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Preparation of High Performance Grccn Alumina Ceramic Balls by Roller Production Waste

Journal of Wuhan University of technology(materials Science) 2008年第1期23卷 134-138页

作者：钟莲云吴伯麟 ZHANG Lianmeng ZHANG Guifang State Key Lab of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Wuhan 430070 China Key Lab of Nonferrous Materials and New Processing Technology （ Guangxi University Guilin University of Technology ） of Ministry of Education Guilin 541004 China School of Chemistry and Ecological Engineering Guangxi University for Nationalities Nanning 530006 China

To reuse roller waste as a raw material of high performance green ceramic balls, three kinds of white alumina ceramic balls whose wear resistance were 2-3 times of the best high alumina ceramic ball with 90% Al2O3 were prepared, and the Al2O3 content of the prepared balls was 75%. It is found that the effect of calcia and magnesia on the wear resistance of ceramic balls is contrast to the accepted one： the wear rate of the ceramic balls prepared in CaO-Al2O3-SiO2 system is the lowest and the wear rate of the ceramic balls prepared in MgO-Al2O3-SiO2 is the highest. The main crystal phase of the ceramic ball is mullite and corundum. The ceramic ball granular is uniform and fine with 4-5 μm average size. The pore diameter is about 2 μm. The wear way of the ceramic balls is mainly transcrystalline fracture.

关键词： roller production waste alumina ceramic ball wear resistance white transcrystalline fracture

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Enhanced photoelectrocatalytic performance of SnO2/TiO 2 rutile composite films

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Journal of materials Chemistry C 2013年第36期1卷 10727-10735页

作者： Yu, Jiaguo Wang, Ying Xiao, Wei State Key Laboratory of Advanced Technology for Material Synthesis and Processing Wuhan University of Technology Wuhan 430070 China Department of Environmental Engineering School of Resource and Environmental Sciences Wuhan University Wuhan 430072 China

Ordered rutile TiO2 nanorods grown on transparent electro-conductive F-doped SnO2-coated (FTO) glass substrates were prepared by a simple hydrothermal method using tetrabutyl titanate as the precursor and then calcined at various temperatures. The prepared SnO 2/TiO2 composite film samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and X-ray photoelectron spectroscopy (XPS). The photoelectrocatalytic (PEC) activity was evaluated by PEC degradation of methylene blue (MB) aqueous solutions under UV-LED light irradiation. The results showed that rutile TiO2 nanorods with diameters of ca. 300-700 nm and lengths of ca. 5 μm vertically grew on the FTO substrate. The resulting rutile TiO2 arrays exhibited excellent stability upon annealing in a temperature range of 300-500 °C. The sample calcined at 400 °C exhibited the highest PEC activity due to the combined effects of several factors including its one-dimensional morphology, high crystallinity, close contact between the TiO2 nanorods and SnO2 layers, SnO2/TiO2 n-n heterojunction and the applied external electrostatic field. The proposed enhanced PEC mechanism was further confirmed by the transient photocurrent response and electrochemical impedance spectroscopy (EIS) experiments. © 2013 The Royal Society of Chemistry.

关键词： Titanium dioxide

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Fabrication and dielectric properties of Si3N 4-MgO-Al2O3 by spark plasma sintering technique

Materials Science

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materials Science 2007年第3期25卷 699-707页

作者： Li, J. Chen, F. Shen, Q. Jiang, H. Zhang, L. State Key Lab of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Wuhan 430070 China School of Chemical Engineering Shandong University of Technology Zibo 255049 China

In the present study, α-Si3N4 was prepared using MgO and Al2O3 as the sintering additives and spark plasma sintering (SPS) technique. The SPS sintering behaviour and mechanism have been discussed. The relationship between the content of sintering additives, sintering temperature, and relative densities of the samples have been analyzed. The phase composition was determined by XRD, the microstructures of the fracture surfaces were observed by SEM and the dielectric properties have been tested. The results suggest that when the sintering temperature is 1300-1500 °C, the content of sintering additives - 6-10%, the relative density of the sintered samples is 64-96%. When the sintering temperature reaches 1400 °C, the content of sintering additives 10%, the samples could be fully dense sintered (the relative density up to 95%) The sintering mechanism is liquid phase sintering. The electric permittivity of the sintered samples is 5-8 being in a close relationship with the relative density. The dielectric loss, influenced by the liquid phase, is less than 1 × 10-2.

关键词： Silicon compounds

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Erratum to:Efficient flexible perovskite solar cells and modules using a stable SnO_(2)-nanocrystal isopropanol dispersion

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Nano Research 2024年第5期17卷 4641-4642页

作者： Zhiwei Su Jing Li Ruixuan Jiang Shujie Zhang Chengkai Jin Feng Ye Bingcan Ke Mengjun Zhou Jinhui Tong Hyesung Park Fuzhi Huang Yi-Bing Cheng Tongle Bu State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of TechnologyWuhan 430070China School of Material Science and Engineering Wuhan University of TechnologyWuhan 430070China Department of Materials Science and Engineering Graduate School of Semiconductor Materials and Devices EngineeringGraduate School of Carbon NerutralityLow Dimensional Carbon Materials CenterUlsan National Institute of Science and TechnologyUlsan 44919Republic of Korea Xianhu Laboratory of the Advanced Energy Science and Technology Guangdong Laboratry Foshan 528200China

Erratum to Nano Research,2024,17(4):2704-2711 https://***/10.1007/s12274-023-6115-y(1)In the article,the table of contents(TOC)image was unfortunately mispresented.

关键词： perovskite dispersion modules

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Preparation of room-temperature ferromagnetic Fe-doped In2O3 films by sol-gel method

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Wuhan Ligong Daxue Xuebao/Journal of Wuhan University of technology 2008年第9期30卷 13-15页

作者： Gao, Hong Chen, Yan-Bing Sun, Zhi-Gang State Key Laboratory of Advanced Technology on Material Synthesis and Processing Wuhan University of Technology Wuhan 430070 China

Transparent Fe-doped In2O3 thin film was prepared by sol-gel method on (general) glass substrate. The structure, morphologies, transmission and magnetic properties of the sample have been characterized by X-ray diffraction, field emission scanning electron microscopy, UV-Vis spectroscopy and vibrating sample magnetometer. XRD result indicated that the sample was single cubic In2O3 phase. FE-SEM clearly showed that the film was homogenous and composed of refining grain with an average size of 14 nm. UV-Vis spectrum indicated that the transmittance of the film was higher than 80% in the visible light, and the Fe-doped In2O3 film arose the optical absorption spectrum red shift. VSM demonstrated the sample was (room temperature ferromagnetic.

关键词： Fe-doped In2O3 Room-temperature ferromagnetism Sol-gel method Transparent thin film

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Fine-structured TiO2 ceramic patterns on the ceramic surface fabricated by replication

Fine-structured TiO2 ceramic patterns on the ceramic surface...

引用

International Symposium on Multifunctional Ceramic materials Based on Nanotechnology, ISMCN 2010

作者： Kim, H.D. Nakayama, T. Hong, B.J. Imaki, K. Yoshimura, T. Suzuki, T. Suematsu, H. Lee, S.W. Fu, Z. Niihara, K. Extreme Energy-Density Research Institute Nagaoka University of Technology 1603-1 Kamitomioka Nagaoka 940-2188 Japan Department of Physics and Electronics Graduate School of Engineering Osaka Prefecture University 1-1 Gakuencho Nakaku Sakai 599-8531 Japan Department of Environmental Engineering Sun Moon University Chungnam 336-708 Korea Republic of State Key Lab. of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Wuhan 430070 China

The ability to fabricate high precision micro- to nanoscale structure in a wide variety of materials is of crucial importance for the advancement of microtechnology, nanotechnology and nanoscience. Also, the ability to create micrometer and sub-micrometer architecture for functional ceramics is a prerequisite of exploring the rich field of ceramic nanotechnology. In this work we fabricated three-dimensional oxide ceramic materials with fine-structure over multiple length scales by combining replication patterning technique, polyvinyl alcohol (PVA), oxide ceramic material (TiO2) nano-sized particles. Our study is based on the idea that PVA can be easily detached from a mold by peeling. We confirmed that micron and sub-micron-sized fine-structured oxide ceramic patterns containing nano-sized pores could be fabricated using this procedure. The results presented demonstrate the compositional and structural diversities that are possible with a facile approach and simple method.

关键词： Ceramic materials

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Influence of sintering on quality factor of Ba(Mg/13Nb/23)O3 ceramic

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Wuhan Ligong Daxue Xuebao/Journal of Wuhan University of technology 2005年第6期27卷 5-7+14页

作者： Tian, Zhong-Qing Liu, Han-Xing Wang, Hao Yu, Hong-Tao School of Materials Science and Engineering Chongqing Institute of Technology Chongqing 400050 China State Key Lab of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Wuhan 430070 China School of Materials Science and Engineering Wuhan University of Technology Wuhan 430070 China

The influences of sintering temperature, soaking time and annealing time on the quality factor of Ba(Mg/13Nb2/3)O3 microwave dielectric ceramic were investigated. The result showed that Qf value increased as the sintering temperature increasing. It was ascribed to the increasing of the relative density and ordering parameter S. The maximum value of Qf, 49500 GHz, was gained at 1550°C. With soaking time increasing, Qf value increased. The increasing of B-site 1:2 ordering degree and grain size should be responsible for the improvement of Qf value. When soaking time was 16 h, Qf value reached 58000 GHz. Annealing time had great effect on Qf value. With annealing time increasing, Qf value increased quickly. This was because of the improvement of B-site 1:2 ordering caused by annealing. A high Qf value, 71500 GHz, was acquired when annealing time was 48 h.

关键词： Ba(Mg/13Nb/23)O3 Microwave dielectric ceramic Quality factor

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Methyl Halide to Olefins and Gasoline over Zeolites and SAPO Catalysts：A New Route of MTO and MTG

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催化学报 2012年第1期33卷 11-21页

作者： WEI Yingxu ZHANG Dazhi LIU Zhongmin SU Bao-Lian Dalian National Laboratory for Clean Energy National Engineering Laboratory for Methanol-to-OlefinsDalian Institute of Chemical PhysicsChinese Academy of SciencesDalian 0LiaoningChina Laboratory of Inorganic Materials Chemistry(CMI) University of Namur(FUNDP)61rue de BruxellesB-5000NamurBelgium State Key Laboratory of Advanced Technology for Material Synthesis and Processing Wuhan University of TechnologyWuhan 430070HubeiChina

到更有用的更高的烃的甲烷的合理、有效的变换是天然气利用的最重要的话题之一。尽管到珍贵混合物的甲烷激活和它的变换吸引增加的注意，甲烷变换经常为 syngas 通过消费精力的步以间接方法被做从甲烷改过的蒸气的生产。一些有希望的结... 详细信息

到更有用的更高的烃的甲烷的合理、有效的变换是天然气利用的最重要的话题之一。尽管到珍贵混合物的甲烷激活和它的变换吸引增加的注意，甲烷变换经常为 syngas 通过消费精力的步以间接方法被做从甲烷改过的蒸气的生产。一些有希望的结果看起来为从甲烷的高增值产品的生产具有为一种选择和潜在的线路的发展的意义。到更高的烃的甲烷的有效变换能作为中介经由甲基卤化物被认识到。在 halomethane 的生产以后，他们能在修改沸石和 SAPO 上被转变到汽油和轻石蜡分子的筛。高变换效率和选择显示了工业申请的可行性。研究在基本研究和工业申请从观点获得了最近成长的兴趣。反应机制上的学习从甲基卤化物使 CC 契约建设的可能的线路清楚些，它是到更高的烃的 C1 反应物变换的重要问题。氢卤化物产生没在反应机制和催化剂的结构稳定性上在甲基卤化物变换期间施加明显的影响。这评论处理这个领域和注释的进化要探索的优点和缺点经由甲基卤化物发送为新、持续的 methane-to-olefins (MTO ) 和 methane-to-gasoline (MTG ) 的开发被阻止。

关键词： methyl halides hydrocarbons zeolite SAPO-34 reaction mechanism

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Thermoelectric properties of p-type rare-earth element cerium-filled skutterudite CeyFexCo4-xSb12

Pan Tao Ti Hsueh Pao/Chinese Journal of Semiconductors

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Pan Tao Ti Hsueh Pao/Chinese Journal of Semiconductors 2006年第6期27卷 1021-1025页

作者： Wang, Kun Tang, Xinfeng Zhang, Qingjie State Key Laboratory of Advanced Technology for Material Synthesis and Processing Wuhan University of Technology Wuhan 430070 China

Cobalt-rich filled skutterudite compounds CeyFexCo4-xSb12 (y=0-0.42) are synthesized using the melting-diffusion method. The structure and thermoelectric properties of the compounds are investigated. Results indicate that the lattice constants increase linearly with the Ce filling fraction. Hall coefficient is positive. Hole concentration and electrical conductivity decreased as the Ce filling fraction increases. Seebeck coefficient increase with the Ce filling fraction. The lattice thermal conductivity reached the minimum value when the Ce filling fraction was about 0.29, indicating that the effect of Ce rattling on phonon scattering is the strongest as Sb-dodecahedron partial voids are filled by Ce. A maximum ZT value of 0.65 is obtained for Ce0.29Fe1.41Co2.59Sb12.32 at 725 K.

关键词： Thermoelectricity

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(Bi_(0.51)Na_(0.47))TiO_(3) based lead free ceramics with high energy density and efficiency

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Journal of Materiomics 2019年第3期5卷 385-393页

作者： Yu Huang Fei Li Hua Hao Fangquan Xia Hanxing Liu Shujun Zhang State Key Lab Silicate Materials for Architecture Center for Smart Materials and Device IntegrationSchool of Materials Science and EngineeringWuhan University of TechnologyWuhan430070China Electronic Materials Research Laboratory Key Lab Ministry of Education and International Center for Dielectric ResearchSchool of Electronic and Information EngineeringXi'an Jiaotong UniversityXi'an710049China School of Chemistry and Chemical Engineering University of JinanJinan250022China State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Center for Smart Materials and Device IntegrationInternational School of Materials Science and EngineeringWuhan University of TechnologyWuhan430070China Institute for Superconducting and Electronic Materials Australian Institute of Innovative MaterialsUniversity of WollongongNSW2500Australia

Dielectric ceramics with high energy storage density and energy efficiency play an important role in high power energy storage *** this work,lead free relaxor ferroelectric ceramics in (1-x) Bi_(0.51)Na_(0.47)TiO_(3-x)Ba(Zr_(0.3)Ti_(0.7))O_(3)(BNT-BZT100x:x=0.20,0.30,0.40 and 0.50)system are fabricated by conventional solid-state sintering *** BNT-BZT100x ceramics are sintered dense with minimal pores,exhibiting pseudocubic symmetry and strong relaxor characteristic.A high energy storage density of 3.1 J/cm^(3) and high energy efficiency of 91% are simultaneously achieved in BNT-BZT40 ceramic with 0.1mm in thickness,at the applied electric field of 280 kV/*** temperature stability of the energy density is studied over temperature range of 20-160℃ ,showing minimal variation below 1.5%,together with the excellent cycling reliability(the variations of both energy density and efficiency are below 3% up to 106 cycles),making BNT-BZT40 ceramic promising candidate for high-temperature dielectric and energy storage applications.

关键词： Energy storage Lead free ceramic Relaxor characteristic

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