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Microstructural and mechanical characterization of superelastic Ni-Free Ti-Nb-based shape memory alloys

materials Today Communications 2025年 47卷

作者： Vitória Hellem Marques Costa Guedes Suelene Silva Araújo Carlos Costa de Carvalho Paulo César Sales da Silva Carlos José de Araújo Postgraduate Program in Materials Science and Engineering (PPG-CEMat) Universidade Federal de Campina Grande Av. Aprígio Veloso 882 Campina Grande PB CEP 58429-140 Brazil Department of Mechanical Engineering Universidade Federal de Campina Grande Av. Aprígio Veloso 882 Campina Grande PB CEP 58429-140 Brazil

Shape Memory Alloys (SMAs) are smart materials that regain their original shape after significant deformation, typically over 1 % under uniaxial tension. Ni-Ti alloys stand out for their low elastic modulus, high recoverable strain, and excellent corrosion resistance. However, nickel raises biocompatibility concerns due to potential adverse effects. As an alternative, Ni-free Ti-Nb-based SMA, composed entirely of biocompatible elements, have emerged as a promising option for biomedical applications. This study investigated and characterized Ti-xNb-based, alloys with x = 23 %, 25 % and 27 % (at%), manufactured by arc melting, cold rolling, and vacuum annealing followed by quenching. The focus was on their mechanical and microstructural properties, particularly cyclic mechanical loading, thermomechanical behavior, and ultramicroindentation, areas still underexplored in the literature. XRD confirmed the predominance of the β phase and EDS verified good compositional homogeneity. Mechanical testing showed that increasing niobium content reduced the elastic modulus, hardness, and reduction modulus due to β-phase stabilization. Tensile tests indicated changes in shape recovery through superelasticity. Overall, Ti-Nb-based alloys presented excellent mechanical properties with potential for biomedical applications.

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Antimicrobial Potential of Linear Low-Density Polyethylene Food Packages with Ag Nanoparticles in Different Carriers (Sio2 and Hap)

SSRN

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SSRN 2023年

作者： da Costa Brito, Sabrina Pereira, Vinicius Alex Cano Prado, Ana Carolina Figueiredo Tobias, Thais Juliana Paris, Elaine Cristina Ferreira, Marcos David São Paulo State University "Julio de Mesquita Filho" Rod. Araraquara Jaú Km 01 SP Araraquara14800-903 Brazil Embrapa Instrumentação Rua XV de Novembro 1452 SP São Carlos13560-970 Brazil Biotechnology Graduate Program Federal University of São Carlos Rod. Washington Luís Km 235 – C. P.676 SP São Carlos13.565-905 Brazil Postgraduate Program in Materials Science and Engineering Federal University of São Carlos Rod. Washington Luís Km 235 – C. P.676 SP São Carlos13.565-905 Brazil Chemistry Graduate Program University of Sao Paulo Av. Trabalhador São-carlense 400 SP São Carlos13.560-970 Brazil Postgraduate Program in Chemistry Federal University of São Carlos Rod. Washington Luís Km 235 – C. P.676 SP São Carlos13.565-905 Brazil

This study intended to verify the antimicrobial efficacy of linear low-density polyethylene films incorporated with silver nanoparticles dispersed in silica and hydroxyapatite carriers at different concentrations. The silver nanoparticles showed a superior inhibitory action on S. aureus and hydroxyapatite was more effective, being this a potential for use in food packaging. © 2023, The Authors. All rights reserved.

关键词： Polymer films

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Synthesis, Characterization, and performance test of modified Zeolite-Si/Al nanocomposite from pumice and waste cans using slow pyrolysis process for removal pollutant parameters from hard water

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Environmental Nanotechnology, Monitoring and Management 2023年 20卷

作者： Gusti Wibowo, Yudha Sudibyo Rianjanu, Aditya Taher, Tarmizi Susanti, Noni Karo Karo, Pulung Suprihatin Iman Supriyatna, Yayat Prasetyo, Erik Bahfie, Fathan Amin, Muhammad Syarifuddin, Hutwan Safitri, Hana Khairurrijal, Khairurrijal Department of Mining Engineering Institut Teknologi Sumatera Lampung-35365 Indonesia Research Center for Mining Technology National Research and Innovation Agency Lampung Indonesia Department of Material Engineering Institut Teknologi Sumatera Lampung-35365 Indonesia Department of Environmental Engineering Institut Teknologi Sumatera Lampung-35365 Indonesia Physics Department Universitas Lampung Lampung Indonesia Department of Environmental Science Postgraduate Program Universitas Jambi Jambi 36122 Indonesia Laboratory of Mine Environmental Department of Mining Engineering Institut Teknologi Sumatera Lampung-35365 Indonesia Department of Physics Institut Teknologi Sumatera Lampung-36365 Indonesia Department of Physics Institut Teknologi Bandung Bandung 40132 Indonesia Center for Green and Sustainable Materials Institut Teknologi Sumatera Indonesia

Hard water is one of crucial problems in the world due to its pollutant parameters. Adsorption is a promising method for treating hard water because of its benefits such as low-cost, easy to use, acceptable, and easy to maintenance. In this study, we utilized zeolite functionalized with silicon/aluminum (Ze-Si/Al) as adsorbent materials for hard water treatment. Ten different ratios of Si/Al were added into zeolite by modifying the solid waste source concentration (pumice and cans). The optimum sample was then further tested with different parameters including contact time, dye concentration, and isotherm models. The zeolite-Si/Al adsorbent was characterized by Scanning Electron Microscope (SEM), X-Ray Diffraction (XRD), and X-Ray Fluorescence (XRF). Results of this study have showed that the best functionalized zeolite was that with Si/Al ratio 0.67, which has higher sorption ability. In contact time test, the equilibrium was reached after 300 min. This study also informed that the concentration of dyes will give impact on removal of pollutant parameters. Isotherm model of Ze-Si/Al fitted with Langmuir method. This study also discussed the potential development and future research direction. Thus, this study is a crucial report to develop the information about waste utilization as source of Si/Al to increasing quality of zeolite. © 2023 Elsevier B.V.

关键词： Adsorption Hard water Wastewater Wastewater treatment zeolite-Si/Al

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Fabrication of silica-nypa membrane applied for water desalination

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AIP Conference Proceedings 2024年第1期2710卷

作者： Muthia Elma Isna Syauqiah Era N. R. Oktaviana Siti Fatimah Aulia Rahma Awali Sir Kautsar Harivram Erdina L. A Rampun Chemical Engineering Department Engineering Faculty Lambung Mangkurat University JL. A. Yani KM 36 Banjarbaru South Kalimantan 70714 Indonesia Materials and Membranes Research Group (M2ReG) Lambung Mangkurat University JL. A.Yani KM 36 Banjarbaru South Kalimantan 70714 Indonesia Doctoral Program of Environmental Science postgraduate Program Lambung Mangkurat University Jl. Brigjen H Hasan Basri Kayutangi Banjarmasin South Kalimantan 70123 Indonesia

Carbon source as a template derived from nypa leaf powder enable to strengthen the silica matrix applied for water desalination. This research aims to synthesize silica-nypa membrane, characterize xerogel silica-nypa leaf and investigate the performance of silica-nypa membrane with various concentration of nypa as a carbon template to treat artificial sea water. The concentrations of nypa leaf as a carbon template are 0.1; 0.5 and 2.5 %wt with a calcination temperature of 350 °C through a rapid thermal processing (RTP) technique. Xerogel characterization using FTIR was employed to analyze a spectrum and Scanning Electron Microscopy (SEM) to investigate the membrane morphology. The result shows that the performance of silica-nypa membrane with water fluxes of 2.1915; 2.0163 and 1.1067 kg.m−2. h−1 (for 0.1; 0.5 and 2.5 %wt. carbon template derived from nypa leaf), and the salt rejection value for all concentrations.

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Date fruit melanin is primarily based on (-)-epicatechin proanthocyanidin oligomers( vol 14 , 4863 , 2024)

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SCIENTIFIC REPORTS 2024年第1期14卷 1-12页

作者： Alam, Muneeba Zubair Okonkwo, Clinton Emeka Cachaneski-Lopes, Joao P. Graeff, Carlos F. O. Batagin-Neto, Augusto Tariq, Saeed Varghese, Sabu O'Connor, Matthew J. Albadri, Abuzar E. Webber, J. Beau W. Tarique, Mohammed Ayyash, Mutamed Kamal-Eldin, Afaf Department of Food Science College of Agriculture and Veterinary Medicine United Arab Emirates University P.O. Box: 15551 Al-Ain United Arab Emirates National Water and Energy Center (NWEC) United Arab Emirates University P.O. Box: 15551 Al-Ain United Arab Emirates Postgraduate Program in Materials Science and Technology (POSMAT) São Paulo State University (UNESP) Bauru SP Brazil Department of Physics School of Sciences São Paulo State University (UNESP) Bauru SP Brazil Institute of Sciences and Engineering São Paulo State University (UNESP) Itapeva SP Brazil Department of Anatomy College of Medicine and Health Sciences United Arab Emirates University Al Ain United Arab Emirates Core Technology Platforms New York University Abu Dhabi 129188 Abu Dhabi United Arab Emirates Department of Chemistry College of Science Qassim University 51452 Buraidah Saudi Arabia Lab-Tools Ltd. Marlowe Innovation Centre Marlowe Way Ramsgate CT12 6FA UK

Plant-based melanin seems to be abundant, but it did not receive scientific attention despite its importance in plant biology and medicinal applications, e.g. photoprotection, radical scavenging, antimicrobial properties, etc. Date fruit melanin (DM) has complex, graphene-like, polymeric structure that needs characterization to understand its molecular properties and potential applications. This study provides the first investigation of the possible molecular composition of DM. High performance size-exclusion chromatography (HPSEC) suggested that DM contains oligomeric structures (569–3236 Da) and transmission electron microscopy (TEM) showed agglomeration of these structures in granules of low total porosity (10–1000 Å). Nuclear magnetic resonance (NMR) spectroscopy provided evidence for the presence of oligomeric proanthocyanidins and electron paramagnetic resonance (EPR) spectroscopy revealed a g-factor in the range 2.0034–2.005. Density functional theory (DFT) calculations suggested that the EPR signals can be associated with oligomeric proanthocyanidin structures having 4 and above molecular units of (−)-epicatechin. The discovery of edible melanin in date fruits and its characterization are expected to open a new area of research on its significance to nutritional and sensory characteristics of plant-based foods.

关键词： Phoenix dactylifera L. (−)-Epicatechin Date fruit Melanin Proanthocyanidins

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Alkali-Activated Eco-Friendly Mixtures with Low-Processed Sugarcane Bagasse Ash—Physical, Mechanical, and Microstructural Properties

SSRN

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SSRN 2022年

作者： Lima, Victor Estolano de Estolano, Amanda Marques Lopes Almeida, Yeda Medeiros Bastos de Henrique, Mariana Alves Araújo, Fernanda Wanderley Corrêa de Melo Neto, Antonio Acacio de Federal University of Pernambuco Department of Civil and Environmental Engineering LabTag Av. da Arquitetura Recife Brazil Federal University of Pernambuco National Institute of Welding Technology and Coating of Materials INTM Rua da Inovação Recife Brazil Federal University of Pernambuco Institute for Petroleum and Energy Research LITPEG Petrochemical Laboratory Av. da Arquitetura Recife Brazil Federal University of Pernambuco Postgraduate Program in Materials Science Av. Jorn. Aníbal Fernandes Recife Brazil Federal Rural University of Pernambuco Department of Rural Technology Rua Cento e Sessenta e Três Cabo de Santo Agostinho Brazil

In this study, sugarcane bagasse ash was used to evaluate the physical, mechanical, and microstructural properties of eco-friendly alkali-activated mixtures with blast furnace slag. Net sodium silicate and solid metasilicate were used as activators to produce conventional and one-part alkali-activated mixtures, respectively. Two types of sugarcane bagasse ash were analyzed: raw (as-received) and calcined. The low number of proposed processes reduces the economic aggregate cost of recycled ash. Further, the blast furnace slag replacement ratios of raw and calcined sugarcane bagasse ash were 10%, 30%, 50%, and 70%. Mortars were prepared for the compressive and flexural strength tests, water absorption, and dry density. Alternatively, X-ray diffraction, thermogravimetry, infrared spectroscopy, and scanning electron microscopy were used to assess the chemical, mineralogical, and microstructural properties of the prepared pastes. In addition, the fresh test was performed using the flow table test, wherein the spread diameter decreased as the SBA content increased, primarily on the raw ash owing to its high organic material content. Moreover, compressive strength results showed that the compressive strength increased after 3 days for mixtures with 10% and 30% SBA. However, at 28 days, there was a decrease with an increase in the SBA content. Similar behavior was observed in the flexural strength and water absorption tests. Tests on pastes verified the probable presence of alternative phases besides C-(A)-S-H, such as pectolite, brucite, hydrotalcite, and zeolites. In addition, through the combination of scanning electron microscopy and energy dispersive spectroscopy techniques, the presence of preserved cellular structure was observed in the alkali-activated matrix, and Ca/Si and Si/Al ratios were calculated. It was concluded that the low reactivity of raw sugarcane bagasse ash and the low reactivity of both ashes significantly decreased mechanical performance. Furthermor

关键词： Slags

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Correction to: SARS-CoV-2 removal with a polyurethane foam composite

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Environmental science and pollution research international 2023年第8期30卷 22033页

作者： Guilherme Pereira Schoeler Thays França Afonso Carolina Faccio Demarco Victor Dos Santos Barboza Tito Roberto Sant'anna Cadaval Andrei Valerão Igansi Marcos Alexandre Gelesky Janice Luehring Giongo Rodrigo de Almeida Vaucher Rafael de Avila Delucis Robson Andreazza Postgraduate Program in Environmental Sciences Center for Engineering Federal University of Pelotas R. Benjamin Constant 989 Pelotas RS CEP 96010-020 Brazil. Postgraduate Program in Materials Science and Engineering Federal University of Pelotas R. Gomes Carneiro 01 Pelotas RS CEP 96010-610 Brazil. Graduate Program in Biochemistry and Bioprospecting Research Laboratory in Biochemical and Molecular Biology of Microorganisms (LaPeBBiOM) Federal University of Pelotas RS Av. Eliseu Maciel Campus Universitário s/n Capão Do Leão CEP 96160-000 Brazil. School of Chemistry and Food Federal University of Rio Grande Av. Itália Km 8 s/n Rio Grande RS CEP 96203-000 Brazil. Postgraduate Program in Environmental Sciences Center for Engineering Federal University of Pelotas R. Benjamin Constant 989 Pelotas RS CEP 96010-020 Brazil. robsonandreazza@yahoo.com.br. Postgraduate Program in Materials Science and Engineering Federal University of Pelotas R. Gomes Carneiro 01 Pelotas RS CEP 96010-610 Brazil. robsonandreazza@yahoo.com.br.

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Coconut waste to green nanomaterial: Large scale synthesis of N-doped graphene nano sheets

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Nano-Structures and Nano-Objects 2023年 36卷

作者： Siburian, Rikson Tang, Liang Wei Alias, Yatimah Tok, Alfred Iing Yoong Goei, Ronn Simanjuntak, Crystina Tarigan, Kerista Paiman, Suriati Goh, Boon Tong Anshori, Isa Kurniawan, Cepi Postgraduate Program Department of Chemistry Faculty of Mathematics and Natural Sciences Universitas Sumatera Utara Medan 20155 Indonesia Department of Chemistry Faculty of Mathematics and Natural Sciences Universitas Sumatera Utara Medan 20155 Indonesia Carbon and Frankincense Research Center Universitas Sumatera Utara Medan 20155 Indonesia Department of Chemistry Faculty of Science Universiti Malaya Kuala Lumpur 50603 Malaysia University Malaya Centre for Ionic Liquids (UMCiL) Universiti Malaya Kuala Lumpur 50603 Malaysia School of Materials Science and Engineering Nanyang Technological University 50 Nanyang Avenue Singapore 639798 Singapore Department of Physics Faculty of Mathematics and Natural Sciences Universitas Sumatera Utara Medan 20155 Indonesia Physics Department Faculty of Science Universiti Putra Malaysia Selangor (Serdang) Seri Kembangan 43400 Malaysia Low Dimensional Materials Research Centre Department of Physics Faculty of Science University of Malaya Kuala Lumpur 50603 Malaysia Biomedical Engineering Department School of Electrical Engineering and Informatics Bandung Institute of Technology Bandung 40132 Indonesia Research Center of Nanoscience and Nanotechnology Bandung Institute of Technology Bandung 40132 Indonesia Chemistry Department Faculty of Mathematics and Natural Sciences Universitas Negeri Semarang Semarang 50229 Indonesia Functional Material Research Center Universitas Negeri Semarang Semarang 50229 Indonesia

In this paper, a breakthrough was achieved in large-scale production of N-doped Graphene Nano Sheets (N-GNS) using coconut fruits. The main objectives were to produce N-GNS on a large scale and assess its electrical conductivity. The process involved two key steps: first, producing GNS from coconut fruits through pyrolysis, and then generating N-GNS by doping with nitrogen using ammonia solution at room temperature. Various analytical techniques were used to characterize the produced N-GNS, including X-ray Diffraction (XRD), Scanning Electron Microscopy with Energy Dispersive Spectroscopy (SEM-EDS), Transmission Electron Microscopy (TEM), X-ray Photoelectron Spectroscopy (XPS), Raman spectroscopy, and electrochemical cyclic voltammetry and electrochemical impedance spectroscopy. The XRD data indicated that the C (002) peak of N-GNS shifted to a higher 2θ value (2θ = 24.72°) compared to GNS (2θ = 23.86°), suggesting an incorporation of nitrogen into carbon structure in N-GNS. This was further supported by XPS data, which identified N-pyridine (BE = 402.0 eV) and C-N (BE = 286.8 eV) in N-GNS. TEM images showed that N-GNS had a flat surface, and the distance between graphene layers slightly expanded (0.36 nm) compared to graphene layers (0.34 nm). SEM images and EDX data validated the morphology, resembling honeycomb lattices, with a significant content of N atoms. Raman data successfully identified the D-band and G-band in N-GNS, further validating its production. Most importantly, N-GNS exhibited electrical conductivity, making it a promising candidate for conductive and supporting materials in various applications. The significance of this research extends beyond N-GNS production, opening up new avenues for the sustainable synthesis of valuable nanomaterials from coconut fruit waste, contributing to both graphene technology and environmental conservation. © 2023 Elsevier B.V.

关键词： C-sp2 Electrical conductivity Graphene nano sheets N-graphene nano sheets N-pyridine XPS

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Flexural properties of recycled ABS/recycled carbon fiber fabric composites

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AIP Conference Proceedings 2023年第1期2884卷

作者： Meire Noriko Hosokawa Jane Maria Faulstich de Paiva Postgraduate Program in Materials Science Federal University of São Carlos João Leme dos Santos Highway (SP 264) 110 18052-780 Sorocaba SP Brazil Department of Production Engineering Federal University of São Carlos João Leme dos Santos Highway (SP 264) 110 18052-780 Sorocaba SP Brazil

The reuse of solid waste is a practice that could reduce the disposal of high-value materials in the environment and also promote the circular economy. The recycling of waste electrical and electronic equipment and carbon-fiber-reinforced polymers wastes can be an alternative to recover materials with good properties (acrylonitrile butadiene styrene and carbon fibers, respectively) and insert them into a new production cycle. In this context, the objective of this study was to develop a composite using a recycled polymer as a matrix (acrylonitrile butadiene styrene) reinforced with recycled carbon fiber fabric and; to evaluate the flexural properties of the materials. The composites were molded by the hot compression method and the bending tests followed the ASTM D790-17 standard. The results showed that the addition of the carbon fiber fabric promoted an increase of up to 13% in the flexural strength of the composite containing a layer of recycled carbon fiber fabric. Thus, remanufacturing can be an alternative to reusing recycled materials that have good mechanical properties and high added value to be used in other applications.

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Reverse electrodialysis membrane for harvesting salinity gradient energy with and without spacer under natural wetland water

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AIP Conference Proceedings 2023年第1期2932卷

作者： Muthia Elma Dwi Resa Lamandau Siti Fatimah Satria Anugerah Suhendra Aulia Rahma Department of Chemical Engineering Faculty of Engineering Lambung Mangkurat University Jl. A. Yani KM 36 Banjarbaru 70714 Indonesia Materials and Membranes Research Group (M2ReG) Lambung Mangkurat University Jl. A. Yani KM 36 Banjarbaru 70714 Indonesia Environmental Science Doctoral and Postgraduate Program Lambung Mangkurat University Jl. Brigjen H. Hasan Basry Banjarmasin 70123 Indonesia

Salinity gradient energy (SGE) allows two solutions with different salt concentration to mixing and directly into electrical energy by reverse electrodialysis (RED) membrane. High power outputs are forecasted theoretically, but in real practice is still relatively low RED power efficiency. In this work, the spacer shadow effects on both membrane and solution compartment resistances are investigated by employing nylon spacer and without spacer. In addition, this experiment also proposes the power density performance of RED membrane under natural wetland water as low saline solution and variation of high saline solution i.e., artificial brackish water (0.3 wt% NaCl) and artificial seawater (3.5 wt% NaCl). The results indicate that the spacer shadow effect on RED membrane has a correlation with energy output generated. The used of spacer led to an increase in stack resistance and decrease in power density compared to without nylon spacer. This result increases the impact of RED renewable power source and brings it closer to practical implementation, especially for the potential natural wetland water as low saline solution. The power output was computed, obtaining a maximum power density of 0.19 W/m2 with variations without spacers, and 0.14 W/m2 with spacers. Results show that of the cell components directly influences the physicochemical principles governing the RED process and is closely related to the cell output parameters. In turn, it is possible to increase the performance of a RED cell by optimizing operation without spacers to avoid the shadow effect.

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