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Food Chemistry Advances 2023年 3卷

作者： Gomes, Bianca Almada Ferreira de Barros, Hanna Elísia Araújo Natarelli, Caio Vinicius Lima Zitha, Elídio Zaidine Maurício Carvalho, Elisângela Elena Nunes de Barros Vilas Boas, Eduardo Valério Food Science Department Federal University of Lavras P.O. Box 3037 Minas Gerais Lavras 37200-900 Brazil Graduate Program in Materials Science and Engineering Federal University of São Carlos São Paulo São Carlos 13565-905 Brazil

The objective of this work was to determine the effect of the binomial time/temperature of hydrocooling (10 and 20 min at 0 °C, 10 °C, and 20 °C) on the shelf life of sorrel, a non-conventional vegetable. The experimental design was entirely randomized in a 2 × 3 × 6 factorial scheme with three repetitions. The vegetables were stored at 10±1 °C and 99% relative humidity for 10 days. The effects of time and temperature of hydrocooling on physical and chemical characteristics were observed. The degradation of bioactive compounds was higher in the control samples and samples hydrocooled at 0 °C, resulting in lower antioxidant capacity at 10 days. Hydrocooling at 20 °C for 10 min maintained the color of the vegetables until the tenth day, with a chlorophyll content of 34.54 mg.100 g⁻¹, related to the reduction of the respiration rate and weight loss. Hydrocooled sorrel for 20 min at the same temperature showed a vitamin C content of 63.71 mg.100 g⁻¹ and total phenolics of 249.57 mg of EAG.100 g⁻¹ of fresh matter, by the Fast Blue method. Thus, 20 °C for 10 or 20 min was the most efficient parameter for preserving sorrel samples. © 2023

关键词： Artificial neural network Bioative compounds Postharvest losses Pre-cooling. Shelf life Unconventional vegetable

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A First-Principles and Calphad-Assisted Phase-Field Model for Microstructure Evolution: Application to Mo-V Binary Alloy Systems

SSRN

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SSRN 2023年

作者： Thakur, Abhishek Kumar Kovacevic, Sasa Manga, Venkateswara Rao Deymier, Pierre Alix Muralidharan, Krishna Department of Materials Science and Engineering University of Arizona TucsonAZ85721 United States Department of Civil and Environmental Engineering Imperial College London LondonSW7 2AZ United Kingdom Lunar and Planetary Laboratory University of Arizona TucsonAZ85721 United States Graduate Interdisciplinary Program in Applied Mathematics India

A multiscale computational framework combining the first-principles calculations and the CALPHAD approach with the phase-field method is presented to simulate the microstructure evolution in multicomponent steel alloys. We demonstrate the potential of the framework by predicting the microstructural evolution in elastically periodic arrays of the Mo-V binary sub-system. The framework utilizes the first-principles calculations using special quasi-random structures. Hitherto unavailable thermodynamic and material properties of the alloy are obtained by employing the first-principles calculations and the CALPHAD approach and fed into the phase-field model to predict the microstructure evolution at different temperatures within the miscibility gap region. In addition to the temperature and cooling rates, the model incorporates the role of mechanical fields in decomposition kinetics in the Mo-V binary alloy system. Regimes for temperatures and cooling rates at which spinodal decomposition occurs are identified. Applying external loading leads to directional phase separation in the Mo-V binary system. The elastic inhomogeneity in terms of material properties between the two phases initiates the directional alignment while eigenstrains and applied external loading control the degree of alignment. The framework developed is general and extendable to higher multicomponent sub-systems in steel alloys. © 2023, The Authors. All rights reserved.

关键词： Temperature

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Effect of pyrolysis temperature on characteristics of tunable magnetic biochar synthesized from watermelon rind and its tetracycline adsorption performance

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Journal of the Taiwan Institute of Chemical Engineers 2024年 160卷

作者： Thairattananon, Phisit Le, Giang T.T. Matsumura, Yukihiko Wu, Kevin C.W. Charinpanitkul, Tawatchai Department of Chemical Engineering Faculty of Engineering Center of Excellence in Particle and Material Processing Technology Chulalongkorn University Bangkok10330 Thailand Institute of Fundamental and Applied Sciences Duy Tan University Ho Chi Minh700000 Viet Nam Faculty of Environmental and Chemical Engineering Duy Tan University Da Nang550000 Viet Nam Mechanical Engineering Program Graduate School of Advanced Science and Engineering Kagamiyama Hiroshima Higashi-Hiroshima739-8527 Japan Department of Chemical Engineering National Taiwan University Taipei10617 Taiwan Department of Chemical Engineering and Materials Science Yuan Ze University Chung-Li Taoyuan Taiwan Research Network of NANOTEC-KU on Nanocatalyst and Nanomaterials for Sustainable Energy and Environment Bangkok10900 Thailand

Background: Tetracycline is an emerging contaminant in water reservoirs, causing undesirable influences on human society. The promising usage of magnetic biochar (MBC) derived from watermelon rind has been explored in the adsorption of various contaminants owing to its high specific surface area and separability;however, the temperature-dependent changes of MBC and its sorption ability toward antibiotics have not been widely examined. Method: Tunable MBCs could be synthesized via simple pyrolysis of watermelon rind impregnated with FeCl3 at different temperatures (700–900 °C). The as-synthesized MBCs were characterized using scanning electron microscopy (SEM), an elemental analyzer, N2 adsorption/desorption, Fourier-transform infrared spectroscopy (FTIR), Raman spectroscopy, X-ray diffractometry (XRD), and vibrating sample magnetometry (VSM). Then Tetracycline, an emerging contaminant in water reservoirs, was employed as the target contaminant, while adsorption kinetics, isotherm, the effect of pH, and reusability were investigated. Significant findings: The tunability of as-synthesized MBCs could be observed by their distinct changes in structural characteristics when varying pyrolysis temperature. MBC synthesized at 900 °C (MBC900) possessed a high-specific surface area (401 m2.g−1) and saturation magnetization (55.29 emu.g−1), resulting in a greater amount of sorption sites. Tetracycline adsorption by MBCs followed a pseudo-second-order kinetic model and fitted well with the Freundlich model. MBC900 is an excellent adsorbent with a maximum adsorption capacity of 77.6 mg.g−1 and could be used for at least five cycles with an insignificant decrease in the adsorption capacity. © 2024 Taiwan Institute of Chemical Engineers

关键词： Adsorption

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Designing the pressure-dependent shear modulus using tessellated granular metamaterials

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Physical Review E 2023年第3期108卷 034901-034901页

作者： Jerry Zhang Dong Wang Weiwei Jin Annie Xia Nidhi Pashine Rebecca Kramer-Bottiglio Mark D. Shattuck Corey S. O'Hern Department of Mechanical Engineering & Materials Science Yale University New Haven Connecticut 06520 USA Benjamin Levich Institute and Physics Department The City College of New York New York New York 10031 USA Department of Physics Yale University New Haven Connecticut 06520 USA Department of Applied Physics Yale University New Haven Connecticut 06520 USA Integrated Graduate Program in Physical and Engineering Biology Yale University New Haven Connecticut 06520 USA

Jammed packings of granular materials display complex mechanical response. For example, the ensemble-averaged shear modulus 〈G〉 increases as a power law in pressure p for static packings of soft spherical particles that can rearrange during compression. We seek to design granular materials with shear moduli that can either increase or decrease with pressure without particle rearrangements even in the large-system limit. To do this, we construct tessellated granular metamaterials by joining multiple particle-filled cells together. We focus on cells that contain a small number of bidisperse disks in two dimensions. We first study the mechanical properties of individual disk-filled cells with three types of boundaries: periodic boundary conditions (PBC), fixed-length walls (FXW), and flexible walls (FLW). Hypostatic jammed packings are found for cells with FLW, but not in cells with PBC and FXW, and they are stabilized by quartic modes of the dynamical matrix. The shear modulus of a single cell depends linearly on p. We find that the slope of the shear modulus with pressure λc<0 for all packings in single cells with PBC where the number of particles per cell N≥6. In contrast, single cells with FXW and FLW can possess λc>0, as well as λc<0, for N≤16. We show that we can force the mechanical properties of multicell granular metamaterials to possess those of single cells by constraining the end points of the outer walls and enforcing an affine shear response. These studies demonstrate that tessellated granular metamaterials provide a platform for the design of soft materials with specified mechanical properties.

关键词： Jamming Granular solids Mechanical metamaterials

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Characterization of the Root Surface of a Friction Stir Welded Uns S32760 Super Duplex Stainless Steel: Insights into its Microstructure and Corrosion Resistance

SSRN

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SSRN 2023年

作者： Vacchi, G.S. de Carvalho, Willian S. Meinhardt, C.P. Bergmann, Luciano A. Amancio-Filho, Sergio T. Rovere, C.A.D. Munir Rachid Corrosion Laboratory Department of Materials Engineering Federal University of São Carlos Rodovia Washington Luis Km 235 SP São Carlos13565-905 Brazil Federal University of São Carlos Graduate Program in Materials Science and Engineering Brazil Graz University of Technology – TU Graz Institute of Materials Science Joining and Forming BMK Endowed Professorship for Aviation Kopernikusgasse 24/1 Graz8010 Austria Federal University of Pampa Department of Mechanical Engineering Avenida Tiarajú 810 RS Alegrete Brazil Helmholtz-Zentrum Hereon Institute of Materials Mechanics Solid State Materials Processing Max-Planck-Straße 1 Geesthacht Germany

The root surface of a friction stir welded super duplex stainless steel (UNS S32760) was thoroughly characterized in this study. The findings revealed a refined grain structure and a conspicuous increase of 50 HV0.3 in the Root's hardness. Interestingly, the volume fraction of the ferrite phase remained largely unchanged. Rapid cooling in the welding process led to the Cr2N precipitation at the ferrite/ferrite grain boundaries in the root area, significantly increasing sensitization, reducing localized corrosion resistance under high potentials in a neutral pH saline environment, and adversely affecting root passivity in a hydrochloric acid environment compared to the base metal. © 2023, The Authors. All rights reserved.

关键词： Friction stir welding

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Preprocessing Techniques for Enhancing Vision-Based Detection System for Tire Sidewall Extraction

Preprocessing Techniques for Enhancing Vision-Based Detectio...

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International Seminar on Research of Information Technology and Intelligent Systems (ISRITI)

作者： Jia Hao Loo Veronica Lestari Jauw Chin Seong Lim Khairul-Rijal Sarmin Nunung Nurul Qomariyah Ahmad Nurul Fajar Department of Mechanical Materials and Manufacturing Engineering University of Nottingham Malaysia Malaysia Continental Tyre Technology Centre Malaysia Petaling Jaya Malaysia Computer Science Department School of Computing and Creative Arts Bina Nusantara University Jakarta Indonesia Information System Management Department BINUS Graduate Program-Master Information Systems Bina Nusantara University Jakarta Indonesia

ISBN: (数字)9798331519643

ISBN: (纸本)9798331519650

This study aims to develop a system for extracting crucial information from tire sidewalls using Optical Character Recognition (OCR). Initially, images of tire were captured manually by smartphone cameras, including Redmi 9T, iPhone 11, and Galaxy S23 Ultra. The captured images are then transferred to a computer for storage. Subsequently, these images were cropped according to the boundaries identified by Hough Circle Transform (HCT). The cropped images were then further pre-processed. During the pre-processing phase, geometrical transformation and image sharpening techniques are applied to enhance the clarity and readability of the text images. The text is then extracted using Google Vision, with the extracted text categorized by size, DOT, brand and pattern. The results indicated that the effectiveness of image pre-processing was constrained by the accuracy of circle detection, which reached a maximum rate of 87.1%. This causes parts of the text to be cut out inaccurately, leading to a suboptimal extraction accuracy of 55.65%. It is also observed that the Redmi 9T camera produced inconsistent results compared to other devices. Specifically, the iPhone 11 and Samsung Galaxy S23 Ultra demonstrated superior extraction accuracies of 69.71% and 66.37%, respectively, whereas the Redmi 9T achieved a lower extraction accuracy of 37.76%.

关键词： Accuracy Optical character recognition Text categorization Lighting Transforms US Department of Transportation Cameras Tires Internet Data mining

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Emulating complex synapses using interlinked proton conductors

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Physical Review Applied 2025年第1期23卷 014027-014027页

作者： Lifu Zhang Ji-An Li Yang Hu Jie Jiang Rongjie Lai Marcus K. Benna Jian Shi Department of Materials Science and Engineering Rensselaer Polytechnic Institute Troy New York 12180 USA Neurosciences Graduate Program University of California San Diego La Jolla California 92093 USA Department of Mathematics Purdue University West Lafayette Indiana 47907 USA Department of Neurobiology School of Biological Sciences University of California at San Diego La Jolla California 92093 USA Department of Physics Applied Physics and Astronomy Rensselaer Polytechnic Institute Troy New York 12180 USA

In terms of energy efficiency and computational speed, neuromorphic electronics based on nonvolatile memory devices are expected to be one of most promising hardware candidates for future artificial intelligence (AI). However, catastrophic forgetting, networks rapidly overwriting previously learned weights when learning new tasks, remains a pivotal obstacle in either digital or analog AI chips for unleashing the true power of brainlike computing. To address catastrophic forgetting in the context of online memory storage, a complex synapse model (the Benna-Fusi model) was proposed recently [M. K. Benna and S. Fusi, Nat. Neurosci. 19, 1697 (2016)], the synaptic weight and internal variables of which evolve following diffusion dynamics. In this work, by designing a proton transistor with a series of charge-diffusion-controlled storage components, we have experimentally realized the Benna-Fusi artificial complex synapse. Memory consolidation from coupled storage components is revealed by both numerical simulations and experimental observations. Different memory timescales for the complex synapse are engineered by the diffusion length of charge carriers and the capacity and number of coupled storage components. The advantages of the demonstrated complex synapse for both memory capacity and memory consolidation are revealed by neural network simulations of face-familiarity detection. Our experimental realization of the complex synapse suggests a promising approach to enhance memory capacity and to enable continual learning.

关键词： Nonvolatile storage

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Wavelength dependence of laser-induced nanowelded microstructures assembled from metal nanoparticles

arXiv

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arXiv 2023年

作者： Rogers, Ariel Niyonshuti, Isabelle I. Ou, Jun Shrestha, Diksha Chen, Jingyi Wang, Yong Department of Physics University of Arkansas FayettevilleAR72701 United States Department of Chemistry and Biochemistry University of Arkansas FayettevilleAR72701 United States School of Engineering California State Polytechnic University Humboldt ArcataCA95521 United States Mechanical Engineering Program California State Polytechnic University Humboldt ArcataCA95521 United States Cell and Molecular Graduate Program University of Arkansas FayettevilleAR72701 United States Materials Science and Engineering Program University of Arkansas FayettevilleAR72701 United States

Light-based nanowelding of metallic nanoparticles is of particular interest because it provides convenient and controlled means for the conversion of nanoparticles into microstructures and fabrication of nanodevices. Here, we demonstrated the wavelength dependence of laser-induced nanowelded shapes of silver nanoparticles (AgNPs). We observed that the nanowelded microstructures illuminated by the 405 nm laser only were more branched than those formed with illumination of both the 405 nm and 532 nm lasers. We quantified this observation by several compactness descriptors and examined the dependence of the power of the 532 nm laser. More importantly, to understand the experimental observations, we formulated and tested a hypothesis by calculating the wavelength-dependent electric field enhancement due to surface plasmon resonance of the AgNPs and nanowelded microstructures when illuminated with lights at the two wavelengths. Based on the different patterns of "hot spots" for welding AgNPs from these calculations, numerical simulations successfully "reproduced" the different shapes of nanowelded microstructures, supporting our hypothesis. This work suggests the possibility of light-based controlling the shapes of laser-induced nanowelded microstructures of metallic nanoparticles. This work is expected to facilitate the development of better nanowelding strategies of metallic nanoparticles for broader applications. Copyright © 2023, The Authors. All rights reserved.

关键词： Surface plasmon resonance

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Room temperature phosphorescence materials based on small organic molecules: Design strategies and applications

Responsive Materials

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Responsive materials 2024年第3期2卷

作者： Meixia He Cong Ding Hexiang Guo Quan Li Institute of Advanced Materials and School of Chemistry and Chemical Engineering Southeast University Nanjing China Materials Science Graduate Program Kent State University Kent Ohio USA

Room-temperature phosphorescence (RTP) materials have attracted significant attention due to their applications in various fields such as information storage and encryption, organic light-emitting diode (OLED), sensing, lighting and display, biological imaging, and photodynamic therapy. Traditionally, RTP materials can be efficiently developed using inorganic systems with noble metals or rare earth elements. Recently, many efforts have been devoted to the development of RTP materials based on small organic molecules. The strategies to construct RTP materials include hydrogen bonding, heavy atom effect, n –π* transitions, π–π stacking, donor–acceptor effect, and host–guest doping. Herein, we summarize the recent examples of RTP materials based on small organic molecules primarily focusing on their design strategies and properties. Moreover, their promising applications in information encryption, OLED, as well as bio-imaging and phototherapy are discussed. The challenges and perspectives are given to provide inspiration toward the future development of organic RTP materials.

关键词： bio-imaging information encryption organic room-temperature phosphorescence persistent room temperature phosphorescence small organic molecule

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Performance comparison of InGaN-based 40–80 μm micro-LEDs fabricated with and without plasma etching

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materials Today Advances 2024年 22卷

作者： Lo, Yu-Yun Chen, Yi-Ho Hsu, Yun-Cheng Lee, Tzu-Yi Hung, Yu-Ying Kao, Yu-Cheng Zan, Hsiao-Wen Wuu, Dong- Sing Kuo, Hao-Chung Samukawa, Seiji Horng, Ray-Hua Institute of Electronics National Yang Ming Chiao Tung University 1001 University Road Hsinchu30010 Taiwan Department of Photonics College of Electrical and Computer Engineering National Yang Ming Chiao Tung University Hsinchu30010 Taiwan Graduate Degree Program of College of Electrical and Computer Engineering National Yang Ming Chiao Tung University Hsinchu30010 Taiwan Department of Materials Science and Engineering National Chung Hsing University Taichung40227 Taiwan Department of Applied Materials and Optoelectronic Engineering National Chi Nan University Nantou54561 Taiwan Semiconductor Research Center Hon Hai Research Institute Taipei11492 Taiwan Institute of Communications Engineering National Yang Ming Chiao Tung University Hsinchu30010 Taiwan

The fabrication of InGaN-based blue 4✕4 array micro-LEDs (μLEDs) with 40 μm ✕40 μm chip size and 2✕2 array μLEDs with 80 μm ✕80 μm chip size etching by the inductive coupled plasma reactive ion etching (ICPRIE) and defect-free neutral beam etching (NBE) processes was studied in this work. In μLEDs of this size, the influence of defects formation in the sidewalls on EQE was evaluated. There was almost no difference in EQE between μLEDs array etched by the NBE process no matter 40 μm ✕40 μm and 80 μm ✕80 μm, but the dependence was observed in the ICPRIE. Even with this size, it was found that the size effect of EQE is smaller than that in case of using ICPRIE for defect-free neutral beam etching. This impact is substantial since μLED predominantly operated at low current density, around 1–5 A/cm2. Consequently, the reduction of defect density, encompassing both internal and sidewall defects, becomes imperative even in 40–80 μm InGaN-based μLEDs. This not only improves the overall efficiency of μLEDs but also fortifies the brightness stability of μLED displays if process etching by NBE. It was also found that the etching shape had an influence on EQE. It could be attributed to fact that the etching profile angle of NBE was more vertical than that of ICPRIE. Because the different angles of the mesa resulted in different light intensity. The μLEDs emitting with a wavelength of 450 nm, the light extraction efficiency and intensity at a mesa angle 58° of NBE etching μLEDs was about 8% lower than those of an angle (38°) of ICPRIE etching μLEDs by simulation. © The Authors

关键词： Light emitting diodes

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