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3D Ordered Macroporous: A Novel 3DOM TiO2Based Multifunctional Photocatalytic and Catalytic Platform for Energy Regeneration and Pollutants Degradation (Adv. Mater. Interfaces 4/2021)

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advanced materials Interfaces 2021年第4期8卷

作者： Yang Ding Lina Huang Tarek Barakat Bao-Lian Su Laboratory of Inorganic Materials Chemistry (CMI) University of Namur 61 rue de Bruxelles Namur B5000 Belgium Guangdong Provincial Key Laboratory of Durability for Marine Civil Engineering Shenzhen Durability Center for Civil Engineering College of Civil Engineering Shenzhen University Shenzhen Guangdong 518060 China State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology 122 Luoshi Road Wuhan Hubei 430070 China

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Correction: Additive-mediated intercalation and surface modification of MXenes

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Chemical Society reviews 2022年第8期51卷 3314页

作者： Jing Zou Jing Wu Yizhou Wang Fengxia Deng Jizhou Jiang Yizhou Zhang Song Liu Neng Li Han Zhang Jiaguo Yu Tianyou Zhai Husam N Alshareef School of Environmental Ecology and Biological Engineering School of Chemistry and Environmental Engineering Key Laboratory of Green Chemical Engineering Process of Ministry of Education Engineering Research Center of Phosphorus Resources Development and Utilization of Ministry of Education Wuhan Institute of Technology Wuhan Hubei 430205 P. R. China. 027wit@***. Key Laboratory of Rare Mineral Ministry of Natural Resources Geological Experimental Testing Center of Hubei Province Wuhan Hubei 430034 P. R. China. Physical Science and Engineering Division Materials Science & Engineering King Abdullah University of Science and Technology (KAUST) Thuwal 23955-6900 Kingdom of Saudi Arabia. husam.alshareef@kaust.edu.sa. State Key Laboratory of Urban Water Resources and Environment School of Environment Harbin Institute of Technology Harbin 150090 P. R. China. Institute of Advanced Materials and Flexible Electronics (IAMFE) School of Chemistry and Materials Science Nanjing University of Information Science & Technology Nanjing 210044 P. R. China. yizhou.zhang@***. Key Laboratory for Organic Electronics & Information Displays and Institute of Advanced Materials Nanjing University of Posts and Telecommunications Nanjing 210023 P. R. China. Institute of Chemical Biology and Nanomedicine (ICBN) State Key Laboratory of Chemo/Biosensing and Chemometrics College of Chemistry and Chemical Engineering Hunan University Changsha 410082 P. R. China. State Key Laboratory of Advanced Technology for Materials Synthesis and Processing State Key Laboratory of Silicate Materials for Architectures Wuhan University of Technology Wuhan Hubei 430070 P. R. China. Shenzhen Engineering Laboratory of Phosphorene and Optoelectronics and Key Laboratory of Optoelectronic Devices and Systems of Ministry of Education and Guangdong Province Shenzhen University Shenzhen 518060 P. R. China. State Key Laboratory of Material Processing and Die & Mould Technology School of Materials Science and Engineering H

Correction for 'Additive-mediated intercalation and surface modification of MXenes' by Jing Zou , , 2022, DOI: 10.1039/d0cs01487g.

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Over 19 % Efficiency Organic Solar Cells Enabled by Manipulating the Intermolecular Interactions through Side Chain Fluorine Functionalization

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Angewandte Chemie 2024年第15期136卷

作者： Prof. Huawei Hu Shuai Liu Jiaoyu Xu Dr. Ruijie Ma Dr. Zhengxing Peng Top Archie Dela Peña Dr. Yongjie Cui Wenting Liang Xiaoli Zhou Dr. Siwei Luo Dr. Han Yu Prof. Mingjie Li Prof. Jiaying Wu Prof. Shangshang Chen Prof. Gang Li Prof. Yiwang Chen State Key Laboratory for Modification of Chemical Fibers and Polymer Materials College of Materials Science and Engineering Donghua University Shanghai 201620 P. R. China Key Lab of Fluorine and Silicon for Energy Materials and Chemistry of Ministry of Education/National Engineering Research Center for Carbohydrate Synthesis Jiangxi Normal University 99 Ziyang Avenue Nanchang 330022 P. R. China Department of Electrical and Electronic Engineering Research Institute for Smart Energy (RISE) Guangdong-Hong Kong-Macao (GHM) Joint Laboratory for Photonic-Thermal-Electrical Energy Materials and Devices The Hong Kong Polytechnic University Hung Hom Kowloon Hong Kong 999077 P. R. China Advanced Light Source Lawrence Berkeley National Laboratory Berkeley CA 94720 USA Function Hub Advanced Materials Thrust The Hong Kong University of Science and Technology Nansha 511400 Guangzhou P. R. China The Hong Kong Polytechnic University Faculty of Science Department of Applied Physics Kowloon Hong Kong 000000 P. R. China Department of Chemistry Hong Kong University of Science and Technology Clear Water Bay Kowloon Hong Kong 999077 P. R. China School of Chemistry and Chemical Engineering Nanjing University Nanjing 210023 P. R. China

Fluorine side chain functionalization of non-fullerene acceptors (NFAs) represents an effective strategy for enhancing the performance of organic solar cells (OSCs). However, a knowledge gap persists regarding the relationship between structural changes induced by fluorine functionalization and the resultant impact on device performance. In this work, varying amounts of fluorine atoms were introduced into the outer side chains of Y-series NFAs to construct two acceptors named BTP-F0 and BTP-F5. Theoretical and experimental investigations reveal that side-chain fluorination significantly increase the overall average electrostatic potential (ESP) and charge balance factor, thereby effectively improving the ESP-induced intermolecular electrostatic interaction, and thus precisely tuning the molecular packing and bulk-heterojunction morphology. Therefore, the BTP-F5-based OSC exhibited enhanced crystallinity, domain purity, reduced domain spacing, and optimized phase distribution in the vertical direction. This facilitates exciton diffusion, suppresses charge recombination, and improves charge extraction. Consequently, the promising power conversion efficiency (PCE) of 17.3 % and 19.2 % were achieved in BTP-F5-based binary and ternary devices, respectively, surpassing the PCE of 16.1 % for BTP-F0-based OSCs. This work establishes a structure-performance relationship and demonstrates that fluorine functionalization of the outer side chains of Y-series NFAs is a compelling strategy for achieving ideal phase separation for highly efficient OSCs.

关键词： non-fullerene acceptors fluorine functionalization intermolecular interactions solar cells molecular packing

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The Nature of Structural Defects in ZIF-8 Revealed with1H and31P MAS NMR and X-Ray Absorption Spectroscopy

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Angewandte Chemie 2024年第2期137卷

作者： Dr. Anton A. Gabrienko Dr. Somboon Chaemchuen Dr. Zongkui Kou Prof. Naoki Ogiwara Prof. Hiroshi Kitagawa Dr. Alexander E. Khudozhitkov Prof. Alexander G. Stepanov Dr. Daniil I. Kolokolov Prof. Francis Verpoort Boreskov Institute of Catalysis Novosibirsk Ac. Lavrentiev av. 5 Novosibirsk 630090 Russia Both authors contributed equally State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Wuhan 430070 China Department of Chemical Engineering Faculty of Engineering Mahidol University Nakhon Pathom 73170 Thailand Department of Basic Science School of Arts and Sciences The University of Tokyo 3-8-1 Komaba Meguro-ku Tokyo 153-8902 Japan Division of Chemistry Graduate School of Science Kyoto University Kitashirakawa-Oiwakecho Sakyo-ku Kyoto 606-8502 Japan School of Chemistry and Chemical Engineering Shandong University of Technology Zibo 255049 China Joint Institute of Chemical Research (FFMiEN) Peoples Friendship University of Russia (RUDN University) 6 Miklukho-Maklaya Str. 117198 Moscow Russia

The metal–organic frameworks (MOFs) attract interest as potential catalysts whose catalytic properties are driven by defects. Several methods have been proposed for the defects-inducing synthesis of MOFs. However, the active species formed on the defective sites remain elusive and uncharacterized, as the spectroscopic fingerprints of these species are hidden by the regular structure signals. In this work, we have performed the synthesis of ZIF-8 MOF with defect-inducing procedures using fully deuterated 2-methylimidazolate ligands to enhance the defective sites′ visibility. By combining 1 H and 31 P MAS NMR spectroscopy and X-ray absorption spectroscopy, we have found evidence for the presence of different structural hydroxyl Zn−OH groups in the ZIF-8 materials. It is demonstrated that the ZIF-8 defect sites are represented by Zn−OH hydroxyl groups with the signals at 0.3 and −0.7 ppm in the 1 H MAS NMR spectrum. These species are of basic nature and may be responsible for the catalytic activity of the ZIF-8 material.

关键词： metal–organic framework defects solid state NMR XAS catalysis

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synthesis,biochemical evaluation and computational simulations of new cytochrome bc1 complex inhibitors based on N-(4-aryloxyphenyl)phthalimides

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Chinese Chemical Letters 2018年第12期29卷 1897-1900页

作者： Hua Cheng Yan Fu Qing Chang Ni Zhang Mengwei Bu Yan Niu Qiongyou Wu Cheng Chen Francis Verpoort Department of Chemical Engineering and Food Science Hubei University of Arts and ScienceXiangyang 441053China State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of TechnologyWuhan 430070China Key Laboratory of Pesticide&Chemical Biology Ministry of EducationCollege of ChemistryCentral China Normal UniversityWuhan 430079China National Research Tomsk Polytechnic University Tomsk 634050Russian Federation Hubei University of Technology Engineering and Technology College Wuhan 430068China

The cytochrome bc1complex(the bc1complex or complex Ⅲ) is an attractive target for the discovery of numerous pharmaceuticals and pesticides. In order to identify new lead structures for this target, a new series of molecules, N-(4-aryloxyphenyl)phthalimides, were designed and synthesized in a straightforward manner. Our design strategy was to introduce a 4-aryloxyphenyl group, a fragment which exhibited promising bc1complex-inhibiting properties, into the aryl group of the valuable N-arylphthalimide backbone. Afterward, the biochemical evaluation of the newly synthesized compounds was carried out,and the results implied that several compounds demonstrated good activities against succinatecytochrome reductase(SCR, a mixture of mitochondrial complex Ⅱ and the bc1complex). Further studies confirmed that 3e’, a representative compound in this paper, was identified as an inhibitor of the bc1complex. Furthermore, computational simulations were also performed to better understand binding of 3e’ to the enzyme complex, which indicated that 3e’ should bind to the Qosite of the ***, we harbor the idea that this paper can provide a solid platform for synthesis and discovery of other bc1complex inhibitors.

关键词： Cytochrome bc_1 complex Inhibitor N-(4-Aryloxyphenyl)phthalimide synthesis Biochemical evaluation Computational simulation

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Full-field X-ray Imaging, a Workhorse Microscopy Beamline at NSLS II for Material Science Researches

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Microscopy and Microanalysis 2019年第S2期25卷 386-387页

作者： Xianghui Xiao Mingyuan Ge Chong Yin Feng Wang Lijie Zou Fei Chen Yu-chen Karen Chen-Wiegart Wah-Keat Lee National Synchrotron Light Source II Brookhaven National Laboratory Upton NY USA. Ningbo Institute of Materials Technology & Engineering Ningbo China. Sustainable Energy Technologies Department Brookhaven National Laboratory NY USA. State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Wuhan China. Department of Materials Science and Chemical Engineering Stony Brook University Stony Brook NY USA.

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Tandem Catalysis for Selective Oxidation of Methane to Oxygenates Using Oxygen over PdCu/Zeolite

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Angewandte Chemie 2022年第24期134卷

作者： Bo Wu Tiejun Lin Min Huang Shenggang Li Ji Li Xing Yu Ruoou Yang Fanfei Sun Zheng Jiang Yuhan Sun Liangshu Zhong CAS Key Laboratory of Low-Carbon Conversion Science and Engineering Shanghai Advanced Research Institute Chinese Academy of Sciences Shanghai 201210 P. R. China University of Chinese Academy of Sciences Beijing 100049 P. R. China School of Physical Science and Technology ShanghaiTech University Shanghai 201210 P. R. China Shanghai Synchrotron Radiation Facility Zhangjiang National Lab Shanghai Advanced Research Institute Chinese Academy of Sciences Shanghai 201204 P. R. China State Key Laboratory of Materials Processing and Die & Mould Technology School of Materials Science and Engineering Huazhong University of Science and Technology Wuhan Hubei 430074 P. R. China

Selective oxidation of methane to oxygenates with O 2 under mild conditions remains a great challenge. Here we report a ZSM-5 (Z-5) supported PdCu bimetallic catalyst (PdCu/Z-5) for methane conversion to oxygenates by reacting with O 2 in the presence of H 2 at low temperature (120 °C). Benefiting from the co-existence of PdO nanoparticles and Cu single atoms via tandem catalysis, the PdCu/Z-5 catalyst exhibited a high oxygenates yield of 1178 mmol g −1 Pd h −1 (mmol of oxygenates per gram Pd per hour) and at the same time high oxygenates selectivity of up to 95 %. Control experiments and mechanistic studies revealed that PdO nanoparticles promoted the in situ generation of H 2 O 2 from O 2 and H 2 , while Cu single atoms not only accelerated the activation of H 2 O 2 for the generation of abundant hydroxyl radicals (⋅OH) from H 2 O 2 decomposition, but also enabled the homolytic cleavage of CH 4 by ⋅OH to methyl radicals (⋅CH 3 ). Subsequently, the ⋅OH reacted quickly with the ⋅CH 3 to form CH 3 OH with high selectivity.

关键词： Methane Oxygenates Reaction Mechanisms Selective Oxidation Tandem Catalysis

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2020 Roadmap on gas-involved photo-and electro-catalysis

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Chinese Chemical Letters 2019年第12期30卷 2089-2109页

作者： Yulu Yang Yang Tang Haomin Jiang Yongmei Chen Pingyu Wan Maohong Fan Rongrong Zhang Sana Ullah Lun Pan Ji-Jun Zou Mengmeng Lao Wenping Sun Chao Yang Gengfeng Zheng Qiling Peng Ting Wang Yonglan Luo Xuping Sun Alexander S.Konev Oleg V.Levin Panagiotis Lianos Zhuofeng Hu Zhurui Shen Qinglan Zhao Ying Wang Nadia Todorova Christos Trapalis Matthew V.Sheridan Haipeng Wang Ling Zhang Songmei Sun Wenzhong Wang Jianmin Ma School of Physics and Electronics Hunan UniversityChangsha 410082China College of Chemistry Beijing University of Chemical TechnologyBeijing 100029China School of Civil and Environmental Engineering Georgia Institute of TechnologyAtlantaGA 30332United States College of Engineering and Applied Sciences and School of Energy ResourcesUniversity of WyomingLaramieWY 82071United States Key Laboratory for Green Chemical Technology of the Ministry of Education School of Chemical Engineering and TechnologyTianjin UniversityTianjin 300072China Collaborative Innovative Center of Chemical Science and Engineering(Tianjin) Tianjin 300072China Institute for Superconducting and Electronic Materials Australian Institute for Innovative MaterialsUniversity of WollongongNSW 2522Australia Laboratory of Advanced Materials Department of ChemistryFudan UniversityShanghai 200438China Institute of Fundamental and Frontier Sciences University of Electronic Science and Technology of ChinaChengdu 610054China Chemical Synthesis and Pollution Control Key Laboratory of Sichuan Province College of Chemistry and Chemical EngineeringChina West Normal UniversityNanchong 637002China Institute of Chemistry St.Petersburg State University7/9 Universitetskaya emb.St.Petersburg 199034Russian Federation Department of Chemical Engineering University of PatrasPatras 26500Greece School of Environmental Science and Engineering Guangdong Provincial Key Laboratory of Environmental Pollution Control and Remediation TechnologySun Yat-sen UniversityGuangzhou 510275China School of Materials Science and Engineering Nankai UniversityTianjin 300350China Department of Chemistry Chinese University of Hong KongHong KongChina Institute of Nanoscience and Nanotechnology NCSR"Demokritos"Athens 15341Greece State Key Laboratory of School of Radiation Medicine and Protection and School for Radiological and interdisciplinary Sciences(RAD-X) Soochow UniversitySuzhou 215123China State Key Laboratory of High Performance Ceramics and Superf

Green reactions not only provide us chemical products without any pollution,but also offer us the viable technology to realize difficult tasks in normal ***-,photoelectro-,and electrocatalytic reactions are indeed powerful tools to help us to embrace bright ***,some gas-involved reactions are extremely useful to change our life environments from energy systems to liquid fuels and cost-effective products,such as H2 evolution(H2 production),02 evolution/reduction,CO2 reduction,N2 reduction(or N2 fixation) *** can provide fuel cells clean H2 for electric vehicles from H2 evolution reaction(HER),at the same time,we also need highly efficient 02 reduction reaction(ORR) in fuel cells for improving the reaction ***,we can get the clean oxidant O2 from water through O2 evolution reaction(OER),and carry out some reactions without posing any pollution to reaction ***,we can translate the greenhouse gas CO2 into useful liquid fuels through CO2 reduction reaction(CRR).Last but not the least,we can get ammonia from N2 reduction reaction(NRR),which can decrease energy input compared to the traditional Hubble *** reactions,such as HER,ORR,OER,CRR and NRR could be realized through solar-,photoelectro-and electro-assisted *** them,the catalysts used play crucial roles in determining the efficiency and kinds of products,so we should consider the efficiency of ***,the cost,synthetic methods of catalysts should also be ***,significant progress has been achieved,however,many challenges still exist,reaction systems,catalysts underlying mechanisms,and so *** extremely active fields,we should pay attention to *** the background,it has motivated us to contribute with a roadmap on ’GasInvolved Photo-and Electro-Catalysis’.

关键词： H2 evolution reaction O2 reduction reaction O2 evolution reaction CO2 reduction reaction N2 reduction reaction Electrocatalysis Photocatalysis Photoelectrocatalysis

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FeVO 4 ⋅nH 2 [email protected] nanocomposite as high performance cathode materials for aqueous Zn-ion batteries

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Journal of Alloys and Compounds 2020年 818卷

作者： Binxu Lan Chen Tang Lineng Chen Wenwei Zhang Wen Tang Chunli Zuo Xudong Fu Shijie Dong Qinyou An Ping Luo Hubei Provincial Key Laboratory of Green Materials for Light Industry Collaborative Innovation Center of Green Light-Weight Materials and Processing School of Materials and Chemical Engineering Hubei University of Technology Hubei Wuhan 430068 PR China State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Wuhan 430070 Hubei China Hubei University of Economics Hubei Wuhan 430205 PR China

Aqueous zinc ion batteries (ZIBs) have recently attracted an increasing attention as an environmental friendliness, low cost and highly potential novel energy storage system. Although vanadium-based materials serve as a capable of arousing and holding the attention cathode materials for ZIBs, whereas low conductivity and confusing zinc ion storage mechanisms remain an obstacle. Herein, FeVO 4 ⋅nH 2 [email protected] composite is employed to evaluate zinc ion storage capability as a cathode for the first time in 2 M Zn(TFSI) 2 electrolyte. Benefiting from the large lattice spacing, dual electrochemical activity and fast electron transfer, the composite delivers excellent rate performance and long life cycle (the capacity retained ∼100 mAh g −1 at 1.0 A g −1 after 1000 cycle). In addition, the electrochemical performance of graphene-modified FeVO 4 ⋅nH 2 O is superior to other precursors for comparison. Furthermore, the intercalated/de-intercalated mechanism of zinc ion is distinct from the traditional conversion reaction, which is confirmed by in-situ X-ray diffraction and various ex-situ techniques.

关键词： FeVO 4 ⋅nH 2 [email protected] Aqueous zinc ion batteries Cathode Energy storage mechanism

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Regulating Non-Equilibrium Solvation Structure in Locally Concentrated Ionic Liquid Electrolytes for Wide-Temperature and High-Voltage Lithium Metal Batteries

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Angewandte Chemie 2024年第1期137卷

作者： Haifeng Tu Zhicheng Wang Jiangyan Xue Zhiyong Tang Yang Liu Xiaofang Liu Lingwang Liu Suwan Lu Shixiao Weng Yiwen Gao Guochao Sun Zheng Liu keyang Peng Xin Zhang Dejun Li Guangye Wu Meinan Liu Jianchen Hu Hong Li Jingjing Xu Xiaodong Wu School of Nano-Tech and Nano-Bionics University of Science and Technology of China Hefei Anhui 230026 China i-lab Suzhou Institute of Nano-Tech and Nano-Bionics Chinese Academy of Sciences Suzhou Jiangsu 215123 China These authors contributed equally to this work: Haifeng Tu Zhicheng Wang Institute of Physics Chinese Academy of Sciences Beijing 100190 China Tianmu Lake Institute of Advanced Energy Storage Technologies Liyang 213300 China Jiangxi Key Laboratory of Flexible Electronics Jiangxi Science & Technology Normal University Nanchang 330013 Jiangxi China State Key Laboratory of Featured Metal Materials and Life-cycle Safety for Composite Structures Guangxi Key Laboratory of Processing for Non-Ferrous Metals and Featured Materials School of Resources Environment and Materials Guangxi University Nanning 530004 China National Engineering Laboratory for Modern Silk College of Textile and Clothing Engineering Research Center of Cooperative Innovation for Functional Organic/Polymer Material Micro/Nanofabrication Soochow University Suzhou 215123 China College of Material Science and Engineering Hohai University Nanjing Jiangsu 210024 China

The development of high-voltage lithium metal batteries (LMBs) encounters significant challenges due to aggressive electrode chemistry. Recently, locally concentrated ionic liquid electrolytes (LCILEs) have garnered attention for their exceptional stability with both Li anodes and high-voltage cathodes. However, there remains a limited understanding of how diluents in LCILEs affect the thermodynamic stability of the solvation structure and transportation dynamics of Li + ions. Herein, we propose a wide-temperature LCILEs with 1,3-dichloropropane (DCP13) diluent to construct a non-equilibrium solvation structure under external electric field, wherein the DCP13 diluent enters the Li + ion solvation sheath to enhance Li + ion transport and suppress oxidative side reactions at high-nickel cathode (LiNi 0.9 Co 0.05 Mn 0.05 O 2 , NCM90). Consequently, a Li/NCM90 cell utilizing this LCILE achieves a high capacity retention of 94 % after 240 cycles at 4.3 V, also operates stably at high cut-off voltages from 4.4 V to 4.6 V and over a wide temperature range from −20 °C to 60 °C. Additionally, an Ah-level pouch cell with this LCILE simultaneously achieves high-energy-density and stable cycling, manifesting the practical feasibility. This work redefines the role of diluents in LCILEs, providing inspiration for electrolyte design in developing high-energy-density batteries.

关键词： Lithium metal batteries locally concentrated ionic liquid electrolyte chloroalkane diluent non-equilibrium solvation structure external electric field

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