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Mofs-Derived Cu/Carbon Membrane as Bi-Functional Catalyst: Improving Catalytic Activity in Detection and Degradation of Pfoa Via Regulation of Reactive Cu Species

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SSRN 2023年

作者： Hou, Chen Chen, Fang Cheng, Daozhen Zou, Shengyang Wang, Jianzhi Shen, Mengxia Wang, Yang College of Bioresources Chemical and Materials Engineering Shaanxi University of Science and Technology Shaanxi Provincial Key Laboratory of Papermaking Technology and Specialty Paper Development Key Laboratory of Paper Based Functional Materials of China National Light Industry National Demonstration Center for Experimental Light Chemistry Engineering Education Xi’an710021 China Key Laboratory for Green Chemical Process of Ministry of Education Hubei Key Laboratory for Novel Reactor and Green Chemistry Technology Hubei Engineering Research Center for Advanced Fine Chemicals School of Chemical Engineering and Pharmacy Wuhan Institute of Technology Wuhan430073 China

Developing bi-functional materials to simultaneously detect and degrade persistent pollutant perfluorooctanoic acid (PFOA) is of significant importance for environmental and human health. In this study, a copper-based mimic enzyme colorimetric detecting sensor coupling with solar photo-electro-Fenton degradation (SPEF) system was built based on Cu/carbon nanofiber (CNF-Cu/C) membrane. Self-supporting flexible CNF-Cu/C membrane was successfully prepared by solvothermal method with further secondary seed growth and in-situ thermal reduction. Based on calcination temperature regulation, the obtained CNF-Cu/C membrane derived from MOFs/polyacrylonitrile (HKUST/PAN) membrane was characterized by 3D carbon fiber network dispersed with porous carbon skeleton embedded copper species, which exhibited good dispersibility, cycling stability and excellent electrical conductivity. With excellent peroxidase-like activity, CNF-Cu/C can rapidly detect PFOA based on the inhibition of color reaction of tetramethylbenzidine (TMB) with detection limit of 0.133 μM. Furthermore, CNF-Cu/C also exhibited outstanding optical properties and oxygen redox reaction (ORR) activity, and the removal efficiency of PFOA in Cu-SPEF system reached 98.22% within 180 min under optimal conditions. Based on the results of free radical quenching experiment, EPR experiment and HPLC-MS experiments, the degradation mechanism and degradation path of PFOA by SPEF system were further speculated. © 2023, The Authors. All rights reserved.

关键词： Membranes

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Facile Construction of 2d/2d Tio2/Znin2s4 Bifunctional Photocatalysts for Simultaneous Pollutant Degradation and H2 Production

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SSRN 2023年

作者： Chen, Yue Zhu, Liezhen Shen, Youliang Qiu, Lingfang Xu, Xun Xi, Jiangbo Men, Dandan Xu, Zili Duo, Shuwang Li, Ping Jiangxi Key Laboratory of Surface Engineering School of Materials and Energy Jiangxi Science and Technology Normal University Nanchang330038 China Key Laboratory of Novel Biomass-Based Environmental and Energy Materials in Petroleum and Chemical Industry Key Laboratory of Green Chemical Engineering Process of Ministry of Education Engineering Research Center of Phosphorus Resources Development and Utilization of Ministry of Education Hubei Key Laboratory of Novel Reactor and Green Chemical Technology School of Chemistry and Environmental Engineering Wuhan Institute of Technology Wuhan430073 China Jiangxi Science and Technology Normal University China

A two-dimensional/two-dimensional (2D/2D) TiO2/ZnIn2S4 photocatalyst was reasonably proposed and constructed by a two-step oil bath-hydrothermal method. TiO2 nanosheets uniformly grown on the surface of ZnIn2S4 nanosheets and a synergetic effect between the TiO2 and ZnIn2S4 could highly contribute to improving the specific surface area and hydrophilicity of ZnIn2S4 as well as accelerating the separation and transfer of photon-generated e−-h+ pairs, and thus enhancing the visible-light photocatalytic degradation and H2 evolution performance of ZnIn2S4. Rhodamine B (RhB) and tetracycline (TC) were simultaneously selected as the target pollutants for degradation in the work. The optimum photocatalytic RhB and TC degradation properties of TiO2/ZnIn2S4-10wt% were almost 3.11 and 8.61 times higher than that of pure ZnIn2S4, separately, while the highest photocatalytic hydrogen evolution rate was also observed in the presence of TiO2/ZnIn2S4-10wt% and 4.28 times higher than that of ZnIn2S4. Moreover, the possible photocatalytic mechanisms for enhanced visible-light photocatalytic degradation and H2 evolution were investigated and proposed in detail. Our research results open an easy pathway for developing efficient bifunctional photocatalysts.A two-dimensional/two-dimensional (2D/2D) TiO2/ZnIn2S4 photocatalyst was reasonably proposed and constructed by a two-step oil bath-hydrothermal method. TiO2 nanosheets uniformly grown on the surface of ZnIn2S4 nanosheets and a synergetic effect between the TiO2 and ZnIn2S4 could highly contribute to improving the specific surface area and hydrophilicity of ZnIn2S4 as well as accelerating the separation and transfer of photon-generated e−-h+ pairs, and thus enhancing the visible-light photocatalytic degradation and H2 evolution performance of ZnIn2S4. Rhodamine B (RhB) and tetracycline (TC) were simultaneously selected as the target pollutants for degradation in the work. The optimum photocatalytic RhB and TC degradation properties of

关键词： Titanium dioxide

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Ultrafast Oxidative Desulfurization of Diesel Fuel Catalyzed by Polyoxometalate-Based Catalyst Immobilized on Functionalized Y-Sba-15

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SSRN 2022年

作者： Zhang, Zhe Wang, Jian Chen, Ming Zhang, Tao Yang, Biao Peng, Xuelian Zhang, Linfeng Wu, Huadong Guo, Jia Engineering Research Center of Phosphorus Resources Development and Utilization of Ministry of Education Key Laboratory of Green Chemical Process of Ministry of Education Hubei Key Laboratory of Novel Chemical Reactor and Green Chemical Technology Wuhan Institute of Technology Wuhan430073 China School of Environment and Natural Resources Renmin University of China Beijing100872 China

Y-SBA-15 was synthesied by doping Yttrium (Y) into SBA-15 using a solvent-free solid-state grinding method, and 1-butyl-3-methylimidazolium phosphomolybdic salt ([Bmim] 3 PMo 12 O 40 , abbreviated to [Bmim]PMoO ) was synthesized, and then it was loaded on Y-SBA-15. [Bmim]PMoO/Y-SBA-15 is a catalyst used for oxidative desulfurization (ODS). The physicochemical characteristics of the catalyst have been investaged by FT-IR, XRD, BET, FESEM, TEM, XPS, Contact angle testing, and EPR etc. The 25[Bmim]PMoO/10Y-SBA-15 showed highly catalytic activity in dibenzothiophene (DBT) ODS, and removing the complete sulfur compounds within 40 min under the conditions: V Oil = 10 mL, m catalyst =0.1 g, m [Bmim]PMoO : m [Bmim]PMoO/10Y-SBA-15 =25%, O/S = 4 (molar ratio). In addition, the concentration of aromatics had little effect on the DBT ODS. Sulfur compounds in real diesel might be reduced from 203 µg/g to 8 µg/g. The ODS reaction mechanism is also investigated. Hydroxyl radical •OH and superoxide radical •O 2− play crucial roles during ODS reaction. © 2022, The Authors. All rights reserved.

关键词： Catalyst activity

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Experimental measurements of CO2 solubility, viscosity, density, sound velocity and evaporation rate for 2-(2-aminoethoxy)ethanol (DGA) + 1-methylpyrrolidin-2-one (NMP) / water + ionic liquid systems

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Fluid Phase Equilibria 2022年 559卷

作者： Ebrahiminejadhasanabadi, Mojgan Nelson, Wayne Michael Naidoo, Paramespri Mohammadi, Amir H. Ramjugernath, Deresh Thermodynamics Research Unit School of Engineering University of KwaZulu-Natal Howard College Campus King George V Avenue Durban4041 South Africa Department of Process Engineering Faculty of Engineering Stellenbosch University Banhoekweg7600 South Africa Department of Chemical Engineering Faculty of Engineering and the Built Environment Durban University of Technology Steve Biko Campus Durban4001 South Africa

Among technologies used to remove carbon dioxide and hydrogen sulfide from natural gas and flue gas emissions, absorption processes based on amine solvents are the most common. This study investigated the potential of new hybrid amine solutions to absorb carbon dioxide compared to conventional solvents. The solubility of carbon dioxide in hybrid solvents with different mixtures of diglycolamine, water, n-methyl-2-pyrrolidone, 1-butyl-3-methylimidazolium trifluoromethanesulfonate and 1-butyl-3-methylimidazolium bis(trifluoromethanesulfonyl)imide was measured at temperatures of (∼298.15 and ∼313.15) K by a static-synthetic method. Furthermore, the viscosity, density, sound velocity and evaporation rate for the mixtures were measured. Although the addition of an ionic liquid to the solvents increased the viscosity of the solution and decreased the solubility with the aqueous diglycolamine solvents, the replacement of water with a mixture of n-methyl-2-pyrrolidone and ionic liquid increased the solubility. The exception however was observed at lower pressures. © 2022 Elsevier B.V.

关键词： Ionic liquids

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Highly Efficient and Selective Reduction of Nitroarenes to N-Arylhydroxylamines Catalysed by Phosphine Oxide-Decorated Polymer Immobilized Ionic Liquid Stabilized Ruthenium Nanoparticles

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SSRN 2022年

作者： Paterson, Reece Alharbi, Husam Y. Wills, Corinne Chamberlain, Thomas W. Bourne, Richard A. Griffiths, Anthony Collins, Sean M. Wu, Kejun Simmons, Matthew D. Knight, Julian G. Doherty, Simon School of Chemistry Newcastle University Bedson Building Newcastle upon TyneNE1 7RU United Kingdom Institute of Process Research & Development School of Chemistry School of Chemical and Process Engineering University of Leeds Woodhouse Lane LS2 9JT United Kingdom

RuNPs stabilised by phosphine oxide decorated PEG-modified polymer immobilised ionic liquid, RuNP@O=PPh2-PEGPIILS, (2) is a remarkably efficient and selective catalyst for the hydrazine hydrate-mediated partial reduction of nitroarenes to the corresponding N-arylhydoxylamine. Near quantitative conversion to N-phenylhydroxylamine with >99% selectivity was obtained after only 2 h when the reaction was conducted at 25 °C in ethanol under an inert atmosphere using 0.1 mol% catalyst. Under these conditions, the composition-time profile showed that the reduction occurred via the direct pathway whereas reactions in air gave a mixture of azoxy-based products due to competing condensation resulting from reversible formation of N-phenylhydroxylamine. The initial TOF of 6,100 h-1 obtained after 10 min at 40 °C with 0.1 mol% 2 is among the highest to be reported for the metal nanoparticle catalysed reduction of nitrobenzene to N-phenylhydroxylamine and a significant improvement on 5 wt% Ru/C which gave a modest conversion of 21% (initial TOF = 240 h-1) to a mixture of N-phenylhydroxylamine and aniline. A broad range of substituted N-aryl and N-heteroaryl nitroarenes were reduced to the corresponding N-arylhydroxylamine in high yield and with excellent selectivity by adjusting the reaction times. However, reduction of electron rich amino-substituted nitroarenes was extremely slow and resulted in reduction to the aniline with no evidence for the corresponding hydroxylamine. Complete reduction of amino substituted nitroarene is proposed to be facilitated by amine-assisted elimination of hydroxide from the hydroxylamine to afford a readily reducible quinondiimine-derived iminium intermediate that reacts with a surface hydride to liberate the amine. Under optimum conditions the catalyst could be reused five times for the reduction of nitrobenzene to N-phenylhydroxylamine with no detectable change in activity and only slight decrease in selectivity. © 2022, The Authors. All rights re

关键词： Reduction

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Electrodeposited Polyaniline on Graphite Felt (Pani/Gf) Improves Start-Up Time and Acetate Productivity of Microbial Electrosynthesis Cell

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SSRN 2024年

作者： Kim, Eunseo Kim, Minsoo Li, Shuwei Song, Young Eun Maile, Nagesh C. Jang, Min Son, Sang Hwan Jae, Jungho Kim, Hyoung-Il Kim, Jung Rae School of Chemical Engineering Pusan National University Busan46241 Korea Republic of School of Chemical Engineering and Technology Xi’an Jiaotong University Xi’an China Department of Gastroenterology First Affiliated Hospital of Xi’an Jiaotong University 277 West Yanta Road Shanxi Xi’an710061 China Advanced Biofuel and Bioproducts Process Development Unit Lawrence Berkeley National Laboratory EmeryvilleCA94608 United States School of Civil & Environmental Engineering Yonsei University Seoul03722 Korea Republic of Institute for Environmental Energy Pusan National University Busan46241 Korea Republic of Kwangwoon University Korea Republic of

Microbial electrosynthesis (MES) for CO2 capture and utilization has been highlighted for carbon-negative intermediate chemical production. Interface engineering of the electrode surface promotes electron uptake by electroactive bacteria through extracellular electron transport systems and is essential for enhancing acetate production from CO2. This study developed a polyaniline (PANI) electrodeposited graphite felt (GF) electrode to enhance acetate production in MES. The high biocompatibility and electrical conductivity of PANI promoted biofilm formation by increasing the interfacial interaction of electroactive bacteria. The physicochemical properties of PANI/GF were analyzed by Eenergy dispersive X-ray spectroscopy, Fourier transform infrared spectrometry, Raman spectroscopy, and X-ray diffraction. PANI/GF produced higher acetate levels (61.8 g/m2cat/day) from CO2 than the unmodified GF (41.6 g/m2cat/day). The specific capacitance (Cp) of PANI/GF (0.018 Fg-1) was 8.7 times higher than that of the unmodified GF (0.002 Fg-1). The PANI/GF electrodes promoted biofilm formation on the surface and improved the enrichment time of MES. In conclusion, the PANI/GF-modified electrodes facilitate electroactive bacteria–electrode interactions and extracellular electron transfer to improve the performance of MES. © 2024, The Authors. All rights reserved.

关键词： Carbon dioxide

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A novel metal hydride reactor design: The effect of using copper, AlN and AlSi10Mg composite fins on the dehydrogenation process of LaNi5-Metal alloy

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International Journal of Hydrogen Energy 2025年 141卷 118-132页

作者： Chibani, Atef Boucetta, Chahrazed Haddad, Mohammed Amin Nassim Boukhari, Ali Fourar, Issam Merouani, Slimane Badji, Riad Adjel, Samir Belkhiria, Sihem Boukraa, Moustafa Bougriou, Cherif Research Center in Industrial Technologies CRTI P.O.Box 64 Cheraga Algiers16014 Algeria Faculty of Exact Sciences and Sciences of Nature and Life Department of Material Sciences University of Larbi Ben M'hidi Oum El Bouaghi04000 Algeria LMSEA Mechanical Engineering Department National Polytechnic School of Constantine Constantine25000 Algeria UDERZA Unit Faculty of Technology University of El Oued El Oued39000 Algeria Laboratory of Environmental Process Engineering Department of Chemical Engineering Faculty of Process Engineering University Salah Boubnider Constantine 3 P.O. Box 72 Constantine25000 Algeria University of Monastir Faculty of Sciences Laboratory of Thermal and Energetic Systems Studies LR99ES31 Monastir5019 Tunisia Mechanical Engineering Department Faculty of Technology University of Mostefa Ben Boulaid Batna 2 Batna05000 Algeria

The optimal design of solid-state hydrogen storage devices is crucial for their effectiveness. This study investigates the thermal management of LaNi5-based metal hydride reactors for solid-state hydrogen storage by incorporating various fin materials: copper, aluminum nitride (AlN), and Aluminum Silicon Magnesium (AlSi10Mg). Utilizing ANSYS FLUENT 15.0 for simulations within a 2D numerical model, User-Defined Functions (UDFs) were employed to access the dehydrogenation process over a half-hour period. The reactor is subjected to an initial temperature of 363 K and heating oil is introduced at a speed of 1 m/s pressures ranging from 1 to 2 bar. The impact of different fin materials on enhancing the reactor's desorption properties was evaluated through key metrics such as hydrogen concentration, forced convection heat transfer coefficient, and average reactor temperature. Results demonstrate a remarkable improvement in hydrogen desorption rates, where copper fins achieve up to 67.6 % reduction in time to reach equilibrium at 1 bar compared to the reactor without fins. Similarly, AlN and AlSi10Mg fins exhibit a 64 % and 62 % reduction, respectively, highlighting their contributions to improved reactor performance. This research contributes to the advancement of hydrogen storage technologies by offering insights into the selection of fin materials and design for efficient. © 2025 Hydrogen Energy Publications LLC

关键词： Forced convection

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Synergistic effect of synthesized ZnO nanoflowers coupled with various antibiotics against pathogenic microbes: Characterization, antibacterial and antifungal activity assessment

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Nano-Structures and Nano-Objects 2023年 36卷

作者： Makaoui, Nassima Moghni, Nassiba Boutemak, Khalida Akkache, Lynda Imoudache, Hicham Zafour, Amel Hadj-Ziane Chemical Engineering Laboratory Process Engineering Department Faculty of Technology University Saad Dahleb Blida 1 BP270 Blida 09000 Algeria Research and Development Center SAIDAL GROUP Algiers Algeria Functional Analysis of Chemical Processes Laboratory Process Engineering Department Faculty of Technology University Saad Dahleb Blida 1 BP270 Blida 09000 Algeria Pharmaceutical Inorganic Chemistry Laboratory Faculty of Medicine University Saad Dahleb Blida 1 BP270 Blida 09000 Algeria

In this study, zinc oxide nanoparticles (denoted as ZnO NPs) were synthesized via a simple sol-gel technique using only two precursors. Various techniques were utilized to characterize the prepared ZnO nanoparticles. X-ray diffraction analysis indicated the formation of nanoparticulated crystallite ZnO, whilst XPS spectra confirmed the occurrence of Zn and O atoms. SEM imaging showed a nanoflower morphology with varying particle sizes at the nanoscale, whereas DLS characterization revealed a mean particle diameter that equalled 19 nm. The EDX technique confirmed the presence of Zn and O with 85.43% and 12.4%, respectively. Meanwhile the adopted colorimetric method revealed a 99.9% ZnO loading, implying the high purity of the synthesized material. The synergetic effect of combining ZnO nanoflowers with antibiotics, namely chlortetracycline hydrochloride, spiramycin and azithromycin, on enhancing the antibacterial activity against various bacterial strains was investigated via the disc diffusion technique. The antifungal activity of the synthesized ZnO-antibiotic was also examined. The antibacterial and antifungal activities of chlortetracycline hydrochloride and spiramycin were enhanced in the presence of the ZnO nanomaterial, confirming the synergistic impact of the ZnO-chlortetracycline and ZnO-spiramycin conjunctions. The ZnO-CTC materials exhibited the best synergistic effect both against gram-negative and gram-positive organisms. The inhibitory zone of ZnO-CTC in Pseudomonas aeruginosa, Staphylococcus aureus, Bacillus subtilis and Escherichia coli plates were 26.3%, 18.3%, 20.0% and 18.3% higher than that of CTC alone. The inhibition zone of ZnO-CTC against Candida albicans, Saccharomyces cerevisiae and Aspergillus brasiliensis increased by 45.0%, 26.3% and 21.5% in comparison to bare ZnO, respectively. This implies the combination of ZnO-CTC outperforms ZnO in terms of antibacterial efficiency. On the other hand, the antibacterial and antifungal efficiencies we

关键词： Antibacterial activity Antibiotics Antifungal activity Nanoflowers Synergistic effect ZnO

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Box-Behnken Design Optimizing Operating Conditions in Bio-Hydrogenated Diesel Production by Using Bhd Product as a Solvent

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SSRN 2023年

作者： Prapainainar, Paweena Ounsuk, Patravee Prapainainar, Chaiwat Hongloi, Nitchakul Sudsakorn, Kandis Lalitpattarakit, Montida Seubsai, Anusorn Kiatkittipong, Worapon Wongsakulphasatch, Suwimol Assabumrungrat, Suttichai Sureeyatanapas, Panitas National Center of Excellence for Petroleum Petrochemicals and Advance Material Department of Chemical Engineering Faculty of Engineering Kasetsart University Chatuchak Bangkok10900 Thailand Department of Chemical Engineering Faculty of Engineering King Mongkut's University of Technology North Bangkok Bangsue Bangkok10800 Thailand Research and Development Center for Chemical Unit Operation and Catalyst Design Science and Technology Research Institute King Mongkut’s University of Technology North Bangkok Bangkok10800 Thailand Research Network of NANOTEC - KU on NanoCatalysts and NanoMaterials for Sustainable Energy and Environment Kasetsart University Bangkok10900 Thailand Department of Chemical Engineering Faculty of Engineering and Industtrial Technology Silpakorn University Nakhon Pathom73000 Thailand Center of Excellence in Catalysis and Catalytic Reaction Engineering Department of Chemical Engineering Faculty of Engineering Chulalongkorn University Bangkok10330 Thailand Bio-Circular-Green-economy Technology & Engineering Center BCGeTEC Department of Chemical Engineering Faculty of Engineering Chulalongkorn University Bangkok10330 Thailand Department of Industrial Engineering Faculty of Engineering Khon kaen University Khon Kaen40002 Thailand

The development of alternative liquid fuels, such as bio-hydrogenated diesel (BHD), is becoming increasingly important to reduce fossil fuel consumption. In addition, BHD components (such as hexadecane) can be used as a solvent to simplify product separation for the first time. This paper demonstrated the influence of several parameters—temperature (250, 200, 350 ◦C), pressure (10, 20, 30 bar), and reactant-to-solvent ratio (1:0, 1:0.5, 1:1)—for BHD production using palmitic acid as the reactant and hexadecane as the solvent with a nickel-on-zirconia catalyst. Response surface methodology was used to determine the optimum conditions for responses (palmitic acid conversion, BHD selectivity, and yield). A set of experiments was established based on a Box-Behnken designs. The results showed that the most significant parameter for palmitic acid conversion and BHD yield was temperature, especially when higher than 300 ◦C, where the BHD yield increased from 45% to 80%. Overall, the optimum operating conditions were 350 ◦C, 17 bar, and a reactant-to-solvent ratio of 1:0.77, revealing the potential for further use of BHD products as solvent. Deoxygenation of palm fatty acid with hexadecane as solvent found highest conversion of 82.7% and BHD selectivity of 84.38% at reaction time 4 hr. © 2023, The Authors. All rights reserved.

关键词： Solvents

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engineering heavy chain antibody-drug conjugates against solid tumors for a one-shot kill

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Cancer Communications 2024年第12期44卷 1444-1448页

作者： Xue Liu Wenjing Ning Lei Wang Han Liu Hongye Zeng Xiaojing Qin Yuanzhi Chen Fentian Chen Lin Xu Yang Zhao Xiaoqing Chen Jixian Tang Yunlong Ren Xiaowen Yan Wenxin Luo Ningshao Xia State Key Laboratory of Vaccines for Infectious Diseases Xiang An Biomedicine LaboratorySchool of Public HealthXiamen UniversityXiamenFujianP.R.China National Institute of Diagnostics and Vaccine Development in Infectious Diseases State Key Laboratory of Molecular Vaccinology and Molecular DiagnosticsNational Innovation Platform for Industry-Education Integration in Vaccine Researchthe Research Unit of Frontier Technology of Structural Vaccinology of Chinese Academy of Medical SciencesXiamen UniversityXiamenFujianP.R.China Department of Chemistry and the MOE Key Laboratory of Spectrochemical Analysis&Instrumentation College of Chemistry and Chemical EngineeringXiamen UniversityXiamenFujianP.R.China Innovation Laboratory for Sciences and Technologies of Energy Materials of Fujian Province(IKKEM) XiamenFujianP.R.China

The inefficient tumor penetration of conventional antibodies has hampered the effective use of antibody-drug conjugates(ADCs)against solid tumors[1-5].Compared with full-length antibodies and single-chain variable fragment(scFv),nanobodies(Nbs)have much smaller molecular weights,allowing them to achieve deeper tissue penetration,and they have become an attractive candidate platform for conjugating small-molecule drugs and tracers because of their favourable thermostability and high bioengineering potential[6,7].

关键词： drug tumors drugs

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