The B4C-ZrB2-SiC ternary composites with super hard and high toughness were obtained by arc melting in argon atmosphere. Microstructures were observed by SEM, and phase compositions were analyzed by XRD. The hardness ...
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The B4C-ZrB2-SiC ternary composites with super hard and high toughness were obtained by arc melting in argon atmosphere. Microstructures were observed by SEM, and phase compositions were analyzed by XRD. The hardness and fracture toughness of ternary composites are 28GPa and 4.5MPa-m1/2. The eutectic mole composition is 0.39B4C-0.25ZrB2-0.36SiC, and the eutectic lamellar microstructure is composed of B4C matrix with the lamellar ZrB2 and SiC grains.
Using steel slag and charcoal as raw materials, the steel slag/charcoal nano-/micro-composites with magnetic-resistance mixed loss mode were fabricated by a high-performance milling process, and then the composition, ...
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Using steel slag and charcoal as raw materials, the steel slag/charcoal nano-/micro-composites with magnetic-resistance mixed loss mode were fabricated by a high-performance milling process, and then the composition, phase structure, morphology, and electromagnetic (EM) characteristics of the products were characterized by XRD, EDS, SEM, and vector network analyzer, respectively. The results showed that EM characteristics of the products were strongly dependent on the content of the charcoal (WCharcoal). The real and imaginary parts of the permittivity of the steel slag/charcoal nano-/micro-composites significantly increased with the increasing WCharcoal. Among them, the steel slag/charcoal composites with WCharcoal=50wt% exhibited the best EM-wave absorption performance, with a maximum reflectivity value of -33.4dB, the effective bandwidth 15.2GHz(<-10dB) and 8.6 GHz (<-20 dB), respectively, which is a consequence of enhanced dielectric loss and a proper EM matching.
Based on a facile glucose-guided hydrolyzing-heat-treating approach, urchin-like α-Fe2O3 nanomaterials with controllable morphology and crystallinity were prepared via adjusting the heat-treating temperature, and the...
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Based on a facile glucose-guided hydrolyzing-heat-treating approach, urchin-like α-Fe2O3 nanomaterials with controllable morphology and crystallinity were prepared via adjusting the heat-treating temperature, and their electrochemical performances were investigated. The results showed that changing the heat-treating temperature can effectively control the structure and electrochemical property of the as-made products. The urchin-like α-Fe2O3 nanomaterials obtained by heat-treating at 300°C, composed of a mass of the shuttle fibrous brunches, had higher initial discharge capacity(1475 mAhg-1) than those consisting of nanorods formed at 700°C. The above difference is ascribed to the urchin-like samples obtained at the relatively low heat-treating temperature, which, with low crystallinity, large SBET, and well-regulated porous, is helpful to the adsorption of electrolyte and the transport of lithium ion, resulting in the high activity and discharge-charge capacity.
作者：
Kaijie LinGuangze TangYujiang WangXinxin MaKen YukimuraSchool of Materials Science and Engineering
Harbin Institute of TechnologyHarbin 150001China National Key Laboratory of Science and Technology on Precision Hot Processing of MetalsHarbin Institute of TechnologyHarbin 150001China National Key Laboratory for RemanufacturingAcademy of Armored Forces EngineeringBeijing 100072China State Key Lab of Advanced Welding Production TechnologyHarbin Institute of TechnologyHarbin 150001China
Effect of stacking layers on the structure and properties of Ca(Mg 1/3Nb2/3)O3/CaTiO3 (CMN/CT) microwave dielectric heterogeneous thin films prepared was investigated. Precursor solutions for CMN and CT synthesis were...
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The Fe2O3 nanoparticles activated V2O5 nanotubes were achieved via a hydrolysis method. The TEM and SEM images of the nanotubes indicated that the Fe2O3 nanoparticles with the particle size of about 15 nm were dispers...
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Lead free textured K_(0.5)Na_(0.5)NbO_(3) piezoelectric ceramics have been prepared by reactive-templated grain growth method by using NaNbO_(3) with different morphologies as templates. The NaNbO_(3) template particl...
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ISBN:
(纸本)9781457711626
Lead free textured K_(0.5)Na_(0.5)NbO_(3) piezoelectric ceramics have been prepared by reactive-templated grain growth method by using NaNbO_(3) with different morphologies as templates. The NaNbO_(3) template particles with different edge length (10-20 (mu)m) and thickness (0.5-2.5 (mu)m) was synthesized through controlling Bi_(1.5)Na_(x-1.5)Nb_(x)O_(3x+3) precursor's layer numbers x from 2 to 6 by two-step molten salt methods. The crystalline phases and microstructure of textured K_(0.5)Na_(0.5)NbO_(3) were characterized by X-ray diffraction and scanning electron microscopy, respectively. It shows that all the K_(0.5)Na_(0.5)NbO_(3) ceramics are orthorhombic perovskite structure with {001} orientation. By using the template particles with a ratio of edge length to thickness (l/h)(velence)approx10, the textured ceramics with optimized piezoelectric properties was prepared. The results indicate that the enhanced properties of textured ceramics are concerned with the template morphology.
A novel way was used to prepare dense B4C ceramics at a lower temperature by reactive sintering from carbon and boron elemental powders. Spark Plasma Sintering (SPS) technique, a rapid and non-conventional powder cons...
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ISBN:
(纸本)9780470927151
A novel way was used to prepare dense B4C ceramics at a lower temperature by reactive sintering from carbon and boron elemental powders. Spark Plasma Sintering (SPS) technique, a rapid and non-conventional powder consolidation method, was employed. The densification, microstructure and mechanical property of the as-prepared B4C ceramics were investigated. The reactive sintering process could be divided into two stages, corresponding to synthesis (1300∼1700°C) and densification (1700∼1900°C), respectively. At those stages, boron first reacted with carbon to form B4C, and then the in-situ densification of the as-synthesized B4C occurred and was enhanced by increasing sintering temperature. B4C ceramics with grain size of several hundred nanometers and high densification (98%) were obtained at 1800°C, a lower sintering temperature as compared with general hot press. Due to the high densification and purity as well as fine texture, the SPS-sintered B4C ceramics had high Vickers hardness (48.8GPa), Young's modulus (264.5GPa), fracture toughness (3.9MPa·m1/2) and flexure strength (450MPa).
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