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Liquid Phase Sintering (LPS) and Dielectric Constant of α-Silicon Nitride Ceramic

Journal of Wuhan University of technology(materials Science) 2006年第2期21卷 98-100页

作者：陈常连 State Key Lab of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Wuhan 430070 China

The spark plasma sintering （SPS） was applied to prepare α-Si3 N4 ceramics of different densities with magnesia, silicon dioxide, alumina as the sintering aids. The mechanism of liquid phase sintering （LPS） wus discussed and the factors influencing the density of the prepared samples were analyzed. The dielectric constant of sintered samples was tested. The experimental results show that the density can be controlled from 2.48 g/ cm^3 to 3.09 g/ cm^3 while the content of the sintering aids and the sintering temperature alter and the dielectric constant is closely dependent on the density of obtained samples.

关键词： liquid phase sintering （LPS） spark plasma sintering （SPS） α-silicon nitride sintering aids dielectric constant

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Preparation, Characterization and Dielectric Properties of Ba_6Mg_(0.67)Nb_(9.33)O_(30) Ceramic

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Journal of Wuhan University of technology(materials Science) 2005年第3期20卷 14-16页

作者：张辉 State Key Lab of Advanced Tech. for Mater. Synthesis and Processing Wuhan University of Technology

A new niobate Ba6Mg0.67Nb9.33O30 was ssnthesized in the BaO-MgO-Nb2O5 system by solid state reaction at 1350 ℃ for 48 b. The strncture and dielectric properties of Ba6Mg0.67Nb9.33O30 were determined by X-ray pouder diffraction, straining electron microscopy and dielectric measurements. The results show that Ba6Mg0.67Nb9.33O30 belongs to ferroelectric phase of filled tetragonal tungsten bronze structure at room temperature with unit cell parameters ： a = 1. 26052（4） nm , c = 0.40045（2） nm, space group P4bm , calculated density 5 . 707g. cm ^-3 . Ba6Mg0.67Nb9.33O30 belongs to relaxor ,ferroetectrics undergoing diffusive phase transition, and the transition temperature （ Tc ） is 30 ℃ observed at 10 kHz. At room temperature, Ba6Mg0.67Nb9.33O30 eeramic has a high dielectric constant 850 at 1 MHz and a low dielectric loss of 0. 0052.

关键词： Niobate tungsten bronze structure dielectric properties XRD retaxor ferroelectrics

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Effect of Ultrafine Grinding on Dissolving-out Quantity of Tanshinone IIA from Radix Salvia Miltiorrhiza

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Journal of Wuhan University of technology(materials Science) 2009年第6期24卷 973-976页

作者：苏艳丽傅正 College of Chemistry Chemical Engineering and Material ScienceSoochow UniversitySuzhou China State Key Laboratory of Advanced Technology for Material Synthesis and Processing Wuhan University of Technology

In order to improve the bioavailab.lity, Radix salvia miltiorrhiza raw powder mixed with distilled water （5.5wt%） was ultrafinely ground to nanosize particles using HSCS pulverizer, and the dissolving-out quantity of tanshinone IIA in the filtrate that obtained from nanoparticles suspension and raw powder marinated in water for different time was determined by HPLC. The experimental results show that raw powder can be ultrafinely ground to 133.5 nm at 1500 r/min for 50 min and the molecular structure of active ingredients doesnot change, and the dissolving-out quantity of tanshinone IIA obtained from the filtrate is increased greatly from 12.77 μg/g to 54.55 μg/g.

关键词： Radix salvia miltiorrhiza tanshinoe IIA HPLC dissolving-out quantity

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Poly(dopamine)-assisted Bioactive Coating on the Surface of Porous Poly (Ether Ether Ketone) to Promote Osteogenic Differentiation of rBMSC

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Journal of Wuhan University of technology(materials Science) 2021年第5期36卷 766-776页

作者： WANG Jin WANG Youfa WU Qingzhi State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Biomedical Material and Engineering Center of Hubei ProvinceWuhan University of TechnologyWuhan 430070China

A facile modification strategy is developed to promote the proliferation and osteogenic differentiation of rat bone marrow stromal cells(rBMSCs)through deposition of a bioactive calcium silicate(CS)coating on the porous surface of poly(ether-ether-ketone)(PEEK)with the assistance of poly(dopamine)(PDA).The porous structures are etched on the surface of PEEK after sulfonation treatment.A poly(dopamine)layer is coated on the porous surface of the sulfonated PEEK(SPEEK),which provides anchoring groups for the subsequent deposition of the CS *** show that the CS coating on the porous surface of SPEEK significantly improve the hydrophilicity and biomineralization formation of *** with PEEK,SPEEK-PDA-CS displays higher bioactivity to promote the proliferation and osteogenic differentiation of rBMSCs,including the increase of ALP activity and formation of calcium nodules,the expression of osteogenic differentiation-related *** results are beneficial to extending clinical applications of PEEK-based implants for bone tissue repair and orthopedic surgery.

关键词： poly(ether-ether-ketone) calcium silicate poly(dopamine) bioactivity osteogenic differentiation

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Three dimensional profile for the valence electronic structure across the triple pocket junction in SrTiO3 ceramic

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Journal of advanced Microscopy Research 2013年第2期8卷 128-136页

作者： Tan, Guo-Long State Key Lab of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Wuhan 430070 China

The three dimensional profile for valence electron structure across the triple pocket junction in SrTiO3 ceramic has been quantitatively determined by analysis of spatially resolved low loss electron energy-loss spectroscopy (EELS) data, which were collected from one front grain across the triple pocket junction to another backside grain by line scan technique. From the experimental data, local complex dielectric functions were determined, from which interband transition strength Jcv spectra can be locally analyzed. A three dimensional surface profile of the interband transition strength spectra across the triple pocket junction has been built up, the front view of which looks like a valley with a horse-hump shaped grooving gap across the triple pocket junction (TPJ). The dramatic change of the valence electronic structure across the triple pocket junction has been observed. The transition strength between the energy range of two major transition peaks at 28.9 eV (F ) and 47.3 eV (H) drops dramatically across the triple pocket junction, a new transition peak E at 15.3 eV appears. This new feature was corresponding to the interband transition relative to one of the splitting O 2s sub-bands of TiO2. The bulk plasmon excitation peak for SrTiO3 disappeared at the central point of the triple pocket junction, where a new plasmon resonance peak at 24.6 eV for TiO2 shows up. The disappearance of peak H at 47.4 eV and the occurrence of a new peak E suggest that TiO2 be the only component at the central point of the triple pocket junction. Copyright © 2013 American Scientific Publishers.

关键词： Perovskite

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Iron Fibers Arrays Prepared by Electrodepositing in Reverse Liquid Crystalline

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Journal of Wuhan University of technology(materials Science) 2006年第2期21卷 66-68页

作者：赵素玲官建国 State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Wuhan 430070 ChinaCenter for Material Research and Testing Wuhan University of Technology Wuhan 430070 China State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Wuhan 430070 China

Ordered iron fiber arrays were electrodeposited on the surface of zinc foils using ＂FeSO4 solution-sodium caprylate-Decanol＂ 3-component reverse hexagonal liquid crystal as soft templates. The structure of the soft templates and the synthesized iron ,fibers were characterized by polarizing microscopy, X-ray diffraction （XRD）, scanning electron microscopy （SEM） and energy dispersive X-ray microanalysis etc. The experimental results shou that the synthesized iron fibers with a crystal phase grew up in the form of fiber clusters of about 200 nm along the direction perpendicular to the cathode surface. Each cluster was composed of several tens of fibers. The fibers had almost the same length of more than 10μm with a diameter of about 50 nm.

关键词： iron fibers arrays reverse hexagonal liquid crystal soft template electrodepositing

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A Flier-plate material with Graded Impedance Used in Dynamic High-pressure Physics

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Journal of Wuhan University of technology(materials Science) 2002年第4期17卷 32-35页

作者：王传彬 State Key Lab of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Wuhan China

By using such flier-plate material,quasi-isentropic compression can be *** on it,hypervelocity launching is further *** a result,an extremely high dynamic pressure can be obtained in lab.ratory,offering a practical method for the comprehensive determination of materials behavior,response,equation-of-state and properties in dynamic loading process.

关键词： flier-plate material with graded impedance quasi-isentropic compression hypervelocity launching

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Enhanced breakdown strength of BaTiO_(3)-based multilayer ceramic capacitor by structural optimization

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Rare Metals 2023年第8期42卷 2552-2561页

作者： Qian Liu Hua Hao Qing-Hu Guo Zhong-Hui Shen Jian Wang Ming-He Cao Zhong-Hua Yao Han-Xing Liu State Key Laboratory of Advanced Technology for Materials Synthesis and Processing School of Material Science and EngineeringWuhan University of TechnologyWuhan 430070China Foshan Xianhu Laboratory of the Advanced Energy Science and Technology Guangdong Laboratory Foshan 528220China Sanya Science and Education Innovation Park of Wuhan University of Technology Sanya 572000China International School of Material Science and Engineering Wuhan University of TechnologyWuhan 430070China State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Center of Smart Materials and DevicesWuhan University of TechnologyWuhan 430070China State Key Laboratory of Advanced Technology for Materials Synthesis and Processing International School of Material Science and EngineeringWuhan University of TechnologyWuhan 430070China

0.5 wt%Nb_(2)O_(5)doped 0.12BiAlO_(3)-0.88BaTiO_(3)(12BA5N)multilayer ceramic capacitor(MLCC-1)was prepared,which satisfied EIA X7R specification(where X is the minimum temperature,R is the percentage of capacitance variation limit)at 1 *** distribution of internal electric field under breakdown voltage was simulated by finite element method(FEM),indicating that the electric field strength increased significantly at the terminal of internal *** areas may become the headstream of breakdown for MLCC-1 due to the shape *** order to improve the breakdown performance of MLCC-1,it was optimized by 12BA5N+2G green sheets(prepared by 12BA5N ceramic powder with 2 wt%B-Al-Si glass additive),then MLCC-2 was obtained which satisfied EIA X8R *** BDS rose from 20 to29.4 kV·mm^(-1),and the electric field distribution of dielectric layer was also analyzed by ***,it was also found that the grain size and the dielectric constants of"core"and"shell"parts for the 12BA5N+2G dielectric layer both contributed to the enhanced BDS of MLCC-2according to the simulation results from FEM.

关键词： Multilayer ceramic capacitor(MLCC) Breakdown strength(BDS) Simulation Grain size Dielectric constant

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Preparation of Nano-sized Zirconium Carbide Powders through a Novel Active Dilution Self-propagating High Temperature synthesis Method

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Journal of Wuhan University of technology(materials Science) 2015年第4期30卷 729-734页

作者：达奥运龙飞 WANG Jilin XING Weihong WANG Yang ZHANG Fan 王为民 FU Zhengyi State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Key Lab of New Processing Technology for Nonferrous Metals & Materials Ministry of Education China Guilin University of Technology

High quality nano-sized zirconium carbide （ZrC） powders were successfully fabricated via a developed chemical active dilution self-propagating high-temperature synthesis （SHS） method assisted by ball milling pretreatment process using traditional cheap zirconium dioxide powder （ZrO2）, magnesium powder （Mg） and sucrose （C12H22Oll） as raw materials. FSEM, TEM, HRTEM, SAED, XRD, FTIR and Raman, ICP- AES, laser particle size analyzer, oxygen and nitrogen analyzer, carbon/sulfur determinator and TG-DSC were employed for the characterization of the morphology, structure, chemical composition and thermal stability of the as-synthesized ZrC samples. The as-synthesized samples demonstrated high purity, low oxygen content and evenly distributed ZrC nano-powders with an average particle size of 50nm. In addition, the effects of endothermic rate and the possible chemical reaction mechanism were also discussed.

关键词： zirconium carbide ZrC self-propagating high-temperature synthesis active dilution nano-powders ball milling

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In-situ Preparation of TiB_2-TiB-Ti Functionally Graded materials by Improved Sintering Process

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Journal of Wuhan University of technology(materials Science) 2015年第4期30卷 710-714页

作者：刘国玺 LI Kezhi ZHANG Jinyong 张帆 School of Materials Science Northwestern Polytechinical University Ningbo Branch of Ordnance Science Institute of China State Key Lab of Advanced Technology for Material Synthesis and Processing Wuhan University of Technology

An improved multi-step sintering process was used to in-situ prepare TiB2-TiB-Ti FGMs. According to the sintering temperatures, the functionally graded materials （FGMs） were divided into three sections. After sintering at a proper temperature, the three sections were sintered together in turn. The experimental results showed that there were no obvious pores and cracks in the whole TiB2-TiB-Ti FGMs, and no delamination was found in the impacting test with good performance features, which indicated that there were no interface effects in FGMs during penetration, so that the TiB2-TiB-Ti FGMs were an ideal FGM.

关键词： FGMs TiB2 Ti Fabrication

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