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Injectable Platelet-Rich Fibrin in Contact with Bone Substitutes, Porous Zirconia, or Laser-Textured Implant Surfaces: A Detailed Morphological Analysis

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Biomedical materials and Devices 2024年第1期2卷 415-426页

作者： Oliveira, Miguel Noronha Varela, Hugo Almeida Nascimento, Rubens M. Sahoo, Narayan Carvalho, Oscar Henriques, Bruno Souza, Júlio C. M. Ceramic and Composite Materials Research Group (CERMAT) Department of Mechanical Engineering (EMC) Federal University of Santa Catarina (UFSC) Post-graduate Program in Materials Science and Engineering Federal University of Rio Grande Norte (UFRN) Center for MicroElectroMechanical Systems (CMEMS-UMINHO) Universidade do Minho LABBELS - Associate Laboratory University of Minho University Institute of Health Sciences (IUCS) CESPU

The aim of the present study was to perform a detailed morphological analysis of an injectable platelet rich fibrin after combination with two different particulate hydroxyapatite-based granules, a porous zirconia block, and laser-textured zirconia or titanium surfaces. Blood samples were harvested from three participants to prepare the flowable injectable PRF in contact or not with particulate hydroxyapatite (Hap), bone mineral granules (DBBM), porous zirconia blocks, laser-textured titanium or zirconia surfaces. Optical and scanning electron microscopy (SEM) were used to evaluate the fibrin network density, fibrin fibers’ diameter, blood cells, and the interaction of PRF with the biomaterials. Histomorphometry of the flowable PRF was also performed using the hematoxylin–eosin staining protocol. Specimens were independently evaluated by two blinded and well-trained researchers in histomorphometry and microscopy. Particulate Hap and DBBM shown different morphological aspects by SEM analyses since DBBM revealed macro- and micro-scale pores while Hap revealed a dense structure. Hydroxyapatite and DBBM granules were entirely embedded by the fibrin-network in the presence of leukocytes and blood platelets. The zirconia porous structured was filled with PRF and its components. Also, the laser-structured zirconia or implant surfaces were entirely coated with the PRF fibrin network embedding leukocytes and blood platelets. Laser-textured titanium surfaces revealed macro- and micro-scale irregularities that increase the surface area and retention of the injectable PRF. Histomorphometric analyses revealed complementary details on the distribution of lymphocytes, red blood cells, and fibrin associated with platelet aggregation. The flowing and viscosity of an injectable platelet rich fibrin provided an agglomeration of synthetic or xenogeneic particulate bone substitutes and the coating of porous zirconia and textured implant surfaces as inspected by scanning electron microsc

关键词： Bone healing Bone substitutes Histology Morphology Platelet-rich fibrin

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Anomalous properties of spark plasma sintered boron nitride solids

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materials Today 2025年 86卷 42-51页

作者： Biswas, Abhijit Serles, Peter Alvarez, Gustavo A. Schimpf, Jesse Hache, Michel Kong, Jonathan Demingos, Pedro Guerra Yuan, Bo Pieshkov, Tymofii S. Li, Chenxi Puthirath, Anand B. Gao, Bin Gray, Tia Zhang, Xiang Murukeshan, Jishnu Vajtai, Robert Dai, Pengcheng Singh, Chandra Veer Howe, Jane Zou, Yu Martin, Lane W. Clancy, James Patrick Tian, Zhiting Filleter, Tobin Ajayan, Pulickel M. Department of Materials Science and Nanoengineering Rice University HoustonTX77005 United States Department of Mechanical & Industrial Engineering University of Toronto 5 King's College Road TorontoM5S 3G8 Canada Sibley School of Mechanical and Aerospace Engineering Cornell University IthacaNY14853 United States Department of Materials Science and Engineering University of California Berkeley94720 United States Department of Materials Science and Engineering University of Toronto 184 College St TorontoM5S 3E4 Canada Department of Physics and Astronomy McMaster University HamiltonL8S 4M1 Canada Applied Physics Graduate Program Smalley-Curl Institute Rice University HoustonTX77005 United States Department of Physics and Astronomy Rice University HoustonTX77005 United States Materials Sciences Division Lawrence Berkeley National Laboratory Berkeley94720 United States

Hexagonal boron nitride (h-BN) is a brittle ceramic with a layered structure, however, recent experiments have suggested that inter-layer structural engineering could be key to new structural and functional properties. Here we report the scalable bulk synthesis of high-density crystalline h-BN solids, by using high-temperature spark plasma sintering (SPS) of h-BN powders, which show high values of mechanical strength, ductility, dielectric constant, thermal conductivity, and exceptional neutron radiation shielding capability. Through exhaustive characterizations we reveal that SPS induces non-basal plane crystallinity, twisting of layers, and facilitates inter-grain fusion with a high degree of in-plane alignment across macroscale dimensions, resulting in near-theoretical density and improved properties. Our findings highlight the importance of material design, via new approaches such as layer twisting and interlayer interconnections, to create novel ceramics with properties that could go beyond their intrinsic limits. © 2025

关键词： Ductility

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Evidence of electronic structural change at the metal-insulator transition in the perovskite NaOsO3

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Physical Review B 2023年第19期108卷 195115-195115页

作者： J.-S. Zhou X.-Y. Li M. D. Johannes Materials Science and Engineering Program Mechanical Engineering University of Texas at Austin Austin Texas 78712 USA Center for Computational Materials Science Naval Research Laboratory Washington D.C. 20375 USA

NaOsO3 exhibits an unusual metal-insulator transition (MIT) that has been touted as Slater type, though there are observations that do not entirely conform to this typing. Consistent with a Slater transition, the cell volume and crystal symmetry show no change on cooling through the transition, but both a and b axes in this Pbnm orthorhombic perovskite show a clear kink, and the splitting between them enlarges slightly. Since atomic positions, determined by fitting the intensity of state-of-the-art neutron diffraction data, exhibit no anomalies within the measurement uncertainty, the origin of the a−b splitting and the kink in the data have not yet been elucidated. Understanding the origin of these subtle structural changes across the transition temperature may provide understanding about the electronic behavior. In this paper, we connect local structural changes to changes in the lattice parameters through (1) well-established structural modeling and (2) density functional theory (DFT) calculations. This approach successfully reveals a subtle but significant change of the O-Os-O bond angle on cooling through TMIT. A Madelung energy calculation suggests that this bond angle change signals electron localization in the t2g orbital complex, and this is verified by DFT, which shows an electronic transition from itinerant to localized electronic behavior along with the bond angle shift. In this detailed structural study, we add an important though heretofore overlooked element in the microscopic picture of the MIT in NaOsO3.

关键词： Density of states Jahn-Teller effect Spin-orbit coupling Mott insulators Strongly correlated systems

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Atomistic observation of in situ fractured surfaces at a V-doped WC–Co interface

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Journal of materials science & Technology 2022年第15期110卷 103-108页

作者： Congying Xiang Min Shen Chongze Hu Lok Wing Wong Hongbo Nie Huasheng Lei Jian Luo Jiong Zhao Zhiyang Yu State Key Laboratory of Photocatalysis on Energy and Environment College of ChemistryFuzhou UniversityFuzhou 350002China Department of NanoEngineering Program of Materials Science and EngineeringUniversity of California San DiegoLa JollaCA 92093United States Department of Applied Physics Hong Kong Polytechnic UniversityHong Kong 999077China School of Materials Science and Engineering Baise UniversityBaise 533000China

*** Cemented carbides are composites of WC ceramic phases and metallic Co binders that endow them with superior hardness and excellent *** metals are widely used as metal cutting and rock drilling tools[1,2].Their hardness is believed to be inversely proportional to the sizes of WC grains^([3]).Grain growth inhibitors are widely employed to achieve smaller grain sizes.

关键词： toughness grain sizes

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High-quality Mid-infrared Chalcogenide Ring Resonator

High-quality Mid-infrared Chalcogenide Ring Resonator

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2024 Conference on Lasers and Electro-Optics, CLEO 2024

作者： Lu, Bright Xu, Bo Krueper, Greg Zohrabi, Mo Gopinath, Juliet T. Park, Wounjhang Department of Electrical Computer and Energy Engineering University of Colorado BoulderCO80309 United States Department of Physics University of Colorado BoulderCO80309 United States Materials Science and Engineering Program University of Colorado BoulderCO80309 United States

ISBN: (纸本)9781957171395

We report Ge23Sb7S70 chalcogenide ring resonators with up to 8 × 104 quality factors operating around 3.6 µm wavelength fabricated through e-beam lithography. Their rib waveguide geometry can be engineered to support close-to-zero dispersion modes needed for mid-infrared microcomb generation. CLEO 2024 © Optica Publishing Group 2024 © 2024 The Author(s)

关键词： Ring lasers

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A physics-constrained deep learning surrogate model of the runaway electron avalanche growth rate

arXiv

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arXiv 2024年

作者： Arnaud, Jonathan Mark, Tyler McDevitt, Christopher J. Nuclear Engineering Program Department of Materials Science and Engineering University of Florida GainesvilleFL32611 United States

A surrogate model of the runaway electron avalanche growth rate in a magnetic fusion plasma is developed. This is accomplished by employing a physics-informed neural network (PINN) to learn the parametric solution of the adjoint to the relativistic Fokker-Planck equation. The resulting PINN is able to evaluate the runaway probability function across a broad range of parameters in the absence of any synthetic or experimental data. This surrogate of the adjoint relativistic Fokker-Planck equation is then used to infer the avalanche growth rate as a function of the electric field, synchrotron radiation and effective charge. Predictions of the avalanche PINN are compared against first principle calculations of the avalanche growth rate with excellent agreement observed across a broad range of parameters. © 2024, CC BY.

关键词： Fokker Planck equation

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Self-Attenuating Graphene-Based Antennas Utilizing Polyvinylidene Fluoride (PVDF) Substrates

Self-Attenuating Graphene-Based Antennas Utilizing Polyvinyl...

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Microwave and Antenna Symposium (IMAS), International

作者： Josef Frankhouse Evans Addo-Mensah Uche Wejinya Department of Mechanical Engineering University of Arkansas - Fayetteville Materials Science and Engineering Graduate Program University of Arkansas - Fayetteville

ISBN: (数字)9798350356359

ISBN: (纸本)9798350356366

In this study, a Terahertz (THz) band antenna which can regulate its own resonant frequency without the requirement of manual adjustment is simulated. A polyvinylidene fluoride (PVDF) substrate is applied onto a rectangular graphene patch antenna. With a voltage potential applied onto the PVDF, the patch antenna can attenuate its frequency by physically changing the shape of the antenna, and in turn its resonant frequency. These antennas are within a 0.1 THz band between 1.32 THz to 1.22 THz measured from a radial bend of a flat surface to r = 75 μm, fitting into a return loss (S11) above -30 dB. Although the return loss did not show consistency, the resonating frequency shifted at a linear rate relative to the cylindrical bending.

关键词： Microwave antennas Patch antennas Graphene Resonant frequency Prototypes Bandwidth Bending Loss measurement Substrates Terahertz communications

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High-quality Mid-infrared Chalcogenide Ring Resonator

High-quality Mid-infrared Chalcogenide Ring Resonator

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CLEO: science and Innovations in CLEO 2024, CLEO: S and I 2024 - Part of Conference on Lasers and Electro-Optics

关键词： Infrared devices

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Density Functional Theory Study of Surface Stability and Phase Diagram of Orthorhombic CsPbI3

arXiv

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arXiv 2024年

作者： Li, Kejia Wang, Mengen Department of Electrical and Computer Engineering and Materials Science and Engineering Program SUNY BinghamtonNY13902 United States

CsPbI3 has been recognized as a promising candidate for optoelectronic device applications. To further improve the efficiency of the devices, it is imperative to better understand the surface properties of CsPbI3, which affect charge carrier transport and defect formation properties. In this study, we perform density functional theory calculations to explore the stability of the (001), (110), and (100) surfaces of orthorhombic CsPbI3, considering different stoichiometries and surface reconstructions. Our results show that, under the chemical potentials confined by the thermodynamically stable region of bulk CsPbI3, the CsI-terminated surfaces of (001) and (110) and the stoichiometric surface of (100) are stable. Among these three surfaces, the CsI-terminated (110) surface has the lowest surface energy and no mid-gap states, which benefits the transport properties of the material. © 2024, CC BY-NC-SA.

关键词： Stoichiometry

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INTER- AND INTRA-LAMINAR PROPERTIES OF AN AFP POST-PROCESSED THERMOPLASTIC COMPOSITE

INTER- AND INTRA-LAMINAR PROPERTIES OF AN AFP POST-PROCESSED...

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SAMPE 2024 Conference and Exhibition

作者： Yap, Timothy S. Heathman, Nathaniel M. Kirchhoff, Joseph G. Tehrani, Mehran Walker Department of Mechanical Engineering The University of Texas at Austin AustinTX United States Department of Structural Engineering University of California La Jolla San DiegoCA United States Program in Materials Science and Engineering University of California La Jolla San DiegoCA United States

ISBN: (纸本)9781934551455

Transitioning to high-performance thermoplastic composites (TPCs) carries great potential due to their enhanced toughness, ease of repairability, and the possibility of bypassing the need for autoclaves that are essential for curing thermosetting composites. Full consolidation of parts may be achieved in-situ using automated fiber placement (AFP) at slow rates;alternatively, with higher rates, consolidation may only occur following vacuum-bag oven processing (vacuum-bag only or VBO) or compression molding (CM) post-processing. This study investigates the CM of AFP carbon fiber LM-PAEK™ composites at a low pressure of 0.2 MPa to simulate VBO post-processing, focusing on their intra- and inter-laminar behavior. Short-beam strength, fracture toughness modes I and II, and transverse tensile and compressive samples were manufactured via AFP using a fast layup rate, followed by low-pressure CM. As compared to previous studies, post-processing resulted in greater interlaminar bonding. This study demonstrates the viability of TPCs for the next generation of aerospace structures with a relatively simple oven post-processing. © 2024 Soc. for the Advancement of Material and Process engineering. All rights reserved.

关键词： Compression molding

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