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Enantioselective Rhodium‐Catalyzed Addition of Arylboroxines to N‐Unprotected Ketimines: Efficient Synthesis of Cipargamin

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Angewandte Chemie 2019年第45期131卷

作者： Jinbin Zhu Linwei Huang Wei Dong Naikai Li Xingxin Yu Wei‐Ping Deng Wenjun Tang Shanghai Key Laboratory of New Drug Design School of Pharmacy East China University of Science and Technology 130 Mei Long Rd Shanghai 200237 China State Key Laboratory of Bio-Organic and Natural Products Chemistry Center for Excellence in Molecular Synthesis Shanghai Institute of Organic Chemistry Chinese Academy of Sciences 345 Ling Ling Rd Shanghai 200032 China

Highly enantioselective rhodium‐catalyzed addition of arylboroxines to N‐unprotected ketimines is realized for the first time by employing chiral BIBOP‐type ligands with a Rh loading as low as 1 mol %. A range of chiral α‐trifluoromethyl‐α,α‐diaryl α‐tertiary amines or 3‐amino‐3‐aryloxindoles were formed with excellent ee values and yields by employing either WingPhos or PFBO‐BIBOP as the ligand. The method has enabled an efficient enantioselective synthesis of cipargamin.

关键词： Asymmetrische Katalyse Enantioselektivität Ketimine P-Liganden Rhodium

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26th Annual computational Neuroscience Meeting (CNS*2017) of the Organization for computational Neuroscience Antwerp, Belgium, July 15-20, 2017

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BMC NEUROSCIENCE 2017年第SUPPL 1期18卷 59-59页

作者： [Anonymous] Indiana University Purdue University Indianapolis Indianapolis IN 46032 USA Stark Neurosciences Research Institute Indiana University School of Medicine Indianapolis IN 46032 USA Department of Mathematics East Carolina University Greenville NC 27858 USA Jülich Supercomputing Centre Forschungszentrum Jülich 52425 Jülich Germany Future Systems Swiss National Supercomputing Centre 8092 Zurich Switzerland User Engagement and Support Swiss National Supercomputing Centre 6900 Lugano Switzerland Institut de Neurosciences des Systèmes Aix Marseille Univ 13005 Marseille France Simulation Lab Neuroscience Forschungszentrum Jülich Jülich Germany Department of Experimental Psychology Ghent University 9000 Ghent Belgium Donders Center for Cognitive Neuroimaging Radboud University 6525HR Nijmegen The Netherlands Department of Electrical Computer and Energy Engineering University of Colorado Boulder CO 80309 USA Department of Neurosurgery Johns Hopkins School of Medicine Baltimore MD 21287 USA Department of Neurology Johns Hopkins School of Medicine Baltimore MD 21287 USA Department of Otolaryngology Johns Hopkins School of Medicine Baltimore MD 21287 USA INSERM U968 Paris France Sorbonne Universités UPMC University Paris 06 UMR_S 968 Institut de la Vision Paris France CNRS UMR_7210 Paris France Department of Computer Architecture and Technology University of Granada (CITIC) Granada Spain Sorbonne Universités UPMC Univ Paris 06 INSERM CNRS Institut de la Vision Paris France Department of Adaptive Machine Systems Osaka University Osaka Japan Department of Computer Science University of Cergy-Pontoise Cergy-Pontoise France Department of Physics and Astronomy College of Charleston Charleston SC 29424 USA School of Physics Faculty of Science University of Sydney Sydney NSW 2006 Australia Center of Excellence for Integrative Brain Function Australian Research Council Sydney Australia Max Planck Institute for Human Cognitive and Brain Sciences Saxony Lei

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EPMA-World Congress 2015 Bonn, Germany. 3-5 September 2015 Abstracts

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EPMA JOURNAL 2016年第SUPPL 1期7卷 9-9页

作者： [Anonymous] Department of Radiology University of Bonn Sigmund-Freud-Str. 25 53105 Bonn Germany Market Access at Unicorn P.O.B. 91 Zhytomyr 10020 Ukraine Nanotechnology & Smart Systems NASA Ames Research Center Moffett Field CA USA Department of Neurosurgery Valparaiso University Medical School Valparaiso Chile Department of Oral Biology College of Dental Medicine Georgia Regents University Augusta Georgia 30912 USA Research Developing and Training Centre of Molecular Microbiology and Mucosal Immunology Uzhhorod National University Uzhhorod Ukraine “Astra-DIA” Medical Diagnostic Centre Uzhhorod Ukraine Cassovia Life Science Kysucké Nové Mesto Slovakia Department of Biomedical Engineering Wroclaw University of Technology Wroclaw Poland Faculty of Physiotherapy Wrocław University School of Physical Education Wroclaw Poland Pavol Jozef Šafárik University Košice Slovakia Uzhhorod National University Uzhhorod Ukraine Clinical Hospital “Pheophania” of State Affairs Department The Centre of Ultrasound Diagnostics and Interventional Sonography Kyiv Ukraine Association “Health and Wealth” Kyiv Ukraine TSBUA “IT Solutions” Kyiv Ukraine Maastricht University Medical Centre Maastricht The Netherlands Fleischhacker GmbH Schwerte Germany RIMS bvba Overijse Belgium German Foundation For the Chronically Ill Fürth Germany Linköping University Norrköping Sweden Medical Faculty Pilsen Pilsen Czech Republic Sananet Care BV Sittard The Netherlands Exploris AG Zürich Switzerland ense.ly San Francisco USA Mulimedica SPA Milano Italy Medtronic Iberica SA Madrid Spain Clinical Hospital “Pheophania” of State Affairs Department Zabolotny Str. 21 Kyiv 03680 Ukraine Zabolotny Institute of Microbiology and Virology National Academy of Sciences of Ukraine 154 Zabolotny st. Kyiv 03680 Ukraine Endocrinology centre Clinical Hospital “Pheophania” of State Affairs Department Zabolotny Str. 21 Kyiv 03680 Ukraine Bogomolets National Medical University T. Shevchenko boulevard 13 Kyi

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31st Annual Meeting and Associated Programs of the Society for Immunotherapy of Cancer (SITC 2016): part two Abstracts

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JOURNAL FOR IMMUNOTHERAPY OF CANCER 2016年第SUPPL 1期4卷 107-221页

作者： [Anonymous] Department of Immunology University of Texas MD Anderson Cancer Center Houston TX USA Department of Cancer Medicine University of Texas MD Anderson Cancer Center Houston TX USA Immune Design Seattle WA USA Innate Pharma Marseille Provence-Alpes-Cote d’Azur France MedImmune Cambridge England UK Georgetown-Lombardi Comprehensive Cancer Center Washington DC USA Westmead and Blacktown Hospitals Melanoma Institute Australia and the University of Sydney Westmead New South Wales Australia University of California Los Angeles CA USA University of Washington Seattle WA USA Dana-Farber Cancer Institute/Brigham and Women’s Hospital Harvard University Boston MA USA University of Texas MD Anderson Cancer Center Houston TX USA Beth Israel Deaconess Medical Center Boston MA USA Gallipoli Medical Research Foundation Greenslopes Private Hospital and the University of Queensland Greenslopes Queensland Australia Olivia Newton-John Cancer Research Institute Heidelberg Victoria Australia Canterbury District Health Board Christchurch Hospital Christchurch New Zealand Waikato Hospital Regional Cancer Centre Hamilton New Zealand Royal Prince Alfred Hospital Melanoma Institute Australia the University of Sydney and Chris O’Brien Lifehouse Camperdown New South Wales Australia Tasman Oncology Research Southport Gold Coast Queensland Australia Merck & Co. Inc. Kenilworth NJ USA Quantitative Solutions A Certara Company Oss Netherlands Melanoma Institute Australia the University of Sydney Mater Hospital and Royal North Shore Hospital Wollstonecraft New South Wales Australia Columbia University Medical Center New York NY USA Institut d’Investigacions Biomediques August Pi i Sunyer Barcelona Catalonia Spain Icahn School of Medicine at Mount Sinai New York NY USA New York Presbyterian/Columbia University Medical Center New York NY USA Memorial Sloan Kettering Cancer Center New York NY USA Peregrine Pharmaceuticals Inc. Tustin CA USA Regeneron Tarrytown NY USA University of

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Symposia lectures

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Journal of biosciences 1999年第1期24卷 5-31页

作者： F. Parak A. Ostermann G. U. Nienhaus Nobuo Niimura William A. Eaton Stephen J. Hagen Eric R. Henry James Hofrichter Gouri Jas Lisa Lapidus Victor Muñoz Chih-chen Wang Abani Bhuyan Javant Udgaonkar Heinz Rüterians Derek N. Woolfson M. D. Finucane J. H. Lees M. J. Pandya G. Spooner M. Tuna Wilma K. Olson K. V. R. Chary E. Westhof I. G. Wool C. C. Correll V. I. Ivanov S. A. Bondarenko E. M. Zdobnov A. D. Beniaminov E. E. Minyat N. B. Ulyanov Dale B. Wigley Nobuo Shimamoto Takashi Kinebuchi Hiroyuki Kabata Osamu Kurosawa Masao Washizu Barbara Baird David Holowka H. Belrhali P. Nollert A. Royant J. P. Rosenbusch E. M. Landau E. Pebav-Peyroula Anil K. Lala Patrick R. D’Silva Daniela Pietrobon Paolo Pinton Paulo Magalhaes Anna Chiesa Marisa Brini Tullio Pozzan Rosario Rizzuto M. Montai Shu-Rong Wang José L. Carrascosa B. Bhattacharyya Ian A. Wilson Dinakar M. Salunke Kurt Drickamer Anne Imberty A. Surolia Louise N. Johnson Michal Neeman S. M. Prince K. McLuskey R. J. Cogdell K. McAuley N. W. Isaacs G. Venturoli F. Drepper J. C. Williams J. P. Allen X. Lin P. Mathis R. van Grondelle Wolfgang Junge T. Tsukihara K. Shinzawa-Itoh R. Nakashima E. Yamashita M. J. Fei N. Inoue T. Tomizaki C. Peters Libeu S. Yoshikawa Patrick Chaussepied Keiichi Namba Marie-France Carlier Fariza Ressacl Valerie Laurent Thomas Loisel Coumaran Egile Philippe Sansonetti Dominique Pantaloni Manju Bansal E. W. Knapp M. G. Ullmann A. Amadei B. L. de Groot M. A. Ceruso M. Paci H. J. C. Berendsen A. Di Nola V. Di Francesco P. J. Munson J. Garnier Sung-Hou Kim Jean-Michel Claverie Ian C. P. Smith P. T. Callaghan Bruce Cornell Ratna S. Phadke Kazuhiko Kinosita D. Goldfarb I. Qromov C. Shutter I. Pecht P. Manikandan R. Carmieli T. Shane David S. Moss Clare E. Sansom Jeremy K. Cockcroft Ian J. Tickle Huub C. P. Driessen J. Raul Grigera Ramen K. Poddar Charles R. Cantor Barry Robson Jean Garnier John Helliwell Sunney I. Chan Ronald Rock Physik-Department El7 Technische Universität München Garching Abteilung Biophysik Universität Ulm Ulm Advanced Science Research Center Japan Atomic Energy Research Institute Japan Laboratory of Chemical Physics NIDDK National Institutes of Health Bethesda USA National Lab of Biomacromolecules Institute of Biophysics Beijing China National Centre for Biological Sciences Bangalore Institute of Biophysical Chemistry University of Frankfurt Frankfurt/Main Germany Centre for Biomolecular Design and Drug Development University of Sussex UK Rutgers University Piscataway USA Department of Chemical Sciences Tata Institute of Fundamental Research Mumbai India IBMC-CNRS Strasbourg France Department of Biochemistry and Molecular Biology The University of Chicago Chicago USA Engelhardt Institute of Molecular Biology RAS Moscow Russia Sir William Dunn School of Pathology University of Oxford Oxford UK Structural Biology Center National Institute of Genetics Japan Faculty of Engineering Kyoto University Kyoto Advance Co. Tokyo Japan Department of Chemistry and Chemical Biology Cornell University Ithaca Institute de Biologie Structurale Joseph Fourier Grenoble Cedex 1 France Biomembrane Lab Department of Chemistry and Biotechnology CenterIndian Institute of Technology Bombay Powai Mumbai India Dept of Biomedical Sciences Univ. of Padova Italy Dept. Exp. Diagn. Med. Sect. Gen. Pathol Ferrara Italy Department of Biology University of California San Diego La Jolla USA Chinese Academy of Sciences Institute of Biophysics Beijing China Centra Nacional de Biotecnología CSIC. Campus de la Universidad Autónoma de Madrid Cantoblanco Spain Dept.of Biochemistry Bose Institute Calcutta-54 India The Scripps Research Institute La Jolla National Institute of Immunology New Delhi India Glycobiology Institute Department of Biochemistry University of Oxford Oxford UK Centre de Recherches sur les Macromolécules Végétales-CNRS Grenoble cedex 9 France Molecular Biophysics Uni

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FERMENTATION AND GENETIC-ENGINEERING - PROBLEMS AND PROSPECTS

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bio-TECHNOLOGY 1983年第10期1卷 847-&页

作者： BULL, DN Daniel N. Bull Ph.D. is a consultant in fermentation technology and president of Satori Corporation P.O. Box 1730 Montclair N.J. 07042. (201) 783-9787.REFERENCES Graff G.M. Short H. and Keene J.1983. Gene-splicing methods move from lab to plant. Chem. Eng.90: 22-27.|ISI|Broda P.1979. p. 1-3. Plasmids. W. H. Freeman Oxford and San Francisco.Donoghue D.J. and Sharp P.A.1978. Construction of a hybrid bacteriophage-plasmid recombinant DNA vector. J. Bact.136: 1192-1196.|PubMed|ISI|ChemPort|Bok S.H. Hoppe D. Mueller D.C. and Lee S.E.1983. Improving the production of recombinant DNA proteins through fermentation development. Abstract from 186th ACS Natl. Mtg. Washington D.C. Sept. 1.Maniatis T. Fritsch E.F. and Sam-brook J.1982. p. 88. Molecular Cloning. Cold Spring Harbor Laboratory. Guidelines for research involving recombinant DNA molecules June 1983 Fed. Reg.48: 24556-24581. Modifications of physical containment recommendations for large-scale uses of organisms containing recombinant DNA molecules. 1983. Recomb. DNA Tech. Bull.6: 69-70.Bull D.N. Thoma R.W. and Stinnett T.E.1983. Bioreactors for submerged culture. In:Adv. in Biotechnological Proc. A. Mizrahi and A. L. van Wezel (eds.) 1: 1-30.Schmidli B.L. and Swartz R.W.1982. Design considerations for aseptic fermentation. Presentation at 184th ACS Natl. Mtg. Kanas City MO.Sittig W.1982. The present state of fermentation reactors. J. Chem. Tech. Biotechnol.32: 47-58.|ISI|Strek F.1963. Intl. Chem. Eng.3: 533.Uhl V.W. and Gray J.B.1996. Mixing Theory and Practice Vol. I. Academic Press New York.Peters M.S. and Timmerhaus K.D.1968. p. 542. Plant Design and Economics for Chemical Engineers. McGraw-Hill New York.Dickey D.S. and Hicks R.W. Fundamentals of agitation. Chem. Eng.83: 93-100.Oldshue J.Y.1983. Fluid mixing technology and practice. Chem. Eng.90: 82-108.Kipke K.D.1981. Heat transfer in aerated non-Newtonian fluids. Abstract from 2nd Eur. Cong. Biotech. Eastbourne UK April 5-10.Blakebrough N. McM

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