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A New Class of Fillers in Mixed Matrix Membranes: Use of Synthetic Silico-Metallic Mineral Particles (Ssmmp) as a Highly Selective Component for Co2/N2 Separation

SSRN

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SSRN 2023年

作者： Ferrari, Henrique Z. Rodrigues, Daniela M. Bernard, Franciele L. dos Santos, Leonardo M. Le Roux, Christophe Micoud, Pierre Martin, François Einloft, Sandra Post-Graduation Program in Materials Engineering and Technology School of Technology Pontifical Catholic University of Rio Grande do Sul – PUCRS Brazil School of Technology Pontifical Catholic University of Rio Grande do Sul - PUCRS Porto Alegre Brazil Université de Toulouse ERT Géomatériaux Toulouse France

Membrane-based CO2 separation technology is a promising technology of low operating and energy costs and high scalability. This work describes the influence of synthetic silico-metallic mineral particles (SSMMP) and SSMMP/ionic liquids (IL) associated with polysulfone (PSF) to produce new mixed matrix membranes (MMM) for post-combustion technology. SSMMP is the precursor of synthetic talc undergoing no hydrothermal process resulting in a low-cost, energy-demanding, and CO2-free emission material due to its synthesis process. SSMMP have many reactive OH groups free on their surface making this material ideal to be compatibilized in a polymeric matrix. IL was immobilized in SSMMP to further improve CO2 affinity. As far as we know is the first time this material is used to obtain MMMs. MMMs were prepared with concentrations of 0.5, 1, 2 and 3 wt% of fillers via melting solution and solvent evaporation. The obtained MMMs were characterized by scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS) with elemental mapping, thermogravimetric analysis (TGA), differential scanning calorimetry (DSC) and X-ray diffraction (XRD). Permeability analyzes were carried out at 25°C and 0.4MPa. The addition of pristine SSMMP and SSMMP/Im(nBu)Tf2N, improved membrane selectivity decreasing the permeability for the majority tested filler content. When using SSMMP/Im(nBu)I to obtain MMMs a different behavior was observed decreasing selectivity (except for MMM with 2% (w/w) of filler) and increasing permeability in all studied concentrations. The best result was obtained for sample SSMMP/Im(nBu)Tf2N (2%w/w) achieving a selectivity of 71.9, four times higher than pristine polysulfone membrane. © 2023, The Authors. All rights reserved.

关键词： Carbon dioxide

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Co2 Capture Using Silica-Immobilized Dicationic Ionic Liquids with Magnetic and Non-Magnetic Properties

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SSRN 2023年

作者： Duarte, Evandro Bernard, Franciele Dos Santos, Leonardo Moreira Polesso, Bárbara B. Duczinski, Rafael Forneck, Vitor Geshev, Julian Einloft, Sandra Post-Graduation Program in Materials Engineering and Technology Pontifical Catholic University of Rio Grande do Sul – PUC RS Brazil School of Technology Pontifical Catholic University of Rio Grande do Sul – PUC RS Brazil Institute of Physics Federal University of Rio Grande do Sul RS Porto Alegre Brazil

The need to find alternative materials to replace aqueous amine solutions for CO2 capture in post-combustion technologies is pressing. This study assesses the CO2 sorption capacity and CO2/N2 selectivity of three dicationic ionic liquids with distinct anions immobilized in commercial mesoporous silica support (SBA-15). The samples were characterized by UART-FTIR, NMR, Raman, FESEM, TEM, TGA, Magnetometry (VSM), BET and BJH. The highest CO2 sorption capacity and CO2/N2 selectivity were obtained for sample SBA@DIL_2FeCl4 [at 1 bar and 25°C;57.31 (±0.02) mg CO2/g;12.27 (±0.72)]. The results were compared to pristine SBA-15 and revealed a similar sorption capacity, indicating that the IL has no impact on the silicás CO2 sorption capacity. On the other hand, the selectivity was improved by approximately 3.8, demonstrating the ionic liquid´s affinity for the CO2 molecule. The material underwent multiple sorption/desorption cycles and proved to be stable and a promising option for use in industrial CO2 capture processes. © 2023, The Authors. All rights reserved.

关键词： Carbon dioxide

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Occurrence and fate of pharmaceutical pollutants in wastewater: Insights on ecotoxicity, health risk, and state–of–the-art removal

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Chemosphere 2024年 354卷 141678页

作者： Nguyen, Minh-Ky Lin, Chitsan Bui, Xuan-Thanh Rakib, Md. Refat Jahan Nguyen, Hoang-Lam Truong, Quoc-Minh Hoang, Hong-Giang Tran, Huu-Tuan Malafaia, Guilherme Idris, Abubakr M. Faculty of Environment and Natural Resources Nong Lam University Hamlet 6 Linh Trung Ward Thu Duc City Ho Chi Minh City700000 Viet Nam Ph.D. Program in Maritime Science and Technology National Kaohsiung University of Science and Technology Kaohsiung81157 Taiwan Department of Marine Environmental Engineering National Kaohsiung University of Science and Technology Kaohsiung81157 Taiwan Linh Trung Ward Thu Duc City Ho Chi Minh City700000 Viet Nam Ho Chi Minh City700000 Viet Nam Department of Environmental Science and Management North South University Dhaka Bashundhara1229 Bangladesh Department of Civil Engineering McGill University Montreal Canada Faculty of Management Science Thu Dau Mot University Binh Duong 75000 Viet Nam Faculty of Medicine Dong Nai Technology University Dong Nai Bien Hoa76100 Viet Nam Laboratory of Ecology and Environmental Management Science and Technology Advanced Institute Van Lang University Ho Chi Minh City700000 Viet Nam Faculty of Applied Technology School of Engineering and Technology Van Lang University Ho Chi Minh City700000 Viet Nam Post-Graduation Program in Ecology Conservation and Biodiversity Federal University of Uberlândia MG Uberlândia Brazil Post-Graduation Program in Biotechnology and Biodiversity Federal University of Goiás GO Goiânia Brazil Post-Graduation Program in Conservation of Cerrado Natural Resources Goiano Federal Institute GO Urutaí Brazil Department of Chemistry College of Science King Khalid University Abha62529 Saudi Arabia King Khalid University Abha62529 Saudi Arabia

Pharmaceutical active compound (PhAC) residues are considered an emerging micropollutant that enters the aquatic environment and causes harmful ecotoxicity. The significant sources of PhACs in the environment include the pharmaceutical industry, hospital streams, and agricultural wastes (animal husbandry). Recent investigations demonstrated that wastewater treatment plants (WWTPs) are an important source of PhACs discharging ecosystems. Several commonly reported that PhACs are detected in a range level from ng L−1 to μg L−1 concentration in WWTP effluents. These compounds can have acute and chronic adverse impacts on natural wildlife, including flora and fauna. The approaches for PhAC removals in WWTPs include bioremediation, adsorption (e.g., biochar, chitosan, and graphene), and advanced oxidation processes (AOPs). Overall, adsorption and AOPs can effectively remove PhACs from wastewater aided by oxidizing radicals. Heterogeneous photocatalysis has also proved to be a sustainable solution. Bioremediation approaches such as membrane bioreactors (MBRs), constructed wetlands (CWs), and microalgal-based systems were applied to minimize pharmaceutical pollution. Noteworthy, applying MBRs has illustrated high removal efficiencies of up to 99%, promising prospective future. However, WWTPs should be combined with advanced solutions, e.g., AOPs/photodegradation, microalgae–bacteria consortia, etc., to treat and minimize their accumulation. More effective and novel technologies (e.g., new generation bioremediation) for PhAC degradation must be investigated and specially designed for a low-cost and full-scale. Investigating green and eco-friendly PhACs with advantages, e.g., low persistence, no bioaccumulation, less or non-toxicity, and environmentally friendly, is also necessary. © 2024 Elsevier Ltd

关键词： Microalgae

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Effects of Sulfamethazine and Tetracycline at Molecular, Cellular and Tissue Levels in Eisenia Fetida Earthworms

SSRN

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SSRN 2024年

作者： Rutkoski, C.F. Vergara-Luis, I. Urionabarrenetxea, Erik García-Velasco, Nerea Zaldibar, B. Anza, M. Olivares, Maitane Prieto, Ailett Epelde, L. Garbisu, C. Almeida, E.A. Soto, Manu Environmental Engineering Post-Graduation Program University of Blumenau SC Blumenau Brazil Department of Natural Science University of Blumenau SC Blumenau Brazil Basque Country Leioa Spain Plentzia Basque Country Spain Basque Country Leioa Spain Parque Científico y Tecnológico de Bizkaia P812 Basque Country DerioE-48160 Spain

Soil contamination by antibiotics is a global issue of great concern that contributes to the rise of bacterial antibiotic resistance and can have toxic effects on non-target organisms. This study evaluated the variations of molecular, cellular, and histological parameters in Eisenia fetida earthworms exposed to sulfamethazine (SMZ) and tetracycline (TC), two antibiotics commonly found in agricultural soils. The earthworms were exposed for 14 days to a series of concentrations (0, 10, 100, and 1000 mg/kg) of both antibiotics. Sulfamethazine and TC did not affect the survival of E. fetida, however, other effects at different levels of biological complexity were detected. The two highest concentrations of SMZ reduced the viability of coelomocytes. At the highest TC concentration, there was a noticeable decline in cell viability, acetylcholinesterase activity, and the relative presence of mucopolysaccharides in the epidermis. Glutathione S-transferase activity decreased in all TC treatments and at the highest SMZ concentration. However, levels of malondialdehyde and protein carbonyls did not change, suggesting an absence of oxidative stress. Tetracycline was neurotoxic to E. fetida and changed the integrity of the epidermis. Both antibiotics altered the intestinal microbiota of E. fetida, leading to a reduction in the relative abundance of bacteria from the phyla Proteobacteria and Bacteroidetes, while causing an increase in the phylum Actinobacteroidota. All observed changes indicate that both SMZ and TC can disrupt the earthworms' immune system and gut microbiome, while fostering the growth of bacteria that harbour antibiotic resistance genes. Finally, both antibiotics exerted additional metabolic and physiological effects that increased the vulnerability of E. fetida to pathogens. © 2024, The Authors. All rights reserved.

关键词： Antibiotics

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Toxicity Induced Via Ingestion of Naturally-Aged Polystyrene Microplastics by a Small-Sized Terrestrial Bird and its Potential Role as Vectors for the Dispersion of These Pollutants

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SSRN 2022年

作者： de Souza, Sindoval Silva Freitas, Ítalo Nascimento de Oliveira Gonçalves, Sandy Luz, Thiarlen Marinho da Araújo, Amanda Pereira da Costa Rajagopal, Rajakrishnan Balasubramani, Govindasamy Rahman, Md Mostafizur Malafaia, Guilherme Laboratory of Toxicology Applied to the Environment Goiano Federal Institute Urutaí GO Brazil Post-Graduation Program in Conservation of Cerrado Natural Resources Goiano Federal Institute Urutaí GO Brazil Post-Graduation Program in Environmental Sciences Federal University of Goiás Goiânia Brazil Department of Botany and Microbiology College of Science King Saud University Riyadh Saudi Arabia Division of Research and Innovation Department of Biotechnology Saveetha School of Engineering Saveetha Institute of Medical and Technical Sciences Sriperambudur Tamil Nadu 600124 India Department of Environmental Sciences Jahangirnagar University Dhaka1342 Bangladesh Laboratory of Environmental Health and Ecotoxicology Department of Environmental Sciences Jahangirnagar University Dhaka1342 Bangladesh Post-Graduation Program in Ecology Conservation and Biodiversity Federal University of Uberlândia Uberlândia MG Brazil Post-Graduation Program in Biotechnology and Biodiversity Federal University of Goiás GO Goiânia Brazil

关键词： Biochemistry

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Dual Synergetic Approach for Targeting Dysfunctional Cells Based on Rare-Earth-Doped Forsterite Nanoparticles

SSRN

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SSRN 2024年

作者： Zampiva, Rúbia Young Sun Kaufmann, Claudir Gabriel Viana, Altevir Rossato Rhoden, Cristiano Rodrigo Bohn Krause, Luciana Maria Fontanari Mortari, Sergio Roberto Rossi, Marco Bergmann, Carlos Pérez Alves, Annelise Kopp Jacinto, Carlos Brazil Post-Graduation Program in Mining Metallurgical and Materials Engineering Federal University of Rio Grande do Sul-UFRGS RS Porto Alegre90035-190 Brazil RS Santa Maria Brazil Group of Cell Culture Bioscience Laboratory Franciscan University -UFN RS Santa Maria97010-032 Brazil Universidade Federal de Alagoas Brazil Department of Basic and Applied Sciences for Engineering University of Rome Sapienza RM Rome00185 Italy

In recent years, forsterite (Fo, Mg₂SiO₄) has emerged as a promising biomaterial for bone tissue engineering scaffolds, demonstrating efficacy in inhibiting the growth of clinical bacterial isolates. Additionally, rare-earth (RE) doped Fo exhibits excitation properties that match the near-infrared (NIR) biological transparency window (700-1800 nm), facilitating deep penetration into biological tissues. Despite these advantageous properties, the literature lacks data on the toxicity of RE-doped forsterite and its effects on damaged or dysfunctional cells, such as cancer cells. This study presents, for the first time, toxicity analyses of RE-doped forsterite nanoparticles (NPs) in cultures of healthy and tumor skin cells. Specifically, forsterite doped with Er³⁺, Yb³⁺, and a combination of Er³⁺/Yb³⁺, produced via reverse strike coprecipitation (RSC), was employed in cytotoxicity assays. The influence of solution pH on the toxicity response was also investigated. The results indicated that all NPs exhibited biocompatibility with keratinocytes, while melanoma cells showed increased cell death. Photoluminescence (PL) analyses revealed that Fo:Yb displayed enhanced blue emission under 980 nm excitation, whereas Fo:Er/Yb exhibited green and red emissions. The study proposes that the combination of the alkalinization effect of forsterite with the upconversion (UC) photoactivity of the NPs could serve as a dual-attack system for in situ oncological treatment. © 2024, The Authors. All rights reserved.

关键词： Nanoparticles

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Theoretical insights into the chemical bonding, electronic structure, and spectroscopic properties of the lanarkite Pb2SO5 structure

arXiv

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arXiv 2023年

作者： Fabris, Guilherme S.L. Ferrer, Mateus M. Sambrano, Julio R. Almeida, Cláudio R.R. Paskocimas, Carlos A. La Porta, Felipe A. Graduate Program in Materials Science and Engineering Technological Development Center Universidade Federal de Pelotas RS Pelotas96010-610 Brazil Modeling and Molecular Simulation Group São Paulo State University Bauru São Paulo17033-360 Brazil Department of Materials Engineering Federal University of Rio Grande do Norte RN Natal59078-970 Brazil Postgraduate Program in Science and Engineering of Materials Federal University of Rio Grande do Norte RN Natal59078-970 Brazil Federal University of Technology - Paraná Nanotechnology and Computational Chemistry Laboratory Avenida dos Pioneiros 3131 CEP PR Londrina86036-370 Brazil State University of Londrina Post-Graduation Program in Chemistry Rodovia Celso Garcia Cid 445 km 380 CEP PR Londrina86057-970 Brazil

Lanarkite is a mineral formed by a combination of lead, sulphur, and oxygen atoms arranged in the general chemical formula Pb2SO5 (PSO) that crystallises with monoclinic symmetry (belonging to the C2/m space group, No. 12). This mineral was first discovered in Lanarkshire, Scotland and was named after its location. PSO has a unique structure comprising alternating penta-coordinated lead [PbO5] and tetra-coordinated sulphur [SO4] clusters. This lanarkite-type structure has recently attracted significant scientific interest and has been the focus of the superconducting material research community. However, its chemistry needs to be explored further. This article presents a comprehensive investigation on the chemical bonding, electronic structure, and spectroscopic properties of the lanarkite-type PSO structure from a computational perspective. Thus, different functionals in the DFT (e.g., PBE, PBE0, PBESOL, PBESOL0, BLYP, WC1LYP37, and B3LYP) were assessed to accurately predict their fundamental properties. All the DFT calculations were performed using a triple-zeta valence plus polarisation basis set. Among all the DFT functionals tested in this study, PBE showed the best agreement with the experimental data available in the literature. Our results also reveal that the [PbO5] clusters are formed with three Pb–O bond lengths, with values of about 2.32, 2.59, and 2.84 Å, respectively, while the [SO4] clusters have the same S–O bond length of 1.57 Å. We performed a complete topological analysis of this system to comprehend these structural differences. Additionally, the PSO structure has an indirect band gap energy of 2.9 eV and an effective mass ratio (mℎ∗ /me∗) of about 0.415 (using PBE calculations) which may, in principle, indicate a low recombination of electron-hole pairs in the lanarkite structure. Therefore, we believe that a detailed understanding of their electronic structures, spectroscopic properties as well as their chemical bonding is critically important

关键词： Lead compounds

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Revolutionary valorization of carbon dioxide into dimethyl carbonate is catalyzed by sodium chloride: cheap, clean, one-pot, and water-free synthesis

arXiv

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arXiv 2023年

作者： Chaban, Vitaly V. Andreeva, Nadezhda A. Santos, Leonardo Moreira dos Einloft, Sandra Yerevan State University Yerevan0025 Armenia Peter the Great St. Petersburg Polytechnic University Saint Petersburg Russia School of Technology Pontifical Catholic University of Rio Grande do Sul - PUCRS Porto Alegre Brazil Post-Graduation Program in Materials Engineering and Technology School of Technology Pontifical Catholic University of Rio Grande do Sul – PUCRS Brazil

The robust valorization of carbon dioxide (CO2) stays at the center of sustainable development. Since CO2 represents a low-energy compound, its transformation into commercially coveted products is cumbersome. In the present work, we report a revolutionary method to obtain dimethyl carbonate (DMC) out of methanol (CH3OH) and CO2 catalyzed by sodium chloride (NaCl) and similar inorganic salts. The computational exploration revealed a mechanism of favorable catalysis, which was subsequently confirmed experimentally. Unlike all competitive syntheses of DMC, the new one does not produce water and, therefore, the hydrolysis of a carbonate does not occur. No dehydrating agents are necessary. The employed catalyst is cheap and permanently exists in the same phase with the reactants and products. The action of NaCl was compared to those of other alkali metal salts, LiI, LiCl, and KI, and competitive performances were recorded. The experimentally obtained result outperforms most competing technologies according to the DMC yield, 19% with molecular sieves and 17% without molecular sieves. All existing competitors are excelled by the simplicity and cleanness of the synthesis. The reported advance substantially simplifies the synthesis of linear organic carbonates and robustly valorizes CO2 © 2023, CC BY.

关键词： Methanol

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Synthesize Palladium Nanoparticles from the Macroalgae Sargassum Fusiforme: An Eco-Friendly Tool in the Fight Against Plasmodium Falciparum?

SSRN

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SSRN 2022年

作者： Kamaraj, Chinnaperumal Ragavendran, Chinnasamy Kumar, R.C. Satish Sabarathinam, Sarvesh Vetrivel, Cittrarasu Vaithiyalingam, Mariyappan Malafaia, Guilherme Drug Testing Laboratory Directorate of Research SRM Institute Science and Technology Tamil Nadu Kattankulathur603 203 India Department of Cariology Saveetha Dental College and Hospitals Tamil Nadu Chennai India Carbon Capture Lab Department of Chemical Engineering SSN College of Engineering Kalavakkam Tamil Nadu Chennai603110 India Department of Chemistry SRM Institute of Science and Technology Kattankulathur Tamilnadu Chengalpattu603203 India Laboratory of Toxicology Applied to the Environment Goiano Federal Institute GO Urutaí Brazil Post-Graduation Program in Conservation of Cerrado Natural Resources Goiano Federal Institute GO Urutaí Brazil Post-Graduation Program in Ecology Conservation and Biodiversity Federal University of Uberlândia MG Uberlândia Brazil Post-Graduation Program in Biotechnology and Biodiversity Federal University of Goiás GO Goiânia Brazil

Although numerous drugs are practiced to control malaria and its vectors, more recently, eco-friendly control tools have been proposed to battle its etiologic agents. Thus, using green bionanotechnology approaches, we aimed to synthesize palladium nanoparticles (Pd NPs) from the macroalgae Sargassum fusiforme (Sf), its potential antiparasitic activity against P. falciparum, as well as its possible cytotoxicity, in HeLa cells. After the biosynthesis of the PdSf NPs, their characterization was carried out by UV–Vis, FESEM, and EDX analyses, and their hydrodynamic size, zeta potential, and surface area were determined. Furthermore, the functional groups of the PdSf NPs were analyzed by FT-IR and GC–MS. While PdSf NPs had an IC50 of 7.68 µg/mL (Chloroquine (C)-s) and 16.42 µg/mL, S. fusiforme extract had an IC50 of 14.38 µg/mL (CQ-s) and 35.27 µg/mL (CQ- r). With an IC50 value of 94.49 µg/mL, PdSf NPs exhibited the least toxic effect on the HeLa cells. The Lipinski rule of five and ADMET prediction were used to assess the in-silico models of caffeine acid hexoside and quercetin 7-O-hexoside for the presence of drug-like properties. Pathogenic proteins, primarily responsible for motility, binding, and disease-causing, were the target of the structurally based docking studies between plant-derived compounds and pathogenic proteins. Thus, our study pioneered promising results that support the potential antiplasmodial activity of eco-friendly synthesized PdSf NPs using S. fusiforme extract against P. falciparum, opening perspectives for further exploration into the use of these NPs in malaria therapy. © 2022, The Authors. All rights reserved.

关键词： Nanoparticles

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Eco-Friendly Bioremediation of Pollutants from Contaminated Sewage Wastewater Using Special Reference Bacterial Strain of Bacillus Cereus Sdn1 and Their Genotoxicological Assessment in Allium Cepa

SSRN

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SSRN 2022年

作者： Anusha, Ponniah Ragavendran, Chinnasamy Kamaraj, Chinnaperumal Natarajan, Devarajan Thesai, Annadurai Sakthi Malafaia, Guilherme Sangeetha, K. Department of Science and Humanities Kongunadu College of Engineering and Technology Tholurpatti Tamil Nadu Trichy621 215 India Kattankulathur Tamil Nadu Chennai603 203 India Natural Drug Research Laboratory Department of Biotechnology School of Biosciences Periyar University Tamil Nadu Salem India Department of Microbiology Sona College of Technology Sona College of Arts and Science Salem636 005 India Laboratory of Toxicology Applied to the Environment Goiano Federal Institute GO Urutaí Brazil Post-Graduation Program in Conservation of Cerrado Natural Resources Goiano Federal Institute GO Urutaí Brazil Post-Graduation Program in Ecology Conservation and Biodiversity Federal University of Uberlândia MG Uberlândia Brazil Post-Graduation Program in Biotechnology and Biodiversity Federal University of Goiás GO Goiânia Brazil

The present study aimed to assess the Bacillus cereus SDN1 native bacterium's ability to clean up contaminated, polluted water. This bacterium was identified by its morphological and biochemical characteristics, which were then confirmed at the genus level. Furthermore, the isolated B. cereus (NCBI accession No: MW828583) was identified genomically by PCR amplifying 16s rDNA using a universal primer. The phylogenetic analysis of the rDNA sequence was conducted to determine the taxonomic and evolutionary profile of the isolate of the previously identified Bacillus sp. Besides, B. cereus and the bacterial consortium were treated using sewage wastewater. After 15 days of treatment, the following pollutants were reduced: total hardness particles removal varied from 63.33% to 67.55%, calcium removal varied from 90% to 93.33%, and total nitrate decreased range from 37.77% to 22.22%, respectively. Electrical conductivity ranged from 1809 mS/cm to 2500 mS/cm, and pH values ranged from 6.5 to 8.95. The outcome of in-situ remediation results suggests that B. cereus has a noticeable remediation efficiency to the suspended particles. A root tip test was also utilized to investigate the genotoxicity of treated and untreated sewage-contaminated waters on onion (Allium cepa) root cells. The highest chromosomal aberrations and mitotic inhibition were found in roots exposed to contaminated water. The study can thus be applied as a biomarker to identify the genotoxic impacts of sewage water pollution on biota. It may be concluded that employing bacterial consortia for domestic wastewater treatment could be a suitable strategy for chemical contaminants removal. Additionally, based on an identified bacterial consortium, this work offers a low-cost and eco-favorable method for treating household effluent. © 2022, The Authors. All rights reserved.

关键词： Bacillus cereus

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