructures and their surface contact properties to effectively concentrate analyte molecules in specific regions for detection at extremely low concentrations. Here we show how single and double femtosecond laser pulse irradiation can be used to achieve different LIPSS morphologies. We generate 1D and 2D periodic nanostructures on 304 stainless steel substrates by adjusting the polarization and inter-pulse delay between fs pulses. From the preliminary experimental results, the dense hotspots in these LIPSS-based sensors allow for the detection of Rhodamine 6G at concentrations as low as 10-10 M, with an analytical enhancement factor of 2 × 107 for consistent and repeatable measurements. These findings provide important insights into the control of laser-induced submicron morphologies by adjusting experimental parameters, offering a straightforward and cost-efficient approach for detecting molecules at ultra-trace levels. © 2025 SPIE.

关键词： Femtosecond lasers

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Bubble-pen lithography:Fundamentals and applications

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Aggregate 2022年第4期3卷 85-100页

作者： Pavana Siddhartha Kollipara Ritvik Mahendra Jingang Li Yuebing Zheng Walker Department of Mechanical Engineering The University of Texas at AustinAustinTexasUSA Department of Electrical and Computer Engineering The University of Texas at AustinAustinTexasUSA Material Science and Engineering Program Texas Materials InstituteThe University of Texas at AustinAustinTexasUSA

Developing on-chip functional devices requires reliable fabrication methods with high resolution for miniaturization,desired components for enhanced performance,and high throughput for fast prototyping and mass ***,laser-based bubble-pen lithography(BPL)has been developed to enable sub-micron linewidths,in situ synthesis of custom materials,and on-demand patterning for various functional components and *** exploits Marangoni convection induced by a laser-controlled microbubble to attract,accumulate,and immobilize particles,ions,and molecules onto different *** years have witnessed tremendous progress in theory,engineering,and application of BPL,which motivated us to write this ***,an overview of experimental demonstrations and theoretical understandings of BPL is ***,we discuss the advantages of BPL and its diverse applications in quantum dot displays,biological and chemical sensing,clinical diagnosis,nanoalloy synthesis,and *** conclude this review with our perspective on the challenges and future directions of BPL.

关键词： additive manufacturing capillary flow lithography marangoni convection microbubbles sensing

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An interpretable deep learning approach for designing nanoporous silicon nitride membranes with tunable mechanical properties

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npj Computational materials 2023年第1期9卷 1524-1533页

作者： Ali KShargh Niaz Abdolrahim Department of Mechanical Engineering University of RochesterRochesterNY 14627USA Materials Science program University of RochesterRochesterNY 14627USA Laboratory for Laser Energetics University of RochesterRochesterNY 14627USA

The high permeability and strong selectivity of nanoporous silicon nitride(NPN)membranes make them attractive in a broad range of *** their growing use,the strength of NPN membranes needs to be improved for further extending their biomedical *** this work,we implement a deep learning framework to design NPN membranes with improved or prescribed strength *** examine the predictions of our framework using physics-based *** results confirm that the proposed framework is not only able to predict the strength of NPN membranes with a wide range of microstructures,but also can design NPN membranes with prescribed or improved *** simulations further demonstrate that the microstructural heterogeneity that our framework suggests for the optimized design,lowers the stress concentration around the pores and leads to the strength improvement of NPN membranes as compared to conventional membranes with homogenous microstructures.

关键词： tunable prescribed strength

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Design and development of an integrated enset processing machine suitable for central highland farmers of west shewa zone Ethiopia

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Discover Agriculture 2025年第1期3卷 1-26页

作者： Jima, Beka Adugna Kolhe, Kishor Purushottam Jiru, Moera Gutu Agricultural Machinery Engineering Program Department of Mechanical Engineering School of Mechanical Chemical and Materials Engineering at Adama Science and Technology University Adama Ethiopia Department of Mechanical Engineering School of Mechanical Chemical and Materials Engineering at Adama Science and Technology University Adama Ethiopia

The development of Integrated Enset processing technology is significant for the easy availability of stable food in the current condition for fulfilling the pangs of hunger in Ethiopia, currently; individual manual technologies such as decortication, corm granting, bulla extraction, and fermenting techniques eventually contribute to utilizing food security such as Kocho, which is not affordable for the marginal farmers of Ethiopia. However, there is a lack of integrated compromise of the all-function process of corm granting, decortication, and pulverization in one machine wholesome of the product such as Kocho, and bulla within consuming time and labor. Therefore, it is decided to design and develop an integrated enset processing machine for central high land of Ethiopian farmers with high-quality production. The physical and mechanical properties of the enset is studied to get an efficient and robust design of the various components. The overall design and development of proposed machine components were carried out at Adama science and Technology University, Ethiopia by using ANSYS 2023 R1 software by considering the engineering economics and material specifications as per ASTM standards. The process parameters of the proposed machine are identified as feed rate, drum speed, concave to drum clearance, power requirement, etc. Also, the enset characteristics were considered as decorticating and granting, fiber cutting resistance, fiber length, dimension, shape, and weight. The overall developed enset integrated machine assembles are analyzed for granting and decorticating with drum clearance and bulla extraction throughput capacity, reliability, simplicity, safety, and overall cost. The machine's safety from a Design Perspective is checked and validated by a simulation study on the critical parts subjected to higher stresses. The cost of available individual decorticators, granting, pulverized, and bulla squeezer machines is costly to the farmer’s community. Theref

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