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Manipulating mechanical properties of graphene/Al composites by an in-situ synthesized hybrid reinforcement strategy

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Journal of Materials science & technology 2022年第28期123卷 13-25页

作者： Lizhuang Yang Bowen Pu Xiang Zhang Junwei Sha Chunnian He Naiqin Zhao School of Materials Science and Engineering Tianjin Key Laboratory of Composite and Functional MaterialsTianjin UniversityTianjin 300072China Joint School of National University of Singapore and Tianjin University International Campus of Tianjin UniversityBinhai New CityFuzhou 350207China Collaborative Innovation Center of Chemical Science and Engineering(Tianjin) Tianjin 300072China Key Laboratory of Advanced Ceramics and Machining Technology Ministry of EducationTianjin UniversityTianjin 300072China

The structural deterioration caused by the relatively weak out-of-plane bending stiffness and the chemically-active edge area of graphene limits its outperformance in strengthening for Al matrix composites(AMCs).Introducing one-dimensional(1D)carbon nanotubes(CNTs)to graphene/metal system is one of the promised strategies to complement the weakness of 2D graphene and make full use of the outstanding intrinsic properties of the both *** date,such synergistic strengthening and toughening mechanisms are largely *** this study,AMCs reinforced by a novel hybrid reinforcement,i.e.,graphene nanosheets decorated with Cu nanoparticles and CNTs(Cu@GNS-CNTs),are fabricated by an in-situ synthesis *** combined contrast experiments validated that the organically integrated reinforcing structure promotes the intrinsic load bearing capacity of GNS and the strain hardening capability of the Al matrix *** a result,the composites achieved excellent tensile strength and uniform elongation with almost no *** strengthening mechanism originated primarily from the hybrid reinforcement exhibits superior load-transfer,fracture inhibition and dislocation storage capability by controlling the interface reaction to construct an effective interface structure without damaging the *** work identifies a promising structural modification strategy for 2D materials and provides mechanistic insights into the synergistic strengthening effect of graphene/CNTs hybrid reinforcement.

关键词： Metal-matrix composites(MMCs) Mechanical properties Graphene Synergistic strengthening Interface

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Layered niobium carbide enabling excellent kinetics and cycling stability of Li-Mg-B-H hydrogen storage material Layered niobium carbide enabling excellent kinetics

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Rare Metals 2024年第3期43卷 1153-1166页

作者： Li-Wen Lu Hui Luo Guang-Xu Li Yun Li Xin-Hua Wang Cun-Ke Huang Zhi-QiangLan Wen-Zheng Zhou Jin Guo Mohammad Ismail Hai-Zhen Liu Guangxi Novel Battery Materials Research Center of Engineering Technology Guangxi Colleges and Universities Key Laboratory of Blue Energy and Systems IntegrationSchool of Physical Science and TechnologyGuangxi UniversityNanning530004China State Key Laboratory of Featured Metal Materials and Life-Cycle Safety for Composite Structures Nanning530004China School of Mechanical and Electrical Engineering Quzhou College of TechnologyQuzhou324000China Department of Materials Science and Engineering Zhejiang UniversityHangzhou310027China Faculty of Ocean Engineering Technology and Informatics Universiti Malaysia Terengganu21030Kuala NerusTerengganuMalaysia Key Laboratory of Advanced Energy Materials Chemistry(Ministry of Education) Nankai UniversityTianjin300071China

The Li-Mg-B-H composite(2LiBH_(4)+MgH_(2))has a high capacity of 11.4 wt%as a hydrogen storage ***,the slow kinetics and poor cycling stability severely restrict its practical *** this work,a layered Nb_(2)C MXene was first synthesized and then introduced to tailor the kinetics and cycling stability of the Li-Mg-B-H *** milled 2LiH+MgB_(2)composites were initially hydrogenated to obtain the 2LiBH_(4)+MgH_(2)*** 2LiBH_(4)+MgH_(2)+5wt%Nb_(2)C can release 9.0 wt%H_(2)in 30 min at 400℃,while it is only 2.7 wt%for the undoped 2LiBH_(4)+MgH_(2).The dehydrogenation activation energies of MgH_(2)and LiBH_(4)are 123 and 154 kJ·mol^(-1)respectively for the 5 wt%Nb_(2)C-doped composite,lower than the undoped composite(164 and 165 kJ·mol^(-1)).The 2LiBH_(4)+MgH_(2)+5 wt%Nb_(2)C possesses excellent cycling stability,with the reversible capacity only slightly reduced from 9.4 wt%for the 1st cycle to 9.3 wt%for the 20th ***_(2)C keeps stable in the composite and acts as an efficient catalyst for the Li-Mg-B-H *** is believed that both the layered structure and the active Nb element contribu te to the enhanced hydrogen storage performances of the Li-Mg-B-H *** work confirms that the Nb_(2)C MXene with layered stru cture has a significant enhancing impact on the Li-Mg-B-H hydrogen storage materials,which is different from the bulk NbC.

关键词： Hydrogen storage Lithium borohydride Magnesium hydride Nb_(2)C MXene

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Different effect of Li^(+),Na^(+),K^(+)-doping on crystal structure and electrical property of Sr_(0.6)Ba_(0.4)Nb_(2)O_(6)

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Journal of Materiomics 2024年第5期10卷 1071-1079页

作者： Jian Guo Xinrui Yang Yulong Yang Shuting Pang Shan-Tao Zhang Bin Yang National Laboratory of Solid State Microstructures College of Engineering and Applied Sciences&Jiangsu Key Laboratory of Artificial Functional Materials&Collaborative Innovation Center of Advanced MicrostructuresNanjing UniversityNanjing210023China Nanjing University(Suzhou)High-tech Institute Suzhou Industrial Park215123China School of Physics Nanjing UniversityNanjing210093China Functional Materials and Acousto-Optic Instruments Institute School of Instrumentation Science and EngineeringHarbin Institute of TechnologyHarbin150080China

Ferroelectric Sr_(0.6)Ba_(0.4)Nb_(2)O_(6)(SBN)shows typical unfilled tetragonal tungsten bronze structure where 1/6 A sites and all C sites are *** presence of such structural vacancy provides the possibility to further modulate the crystal structure and electrical *** this work,alkali ions(Li^(+),Na^(+),K^(+))doped SBN ceramics have been fabricated via solid-solution reaction *** general,each doping promotes the crystal structure evolves from unfilled toward filled tungsten ***,the different doping ion radius causes the differences in occupying initial structural vacancies,resulting in significantly different electrical properties,Li^(+)doping enhances relaxor characteristic whereas Na+and K^(+)doping lead to normal ferroelectric behavior,accompanying an increase in Curie temperature(TC)from 36℃ of SBN to 40,212,148℃ of Li^(+),Na^(+)and K^(+)doping,*** from improved relaxor degree and high density,the Li^(+)doped SBN displays a good energy storage *** the ratio of Sr/Ba and(Sr+Ba)/Nb has not been changed,this work presents direct evidence for the effect of structural vacancy on crystal structure and properties,as well as inspiration for further work on unfilled tungsten bronze.

关键词： Sr_(0.6)Ba_(0.4)Nb_(2)O_(6) oxides Structural vacant Alkali ions doping

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Stiffness and toughness of soft/stiff suture joints in biological composites

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Applied Mathematics and Mechanics(English Edition) 2022年第10期43卷 1469-1484页

作者： Dong WU Yixing HUANG Ming LEI Zeang ZHAO Xiaogang GUO Daining FANG State Key Laboratory for Turbulence and Complex Systems&Center for Applied Physics and Technology College of EngineeringPeking UniversityBeijing 100871China Beijing Key Laboratory of Lightweight Multi-functional Composite Materials and Structures Beijing Institute of TechnologyBeijing 100081China State Key Laboratory of Explosion Science and Technology Beijing Institute of TechnologyBeijing 100081China School of Astronautics Northwestern Polytechnical UniversityXi’an 710072China

Biological composites can overcome the conflict between strength and toughness to achieve unprecedented mechanical properties in engineering *** suture joint,as a kind of heterogeneous architecture widely existing in biological tissues,is crucial to connect dissimilar components and to attain a tradeoff of all-sided functional ***,the suture joints have attracted many researchers to theoretically investigate their mechanical ***,most of the previous models focus on the sutural interface between two chemically similar stiff phases with(or without)a thin adhesive layer,which are under the framework of linear elasticity and small ***,a general model based on the finite deformation framework is proposed to explore the stiffness and toughness of chemically dissimilar suture joints connecting soft and stiff *** tension tests are conducted to investigate the tensile response of the suture joints,and finite element simulations are implemented to explore the underlying mechanisms,considering both material nonlinearity and cohesive properties of the *** failure modes are quantitively captured by our *** stored elastic energy in the soft phase competes with the energy dissipation due to the interface debonding,which controls the transition among different failure *** toughness of the suture joints depends on not only the intrinsic strengths of the constituent materials and their cohesive strength,but also the interfacial *** work provides the structureproperty relationships of the soft/stiff suture joints and gives a foundational guidance of mechanical design towards high-performance bioinspired composites.

关键词： suture joint biological composite finite deformation toughness

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Dynamic stretching–electroplating metal-coated textile for a flexible and stretchable zinc–air battery

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Carbon Energy 2022年第5期4卷 867-877页

作者： Shengxiang Qu Jie Liu Xiaopeng Han Yida Deng Cheng Zhong Wenbin Hu Key Laboratory of Advanced Ceramics and Machining Technology(Ministry of Education) School of Materials Science and EngineeringTianjin UniversityTianjinChina Tianjin Key Laboratory of Composite and Functional Materials School of Materials Science and EngineeringTianjin UniversityTianjinChina Joint School of National University of Singapore and Tianjin University International Campus of Tianjin UniversityFuzhouFujianChina

A metal electrode is a significant component of a zinc–air battery(ZAB),but the metal material is usually not elastic,which severely restricts the application of flexible and stretchable ZABs in the field of wearable electronic ***,we report a flexible and stretchable metal-coated textile prepared by a dynamic stretching–electroplating based on a wavy spandex textile *** from the unique woven and wavy structure,the metal-coated textile shows a high stretchability of 100%and stable *** situ scanning electron microscope observation during stretching showed that the tensile strain of the metal-coated textile is mainly attributed to the deformation of the microfiber network at the bottom position of the wave *** addition,a sodium carboxymethyl cellulose–polyacrylic acid–potassium hydroxide composite hydrogel has been used as the *** hydrogel shows excellent ionic conductivity,mechanical properties,and water retention properties,which makes it suitable for the semi-open system of ***,a flexible and stretchable sandwich-structure ZAB,assembled using the above-mentioned electrodes and electrolyte,operates stably even under rapid stretching/releasing cycle *** of its facile preparation and low cost,this flexible and stretchable ZAB is suitable for fabrication of large-area batteries to obtain higher output current and power to drive wearable electronic devices.

关键词： dynamic stretching–electroplating hydrogel electrolyte metal-coated textile prestrain–load–recovery zinc–air battery

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Far-from-equilibrium electrosynthesis ramifies high-entropy alloy for alkaline hydrogen evolution

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Journal of Materials science & technology 2023年第35期166卷 234-240页

作者： Yunan Wang Hao Yang Zhe Zhang Xiangying Meng Tao Cheng Gaowu Qin Song Li Key Lab for Anisotropy and Texture of Materials(MoE) School of Material Science and EngineeringNortheastern UniversityShenyang 110819China Institute of Functional Nano&Soft Materials(FUNSOM) Jiangsu Key Laboratory for Carbon-Based Functional Materials&DevicesSoochow UniversitySuzhou 215123China Jiangsu Key Laboratory of Advanced Negative Carbon Technologies Soochow UniversitySuzhou 215123China Institute of Materials Intelligent Technology Liaoning Academy of MaterialsShenyang 110004China

High-entropy alloys(HEAs)provide an ideal platform for developing highly active electrocatalysts and investigating the synergy of mixed ***-from-equilibrium synthesis holds great potential for fabricating HEAs at the nanoscale by rapidly shifting the thermodynamic conditions and manipulat-ing the growth *** far-from-equilibrium synthesis of nanomaterials has been successful un-der thermochemical conditions,it is markedly challenging under electrochemical environments,as the use of an electrolyte limits the accessible temperature window and the temporal tunability of ***,we demonstrate that applying a large electrochemical overpotential would create a far-from-equilibrium condition as changing the temperature of the system by considering the equation △G=△H−T△S+nF△ψ.An electrochemical far-from-equilibrium approach is thus setup for construct-ing hierarchical and self-supporting high-entropy alloy *** large overpotential drives the simultaneous reduction of multiple cations and the subsequent formation of a single-phase *** a proof-of-concept,hierarchical Fe_(0.22)Co_(0.18)Ni_(0.18)Cr_(0.14)Cu_(0.28)was fabricated and used as an electrocatalyst for the hydrogen evolution reaction in alkaline *** noble-metal-free HEA exhibits an overpoten-tial of 84 mV at a current density of 10 mA cm^(-2),which is among the lowest even compared to noble metal-based *** work opens a new avenue for building a variety of HEAs for energy and catalysis applications.

关键词： High-entropy alloys Nanostructures Electrocatalysis Hydrogen evolution reaction Far-from-equilibrium synthesis

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Solar-powered miniature robot for on-site oil spill treatment under magnetic steering

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science China(Technological sciences) 2024年第7期67卷 2164-2175页

作者： WANG Ben CHEN YunRui WANG Yun JI FengTong LI HongYuan NIU ShiChao HAN ZhiWu ZHANG YaBin GUO ZhiGuang College of Chemistry and Environmental Engineering Shenzhen UniversityShenzhen 518060China State Key Laboratory of Featured Metal Materials and Life-cycle Safety for Composite Structures Ministry of Education Key Laboratory of New Processing Technology for Nonferrous Metals and Materialsand School of ResourcesEnvironment and MaterialsGuangxi UniversityNanning 530004China Key Laboratory for Bionic Engineering Ministry of Education Jilin UniversityChangchun 130022China Hubei Collaborative Innovation Centre for Advanced Organic Chemical Materials Ministry of Education Key Laboratory for the Green Preparation and Application of Functional MaterialsHubei UniversityWuhan 430062China Wellcome Trust/Cancer Research UK Gurdon Institute University of CambridgeCambridge CB21QNUK Department of Physiology Development and NeuroscienceUniversity of CambridgeCambridge CB21QNUK State Key Laboratory for Turbulence and Complex Systems Department of Mechanics and Engineering ScienceBeijing Innovation Center for Engineering Science and Advanced TechnologyCollege of EngineeringPeking UniversityBeijing 100871China

Walking on the water surface is an effective method for miniature robots to transport payloads with dramatically decreased interfacial drag. Current aquatic robots reported are generally actuated by a beam of focused light that can trigger asymmetrical deformation, enabling the directional movement through horizontal momentum transfer of photoinduced actuation force to the water. However, the operations are heavily dependent on manual manipulation of the focused light, making the long-term actuation and application of the aquatic robots in vast scenarios challenging. Herein, we developed a kind of water striderinspired robot that can autonomously manage the motion on the water surface under solar irradiation, with their direction steerable by a magnetic field. The motion of this bioinspired robot on the water surface was achieved by the use of a solar cell panel as a driving module to enable propulsive motion based on the conversion of light-electric-mechanical energies. The superhydrophobic design of its leg surfaces enables the aquatic robots with weight-bearing and drag-reducing abilities. With the assistance of magnetic navigation, the bioinspired robot can continuously and controllably locomote to the oily spill floating on the water body and collect them with high efficiency. For further demonstration, the treatment of oil spills in a campus pool with high efficiency has also been achieved. This on-site oil-spill treating strategy, taking advantage of a home-made bioinspired robot actuated by natural sunlight under magnetic steering, shows great potential applications in water-body remediation.

关键词： miniature robot superhydrophobic water strider interfacial friction magnetic actuation

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基于在位力热同步实验装置的动态断裂起裂机理研究

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Acta Mechanica Sinica 2023年第8期39卷 1-8页

作者：刘伟李隆康杨恒陈满喜伊凯齐伟朱盛鑫曾庆磊陈浩森 School of Mechanics and Civil Engineering China University of Mining and Technology (Beijing) Beijing 100083 China Institute of Advanced Structure Technology Beijing Key Laboratory of Lightweight Multi-functional Composite Materials and Structures Beijing Institute of Technology Beijing 100081 China

作为一种典型的失效行为,动态断裂对于材料安全评估和设计至关重要,而动态断裂的瞬时性给实验表征裂纹尖端局部温度场演化带来了巨大挑战.研究人员指出温度对断裂韧性有显著影响,但在动态断裂起裂过程中,温度升高和裂纹尖端区域热软化... 详细信息

作为一种典型的失效行为,动态断裂对于材料安全评估和设计至关重要,而动态断裂的瞬时性给实验表征裂纹尖端局部温度场演化带来了巨大挑战.研究人员指出温度对断裂韧性有显著影响,但在动态断裂起裂过程中,温度升高和裂纹尖端区域热软化效应的作用仍需阐明.本工作旨在评估温升效应对TC4(Ti-6Al-4V)合金受冲击动态断裂起裂的影响.我们开发了一种力/热耦合在位测试装置,获得了高时间/空间分辨率的动态I型断裂的同步COD(裂纹尖端张开位移)和温度场演化过程,并进行了相应的模拟,分析了动态断裂起裂时的热软化效应的作用.对于TC4合金,起裂时刻测得的最高温度约为130,热效应对材料性能的影响较小.本工作的结果为研究金属的力/热耦合断裂行为提供了数据支持.

关键词：热软化效应 TC4合金裂纹尖端张开位移动态断裂温升效应热耦合断裂韧性失效行为

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Fluorine Substitution Effect on the Material Properties in Transparent Aromatic Polyimides

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Chinese Journal of Polymer science 2022年第7期40卷 781-788页

作者： Wei-Feng Peng Huan-Yu Lei Xin-Xin Zhang Lu-Hao Qiu Ming-Jun Huang South China Advanced Institute for Soft Matter Science and Technology School of Emergent Soft MatterSouth China University of TechnologyGuangzhou510640China Guangdong Provincial Key Laboratory of Functional and Intelligent Hybrid Materials and Devices South China University of TechnologyGuangzhou510640China

The recent development of flexible display technology raised additional requirements for optical and electric properties of polyimides,accelerating the structure and property tunning of transparent *** unique electronic effect and steric hindrance effect of fluorine substitutions make fluorine-containing polyimides occupy an important position in the transparent polyimide *** this work,a series of transparent aromatic polyimides were prepared from a fixed 4,4’-(hexafluoroisopropylidene)diphthalic anhydride(6FDA)and biphenyl diamines with different substitute groups at the 2,2’,6,6’-*** systematically studied the effects of pendant groups on the thermal,mechanical,optical and dielectric properties of these 6FDA-based polyimides with the aid of density function theory(DFT)*** particular,we paid special attention to the simple but compact fluoro group *** simple fluoro substitution brought the advantages of maintaining the linearity of the backbone and dense polymer chain packing,which would minimize the weakening of polyimides’inherent thermal,dimensional and mechanical *** with trifluoromethyl substituted polyimides with the best optical transparency,polyimides containing fluoro substitutes exhibited slightly decreased optical transparency,but increased thermal and dimensional stability and higher mechanical *** results could shed light on the ultimate transparent polyimide film development toward the application in extreme working condition,e.g.,the colorless polyimide substrate film for the flexible display technology.

关键词： Polyimides Fluorine substitution Transparent Dielectric Colorless

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Recent Progresses in Liquid-Free Soft Ionic Conductive Elastomers

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Chinese Journal of Chemistry 2023年第7期41卷 835-860页

作者： Chuan Luo Zhenkai Huang Zi-Hao Guo Kan Yue South China Advanced Institute for Soft Matter Science and Technology School of Emergent Soft MatterSouth China University of TechnologyGuangzhouGuangdong510640 China School of Materials Science and Hydrogen Energy Foshan UniversityFoshanGuangdong528000 China Guangdong Provincial Key Laboratory of Functional and Intelligent Hybrid Materials and Devices South China University of TechnologyGuangzhouGuangdong510640 China

Comprehensive Summary With the rapid growth of soft electronic and ionotronic devices such as artificial tissues,soft luminescent devices,soft robotics,and human-machine interfaces,there is a demanding need to accelerate the development of soft ionic conductive *** date,the first-generation ionotronic devices are mainly based on hydrogels or ***,due to their intrinsic drawbacks,such as freezing or volatilization at extreme temperatures,and the leakage problem under external mechanical forces,the reliability of ionotronic devices under harsh conditions remains a great *** advent of liquid-free ionic conductive elastomers(ICEs)has the potentials to solve the issues related to the gel-type soft conductive *** free ions shuttling within the ion-dissolvable polymer network enable liquid-free ICEs to exhibit unparalleled ionic conductivity and ***,by tuning the composition and structure of the polymeric network,it is also feasible to integrate other desirable properties,such as self-healing ability,transparency,biocompatibility,and stimulus responsiveness,into liquid-free ICE *** this review,we summarize the design strategies of recently reported liquid-free ICEs,and further explore the methods to introduce multifunctionality,which originate from the rational molecular design and/or the synergy with other ***,we highlight the representative applications of liquid-free ICEs in soft *** is believed that liquid-free ICEs might provide a unique material platform for the next-generation ionotronics.

关键词： Liquid-free Elastomer lonic conductorSoft materials lonotronics

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