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Thermomechanical Behavior and Corrosion Resistance of a 316 L Austenitic Stainless Steel

materials sciences and Applications 2020年第4期11卷 217-233页

作者： Rafael P. Ferreira Carmem C. F. Nascimento Gedeon S. Reis Eden S. Silva Samuel F. Rodrigues Graduate Program in Materials Engineering Federal Institute of Education Science and Technology of Maranhao (IFMA) Sao Luis Brazil

Hot-formed components are constantly exposed to hostile environments with corrosive substances. Microstructural changes caused by thermomechanical processing can be predicted to increase the corrosion resistance of austenitic stainless steels. The objective of this study is to understand the relationship between the dynamic softening mechanisms and corrosion resistance, thus optimizing the hot-forming process. In the current work, the dynamic recrystallization (DRX) behavior of AISI 316 L austenitic stainless steel was studied in the temperature range of 1273 - 1423 K and strain-rate range of 0.1 - 5.0 s-1 using physical simulation. Subsequently, potentiodynamic polarization tests and scanning electron microscopy were performed on the hot-deformed samples to investigate the influence of temperature and strain-rate on the corrosion resistance and mechanical properties. The results indicated that the DRX fractions increased under low-temperature and high strain-rate conditions, resulting in grain refinement. The potentiodynamic polarization tests indicated that the dynamically recovered samples demonstrated high resistance to corrosion compared with the DRX samples. The best route found for the investigated alloy was for the strain to be applied at a temperature of 1423 K and a strain rate of 0.1 s-1.

关键词： 316 L Austenitic Stainless Steel Softening Phenomena Corrosion

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Characterization of FeCr and FeCoCr alloy coatings of carbon steels for marine environment applications

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Applied Adhesion science 2013年第1期1卷 1-10页

作者： Antunes, Fernando José de Sá Brito, Vinícius Ribeiro dos Santos Bastos, Ivan Napoleão Costa, Hector Reynaldo Meneses Centro Federal de Educação Tecnológica Celso Suckow da Fonseca Graduate Program in Mechanical Engineering and Materials Technology Av. Maracanã 229 Rio de Janeiro RJ – 20271-110 Brazil Universidade do Estado do Rio de Janeiro Graduate Program in Materials Science and Technology Rua Bonfim 25 Nova Friburgo RJ – 28625-570 Brazil

This paper presents the adhesive strength results of FeCr and FeCoCr deposits produced by electric arc thermal spray process on carbon steel plates. Five chemical compositions were tested to give a large panel of possibility. Coatings were characterized by several methods to result in a performance screening. The main assessment of microstructural morphology was made by scanning electron microscopy (SEM). The mechanical strength of coatings was evaluated by standard pull-off test. The corrosion resistance was analyzed in salt-spray test. The morphology of coatings exhibits characteristics of lamellar microstructures with incompletely melted particles together with a distribution of similarly oriented oxides. The adhesive strength of FeCoCr alloy coatings was higher amongst all studied conditions. All sealed conditions presented low corrosion in salt-spray exposure. Additionally, a new FeCoCr alloy was studied to reduce pores and microcracks that are frequently found in traditional FeCr and FeCrNi alloys. Based on the performed characterizations, the findings suggested that the FeCoCr deposition, with an epoxy sealing, is suitable to be used as an efficient coating of carbon steel in aggressive marine environments. © 2013, Antunes et al.;licensee Springer.

关键词： Adhesion test Carbon steel FeCoCr coating Salt-spray test Thermal spray

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Influence of Al-5.0Nb-0.5B inoculant on the microstructure and mechanical properties of AA 2017 alloy fabricated using laser-based powder bed fusion

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Journal of Alloys and Compounds 2025年 1032卷

作者： Pamela Karina dos Santos Bomfim Bruna Fernanda Batistão Aylanna Priscila Marques de Araújo Leandro Henrique Pereira Ricardo Henrique Buzolin Sergio T. Amancio-Filho Conrado Ramos Moreira Afonso Claudemiro Bolfarini Claudio Shyinti Kiminami Francisco Gil Coury Piter Gargarella Graduate Program in Materials Science and Engineering Federal University of São Carlos Rod.Washington Luis Km 235 São Carlos SP 13565-905 Brazil High Performance and Lightweight Materials Group kopernikusgasse 24 Graz 8010 Austria BMK Endowed Professorship for Aviation Kopernikusgasse 24 Graz 8010 Austria Institute of Materials Science Joining and Forming Graz University of Technology Kopernikugasse 24/l Graz 80210 Austria Department of Materials Engineering (DEMa) Federal University of São Carlos (UFSCar) Rod. Washington Luiz km 235 São Carlos 13565-905 Brazil Center of Characterization and Development of Materials Federal University of São Carlos Rod. Washington Luiz km 235 SP-310 São Carlos SP 13565-905 Brazil

This study investigated the influence of the inoculant Al-5.0Nb-0.5B on the microstructure and mechanical properties of the AA 2017 alloy fabricated using laser-based powder bed fusion (L-PBF). The AA 2017 alloy powder was obtained through gas atomization and then mixed with 2 wt% of Al-5.0Nb-0.5B powder (20–53 µm) and synthesized using the L-PBF technique. The small addition of the Al-5.0Nb-0.5B, coupled with specific processing parameters, led to a reduction in the fraction of cracks and transformed the solidification structure from cellular to equiaxial. Additionally, it resulted in a grain size reduction down to 4.0 ± 2.9 µm and a low fiber texture. Due to the refined grains, the AA 2017 samples with 2 wt% Al-5.0Nb-0.5B exhibited a high yield strength of 215 ± 33 MPa and ultimate compressive strength of 602 ± 47 MPa, compared to the AA 2017 alloy samples, which exhibited yield strength of 171 ± 8 MPa and ultimate compressive strength of 427 ± 46 MPa. The addition of a small fraction of Al-5.0Nb-0.5B to the AA 2017 alloy, produced by L-PBF, is a promising alternative for manufacturing lightweight parts with a lower amount of hot cracks and equiaxial microstructure. The results show that the use of inoculant with the micrometric size is an effective alternative to the use of nanoparticles, which has a higher safety risk, is usually difficult to homogenize and may promote agglomeration.

关键词： Compressive strength

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Analysis of Temiki (Melastoma Candidum) Extract Compounds as Corrosion Inhibitors Using GC–MS 4th

Analysis of Temiki (Melastoma Candidum) Extract Compounds as...

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4th International Conference on Experimental and Computational Mechanics in engineering, ICECME 2022

作者： Supardi, Joli Rizal, Samsul Ali, Nurdin Fonna, Syarizal Ikramullah, Ikramullah Arifin, A.K. Doctoral Program School of Engineering Post Graduate Program Syiah Kuala University Banda Aceh23111 Indonesia Department of Mechanical Engineering Teuku Umar University Meulaboh23615 Indonesia Department of Mechanical and Industrial Engineering Syiah Kuala University Banda Aceh23111 Indonesia Department of Mechanical and Materials Engineering Universiti Kebangsaan Malaysia Selangor DE Bangi43600 Malaysia

ISBN: (纸本)9789819974948

Temiki (Melastoma Candidum) is one of the unutilized wild plants observed to be turning pests on plantations. It has only been used for medicine and not for engineering purposes. Therefore, this study aims to identify and analyze Temiki’s chemical compounds, which are useful as corrosion inhibitors. The plant was washed, dried, then blended until it became a fine powder, and was further extracted by employing the maceration method with ethanol as solvent. The extracted compounds were also analyzed using Gas Chromatography-Mass Spectrophotometry (GC–MS) and the results obtained include, 2-Furancarboxaldehyde (CAS) Furfural, 1,2,3-Propanetriol (CAS) Glycerol, Acetic acid,1-(2-methyltetrazole-5-yl) etheny, 4H-Pyran-4one,2,3-dihydro-3,5-dihydroxy, 5-Hydroxymethylfurfural, cis-dimethylmorpholine, 3-penten-1-ol,2,2,4-trimethyl-(CAS)2,2,4, 2-AMINO-9-(3,4-DIHYDROXY-5-HYDORO, D-Allose, beta-D-Glucopyranoside, methyl, Hexadecanoic acid, methyl ester, 9,12,15-Octadecatrienoic acid, methyl ester. In conclusion, these chemical compounds were useful as corrosion inhibitors. © The Author(s), under exclusive license to Springer Nature Singapore Pte Ltd. 2024.

关键词： Corrosion

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Role of delamination fracture for enhanced impact toughness in 0.05 %P doped high strength steel with ultrafine elongated grain structure

Role of delamination fracture for enhanced impact toughness ...

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7th International Conference on Processing and Manufacturing of Advanced materials, THERMEC'2011

作者： Jafari, Meysam Kimura, Yuuji Tsuzaki, Kaneaki Doctoral Program in Materials Science and Engineering Graduate School of Pure and Applied Science University of Tsukuba 1-2-1 Sengen Tsukuba Ibaraki 305-0047 Japan Structural Metals Center National Institute for Materials Science 1-2-1 Sengen Tsukuba Ibaraki 305-0047 Japan

ISBN: (纸本)9783037853047

Ultrafine elongated grain (UFEG) structures with strong 〈110〉// rolling direction (RD) fiber deformation texture were produced by warm caliber-rolling at 773 K, namely tempforming in the 1200 MPa-class medium-carbon low-alloy steel with phosphorous (P) contents of 0.001 and 0.053 mass%. Charpy impact tests were performed at temperature range of -196 to 150 °C on the UFEG structure. Regardless of P content, high upper shelf energy about 145 J and a very low ductile to brittle transition temperature (DBTT) of around -175 °C were obtained. P segregation embrittlement completely disappeared in the 0.053 %P steel and both steels showed ductile fracture on the planes normal to RD at temperature range of -150 to 150 °C. The main reason for the high upper shelf energy and very low DBTT in the 0.053 %P steel would be delamination fracture along RD when both 0.001 and 0.053 %P steels showed quite similar microstructures including texture. Since the occurrence of delamination requires relatively weak interfaces or planes, P segregated to the ferrite grain boundaries and interfaces of cementite particles-ferrite matrix and made them feasible paths for crack branching and consequently delamination occurred. We showed in this work the advantage of delamination (crack arrester-type) on the high absorbed energy obtained by 0.053 %P steel in comparison with 0.001 %P steel. © (2012) Trans Tech Publications, Switzerland.

关键词： Fracture toughness

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Neuromodulation of the peripheral nervous system:Bioelectronic technology and prospective developments

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BMEMat(BioMedical engineering materials) 2024年第1期2卷 88-114页

作者： Hayoung Song Moohyun Kim Enji Kim Jakyoung Lee Inhea Jeong Kyeonghee Lim Seoung Young Ryu Myoungjae Oh Younhee Kim Jang-Ung Park Department of Materials Science and Engineering Yonsei UniversitySeoulSouth Korea Center for Nanomedicine Institute for Basic Science(IBS)SeoulSouth Korea Department of Neurosurgery Yonsei University College of MedicineSeoulSouth Korea Graduate Program of Nano Biomedical Engineering(NanoBME) Advanced Science InstituteYonsei UniversitySeoulSouth Korea

The peripheral nervous system(PNS)is a fascinatingly complex and crucial component of the human body,responsible for transmitting vital signals throughout the body's intricate network of *** efficient functioning is paramount to our health,with any dysfunction often resulting in serious medical conditions,including motor disorders,neurological diseases,and psychiatric *** strides in science and technology have made neuromodulation of the PNS a promising avenue for addressing these health *** involves modifying nerve activity using a range of techniques,such as electrical,chemical,optical,and mechanical *** plays a critical role in this effort,allowing for precise,controlled,and sustained stimulation of the *** paper provides an overview of the PNS,discusses the current state of neuromodulation devices,and presents emerging trends in the field,including advances in wireless power transfer and materials,that are shaping the future of neuromodulation.

关键词： bioelectronics neuromodulation peripheral nervous system

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Effects of spatial uniformity of continuous and pulse laser irradiation on the microstructure and mechanical properties of Ti-6Al-4V in powder bed fusion

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materials Today Communications 2025年 46卷

作者： Seunghwan Moon Seungmuk Ji Yoonseok Ko Min-Su Lee Tea-Sung Jun Dong-Ik Kim Jong-Souk Yeo School of Integrated Technology College of Computing Yonsei University Seoul 03722 Republic of Korea BK21 Graduate Program in Intelligent Semiconductor Technology Yonsei University Seoul 03722 Republic of Korea Center for Energy Materials Research Korea Institute of Science and Technology Seoul 02792 Republic of Korea Department of Mechanical Engineering Incheon National University Incheon 22012 Republic of Korea

Powder bed fusion of metals with laser beam (PBF-LB/M) using Ti-6Al-4V (Ti64) has enabled delicate fabrication of biocompatible medical implants. This research focuses on how the spatial uniformity of laser irradiation affects material under continuous wave (CW) and pulse width modulated (PWM) laser conditions, using a self-developed PBF-LB/M system. The volumetric energy density (VED) was used as a reference parameter in order to accurately compare the effects of CW and PWM lasers, but limitations of VED, which does not include spatial and kinetic factors, which are reinforced in the PWM laser process, were also considered. Results revealed that the uniform distribution of energy irradiation across the entire region brought similar porosities and Vickers hardness tendencies for CW and PWM laser processes. In contrast, the spatially nonuniform energy transfer resulted in a significantly higher porosity in the specimen fabricated using the PWM laser than that produced using the CW laser at the same VED, reducing compressive yield strength. The electron backscattered diffraction analysis showed no significant differences in the average grain size, phase distribution, and misorientation angle of the samples produced using CW and PWM lasers under the same VED. However, sharper grains with an aspect ratio of less than 0.3 were 7 % higher in specimens produced using the PWM laser. This study highlights the possibility of controlling the microstructure and mechanical properties in a wider range when using the PWM laser with spatially nonuniform irradiation.

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Finite-temperature anisotropic elastic properties of Ni-Mn-In magnetic shape memory alloy

Finite-temperature anisotropic elastic properties of Ni-Mn-I...

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作者： Williams, Kristen S. Cagin, Tahir Materials Science and Engineering Graduate Program Texas A and M University College Station TX United States Department of Chemical Engineering Texas A and M University College Station TX United States

ISBN: (纸本)9781617822018

Designing magnetic shape memory materials with practicable engineering applications requires a thorough understanding of their electronic, magnetic, and mechanical properties. Experimental and computational studies on such materials provide differing perspectives on the same problems, with theoretical approaches offering fundamental insight into complex experimental phenomena. Many recent computational approaches have focused on first-principles calculations, all of which have been successful in reproducing ground-state structures and properties such as lattice parameters, magnetic moments, electronic density of states, and phonon dispersion curves. With all of these successes, however, such methods fail to include the effects of finite temperatures, effects which are critical in understanding how these properties couple to the experimentally-observed martensitic transformation. To this end, we apply the quasi-harmonic theory of lattice dynamics to predict the finite-temperature mechanical properties of Ni-Mn-In magnetic shape memory alloy. We employ first-principles calculations in which we include vibrational contributions to the free energy. By constructing a free energy surface in volume/temperature space, we are able to evaluate key thermodynamic properties such as entropy, enthalpy, and specific heat. We further report the elastic constants for the austenite and martensite phases and evaluate their role as a driving force for martensitic transformation. © 2010 materials Research Society.

关键词： Magnetic moments

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Low-temperature sintered LZSA cellular glass ceramics

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6th Pacific Rim Conference on Ceramic and Glass Technology, PacRim6

作者： Sousa, E. Rambo, C.R. Hotza, D. De Oliveira, A.P. Novaes Fey, T. Graduate Program on Materials Science and Engineering - PGMAT Department of Chemical Engineering - EQA Federal University of Santa Catarina P.O. Box 476 88040-900 Florianópolis SC Brazil Department of Materials Science Glass and Ceramics University of Erlangen-Nuremberg Martensstrasse 5 D-91058 Erlangen Germany

ISBN: (纸本)0470080507

Commercial polyurethane foams with a monomodal pore size distribution were used to produce LZSA glass ceramic foams by the polymeric sponge method. A suspension containing LZSA glass ceramic, bentonite and sodium silicate, was prepared in water and isopropanol media to impregnate the polymeric foams by dip coating. The suspension was characterized by Theological measurements. The effect of the solvent on the microstructure and physical properties on the LZSA foams was also evaluated. The cellular microstructure of the glass-ceramic foams was characterized by scanning electron microscopy (SEM) and micro-computer X-ray tomography (μ-CT). The LZSA foam prepared with isopropanol suspension exhibited higher mechanical strength under compression than those prepared with water.

关键词： Glass ceramics

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Microencapsulated phenolic-rich extract from juice processing grape pomace(Vitis *** Var):Effects on oxidative stability of raw and pre-cooked bovine burger

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Food Bioscience 2022年第6期50卷 2120-2129页

作者： Marcelo Edvan dos Santos Silva Rodrigo Lira de Oliveira Thamyres Cesar de Albuquerque Sousa Cristiani Viegas Brandão Grisi Valquíria Cardoso da Silva Ferreira Tatiana Souza Porto Marta Suely Madruga Suzana Pedroza da Silva Fábio Anderson Pereira da Silva Post-Graduate Program in Food Science and Technology Department of Food EngineeringTechnology CentreFederal University of ParaibaJoão PessoaParaiba58051-900Brazil Northeast Biotechnology Network/RENORBIO Federal Rural University of Pernambuco (UFRPE)Dom Manoel de MedeirosDois Irmãos52171-900RecifePEBrazil Federal University of Pernambuco's Agreste (UFAPE) GaranhunsAv.Bom PastorBoa Vista55296-901 GaranhunsPEBrazil Post-Graduate Program in Agrifood Technology Federal University of ParaibaCampus Universitario IIIBananeirasPBBrazil

Grape processing generates residues rich in bioactive compounds with potential application in the meat ***,these substances are unstable and needs to be treated to allow their action during the processing and storage of meat *** this sense,a phenolic-rich extract from grape pomace was microencapsulated and evaluated for its potential to inhibit the oxidative process in raw and precooked beef burgers during cold *** hamburger formulations containing lyophilized extract(LEB),microencapsulated extract(MEB)and synthetic antioxidant sodium erythorbate(SEB)were prepared,pre-cooked,and evaluated for lipid and protein *** microencapsulation,with 95.0%efficiency,provided a material with a crystalline structure,rich in phenolics and with high antioxidant potential,showing 377.4±0.01,1768.1±0.07 and 1185.0±0.20μmol TEAC.100 g^(−1) for DPPH,ABTS and FRAP,*** values of malonaldehyde were found in LEB and MEB(2.9±0.3 and 1.4±0.5 mg ***^(−1),respectively)at the end of storage,with emphasis on for the hamburgers that received the microencapsulated *** behavior was observed for the analysis of carbonyl compounds,with values of 11.1±1.1,8.7±1.4 and 6.8±1.0 nM ***^(−1) in SEB,LEB and MEB,***,the freeze-dried and microencapsulated grape extracts showed superior results when compared to the synthetic antioxidant,increasing the oxidative stability of hamburgers,and avoiding significant color changes during the cold *** results indicate the high potential of the microencapsulated material to be used as a natural antioxidant in the meat industry.

关键词： Lipid oxidation Protein oxidation Meat products Natural antioxidant Encapsulation

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