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High performance gamma-ray spectrometer based on Cs3Cu2I5 single crystal grown by room-temperature vacuum solvent-evaporation method

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Journal of Alloys and Compounds 2025年 1027卷

作者： Seo, Jiwon Song, Seungho Park, Minhwan Byun, Jangwon Park, Beomjun Park, Chansun Jang, Mee Yeom, Jung-Yeol Dept. of Health and Safety Convergence Science Korea University Seoul02841 Korea Republic of Interdisciplinary Program in Precision Public Health Korea University Seoul02841 Korea Republic of Dept. of Bioengineering Korea University Seoul02841 Korea Republic of Dept. of Materials Science and Engineering Korea University Seoul02841 Korea Republic of The Institute for High Technology Materials and Devices Korea University Seoul02841 Korea Republic of Global Health Technology Center Korea University Seoul02841 Korea Republic of Daejeon34057 Korea Republic of School of Biomedical Engineering Korea University Seoul02841 Korea Republic of

In this study, the properties of Cs3Cu2I5 (CCI) crystals grown using the Slow Vacuum Evaporation Technique (SVET) were examined. Crystals were grown at room temperature (300 K, 27 °C) under vacuum conditions, producing single crystals with maximum diameter of 13 mm over 23 days. We confirmed excellent crystallinity via X-ray diffraction (XRD), compositional uniformity via X-ray photoelectron spectroscopy (XPS), and homogeneity via electron probe micro analyzer (EPMA). UV-Vis measurements indicated a high transmittance of 83 % and a bandgap of 3.64 eV. The Stokes shift of 110 nm, smaller than previously reported values, contributed to faster decay times and improved low-energy detection feasibility. Time-resolved photoluminescence (TR-PL) showed a rapid decay component (4.1 ns), accounting for 95.11 % of the total decay, demonstrating superior properties compared to existing reports. The gamma-ray detection capabilities of the CCI crystals were evaluated using six radioactive sources (Am-241, Ba-133, Co-57, Na-22, Cs-137, and Mn-54), achieving excellent energy resolution, including 5.2 % at 662 keV. The crystals displayed a highly linear response to gamma radiation (R² = 0.99998) with a light yield of 55,613 photons/MeV. Moreover, assessments of multiple crystals grown under identical conditions showed consistent performance with a coefficient of variation (CV) of 1.23 %. These findings confirm that SVET is a highly effective and cost-efficient method for producing high-quality CCI crystals, offering significant advantages over other growth techniques. © 2025 Elsevier B.V.

关键词： Gamma ray spectrometers

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Phonon dynamics and magnetodielectric relaxation in distorted honeycomb ferrimagnet Ni4Nb2O9: Experiment and first-principles study

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Physical Review materials 2025年第4期9卷 045202-045202页

作者： Harshita Singh Sobhit Singh Sayandeep Ghosh Prativa Pramanik Vasant Sathe Roland Mathieu Wilfrid Prellier Subhash Thota Department of Physics Indian Institute of Technology Guwahati Assam 781039 India Department of Mechanical Engineering University of Rochester Rochester New York 14627 USA Materials Science Program University of Rochester Rochester New York 14627 USA Department of Physics Chungnam National University Daejeon 34134 Republic of Korea Department of Physics Kunsan National University Gunsan 54150 Republic of Korea Department of Materials Science and Engineering Uppsala University Uppsala SE-75103 Sweden UGC DAE Consortium for Scientific Research Indore 452 001 India Laboratoire CRISMAT ENSICAEN CNRS Université de Caen Normandie Université Caen France

We present the experimental and theoretical studies of lattice dynamics, electronic structure, and magnetodielectric relaxation in the ferrimagnetic (FiM) Ni4Nb2O9. This system exhibits a distorted honeycomb lattice with the space group Pbcn (no. 60) and undergoes FiM ordering below 76 K (TFN), accompanied by a magnetic compensation at 33 K (TCOM). By employing density-functional theory (DFT+U) calculations and vibrational spectroscopy, we study all the allowed Raman and infrared phonon modes in Ni4Nb2O9. Temperature-dependent analysis of Raman-active phonon frequencies provides evidence of spin-phonon coupling in Ni4Nb2O9. Interestingly, we observe a nonlinear mode softening phenomenon in both frequencies ω(T) and their linewidths δωF(T), which can be described using three-phonon anharmonic processes. Contrary to the behavior of the remaining modes, 510 cm−1 mode shows a blue shift and effectively acts as a breathing mode for Ni atoms of two sublattices, and hence plays a crucial role in stabilizing the FiM ground state, thus explaining the strong sensitivity of this Ag mode to temperature. Our investigation of the temperature- and field-dependent relative dielectric permittivity and loss-tangent data reveals the absence of magnetodielectric coupling and the presence of dipole relaxation behavior in Ni4Nb2O9. Additionally, the theoretically determined indirect band gap is about 2.7 eV. Overall, our study helps to fill the existing knowledge gap and provides valuable insights into the electronic, vibrational, and magnetodielectric properties of Ni4Nb2O9, shedding light on its potential applications in dielectric-ceramic resonators and electrochemical sensors.

关键词： Local density approximation

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Propolis nanoemulsion extract from celebes stingless bee (Tetragonula biroi) phytochemistry and antibacterial analysis to periodontopathogen bacteria

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Journal of Oral Biology and Craniofacial Research 2025年第3期15卷 576-584页

作者： Amalia, Nadya Rafika Budhy, Theresia Indah Ridwan, Rini Devijanti Rianti, Devi Bramantoro, Taufan Luthfi, Muhammad Ramadhani, Nastiti Faradilla Pramusita, Adya Putranti, Nurul Aisyah Rizki Nugraha, Albertus Putera Situmorang, Putri Cahaya Shariff, Khairul Anuar Nugraha, Alexander Patera Dental Health Science Study Program Faculty of Dental Medicine Universitas Airlangga Surabaya Indonesia Department of Oral and Maxillofacial Pathology Faculty of Dental Medicine Universitas Airlangga Surabaya Indonesia Department of Oral Biology Faculty of Dental Medicine Universitas Airlangga Surabaya Indonesia Department of Dental Material Faculty of Dental Medicine Universitas Airlangga Surabaya Indonesia Department of Dental Public Health Faculty of Dental Medicine Universitas Airlangga Surabaya Indonesia Department of Dentomaxillofacial Radiology Faculty of Dental Medicine Universitas Airlangga Surabaya Indonesia Department of Orthodontic Faculty of Dental Medicine Universitas Airlangga Surabaya Indonesia Faculty of Medicine Universitas Airlangga Surabaya Indonesia Biology Study Program Faculty of Mathematics and Natural Sciences Universitas Sumatera Utara Medan Indonesia School of Materials and Mineral Resources Engineering Engineering Campus Universiti Sains Malaysia Penang Nibong Tebal 14300 Malaysia

Background: Propolis from Sulawesi's stingless bees (Tetragonula biroi) contains antioxidants, more flavonoids than propolis from Apis bees, and the antibacterial ability. Objective: to examine the antibacterial properties of Propolis Nanoemulsion Extract (PNE), which is extracted from the Celebes Stingless Bee (T. biroi), in relation to the periodontopathogen bacteria such as Fusobacterium nucleatum (Fn), Porphyromonas gingivalis (Pg), Aggregatibacter actinomycetemcomitans (Aa), and Provotella intermedia (Pi). This investigation also examines PNE's phytochemistry, particle size analysis (PSA), and zeta potential. Methods: The maceration process with 96 % ethanol was used to create PNE from Celebes stingless bee (T. biroi), which was then subjected to zeta potential measurement and PSA. Phytochemical analysis was used to identify phytochemical constituents in the PNE (T. biroi). Diffusion zone, minimum bactericidal concentration (MBC), and minimum inhibitory concentration (MIC) were used to assess antibacterial efficacy against Aa, Pg, Pi, and Fn. Furthermore, the statistical analysis was used to extract the data. Results: Phenols, alkaloids, and flavonoids were identified;however, triterpenoids and saponins were not. Between 151.28 and 182.2 diameter nanometers (***) was the range of the PNE's diameter. At 1.56 % propolis (T. biroi) concentration, the MIC, MBC, and diffusion zone analysis performed better than at 0.76 %, with a significant difference (p:0.01;p < 0.05) to Aa, Pg, Pi, and Fn. Conclusions: The highest antibacterial activity against Aa, Pg, Pi, and Fn as periodontopathogen bacteria is demonstrated by alkaloids, flavonoids, and phenols in PNE from Celebes (T. biroi) at a concentration of 1.56 %. © 2025 The Authors

关键词： Antibacterial Communicable disease Infectious disease Medicine Periodontal disease

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Stress relaxation and creep in an impression test

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JOURNAL OF ELECTRONIC materials 1997年第7期26卷 827-832页

作者： Li, JCM Materials Science Program Department of Mechanical Engineering University of Rochester Rochester

A localized stress relaxation technique is described suitable for testing miniature structures and components. The actual size of the area that can be tested depends on the size of the indenter and the sensitivity of the load measurement device. However, the indenter should not be so small that macroscopic theory of deformation cannot be used. The technique described includes a quantitative treatment of the data which can be handled by a computer. Extensive data collection can be made so that many deformation parameters can be examined by using this simple test.

关键词： creep dislocation dynamics impression test interfacial sliding LiF Sn-Pb alloy solder stress relaxation superplasticity

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Disparities in carbon emissions across households: insights from daily diet

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Frontiers of Environmental science and engineering 2025年第7期19卷 87-87页

作者： Yue, Jia Weng, Zhixiong Chen, Siyao Tong, Dan Xie, Yang Xu, Meng Ma, Hao School of Business Xiangtan Institute of Technology Xiangtan411100 China Graduate School University of Perpetual Help System DALTA Las Piñas1740 Philippines Institute of Circular Economy Beijing University of Technology Beijing100124 China State Key Laboratory of Materials Low-Carbon Recycling Beijing University of Technology Beijing100124 China Department of Earth System Science Ministry of Education Key Laboratory for Earth System Modeling Institute for Global Change Studies Tsinghua University Beijing100084 China School of Economics and Management Beihang University Beijing100191 China School of Environmental Sciences and Engineering Peking University Beijing100871 China BGRIMM Technology Group Beijing100160 China

This study examines household food carbon emissions in rural China, focusing on the inequality of these emissions and the influence of household characteristics on their variation. Our findings indicate that the average food consumption per rural household is 1031.66 kg. Among all food types, pork contributes the highest share of carbon emissions at 39.75%, followed by beef and mutton at 15.14%, while milk accounts for the lowest share at just 1.38%. Additionally, as household income increases, both food consumption and associated carbon emissions rise accordingly. The food-related carbon emissions tend to be higher in households that are more educated, younger, and larger in size. There are notable regional and income disparities in rural food-related carbon emissions. The regional inequalities appear primarily driven by interactions between different regions, while income inequality is influenced by both intra-group disparities and overlaps among income groups. The results from our threshold regression suggest that carbon emissions are particularly elevated in households where the head has a college-level education or higher, is aged between 32.80 and 33.25 years, and has a household size of three to five members. It is essential to develop and implement flexible policies aimed at reducing the consumption of high-carbon foods. By taking these steps, we can work toward a more sustainable future and promote greater equity in food-related carbon emissions. © Higher Education Press 2025.

关键词： Beef

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Comparison of CMAS corrosion and sintering induced microstructural characteristics of APS thermal barrier coatings

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Journal of materials science & Technology 2019年第3期35卷 440-447页

作者： Yiyou Wu Hua Luo Canying Cai Yanguo Wang Yichun Zhou Li Yang Guangwen Zhou School of Materials Science and Engineering Xiangtan University Key Laboratory of Low Dimensional Materials & Application Technology of Ministry of Education Xiangtan University Department of Mechanical Engineering & Materials Science and Engineering Program State University of New York at Binghamton

The microstructural features of high-temperature sintered and CaO-MgO-Al_2O_3-SiO_2(CMAS) corroded air plasma sprayed Y_2O_3 stabilized ZrO_2(YSZ) thermal barrier coatings(TBCs) under the thermal gradient condition were comparatively studied. As-sprayed YSZ has a lamellar structure and the lamellae are composed of closely aligned columnar crystals. The sintered and the CMAS corroded YSZ coatings maintain the t'-ZrO_2 phase as the as-sprayed YSZ coating. The sintered YSZ remains the lamellar structure with reduced interlamellar gaps and grains coarsening. After the CMAS corrosion, the top layer of the YSZ coating keeps its lamellar structure consisting of some columnar grains with the CMAS infiltration into the intergrain gaps and the formation of striped Zr_2Y_2 O_7. The typical lamellar structure transforms into more equiaxed grains in the middle and bottom layers of the ceramic coating along with significant infiltration of amorphous CMAS and anorthite formation in the bottom layer owing to the high contents of Ca and Al.

关键词： YSZ thermal barrier coating APS CMAS corrosion Anorthite

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Universal whirling magnetic orders in non-Heisenberg Tsai-type quasicrystal approximants

arXiv

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arXiv 2025年

作者： Labib, Farid Nawa, Kazuhiro Nambu, Yusuke Takakura, Hiroyuki Ikeda, Yoichi Deguchi, Kazuhiko Matsuura, Masato Ishikawa, Asuka Kajimoto, Ryoichi Ikeuchi, Kazuhiko Sato, Taku J. Tamura, Ryuji Research Institute of Science and Technology Tokyo University of Science Tokyo125-8585 Japan Tohoku University Sendai980-8577 Japan Institute for Materials Research Tohoku University Miyagi Sendai980-8577 Japan Organization for Advanced Studies Tohoku University Miyagi Sendai980-8577 Japan FOREST Japan Science and Technology Agency Saitama Kawaguchi332-0012 Japan Division of Applied Physics Faculty of Engineering Hokkaido University Sapporo060-8628 Japan Department of Physics Graduate School of Science Nagoya University Nagoya464-8602 Japan Ibaraki Tokai319-1106 Japan Materials and Life Science Division J-PARC Center Japan Atomic Energy Agency Ibaraki Tokai319-1195 Japan 319-1106 Japan Department of Materials Science and Technology Tokyo University of Science Tokyo125-8585 Japan

Magnetic orders of non-Heisenberg Tsai-type 1/1 approximant crystals (ACs) in the Au-Ga-Dy system were studied through bulk magnetization, neutron diffraction, and inelastic neutron scattering techniques. The results uncovered noncoplanar, ferromagnetic (FM) and antiferromagnetic (AFM) spin configurations whirling along [111] crystallographic axis, which is analogous to those observed in the Tb- and Ho-contained counterparts. The crystal electric field excitations similar to those in the Tb-based counterpart are also observed indicating the strong Ising-like magnetic anisotropy. These comprehensive experiments and analyses have revealed the existence of a universal mechanism that stabilizes noncoplanar FM and AFM structures in non-Heisenberg Tsai-type ACs, independent of the rare-earth species (Tb, Dy, Ho);FM intra-cluster interactions and strong Ising-like anisotropy. Copyright © 2025, The Authors. All rights reserved.

关键词： Magnetic anisotropy

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Antibacterial evaluation of radiolytically synthesized silver nanoparticles with ι-carrageenan stabilizers

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Radiation Physics and Chemistry 2025年 236卷

作者： Gili, Mon Bryan Z. Manuel, Wendell A. Guillermo, Neil Raymund D. Shankaregowda, Rakshith Gowda H. Phan, Manh-Huong Conato, Marlon T. Vega, Marienette M. Department of Science and Technology Philippine Nuclear Research Institute Commonwealth Avenue Diliman Quezon City 1101 Philippines Materials Science and Engineering Program College of Science University of the Philippines Diliman Diliman Quezon City 1101 Philippines Department of Physics University of South Florida 4202 East Fowler Avenue Tampa 33620 FL United States Institute of Chemistry College of Science University of the Philippines Diliman Diliman Quezon City 1101 Philippines

The synthesis of silver nanoparticles (AgNPs) using green, eco-friendly methods has garnered significant attention due to the potential advantages of using natural polymers, such as ι-carrageenan, as stabilizing agents. However, challenges remain in controlling the size, distribution, and stability of the nanoparticles, as well as optimizing their antimicrobial activity. In this study, gamma irradiation of ι-carrageenan solutions was investigated as a method for synthesizing AgNPs and exploring their antimicrobial properties. The primary objective was to assess how varying radiation doses and ι-carrageenan concentrations affect the formation, size distribution, and antimicrobial activity of the AgNPs. ι-Carrageenan solutions (0.1, 0.5, and 1.0 w/v %) were mixed with 0.2 M silver nitrate (AgNO₃) solutions and irradiated at doses ranging from 0 to 20 kGy using Co-60. UV–vis spectroscopic analysis indicated the successful formation of AgNPs, with surface plasmon resonance (SPR) peaks appearing between 402 and 418 nm. These peaks shifted slightly towards shorter wavelengths as the irradiation rose, signaling a reduction in nanoparticle size. The optimal synthesis of AgNPs occurred at 0.5 % ι-carrageenan concentration and a dose of 15 kGy, where the SPR peak intensity and nanoparticle formation were most pronounced. XRD confirmed the presence of silver nanoparticles with face-centered cubic (FCC) structure. Particle size analysis, using dynamic light scattering (DLS), revealed that AgNPs ranged in size from 85 to 142 nm, with smaller particles forming at higher doses. At a 1 kGy dose, the nanoparticle size averaged 114 nm, but increased doses (15–20 kGy) led to a significant reduction in particle size to 85 nm. This size reduction was attributed to the fragmentation of larger particles as the irradiation dose increased. Fourier-transform infrared (FTIR) spectroscopy showed notable changes in the ι-carrageenan structure, with the formation of new functional gro

关键词： Antimicrobial Gamma-irradiation Radiolysis Silver nanoparticles Ι-Carrageenan

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Vertically aligned two-dimensional materials-based thick electrodes for scalable energy storage systems

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Nano Research 2021年第10期14卷 3562-3575页

作者： Zhengyu Ju Xiao Zhang Jingyi Wu Guihua Yu Materials Science and Engineering Program Texas Materials InstituteThe University of Texas at AustinAustinTexas 78712USA

Together with the blooming of portable smart devices and electric vehicles in the last decade,electrochemical energy storage(EES)devices capable of high-energy and high-power storage are urgently ***-dimensional(2D)materials,benefiting from the short solid-state diffusion distance,are well recognized to possess excellent electrochemical ***,liquid diffusion,the rate-determining process in thick electrodes,is notably slow in 2D materials-based electrodes stemming from their stacking during electrode processing,which considerably limits their applications for high energy *** fully exploit intrinsic advantages of 2D materials for scalable energy storage devices,this review summarizes several important strategies,ranging from assembly to template methods,to fabricate vertically aligned 2D materials-based *** further discuss the advantages and challenges of these methods in terms of key features of thick electrodes and illustrate the design principles for high-energy/power devices.

关键词： two-dimensional materials energy storage alignment assembly high energy/power

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Design and applications of lattice plasmon resonances

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Nano Research 2018年第9期11卷 4423-4440页

作者： Bharath Bangalore Rajeeva Linhan Lin Yuebing Zheng Materials Science and Engineering Program Department of Mechanical Engineering The University of Texas at Austin Austin Texas78712 USA

With their unique optical properties associated with the excitation of surface plasmons, metal nanoparticles （NPs） have been used in optical sensors and devices. The organization of these NPs into arrays can induce coupling effects to engineer new optical responses. In particular, lattice plasmon resonances （LPRs）, which arise from coherent interactions and coupling among NPs in periodic arrays, have shown great promise for realizing narrow linewidths, angle-dependent dispersions, and high wavelength tunability of optical spectra. By engineering the materials, shapes, sizes, and spatial arrangements of NPs within arrays, one can tune the LPR-based spectral responses and electromagnetic field distributions to deliver a multitude of improvements, including a high figure-of-merit, superior light-matter interaction, and multiband operation. In this review, we discuss recent progress in designing and applying new metal nanostructures for LPR-based applications. We conclude this review with our perspective on the future opportunities and challenges of LPR-based devices.

关键词： plasmonics,lattice plasmon resonance,nanoparticle array coupling,sensors

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