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Shortening the manufacturing process of degradable magnesium alloy minitube for vascular stents by introducing cyclic extrusion compression

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Journal of Magnesium and Alloys 2024年第8期12卷 3204-3215页

作者： Kun Sheng Wenkai Li Peihua Du Di Mei Shijie Zhu Liguo Wang Shaokang Guan School of Materials Science and Engineering&Henan Key Laboratory of Advanced Magnesium Alloys Zhengzhou UniversityZhengzhou 450001China Key Laboratory of Advanced Materials Processing&Mold Ministry of Education Zhengzhou 450002China

Due to its excellent biocompatibility and biodegradability,Mg and its alloys are considered to be promising materials for manufacturing of vascular ***,the manufacture of high-precision and high-performance Mg alloys minitubes is still a worldwide problem with a long manufacturing processing caused by the poor workability of Mg *** solve this problem,the cyclic extrusion compression(CEC)was used to pretreat the billet by improving the workability of Mg alloys,finally shortening the manufacturing *** CEC treatment,the size of grains and second phase particles of Mg alloys were dramatically refined to 3.2μm and 0.3μm,*** after three passes of cold drawing,the wall thickness of minitube was reduced from 0.200 mm to 0.135 mm and a length was more than 1000 *** error of wall thickness was measured to be less than 0.01 mm,implying a high dimensional *** yield strength(YS),ultimate tensile strength(UTS)and elongation of finished minitube were 220±10 MPa,290±10 MPa and 22.0±0.5%,*** addition,annealing can improve mechanical property and corrosion resistance of minitubes by improving the homogeneity of the microstructure and enhancing the density of basal texture.

关键词： CEC ZE21B Mg alloy Minitube Shortened procedure Cold drawing Annealing

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A novel MgF2/PDA/S-HA coating on the bio-degradable ZE21B alloy for better multi-functions on cardiovascular application

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Journal of Magnesium and Alloys 2023年第2期11卷 480-492页

作者： Yang Yu Shi-Jie Zhu Hao-Tian Dong Xue-Qi Zhang Jing-An Li Shao-Kang Guan School of Materials Science and Engineering&Henan Key Laboratory of Advanced Magnesium Alloy&Key Laboratory of Materials Processing and Mold Technology(Ministry of Education) Zhengzhou UniversityZhengzhou 450001China

Recently, functional molecules such as Polydopamine(PDA), Hyaluronic Acid(HA) and heparin have been widely studied in the field of surface modification of magnesium(Mg) alloy stents for better degradation behavior and biocompatibility, but their further application is limited by undesirable anticoagulant function, uncontrollable degradation and easy bleeding, *** to this consideration, a magnesium Fluoride/Polydopamine/Sulphonated hyaluronic acid(Mg F2/PDA/S-HA) composite coating was successfully prepared by applying S-HA with sulfur content of 9.71 wt% on the surface of ZE21B alloy in this study. The results showed that the composite coating with a unique mesh structure not only inherited the anticoagulant effect of sulfonic acid group and the excellent cyto-compatibility of S-HA with high sulfur content, but also significantly improved the corrosion performance of ZE21B *** results indicate a great application potential of the composite coating in the field of cardiovascular biomaterials.

关键词： Bio-degradable magnesium alloy Cardio-vascular stents Composite coating Sulphonated hyaluronic acid

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Mg alloy cardio-/cerebrovascular scaffolds: Developments and prospects

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Journal of Magnesium and Alloys 2023年第11期11卷 4011-4042页

作者： Shaokang Guan Di Mei Jianfeng Wang Zhaoqi Zhang Peihua Du Lingchuang Bai Chao Yan Jingan Li Jun Wang Shijie Zhu School of Materials Science and Engineering&Henan Key Laboratory of Advanced Magnesium Alloy Zhengzhou UniversityZhengzhou 450001China Key Laboratory of Materials Processing and Mold Technology Ministry of EducationZhengzhou 450002China

Vascular scaffolds are one of the important application fields of biodegradable Mg alloys, and related research has been carried out for more than 20 years. In recent years, the application expansion of Mg alloy vascular scaffolds has brought new challenges to the research of related fields. This review focuses on the relevant advances in the field of Mg alloys for both cardio-/cerebrovascular scaffolds. The frequently investigated alloy series for vascular scaffolds were reviewed. The bottleneck of processing of Mg alloy minitubes was *** idea of functionalized surface modification was also pointed out in this review, and the authors put forward guidelines based on research experience in terms of scaffold structural design and degradation behavior evaluation. Finally, suggestions for further research directions of Mg alloy vascular scaffolds were provided.

关键词： Magnesium alloys Vascular scaffolds Cardiovascular Cerebrovascular Surface modification Degradation evaluation

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Effects of diamond particle size on microstructure and properties of diamond/Al-12Si composites prepared by vacuum-assisted pressure infiltration

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China Foundry 2024年第4期21卷 360-368页

作者： Jia-ping Fu Can-xu Zhou Guo-fa Mi Yuan Liu School of Materials Science and Engineering Henan Polytechnic UniversityJiaozuo 454100HenanChina School of Materials Science and Engineering Tsinghua UniversityBeijing 100084China Key Laboratory for Advanced Materials Processing Technology Ministry of EducationBeijing 100084China

Diamond/aluminium composites have attracted attention in the field of thermal management of electronic packaging for their excellent *** order to solve the interfacial problem between diamond and aluminium,a novel process combining pressure infiltration with vacuum-assisted technology was proposed to prepare diamond/aluminum *** effect of diamond particle size on the microstructure and properties of the diamond/Al-12Si composites was *** results show that the diamond/Al-12Si composites exhibit high relative density and a uniform *** thermal conductivity and coefficient of thermal expansion increase with increasing particle size,while the bending strength exhibits the opposite *** the average diamond particle size increases from 45μm to 425μm,the thermal conductivity of the composites increases from 455 W·m^(-1)·K^(-1)to 713 W·m^(-1)·K^(-1)and the coefficient of thermal expansion increases from 4.97×10^(-6)K^(-1)to 6.72×10^(-6)K^(-1),while the bending strength decreases from 353 MPa to 246 *** research demonstrates that high-quality composites can be prepared by the vacuum-assisted pressure infiltration process and the thermal conductivity of the composites can be effectively improved by increasing the diamond particle size.

关键词： diamond/aluminum composites thermal conductivity electronic packaging vacuum-assisted pressure infiltration

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In-situ polymerized PEO-based solid electrolytes contribute better Li metal batteries:Challenges,strategies,and perspectives

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Journal of Energy Chemistry 2024年第5期92卷 548-571页

作者： Zhihui Jia Yong Liu Haoming Li Yi Xiong Yingjie Miao Zhongxiu Liu Fengzhang Ren School of Materials Science and Engineering Henan Key Laboratory of Non-Ferrous Materials Science&Processing TechnologyHenan University of Science and TechnologyLuoyang 471023HenanChina Provincial and Ministerial Co-construction of Collaborative Innovation Center for Non-ferrous Metal new Materials and Advanced Processing Technology Henan University of Science and TechnologyLuoyang 471023HenanChina

Polyethylene oxide(PEO)-based solid polymer electrolytes(SPEs)with good electrochemical stability and excellent Li salt solubility are considered as one of the most promising SPEs for solid-state lithium metal batteries(SSLMBs).However,PEO-based SPEs suffer from low ionic conductivity at room temperature and high interfacial resistance with the electrodes due to poor interfacial contact,seriously hindering their practical *** an emerging technology,in-situ polymerization process has been widely used in PEO-based SPEs because it can effectively increase Li-ion transport at the interface and improve the interfacial contact between the electrolyte and ***,we review recent advances in design and fabrication of in-situ polymerized PEO-based SPEs to realize enhanced performance in *** merits and current challenges of various SPEs,as well as their stabilizing strategies are ***,various in-situ polymerization methods(such as free radical polymerization,cationic polymerization,anionic polymerization)for the preparation of PEO-based SPEs are *** addition,the application of in-situ polymerization technology in PEO-based SPEs for adjustment of the functional units and addition of different functional filler materials was systematically discussed to explore the design concepts,methods and working ***,the challenges and future prospects of in-situ polymerized PEO-based SPEs for SSLMBs are also proposed.

关键词： In-situ polymerization Polyethylene oxide Solid polymer electrolytes Lithium metal anodes

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Heterobimetallic[NiCo]integration in a hydrogenase mimic for boosting light-driven hydrogen evolution in CaTiO_(3)

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Nano Research 2024年第8期17卷 6888-6894页

作者： Kang Li Juanji Hong Ningning Song Zhanjun Guo Minmin Liang Experimental Center of Advanced Materials School of Materials Science&EngineeringBeijing Institute of TechnologyBeijing 10081China

Light-drive hydrogen production using titanium-based perovskite is one sustainable way to reduce current reliance on fossil fuels,but its wide applications are still limited by high electron−hole recombination and sluggish surface ***,the developments for low-cost and highly efficient co-catalysts remain *** by natural[NiFe]-hydrogenase active center structure,a hydrogenase-mimic,NiCo_(2)S_(4) nanozyme was synthesized,and subsequently decorated onto the CaTiO_(3) to catalyze the hydrogen evolution reaction(HER).Among the following test,CaTiO_(3)with a 15%loading of NiCo_(2)S_(4) nanozyme exhibited the highest HER rate of 307.76μmol·g^(–1)·h^(–1),which is 60 times higher than that of the CaTiO_(3) *** results reveal that NiCo_(2)S_(4) not only significantly increased the charge separation efficiency of the photogenerated carriers,but also substantively lowered the HER activation *** studies show that NiCo_(2)S_(4) readily splits H_(2)O by forming the Ni(OH)-Co intermediate and only Ni in the bimetallic center alters the oxidation state during the HER process in a manner analogous to the[NiFe]-*** contrast to the often-expensive synthetic catalysts that rely on rare elements such as ruthenium and platinum,this study shows a promising way to develop the nature-inspired cocatalysts to enhance the photocatalysts’HER performance.

关键词： hydrogen evolution reaction hydrogenase-mimic nanozyme photocatalyst water-splitting

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Tracing monoclinic distortion in NCM532 cathode materials by in situ high-energy synchrotron X-ray diffraction

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Progress in Natural science:materials International 2024年第2期34卷 274-279页

作者： Min Dong Qingya Sun Zhihua Wang Zixin Rui Zhe Zhang He Zhu Si Lan Herbert Gleiter Institute of Nanoscience School of Materials Science and Engineering Nanjing University of Science and Technology School of Mechanical Engineering Nanjing University of Science and Technology School of Materials Science and Engineering Henan University of Technology Center for Neutron Scattering City University of Hong Kong Shenzhen Research Institute

Layered LiNixCoyMnzO2（NCM） cathode materials have emerged as the best choice for high-energy-density lithium-ion batteries for powering electric *** significant research efforts,the understanding of complex structural dynamics during lithium（de-） intercalation still remains a subject of debate,especially in scenarios where morphology and composition *** this study,we carried out in situ high-energy synchrotron X-ray diffraction experiments on commercial NCM523cathode materials in both single crystal and polycrystalline forms to probe the structural changes during charging and discharging in *** findings reveal that both single crystal and polycrystalline materials exhibit typical H1-H2-H3 phase ***,in polycrystalline NCM532,a monoclinic intermediate phase emerges between the H1 and H2 *** this process,symmetry reduces from R-3m to C2/m,which is attributed to a shear distortion along the ab *** contrast,for single crystal materials,the H1 phase directly transforms into the H2 phase without the monoclinic *** observed monoclinic distortion significantly impacts structural stability and material cycling *** study provides new insight into the structural dynamics in NCM532 cathode materials,particularly concerning morphology-dependent behaviors,which could deepen our understanding of the relationship between NCM material structures and their performance.

关键词： Single crystals

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Modeling bacterial adhesion on the nanopatterned surface by varying contact area

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Journal of materials science & technology 2024年第29期196卷 137-147页

作者： Kun Yang Lei Wang Xianrui Zou Hongshui Wang Chunyong Liang Dawei Zhang Lu-Ning Wang Beijing Advanced Innovation Center for Materials Genome Engineering State Key Laboratory for Advanced Metals and MaterialsSchool of Materials Science and EngineeringUniversity of Science and Technology BeijingBeijing 100083China School of Materials Science and Engineering Hebei University of TechnologyTianjin 300130China School of Health Sciences and Biomedical Engineering Hebei University of TechnologyTianjin 300130China Institute for Advanced Materials and Technology University of Science and Technology BeijingBeijing 100083China Institute of Materials Intelligent Technology Liaoning Academy of MaterialsShenyang 110004China

Bacterial adhesion is a critical process in many fields,such as implant infections,microbiologically influenced corrosion and bioelectricity generation in microbial fuel *** bacterial adhesion,the contact area between the attached bacteria and the patterned surface plays an important *** this study,different surface topographies and treatments were employed to simulate three circumstances with different contact areas.A nanostripe structure with a period of 576.9 nm and a height of 203.5 nm was fabricated on pure titanium by femtosecond laser *** in liquid attached to the peaks of the nanostripe structure and were stretched on the two adjacent *** with the polished surface,the contact area between bacteria and the nanostripe surface was reduced to 50%,resulting in a reduction(about 50%)in the coverage rate of attached *** addition,the nanostripe surface was a hydrophobic surface with a water contact angle(WCA)of 112.1°,and the surface potential of the nanostripe surface was higher than that of the polished ***,the surface potential and wettability of the nanostripe surface played a minor role in the bacterial adhesion due to the reduced contact *** drying,the attached bacteria on the nanostripe surface sank into the valley region and the contact area was about 40%larger than that on the polished *** lateral strength of bacterial adhesion on nanostripe surfaces was higher than that on polished surfaces,due to the larger contact *** applying a lateral force of 10.0 nN,the percentage of bacteria remaining on the nanostripe surface(31.1%)was higher than that on the polished surface(11.9%).Hence,the bacterial adhesion on the nanopatterned surface was mainly determined by the contact *** in-depth exploration of the relation between bacterial adhesion on the nanopatterned surface and the contact area enables the rational surface designs of biomaterials to regulate bacterial adhesion.

关键词： Bacterial adhesion Contact area Nanopatterned surface Atomic force microscope

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Optimizing the overall performance of Cu–Ni–Si alloy via controllingnanometer-lamellar discontinuous precipitation structure

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International Journal of Minerals,Metallurgy and materials 2025年第4期32卷 915-924页

作者： Jinyu Liang Guoliang Xie Feixiang Liu Wenli Xue Rui Wang Xinhua Liu Key Laboratory for Advanced Materials Processing(MOE) Institute for Advanced Materials and TechnologyUniversity of Science and Technology BeijingBeijing 100083China Beijing Laboratory of Metallic Materials and Processing for Modern Transportation Institute for Advanced Materials and TechnologyUniversity of Science and Technology BeijingBeijing 100083China State Key Laboratory for Advanced Metals and Materials University of Science and Technology BeijingBeijing 100083China Beijing Advanced Innovation Center for Materials Genome Engineering University of Science and Technology BeijingBeijing 100083China Institute of Materials Genome Engineering Henan Academy of SciencesZhengzhou 450046China

Simultaneously achieving high strength and high electrical conductivity in Cu–Ni–Si alloys pose a significant challenge, which greatly constrains its applications in the electronics industry. This paper offers a new pathway to improve properties, by preparation of nanometer lamellar discontinuous precipitates(DPs) arranged with the approximate same direction through a combination of deformationaging and cold rolling process. The strengthening effect is primarily attributed to nanometer-lamellar DPs strengthening and dislocation strengthening mechanism. The accumulation of dislocations at the interface between nanometer lamellar DPs and matrix during cold deformation process can results in the decrease of dislocation density inside the matrix grains, leading to the acceptably slight reduction of electrical conductivity during cold rolling. The alloy exhibits an electrical conductivity of 45.32%IACS(international annealed copper standard, IACS), a tensile strength of 882.67 MPa, and a yield strength of 811.33 MPa by this method. This study can provide a guidance for the composition and microstructure design of a Cu–Ni–Si alloy in the future, by controlling the morphology and distribution of DPs.

关键词： Cu–Ni–Si alloys discontinuous precipitates nanometer-lamellar strengthening dislocation strengthening

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Post-tunable salt gel electrolytes toward flexible supercapacitor switches

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Journal of Energy Chemistry 2025年第1期100卷 114-124页

作者： Hui Wang Shuang Chen Xuming Liu Qin Zhang Xin Liu Polymeric and Soft Materials Laboratory School of Chemistry and Life Science and Advanced Institute of Materials ScienceChangchun University of TechnologyChangchun 130012JilinChina Polymeric and Soft Materials Laboratory School of Chemical Engineering and Advanced Institute of Materials ScienceChangchun University of TechnologyChangchun 130012JilinChina

Convertible hydrogel supercapacitors have emerged as promising energy storage devices in switches,diodes,and ***,inherent weaknesses in ionic conductivity,mechanical properties,and water retention of hydrogel electrolytes seriously hinder their *** by the hardness conversion of sea cucumber skin,a conductivity and mechanics dual-tunable salt gel electrolyte is successfully *** salt gel presents a reversible switching of conductors-insulators and a mechanical regulation between softness and hardness via the dissolution-crystallization transition of sodium acetate trihydrate(SAT).Meanwhile,the salt gels spontaneously grow a layer of“armor”through saturated phase-change salt crystals effectively reducing water evaporation of hydrogel ***,this phase-change soft-rigid conversion strategy will expand the capabilities of gel-based flexible supercapacitors(area capacitance:258.6 mF cm^(-2)),and the capacitance retention rate could still reach 86.9%after 3000 cycles at high ***,the salt gel supercapacitor is potentially used in over-heat alarm *** is anticipated that the strategy of conductivity and mechanics of dual-tunable salt gel would provide a new perspective on the development of energy storage devices,wearable electronics,and flexible robots.

关键词： Supercapacitors Salt gels Reversible phase transition Post-tuning Conductivity switching

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